#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105133.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105133_Fobs loop_ _publ_author_name 'Merlini, Marco' 'Perchiazzi, Natale' 'Hanfland, Michael' 'Bossak, Alexei' _publ_section_title ; Phase transition at high pressure in Cu~2~CO~3~(OH)~2~ related to the reduction of the Jahn--Teller effect ; _journal_coeditor_code PS5017 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 266 _journal_page_last 274 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _[local]_cod_data_source_file ps5017malachite_p2sup4.hkl _[local]_cod_data_source_block malachite_p2 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status _jana_refln_twin_domain 0 0 -1 724.16 656.96 15.92 o 1 0 0 1 724.16 623.05 14.72 o 1 0 0 2 291.31 274.90 22.52 o 1 0 0 -2 291.31 314.57 24.53 o 1 0 0 -3 4.12 36.06 32.96 < 1 0 0 3 4.12 2.98 25.65 < 1 0 0 -4 3278.65 3477.66 74.48 o 1 0 -1 1 299.10 323.25 12.86 o 1 0 1 1 299.10 326.85 18.52 o 1 0 -1 -1 299.10 314.21 15.99 o 1 0 -1 -2 13678.29 13966.26 65.95 o 1 0 1 2 13678.29 14260.98 69.32 o 1 0 -1 2 13678.30 14132.79 61.24 o 1 0 1 -2 13678.30 14255.75 63.24 o 1 0 -1 -3 69.92 62.17 29.78 < 1 0 1 -3 69.92 85.12 32.89 < 1 0 1 3 69.92 87.87 42.87 < 1 0 -1 3 69.92 57.41 28.61 < 1 0 -1 -4 200.58 128.76 48.53 < 1 0 -2 2 201.21 183.07 20.92 o 1 0 2 2 201.21 197.31 40.72 o 1 0 -2 -2 201.21 202.87 28.18 o 1 0 2 3 797.64 854.90 62.62 o 1 0 -2 3 797.64 802.47 43.30 o 1 0 -2 -3 797.64 759.25 45.80 o 1 0 -2 -4 170.84 165.63 43.70 o 1 0 -3 -2 143.58 169.16 30.66 o 1 0 -3 -3 1160.69 1363.78 54.21 o 1 0 -3 3 1160.69 1192.74 44.25 o 1 -1 -1 4 20.20 21.22 41.62 < 1 1 -1 -4 20.20 22.45 35.19 < 1 -1 -1 3 988.28 961.97 39.62 o 1 1 1 -3 988.28 912.41 42.25 o 1 1 -1 -3 988.28 872.64 34.79 o 1 -1 -1 2 2435.81 2631.60 31.31 o 1 1 -1 -2 2435.81 2477.71 35.61 o 1 1 1 -2 2435.81 2539.50 30.66 o 1 -1 -1 -1 2604.00 2533.42 28.13 o 1 1 1 1 2604.00 2447.67 29.06 o 1 -1 1 -1 2603.99 2558.17 30.63 o 1 1 -1 1 2603.99 2490.42 29.11 o 1 1 -1 2 3662.59 3652.85 45.35 o 1 -1 -1 -2 3662.59 3840.88 48.60 o 1 1 1 2 3662.59 3876.14 51.46 o 1 -1 1 -2 3662.59 3789.95 45.45 o 1 1 -1 3 98.38 100.83 35.09 < 1 1 1 3 98.38 102.86 40.12 < 1 -1 1 -3 98.38 105.84 35.51 < 1 -1 -1 -3 98.38 113.05 38.92 < 1 1 -2 -4 623.30 427.39 51.46 o 1 -1 -2 3 9.86 22.15 26.93 < 1 1 -2 -3 9.86 20.75 29.43 < 1 -1 -2 2 685.01 613.34 24.28 o 1 1 -2 -2 685.00 612.99 29.83 o 1 1 2 1 15.81 16.24 19.25 < 1 -1 -2 -1 15.81 14.14 13.81 < 1 1 -2 2 700.82 776.21 36.69 o 1 -1 -2 -2 700.82 737.30 37.54 o 1 1 2 2 700.82 838.63 43.22 o 1 1 2 3 708.37 823.39 60.97 o 1 1 -2 3 708.37 766.75 49.68 o 1 -1 -2 -3 708.37 785.47 51.63 o 1 1 -3 -4 168.39 126.56 42.87 < 1 -1 -3 3 162.85 141.90 28.93 o 1 1 -3 -3 162.86 178.44 38.82 o 1 1 3 2 284.90 335.61 48.08 o 1 -1 -3 -2 284.90 257.33 29.71 o 1 1 -3 3 41.54 22.57 34.84 < 1 1 3 3 41.54 76.11 65.70 < 1 -1 -3 -3 41.54 38.64 43.77 < 1 -1 -4 3 502.62 491.26 36.44 o 1 -1 -4 -3 321.93 237.91 48.80 o 1 2 0 -3 2102.39 1749.69 37.04 o 1 2 0 -2 843.46 803.82 20.20 o 1 2 0 0 950.17 842.89 11.04 o 1 -2 0 0 950.17 793.96 12.41 o 1 -2 0 -1 10606.38 10807.52 52.28 o 1 2 0 1 10606.38 10781.79 54.33 o 1 2 0 2 194.36 196.04 34.31 o 1 -2 0 -2 194.36 183.97 28.68 o 1 2 0 3 1835.33 1953.01 56.14 o 1 -2 0 -3 1835.33 2088.38 60.12 o 1 2 -1 -4 33.12 10.11 28.53 < 1 2 -1 -3 3898.10 3584.60 46.90 o 1 2 1 -3 3898.10 3972.90 52.66 o 1 -2 -1 3 3898.10 4531.85 58.14 o 1 -2 -1 2 149.48 134.87 16.89 o 1 2 -1 -2 149.48 117.50 16.97 o 1 2 1 -2 149.48 117.63 15.89 o 1 -2 -1 0 36.73 45.32 8.33 o 1 2 1 0 36.73 39.04 8.51 o 1 2 -1 1 5536.00 5646.01 43.52 o 1 -2 -1 -1 5535.99 5867.50 44.70 o 1 -2 1 -1 5536.00 5714.56 46.12 o 1 2 1 1 5535.99 5756.43 43.65 o 1 -2 -1 -2 540.75 494.79 35.19 o 1 -2 1 -2 540.75 495.14 34.39 o 1 2 1 2 540.75 442.70 37.22 o 1 2 -1 2 540.75 485.25 31.18 o 1 -2 1 -3 1517.12 1845.15 76.18 o 1 -2 -1 -3 1517.12 1756.48 62.14 o 1 2 1 3 1517.12 1758.40 62.12 o 1 2 -1 3 1517.12 1670.53 61.37 o 1 2 -2 -4 687.71 581.35 42.97 o 1 -2 -2 4 687.71 4.23 17.89 < 1 2 -2 -3 570.31 465.48 32.66 o 1 -2 -2 3 570.31 509.60 31.38 o 1 -2 -2 2 65.58 43.65 13.01 o 1 -2 -2 0 11900.97 10031.63 32.89 o 1 2 2 0 11900.97 9673.17 41.47 o 1 2 2 1 4187.86 4806.15 48.28 o 1 -2 -2 -1 4187.86 5042.76 45.30 o 1 -2 -2 -2 42.33 33.56 28.68 < 1 2 -2 2 42.33 22.75 27.58 < 1 2 2 2 42.33 30.88 28.91 < 1 -2 -2 -3 1.78 22.90 36.01 < 1 2 2 3 1.78 41.97 49.70 < 1 2 -2 3 1.78 30.73 39.82 < 1 2 -3 -4 98.52 35.99 31.98 < 1 -2 -3 3 96.75 106.32 23.75 o 1 -2 -3 2 4914.89 5038.78 36.01 o 1 2 3 1 665.98 831.93 41.19 o 1 -2 -3 -1 665.98 811.88 32.49 o 1 -2 -3 -2 6716.64 7373.68 69.80 o 1 2 3 2 6716.64 7958.76 88.40 o 1 2 3 3 25.98 11.76 51.23 < 1 -2 -3 -3 25.98 27.50 42.75 < 1 -2 -4 3 0.76 15.02 20.17 < 1 2 4 2 258.57 279.03 58.01 o 1 -2 -4 -2 258.57 186.28 32.21 o 1 -2 -4 -3 120.84 19.70 35.06 < 1 3 -1 -3 800.41 658.56 31.18 o 1 -3 -1 0 2802.76 2650.82 25.50 o 1 3 1 0 2802.76 2680.20 24.10 o 1 -3 -1 -1 4146.10 4746.36 48.53 o 1 3 1 1 4146.10 4484.55 47.13 o 1 3 -1 1 4146.09 4553.70 45.42 o 1 -3 -1 -2 1124.92 1300.53 53.88 o 1 3 -1 2 1124.92 1329.01 49.98 o 1 3 1 2 1124.92 1253.51 48.18 o 1 -3 1 -2 1124.92 1281.76 53.73 o 1 -3 1 -3 297.84 344.47 59.54 o 1 -3 -1 -3 297.85 390.45 53.18 o 1 3 -2 -3 1348.73 1158.85 37.02 o 1 -3 -2 0 2733.16 2584.62 26.88 o 1 3 2 0 2733.16 2453.53 25.90 o 1 -3 -2 -1 5533.26 5865.42 54.73 o 1 3 2 1 5533.26 6374.55 54.38 o 1 3 2 2 876.42 897.87 49.60 o 1 -3 -2 -2 876.42 974.90 49.15 o 1 3 -2 3 609.21 12.81 44.25 < 1 -3 -3 3 24.24 14.57 13.97 < 1 -3 -3 0 3803.74 3326.45 32.69 o 1 3 3 0 3803.74 3315.54 41.14 o 1 3 3 1 1.72 10.44 26.78 < 1 -3 -3 -1 1.72 20.20 22.62 < 1 3 3 2 523.27 652.63 48.08 o 1 -3 -3 -2 523.27 549.32 44.35 o 1 -3 -4 3 75.15 93.95 19.67 o 1 -3 -4 -1 243.52 266.96 33.69 o 1 3 4 1 243.52 247.52 41.14 o 1 3 4 2 2614.17 3044.69 90.82 o 1 -3 -4 -2 2614.17 2774.93 70.80 o 1 3 4 3 804.31 7.66 25.75 < 1 -3 -5 -2 1066.98 1151.15 57.01 o 1 4 0 -3 269.85 285.03 19.40 o 1 4 0 -2 913.66 772.34 14.42 o 1 4 0 0 10625.35 8045.06 45.70 o 1 4 0 1 745.98 788.30 33.16 o 1 -4 0 -1 745.98 745.78 35.46 o 1 4 0 2 20.55 18.70 30.81 < 1 -4 0 -2 20.55 8.91 30.58 < 1 4 0 3 75.61 2.50 17.32 < 1 4 -1 -3 0.97 17.34 19.90 < 1 4 1 -1 418.97 344.07 13.71 o 1 4 1 0 182.69 201.07 18.77 o 1 -4 -1 0 182.69 189.66 19.42 o 1 4 1 1 128.27 114.62 28.48 o 1 -4 -1 -1 128.27 136.50 30.93 o 1 4 -1 2 2369.79 2719.77 69.27 o 1 -4 1 -2 2369.79 2767.17 80.81 o 1 -4 -1 -2 2369.79 2700.02 65.57 o 1 4 1 2 2369.79 2687.41 64.19 o 1 4 -1 3 194.66 0.48 15.22 < 1 4 1 3 194.66 6.56 14.24 < 1 4 2 -1 4607.60 3700.13 31.11 o 1 -4 -2 1 4607.60 3810.27 27.78 o 1 -4 -2 0 3783.32 4130.89 37.67 o 1 4 2 0 3783.32 3765.90 36.39 o 1 -4 -2 -1 1747.46 1892.50 46.12 o 1 4 2 1 1747.46 1830.01 43.17 o 1 -4 -2 -2 239.43 201.57 38.32 o 1 4 2 2 239.43 195.64 40.59 o 1 4 -2 3 788.23 5.61 14.74 < 1 -4 -3 1 3752.49 3478.99 30.01 o 1 4 3 0 998.46 908.86 33.59 o 1 -4 -3 0 998.46 887.34 28.81 o 1 -4 -3 -1 8908.82 9875.61 76.36 o 1 4 3 1 8908.82 9637.18 77.18 o 1 4 3 2 10.20 21.82 39.42 < 1 -4 -3 -2 10.20 20.02 37.52 < 1 4 4 0 49.78 17.79 27.93 < 1 -4 -4 0 49.78 16.39 19.77 < 1 4 4 1 2573.25 2526.48 60.54 o 1 -4 -4 -1 2573.25 2648.42 57.84 o 1 -4 -4 -2 36.69 50.60 45.05 < 1 4 4 2 36.69 51.43 46.88 < 1 -4 -5 3 591.37 445.16 17.54 o 1 4 5 1 942.17 946.07 71.65 o 1 -4 -5 -1 942.17 904.70 48.03 o 1 -4 -5 -2 111.62 129.64 45.12 < 1 5 -1 -3 645.76 586.48 24.55 o 1 5 1 -1 67.86 23.23 14.67 < 1 -5 -1 0 1024.04 1109.98 30.98 o 1 5 1 0 1024.04 1162.43 33.29 o 1 5 1 1 3551.74 4196.64 56.71 o 1 -5 -1 -1 3551.74 4374.36 59.44 o 1 5 1 2 349.42 419.63 54.43 o 1 -5 -1 -2 349.42 461.67 62.47 o 1 -5 1 -2 349.42 465.93 60.82 o 1 5 -1 2 349.42 362.14 50.25 o 1 5 2 -1 7199.21 6857.09 40.04 o 1 -5 -2 1 7199.21 6899.82 40.34 o 1 -5 -2 0 5912.53 6192.35 53.38 o 1 5 2 0 5912.53 6322.34 48.00 o 1 -5 -2 -1 0.55 8.23 26.18 < 1 5 2 1 0.55 39.94 32.56 < 1 -5 -2 -2 19.51 36.14 45.30 < 1 5 2 2 19.51 9.96 34.24 < 1 5 3 -1 754.83 571.87 27.98 o 1 -5 -3 1 754.83 594.94 23.18 o 1 -5 -3 0 1365.73 1744.44 41.09 o 1 5 3 0 1365.73 1555.43 43.77 o 1 -5 -3 -1 4392.29 5193.87 70.78 o 1 5 3 1 4392.29 5390.36 73.10 o 1 -5 -3 -2 383.87 357.31 52.86 o 1 -5 -4 1 182.55 138.75 22.72 o 1 5 4 0 737.36 717.73 49.50 o 1 -5 -4 0 737.36 790.93 43.85 o 1 -5 -4 -1 2910.48 3254.87 66.67 o 1 5 4 1 2910.48 3404.83 74.88 o 1 -5 -5 1 2544.82 2174.05 40.24 o 1 -5 -5 0 11089.83 12266.25 78.06 o 1 5 5 1 145.21 132.39 62.34 < 1 -5 -5 -1 145.21 154.94 45.52 o 1 -5 -6 -1 382.62 524.04 52.08 o 1 6 0 0 439.29 628.08 34.84 o 1 -6 0 -1 1508.31 1925.21 67.62 o 1 6 0 1 1508.31 1832.03 57.39 o 1 6 1 -1 1437.96 1255.98 30.56 o 1 -6 -1 0 411.63 287.39 35.34 o 1 6 1 0 411.63 308.08 30.38 o 1 -6 -1 -1 2431.56 2901.76 64.87 o 1 6 1 1 2431.56 2808.84 59.51 o 1 -6 -2 1 443.04 358.74 29.31 o 1 6 2 -1 443.04 364.34 23.58 o 1 6 2 0 5198.03 6012.48 59.69 o 1 -6 -2 0 5198.03 5983.98 58.96 o 1 -6 -2 -1 465.51 514.31 46.53 o 1 6 2 1 465.51 472.46 48.30 o 1 6 3 -1 52.16 10.69 20.30 < 1 -6 -3 1 52.16 10.66 18.24 < 1 -6 -3 0 1359.92 1510.58 54.41 o 1 6 3 0 1359.92 1502.43 48.85 o 1 -6 -3 -1 250.31 263.41 40.84 o 1 6 3 1 250.31 208.53 44.07 o 1 6 3 2 4041.31 4.63 15.69 < 1 -6 -4 1 389.56 270.44 27.25 o 1 -6 -4 0 11304.48 13741.47 85.69 o 1 6 4 0 11304.48 12221.77 92.88 o 1 -6 -4 -1 2.39 1.73 32.51 < 1 6 4 1 2.39 19.20 35.41 < 1 -6 -5 2 477.34 312.19 18.02 o 1 -6 -5 1 185.45 138.10 23.85 o 1 -6 -5 0 312.95 311.61 47.03 o 1 6 5 0 312.95 289.96 52.43 o 1 -6 -5 -1 101.31 110.07 47.28 < 1 6 5 1 101.31 96.38 49.68 < 1 -6 -6 2 285.47 199.94 23.13 o 1 -6 -6 1 392.80 416.40 40.64 o 1 -6 -6 0 6.16 10.91 24.90 < 1 6 6 1 29.60 9.69 53.01 < 1 -6 -6 -1 29.60 26.13 40.04 < 1 7 1 -2 441.41 279.35 18.22 o 1 7 1 -1 6.81 15.29 24.15 < 1 -7 -1 0 3197.86 3040.62 60.69 o 1 7 1 0 3197.86 3830.34 56.69 o 1 7 1 1 85.13 80.64 43.10 < 1 -7 -1 -1 85.13 87.97 40.84 < 1 7 2 -2 3402.31 2183.54 27.98 o 1 7 2 -1 550.85 431.89 31.16 o 1 7 2 0 3202.65 3677.50 56.44 o 1 -7 -2 0 3202.65 3556.37 67.05 o 1 7 2 1 17.73 28.01 39.52 < 1 -7 -2 -1 17.73 14.34 35.69 < 1 -7 -3 1 243.12 72.15 25.15 < 1 7 3 -1 243.12 66.05 26.88 < 1 -7 -3 0 5183.00 5807.63 68.82 o 1 7 3 0 5183.00 5917.75 76.23 o 1 -7 -3 -1 12.47 21.20 40.49 < 1 7 3 1 12.47 17.57 34.84 < 1 -7 -4 1 2308.46 2306.42 50.40 o 1 7 4 -1 2308.46 2467.85 70.43 o 1 7 4 0 778.62 667.32 53.78 o 1 -7 -4 0 778.62 711.65 55.03 o 1 -7 -4 -1 357.09 242.44 59.46 o 1 -7 -5 2 605.56 378.06 23.80 o 1 -7 -5 1 1343.79 1073.89 46.53 o 1 -7 -5 0 8.25 18.92 33.81 < 1 7 5 0 8.25 28.86 47.28 < 1 -7 -5 -1 3326.65 7.08 37.07 < 1 -7 -6 2 106.09 33.39 18.22 < 1 -7 -6 1 2121.06 2063.16 56.39 o 1 -7 -6 0 165.00 79.74 44.25 < 1 7 6 0 165.00 117.53 66.40 < 1 -7 -7 2 34.87 19.12 22.65 < 1 -7 -7 1 1080.24 1141.59 57.86 o 1 -7 -7 0 785.77 833.08 68.67 o 1 8 1 -2 2173.50 1909.92 36.71 o 1 8 1 -1 893.38 706.34 41.09 o 1 8 1 0 1197.50 1291.40 63.24 o 1 8 2 -2 21.25 13.34 15.64 < 1 8 2 -1 798.92 729.71 42.02 o 1 8 2 0 1073.79 1335.02 62.84 o 1 -8 -2 0 1073.79 1160.53 52.81 o 1 -8 -3 1 454.33 380.94 43.32 o 1 8 3 -1 454.33 352.03 37.54 o 1 -8 -3 0 977.85 936.79 60.74 o 1 8 3 0 977.85 1139.41 65.82 o 1 8 4 -1 2438.96 2219.05 65.92 o 1 -8 -4 1 2438.96 2029.90 58.24 o 1 -8 -4 0 276.08 210.85 48.45 o 1 8 4 0 276.08 202.69 50.00 o 1 8 4 1 572.84 8.36 16.89 < 1 -8 -5 2 10.69 20.42 19.30 < 1 -8 -5 1 1121.04 866.51 55.74 o 1 8 5 -1 1121.04 772.06 68.80 o 1 8 5 0 10.75 46.88 48.58 < 1 -8 -5 0 10.75 23.60 34.84 < 1 -8 -6 2 90.85 52.21 24.05 < 1 -8 -6 1 251.13 129.34 41.19 o 1 8 6 0 559.16 361.39 84.19 o 1 -8 -6 0 559.16 506.55 66.90 o 1 -8 -7 2 138.76 47.10 25.55 < 1 -8 -7 1 27.06 41.54 38.39 < 1 -8 -7 0 835.69 857.40 70.35 o 1 9 1 -2 37.07 21.72 22.37 < 1 9 1 -1 160.31 70.15 35.29 < 1 9 1 0 48.72 46.90 43.82 < 1 9 2 -2 103.93 29.76 22.12 < 1 9 2 -1 2217.02 1791.21 61.72 o 1 9 2 0 107.03 60.27 47.28 < 1 -9 -2 0 107.03 44.40 45.35 < 1 9 3 -2 10.82 35.94 34.61 < 1 -9 -3 1 431.96 420.76 56.66 o 1 9 3 -1 431.96 426.34 49.75 o 1 -9 -3 0 45.99 25.65 45.40 < 1 9 3 0 45.99 31.71 44.17 < 1 9 4 -1 7.61 15.99 26.53 < 1 -9 -4 1 7.61 10.29 27.60 < 1 9 4 0 366.48 351.03 64.52 o 1 -9 -4 0 366.48 278.45 56.14 o 1 9 5 -1 42.92 17.14 42.95 < 1 -9 -5 1 42.92 25.78 34.69 < 1 -9 -5 0 4368.62 5692.43 111.70 o 1 9 5 0 4368.62 13.01 35.44 < 1 -9 -6 1 2.25 17.07 31.63 < 1 -9 -6 0 99.76 3.30 35.84 < 1 -9 -7 2 183.02 24.70 10.59 < 1 -9 -7 1 264.16 132.64 46.05 < 1 -9 -8 1 1421.75 1473.67 78.41 o 1 10 1 -2 357.97 158.22 34.74 o 1 10 1 -1 157.68 75.78 37.47 < 1 10 2 -2 5.27 11.06 22.75 < 1 10 2 -1 260.71 99.81 41.92 < 1 -10 -2 0 1236.22 20.00 35.81 < 1 10 3 -1 685.30 502.57 54.43 o 1 10 4 -1 371.03 204.72 48.13 o 1 -10 -4 1 371.03 210.28 49.50 o 1 10 5 -1 1.86 27.15 44.95 < 1 -10 -5 1 1.86 17.37 34.99 < 1 10 5 0 5.96 3.73 13.16 < 1 -10 -6 1 477.63 269.89 58.21 o 1 -10 -7 1 83.10 32.01 37.92 < 1 -10 -8 1 160.54 55.31 45.65 < 1 11 2 -1 246.59 53.46 43.95 < 1 11 3 -1 0.89 46.20 42.32 < 1 11 4 -1 730.27 571.59 67.20 o 1 11 5 -1 504.31 329.41 70.35 o 1 -11 -5 1 504.31 372.45 58.01 o 1 0 0 1 367.03 341.99 13.12 o 2 0 0 -1 367.03 319.08 9.09 o 2 0 0 2 147.65 112.56 30.34 o 2 0 0 -2 147.65 185.40 15.30 o 2 0 0 -3 2.09 34.55 19.49 < 2 0 1 1 151.60 182.31 8.64 o 2 0 1 2 6932.74 7744.10 44.44 o 2 0 -1 -2 6932.74 7813.71 43.48 o 2 0 1 -2 6932.75 7782.09 43.05 o 2 0 1 -3 35.44 25.46 18.25 < 2 0 -1 -3 35.44 114.54 29.28 o 2 0 1 3 35.44 21.80 34.47 < 2 0 2 2 101.98 117.75 14.51 o 2 0 2 -3 404.28 444.69 33.37 o 2 0 2 3 404.28 391.51 33.75 o 2 0 3 2 72.77 50.06 16.53 o 2 0 3 3 588.29 664.44 27.52 o 2 0 4 3 500.92 593.25 28.01 o 2 1 1 -4 33.14 16.79 23.62 < 2 -1 1 3 500.90 436.24 39.29 o 2 1 1 -3 500.90 476.81 31.65 o 2 1 -1 -3 500.90 392.88 42.03 o 2 1 1 -2 1234.57 1373.33 30.38 o 2 -1 1 2 1234.57 1155.76 27.81 o 2 1 -1 -2 1234.57 1289.97 31.36 o 2 -1 -1 2 1234.57 1314.94 53.65 o 2 -1 -1 1 29.05 31.51 16.63 < 2 -1 1 1 29.05 18.65 8.34 < 2 1 -1 -1 29.05 14.94 16.24 < 2 1 1 -1 29.05 24.54 10.11 < 2 -1 -1 -2 1856.36 1958.64 24.85 o 2 -1 1 -2 1856.36 2026.53 33.94 o 2 -1 1 -3 49.86 43.76 18.20 < 2 1 2 -4 688.20 186.28 36.70 o 2 -1 2 4 688.20 2.17 17.51 < 2 1 2 -3 5.00 5.88 18.31 < 2 -1 2 3 5.00 20.80 21.17 < 2 -1 2 2 347.19 287.96 20.45 o 2 1 2 -2 347.19 301.14 22.94 o 2 1 2 2 355.20 290.95 11.54 o 2 -1 2 -3 359.03 352.75 26.97 o 2 1 3 -3 82.54 53.33 26.34 < 2 -1 3 3 82.54 46.05 21.72 < 2 1 3 2 144.40 134.91 11.79 o 2 1 3 3 21.05 11.73 17.49 < 2 -1 4 3 254.75 194.04 26.17 o 2 1 4 3 163.17 81.44 14.71 o 2 1 5 3 766.32 762.96 28.44 o 2 2 0 -4 0.92 23.13 37.70 < 2 2 0 -3 1065.58 848.51 36.72 o 2 -2 0 3 1065.58 1043.63 56.88 o 2 2 0 -2 427.50 481.21 29.22 o 2 -2 0 2 427.50 450.93 27.26 o 2 -2 0 1 16792.11 18188.01 45.79 o 2 2 0 -1 16792.11 18059.92 51.10 o 2 -2 0 -2 98.51 71.12 10.46 o 2 -2 0 -3 930.22 977.69 24.66 o 2 -2 1 4 20.19 28.16 58.46 < 2 2 1 -4 20.19 30.06 28.83 < 2 2 1 -3 1975.72 1949.06 53.86 o 2 -2 -1 3 1975.72 1809.51 79.09 o 2 -2 1 3 1975.72 1925.64 49.75 o 2 2 -1 -3 1975.72 2047.56 62.05 o 2 -2 1 2 75.76 75.29 19.55 o 2 -2 -1 2 75.76 71.80 27.11 < 2 2 1 -2 75.76 68.55 17.78 o 2 2 -1 -2 75.76 37.21 26.01 < 2 -2 -1 1 5450.08 5309.76 30.71 o 2 -2 1 1 5450.09 5016.79 36.23 o 2 2 -1 -1 5450.09 4944.36 52.92 o 2 2 1 -1 5450.08 5283.75 29.99 o 2 -2 1 -3 768.94 810.30 28.40 o 2 2 2 -4 622.88 475.49 46.50 o 2 -2 2 3 289.06 201.01 32.10 o 2 2 2 -3 289.06 247.67 31.38 o 2 -2 -2 2 33.24 24.27 37.76 < 2 2 2 -2 33.24 39.11 23.05 < 2 -2 2 2 33.24 28.16 20.82 < 2 -2 -2 1 136.52 90.35 22.52 o 2 2 2 -1 136.52 91.04 14.45 o 2 2 3 -4 168.28 98.38 32.10 o 2 2 3 -3 49.04 23.70 30.81 < 2 -2 3 3 49.04 41.48 26.21 < 2 2 3 -2 2491.08 2530.91 48.61 o 2 2 5 3 4.13 7.99 6.78 < 2 3 1 -4 200.21 14.06 40.54 < 2 -3 -1 3 405.68 362.48 52.94 o 2 3 1 -3 405.68 360.92 41.62 o 2 3 -1 -3 405.68 277.03 50.98 o 2 -3 1 3 405.68 343.84 38.06 o 2 3 -1 -2 214.94 224.52 38.58 o 2 -3 -1 2 214.94 190.03 25.89 o 2 3 1 -2 214.94 220.68 28.18 o 2 -3 1 2 214.94 222.11 23.52 o 2 3 1 -1 800.73 1026.67 22.80 o 2 -3 1 1 800.73 771.56 27.48 o 2 -3 -1 1 800.73 755.60 22.27 o 2 3 -1 -1 800.73 830.73 43.54 o 2 -3 -1 -1 2101.42 2171.60 14.28 o 2 3 2 -4 170.46 40.25 36.53 < 2 -3 2 3 683.59 583.53 40.72 o 2 -3 -2 3 683.59 546.20 75.31 o 2 3 2 -3 683.59 694.74 40.78 o 2 3 2 -2 230.04 153.93 24.74 o 2 -3 2 2 230.04 146.90 26.87 o 2 -3 -2 2 230.04 203.79 40.17 o 2 -3 -2 1 1038.34 1003.11 30.40 o 2 3 2 -1 1038.34 1010.00 24.38 o 2 -3 -2 -1 2804.49 2061.33 29.32 o 2 3 2 1 2804.49 2438.90 15.83 o 2 3 3 -3 12.28 19.80 27.24 < 2 -3 3 3 12.28 12.20 21.07 < 2 3 3 -2 14.57 24.29 25.48 < 2 -3 -3 2 14.57 0.67 40.00 < 2 -3 -3 1 1906.59 1614.37 53.53 o 2 3 3 -1 1906.59 1914.14 32.89 o 2 3 3 1 0.87 9.30 10.15 < 2 3 4 -3 38.09 48.63 37.92 < 2 3 4 -2 874.07 770.84 38.70 o 2 4 0 -3 136.77 54.41 40.92 < 2 -4 0 3 136.77 99.42 33.63 < 2 4 0 -2 463.08 386.02 42.82 o 2 -4 0 2 463.08 385.20 30.12 o 2 4 0 -1 384.12 350.03 29.61 o 2 -4 0 1 384.12 430.39 21.74 o 2 4 1 -3 0.49 19.47 30.46 < 2 -4 -1 3 0.49 24.76 41.33 < 2 4 -1 -3 0.49 11.05 36.55 < 2 -4 1 3 0.49 8.64 26.97 < 2 4 1 -2 2637.20 2555.98 55.39 o 2 4 -1 -2 2637.20 2436.62 69.82 o 2 -4 1 2 2637.20 2646.92 48.91 o 2 -4 -1 2 2637.20 2478.24 51.71 o 2 4 1 -1 212.35 193.88 24.11 o 2 -4 -1 1 212.35 202.56 23.05 o 2 -4 1 1 212.35 188.99 28.58 o 2 4 -1 -1 212.35 153.91 40.68 o 2 -4 -1 -1 65.01 35.39 11.24 o 2 -4 2 3 124.03 62.97 34.12 < 2 -4 -2 3 124.03 109.04 63.19 < 2 4 2 -3 124.03 75.17 32.28 < 2 4 2 -2 244.43 174.18 25.99 o 2 -4 -2 2 244.43 188.91 49.36 o 2 -4 2 2 244.43 144.55 34.90 o 2 4 2 -1 2335.33 2795.62 37.21 o 2 -4 -2 1 2335.33 2557.35 35.94 o 2 -4 -2 -1 885.69 739.11 18.74 o 2 4 2 1 885.69 729.39 23.21 o 2 -4 -3 3 1447.07 1321.03 111.48 o 2 4 3 -3 1447.07 1588.72 54.51 o 2 -4 3 3 1447.06 1599.43 54.43 o 2 4 3 -2 10.72 30.18 30.89 < 2 -4 -3 2 10.72 41.76 51.71 < 2 -4 -3 1 1901.92 1724.23 43.03 o 2 4 3 -1 1901.92 1712.95 36.14 o 2 4 3 1 4515.38 5294.92 27.71 o 2 4 4 -3 42.71 27.24 34.82 < 2 -4 -4 2 383.98 231.65 66.65 o 2 4 4 -2 383.98 377.11 38.19 o 2 -4 -4 1 4751.14 4832.45 90.86 o 2 4 4 -1 4751.14 4750.64 50.43 o 2 4 4 1 1304.23 1267.05 24.50 o 2 4 5 2 56.57 33.67 10.32 o 2 -5 1 3 327.30 185.13 42.07 o 2 5 -1 -3 327.30 146.47 71.88 < 2 -5 -1 3 327.30 5.13 27.95 < 2 5 1 -3 327.30 243.20 46.87 o 2 -5 1 2 376.18 348.44 40.80 o 2 5 1 -2 376.18 343.41 45.46 o 2 -5 -1 2 376.18 327.64 40.15 o 2 5 -1 -2 376.18 152.36 51.83 < 2 -5 -1 1 34.39 13.16 19.63 < 2 5 1 -1 34.39 12.95 18.45 < 2 -5 -1 -1 1800.18 1783.87 28.46 o 2 -5 -1 -2 177.10 179.57 11.89 o 2 5 2 -3 0.84 39.00 43.19 < 2 -5 2 3 0.84 30.53 35.04 < 2 -5 -2 2 4.75 9.07 26.75 < 2 5 2 -2 4.75 13.71 26.11 < 2 5 2 -1 3648.87 3824.25 49.93 o 2 -5 -2 1 3648.87 4180.70 50.18 o 2 5 2 1 0.28 15.57 22.97 < 2 -5 -2 -1 0.28 12.59 13.55 < 2 5 3 -2 408.73 343.44 41.93 o 2 -5 -3 2 408.73 273.83 59.09 o 2 5 3 -1 382.58 345.15 32.04 o 2 -5 -3 1 382.58 334.49 42.68 o 2 -5 -3 -1 2226.20 2377.98 45.09 o 2 5 3 1 2226.20 2361.75 27.03 o 2 -5 -4 3 549.82 5.46 21.02 < 2 5 4 -2 1306.22 1218.60 58.54 o 2 -5 -4 2 1306.22 1086.17 103.08 o 2 -5 -4 1 92.53 73.19 48.36 < 2 5 4 -1 92.53 56.74 26.13 < 2 5 4 1 1475.16 1791.45 30.63 o 2 -5 -5 2 436.11 176.35 89.37 < 2 5 5 -2 436.11 383.87 47.50 o 2 -5 -5 1 1289.83 1002.30 70.78 o 2 5 5 -1 1289.83 1226.65 42.46 o 2 5 5 1 73.60 55.92 19.94 < 2 5 5 2 401.19 396.56 19.51 o 2 5 6 2 1352.81 1456.22 31.06 o 2 -6 0 2 309.52 261.36 44.97 o 2 6 0 -2 309.52 145.62 40.41 o 2 6 0 -1 1395.80 1615.63 67.22 o 2 -6 0 1 1395.80 1316.64 46.28 o 2 -6 -1 3 504.05 6.29 12.69 < 2 6 -1 -2 138.76 61.17 60.03 < 2 6 1 -2 138.76 39.60 34.79 < 2 -6 1 2 138.76 104.41 36.25 < 2 -6 -1 2 138.76 36.31 33.18 < 2 -6 -1 1 728.82 780.33 42.17 o 2 6 1 -1 728.82 541.89 46.69 o 2 -6 -1 -1 1232.42 1329.59 33.90 o 2 -6 -1 -2 92.07 82.50 13.85 o 2 -6 -2 3 199.94 10.87 18.08 < 2 6 2 -2 123.97 74.11 40.01 < 2 -6 -2 2 123.97 73.76 33.32 < 2 6 2 -1 224.55 155.79 32.12 o 2 -6 -2 1 224.55 187.93 36.55 o 2 -6 -2 -1 235.94 217.27 26.87 o 2 -6 -2 -2 0.90 16.80 15.90 < 2 -6 -3 2 3003.94 3154.97 100.97 o 2 6 3 -2 3003.94 3310.42 70.57 o 2 6 3 -1 26.44 17.76 22.41 < 2 -6 -3 1 26.44 7.99 24.33 < 2 6 3 1 126.87 70.98 25.09 < 2 -6 -3 -1 126.87 61.70 22.37 < 2 6 4 -2 421.87 367.63 51.06 o 2 6 4 -1 197.44 149.87 32.59 o 2 -6 -4 1 197.44 117.48 40.66 < 2 6 4 1 1.21 8.27 18.61 < 2 -6 -4 -1 1.21 24.68 37.57 < 2 -6 -5 1 93.99 52.65 72.66 < 2 6 5 -1 93.99 57.94 33.86 < 2 6 5 1 51.35 40.72 22.43 < 2 6 5 2 191.77 88.57 19.41 o 2 6 6 -1 199.09 174.55 37.43 o 2 6 6 1 15.00 19.90 22.41 < 2 6 6 2 338.85 283.55 26.95 o 2 6 7 2 241.49 220.40 25.07 o 2 7 -1 -2 223.73 78.64 74.13 < 2 7 1 -2 223.73 82.18 51.22 < 2 -7 -1 1 3.45 13.96 27.68 < 2 7 1 -1 3.45 17.43 31.12 < 2 -7 -1 -1 43.15 33.83 21.29 < 2 -7 -1 -2 231.34 292.85 25.89 o 2 7 2 -2 1724.44 11.69 29.79 < 2 7 2 -1 279.19 138.38 31.75 o 2 -7 -2 1 279.19 154.46 42.40 o 2 -7 -2 -1 8.99 5.95 19.80 < 2 -7 -2 -2 1101.17 1210.64 34.10 o 2 7 3 -1 123.22 37.94 34.88 < 2 -7 -3 1 123.22 50.57 33.51 < 2 7 3 1 6.32 20.10 30.06 < 2 -7 -3 -1 6.32 9.58 18.76 < 2 -7 -4 2 139.80 7.21 19.12 < 2 -7 -4 1 1170.03 1236.63 72.12 o 2 7 4 -1 1170.03 1324.44 51.14 o 2 -7 -4 -1 180.99 62.99 35.49 < 2 7 4 1 180.99 64.65 24.97 < 2 7 5 -1 681.09 593.78 49.65 o 2 -7 -5 1 681.09 544.36 80.62 o 2 7 5 1 1686.09 1975.31 49.49 o 2 7 6 -1 1075.04 993.59 64.63 o 2 7 6 1 564.89 794.03 42.72 o 2 7 6 2 34.17 17.55 22.60 < 2 7 7 1 495.67 451.29 42.85 o 2 7 8 2 437.31 9.56 7.38 < 2 -8 0 2 301.33 3.80 11.89 < 2 8 0 -1 8.72 31.89 60.70 < 2 -8 0 1 8.72 17.35 31.12 < 2 -8 -1 1 452.81 364.95 44.09 o 2 8 1 -1 452.81 289.31 58.74 o 2 -8 -1 -1 2.50 19.06 25.78 < 2 -8 -1 -2 1150.30 1895.77 47.77 o 2 -8 -2 1 404.93 291.15 47.03 o 2 8 2 -1 404.93 239.27 56.43 o 2 -8 -2 -1 323.97 327.09 36.76 o 2 -8 -2 -2 1.31 11.60 19.47 < 2 8 3 -1 230.27 130.17 45.15 < 2 -8 -3 1 230.27 10.34 22.33 < 2 8 3 1 1054.35 1070.84 80.62 o 2 -8 -3 -1 1054.35 1231.39 44.34 o 2 -8 -3 -2 6.54 36.57 35.02 < 2 8 4 -1 1236.17 1051.04 64.56 o 2 -8 -4 -1 290.34 212.18 52.41 o 2 8 4 1 290.34 184.78 44.21 o 2 -8 -5 -1 7.19 14.04 53.67 < 2 8 5 1 7.19 18.69 23.70 < 2 -8 -6 1 127.28 9.97 31.53 < 2 8 6 1 122.54 32.65 27.77 < 2 8 7 1 527.77 680.80 44.91 o 2 8 8 1 51.48 29.58 30.83 < 2 -9 -1 -1 392.59 406.92 37.76 o 2 -9 -2 -1 192.70 104.94 35.14 < 2 -9 -3 1 218.93 5.33 13.10 < 2 -9 -3 -1 387.47 346.40 40.17 o 2 -9 -4 1 3.86 1.00 10.85 < 2 9 4 1 4.13 39.78 42.82 < 2 -9 -4 -1 4.13 27.54 40.60 < 2 9 5 1 51.88 36.10 36.27 < 2 -9 -5 -1 51.88 22.64 49.67 < 2 9 6 1 166.36 90.43 38.88 < 2 9 7 1 135.22 105.47 41.11 < 2 9 8 1 214.61 252.70 43.56 o 2 -10 -2 -1 192.89 103.45 39.58 < 2 -10 -3 -1 79.99 32.32 31.08 < 2 -10 -4 -1 183.72 110.70 51.41 < 2 10 4 1 183.72 72.27 65.93 < 2 -10 -5 -1 5.20 58.80 54.68 < 2 10 5 1 5.20 25.36 37.27 < 2 10 6 1 2.28 30.05 42.05 < 2 -10 -6 -1 2.28 43.58 66.73 < 2