#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180910 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105136.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105136_Fobs loop_ _publ_author_name 'Merlini, Marco' 'Perchiazzi, Natale' 'Hanfland, Michael' 'Bossak, Alexei' _publ_section_title ; Phase transition at high pressure in Cu~2~CO~3~(OH)~2~ related to the reduction of the Jahn--Teller effect ; _journal_coeditor_code PS5017 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 266 _journal_page_last 274 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cod_data_source_file ps5017malachite_p5sup7.hkl _cod_data_source_block malachite_p5 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status _jana_refln_twin_domain 0 0 -1 514.46 489.63 10.99 o 1 0 0 1 514.46 494.56 11.91 o 1 0 0 -2 159.49 150.06 19.65 o 1 0 0 2 159.49 132.46 16.14 o 1 0 0 3 0.18 20.95 21.56 < 1 0 0 -3 0.18 22.10 25.00 < 1 0 -1 1 252.29 286.38 11.14 o 1 0 1 -1 252.29 263.10 8.66 o 1 0 -1 -1 252.28 257.22 9.88 o 1 0 1 1 252.28 287.56 12.90 o 1 0 1 2 11635.99 10081.98 43.58 o 1 0 1 -2 11635.99 9390.01 39.00 o 1 0 -1 -2 11635.99 9944.06 47.63 o 1 0 -1 2 11635.99 9998.25 41.86 o 1 0 1 3 20.75 11.07 27.67 < 1 0 1 -3 20.75 17.02 23.55 < 1 0 -1 -3 20.75 16.22 23.74 < 1 0 -1 3 20.75 10.27 18.59 < 1 0 -2 2 761.62 38.62 16.22 < 1 0 -2 -2 761.62 33.32 20.61 < 1 0 -2 -3 895.45 868.94 37.51 o 1 0 -2 3 895.46 952.67 35.42 o 1 0 -3 -3 348.12 376.67 29.35 o 1 0 -3 3 348.12 418.31 32.44 o 1 1 -1 -3 552.01 508.22 25.91 o 1 1 1 -3 552.01 557.30 27.63 o 1 -1 -1 3 552.01 549.78 25.68 o 1 1 -1 1 2078.34 2088.97 20.57 o 1 -1 1 -1 2078.34 1979.71 19.39 o 1 1 1 1 2078.34 2102.06 21.98 o 1 -1 -1 -1 2078.34 1967.69 21.33 o 1 -1 -1 -2 2689.23 2834.30 35.68 o 1 -1 1 -2 2689.23 2685.96 30.53 o 1 1 -1 2 2689.23 2894.56 35.84 o 1 1 1 2 2689.23 2807.74 35.19 o 1 1 -1 3 20.12 14.88 26.18 < 1 -1 -1 -3 20.12 22.59 30.95 < 1 1 1 3 20.12 25.53 23.85 < 1 -1 1 -3 20.12 18.59 25.61 < 1 1 -2 -3 32.69 76.33 27.06 < 1 -1 -2 3 32.69 78.73 19.39 o 1 1 -2 -2 755.67 834.06 23.01 o 1 -1 -2 2 755.66 776.20 19.27 o 1 1 2 1 27.68 44.61 12.21 o 1 -1 -2 -1 27.68 43.51 14.01 o 1 1 -2 2 247.75 227.83 22.63 o 1 -1 -2 -2 247.75 210.09 21.87 o 1 1 2 2 247.75 207.30 21.18 o 1 -1 -2 -3 490.40 700.45 33.05 o 1 1 -2 3 490.40 709.87 36.33 o 1 1 2 3 490.40 795.47 40.83 o 1 -1 -3 3 125.67 172.69 24.31 o 1 1 -3 -3 125.67 166.39 27.86 o 1 -1 -3 2 83.82 7.40 11.03 < 1 1 -3 3 91.03 65.14 29.31 < 1 -1 -3 -3 91.03 99.99 33.20 o 1 -1 -4 3 380.80 362.70 26.52 o 1 -1 -4 -3 61.61 53.01 36.94 < 1 2 0 -3 3168.45 3346.41 37.90 o 1 2 0 -2 672.61 573.63 15.23 o 1 -2 0 0 825.68 791.89 11.11 o 1 2 0 0 825.68 662.44 9.46 o 1 2 0 1 6520.19 7319.35 36.60 o 1 -2 0 -1 6520.19 7388.81 36.64 o 1 2 0 2 184.24 144.37 21.87 o 1 -2 0 -2 184.24 132.85 21.45 o 1 2 0 3 2217.14 3214.18 59.88 o 1 -2 0 -3 2217.14 2414.77 44.84 o 1 2 -1 -3 1364.72 1305.29 29.77 o 1 2 1 -3 1364.72 1375.21 27.10 o 1 2 1 0 51.36 60.60 6.87 o 1 -2 -1 0 51.36 65.68 7.48 o 1 2 -1 1 4894.77 5150.80 32.10 o 1 -2 1 -1 4894.77 5282.01 34.35 o 1 -2 -1 -1 4894.76 5225.80 34.19 o 1 2 1 1 4894.76 5287.12 36.22 o 1 -2 -1 -2 868.37 571.34 31.41 o 1 2 1 2 868.37 658.73 36.90 o 1 -2 1 -2 868.37 557.98 28.43 o 1 2 -1 2 868.37 619.31 33.70 o 1 2 -1 3 727.95 857.03 44.38 o 1 -2 -1 -3 727.95 883.55 44.15 o 1 -2 1 -3 727.95 867.87 40.57 o 1 2 1 3 727.95 843.02 38.54 o 1 2 -2 -3 673.41 637.32 31.29 o 1 -2 -2 3 673.41 626.79 22.17 o 1 -2 -2 2 250.76 9.88 9.16 < 1 2 2 0 12186.77 9593.15 31.64 o 1 -2 -2 0 12186.77 9712.71 28.01 o 1 2 2 1 2967.10 3595.85 33.09 o 1 -2 -2 -1 2967.10 3954.43 36.60 o 1 2 2 2 374.05 229.32 29.12 o 1 -2 -2 -2 374.05 172.42 23.47 o 1 2 -2 2 374.05 295.34 32.13 o 1 2 2 3 13.82 31.48 27.90 < 1 -2 -2 -3 13.82 40.49 34.73 < 1 2 -2 3 13.82 17.97 28.66 < 1 -2 -3 3 112.65 191.24 24.23 o 1 -2 -3 2 4563.18 4729.56 28.05 o 1 2 3 1 506.81 689.11 26.94 o 1 -2 -3 -1 506.81 653.62 21.22 o 1 -2 -3 -2 4520.55 5227.55 50.53 o 1 2 3 2 4520.55 5130.85 55.15 o 1 2 3 3 19.46 3.55 30.80 < 1 -2 -3 -3 19.46 23.13 32.90 < 1 2 -3 3 19.46 16.03 28.13 < 1 -2 -4 3 45.49 14.27 17.86 < 1 -2 -4 -3 85.35 17.82 32.25 < 1 3 -1 -3 236.55 215.97 22.63 o 1 3 1 0 2730.86 2344.40 19.27 o 1 -3 -1 0 2730.86 2582.00 21.33 o 1 3 -1 1 3272.45 3796.62 32.78 o 1 -3 -1 -1 3272.45 3856.69 36.87 o 1 3 1 1 3272.45 3401.14 31.75 o 1 -3 1 -1 3272.45 3743.77 33.32 o 1 3 -1 3 70.46 9.66 28.47 < 1 -3 1 -3 70.46 129.75 37.93 o 1 -3 -1 -3 70.46 115.18 32.21 o 1 3 -2 -3 1071.45 1260.19 36.48 o 1 -3 -2 0 3312.07 2612.69 20.26 o 1 3 2 0 3312.07 2788.16 21.98 o 1 -3 -2 -1 3853.36 4293.32 43.32 o 1 3 2 1 3853.36 4809.40 40.49 o 1 3 -2 2 1528.70 1578.58 44.38 o 1 3 2 2 1528.70 1189.28 34.16 o 1 -3 -2 -2 1528.70 1357.16 46.25 o 1 3 -2 3 839.28 12.90 33.35 < 1 3 3 0 3836.59 3382.21 30.19 o 1 -3 -3 0 3836.59 3306.23 25.57 o 1 3 3 1 14.98 17.78 21.18 < 1 -3 -3 -1 14.98 1.79 15.46 < 1 3 3 2 221.79 272.22 32.32 o 1 -3 -3 -2 221.79 228.90 29.81 o 1 -3 -4 3 5.73 18.24 13.74 < 1 3 4 1 277.57 295.42 30.26 o 1 -3 -4 -1 277.57 237.76 22.17 o 1 3 4 2 2297.52 2207.20 62.28 o 1 -3 -4 -2 2297.52 2312.15 58.81 o 1 3 4 3 368.89 3.55 15.53 < 1 -3 -5 3 1885.80 1985.82 26.33 o 1 -3 -5 -2 1100.01 1260.03 53.08 o 1 4 0 -3 141.36 104.87 13.43 o 1 4 0 1 918.11 893.93 29.31 o 1 4 0 2 84.44 93.39 26.07 o 1 -4 0 -2 84.44 97.66 24.50 o 1 4 0 3 17.35 6.72 12.40 < 1 4 -1 -3 93.21 43.89 15.49 < 1 4 1 -1 468.62 449.83 11.79 o 1 4 1 0 331.81 311.72 13.62 o 1 -4 -1 0 331.81 287.25 15.80 o 1 4 1 1 65.57 68.62 21.64 o 1 -4 -1 -1 65.57 86.78 25.15 o 1 4 1 2 2227.15 2156.33 48.54 o 1 -4 1 -2 2227.15 2142.98 47.09 o 1 -4 -1 -2 2227.15 2130.57 49.31 o 1 4 -1 2 2227.15 2241.74 51.83 o 1 4 -1 3 98.04 5.99 12.29 < 1 4 2 -1 2353.84 2208.31 17.71 o 1 -4 -2 1 2353.84 2131.60 16.83 o 1 4 2 0 3203.57 3284.86 30.49 o 1 -4 -2 0 3203.57 2933.72 28.28 o 1 4 2 1 1240.76 1608.39 38.77 o 1 -4 -2 -1 1240.76 1445.16 32.67 o 1 -4 -2 -2 160.98 130.82 30.87 o 1 4 2 2 160.98 119.60 32.86 o 1 4 -2 3 701.36 2.10 13.28 < 1 -4 -3 1 4349.16 3841.01 24.77 o 1 -4 -3 0 1083.81 1150.66 21.71 o 1 4 3 0 1083.81 1209.20 23.20 o 1 -4 -3 -1 6792.01 7721.48 57.02 o 1 4 3 1 6792.01 7979.84 57.02 o 1 4 3 2 251.12 76.67 34.54 < 1 -4 -3 -2 251.12 32.29 30.15 < 1 -4 -4 1 6051.77 6727.25 35.38 o 1 4 4 0 60.09 19.35 18.32 < 1 -4 -4 0 60.09 22.29 15.23 < 1 4 4 1 1557.91 1505.61 35.42 o 1 -4 -4 -1 1557.91 1701.12 40.87 o 1 -4 -4 -2 1713.98 1068.61 48.20 o 1 4 5 1 547.17 638.16 39.73 o 1 -4 -5 -1 547.17 547.41 37.13 o 1 -4 -5 -2 1338.06 516.65 52.05 o 1 5 -1 -3 396.76 478.95 20.80 o 1 5 1 -1 0.96 3.89 8.82 < 1 -5 -1 0 674.66 461.47 16.98 o 1 5 1 0 674.66 672.51 23.13 o 1 -5 -1 -1 2606.50 3265.05 40.07 o 1 5 1 1 2606.50 3081.56 43.66 o 1 -5 1 -2 325.39 339.96 42.21 o 1 5 1 2 325.39 323.13 42.06 o 1 -5 -1 -2 325.39 289.85 35.57 o 1 5 -1 2 325.39 309.58 42.21 o 1 -5 -2 1 6115.38 6906.16 36.18 o 1 5 2 -1 6115.38 7301.60 40.53 o 1 5 2 0 5873.78 6348.75 47.67 o 1 -5 -2 0 5873.78 5990.62 44.00 o 1 5 2 1 12.18 13.70 24.65 < 1 -5 -2 -1 12.18 13.93 23.62 < 1 5 2 2 92.41 9.04 30.11 < 1 -5 -2 -2 92.41 71.48 41.67 < 1 -5 -3 1 191.59 133.30 16.03 o 1 5 3 -1 191.59 143.84 17.59 o 1 -5 -3 0 1350.25 1549.12 29.58 o 1 5 3 0 1350.25 1398.79 29.00 o 1 -5 -3 -1 3456.04 4548.59 54.57 o 1 5 3 1 3456.04 4418.91 51.90 o 1 -5 -4 1 265.71 253.48 16.79 o 1 -5 -4 0 1175.77 1403.07 31.06 o 1 5 4 0 1175.77 1160.73 29.54 o 1 -5 -4 -1 2118.13 2157.78 50.72 o 1 5 4 1 2118.13 2565.94 54.61 o 1 -5 -5 2 1338.23 1138.33 15.84 o 1 -5 -5 1 1619.38 1424.10 28.51 o 1 -5 -5 0 11255.18 12774.47 72.74 o 1 5 5 1 111.90 122.12 31.48 o 1 -5 -5 -1 111.90 116.28 37.67 o 1 -5 -6 -1 249.40 401.17 45.49 o 1 6 0 0 429.65 577.71 32.25 o 1 6 0 1 1223.94 1427.34 44.50 o 1 -6 0 -1 1223.94 1559.04 47.59 o 1 6 1 -1 1372.04 1364.18 27.94 o 1 -6 -1 0 873.13 746.24 24.96 o 1 6 1 0 873.13 807.15 28.24 o 1 -6 -1 -1 1787.77 1891.33 41.56 o 1 6 1 1 1787.77 1940.79 45.68 o 1 6 2 -1 179.88 128.57 18.85 o 1 6 2 0 4609.24 4942.62 43.09 o 1 -6 -2 0 4609.24 4747.99 42.55 o 1 6 2 1 369.43 472.50 41.79 o 1 -6 -2 -1 369.43 449.14 38.39 o 1 6 2 2 2075.54 1.11 10.84 < 1 -6 -3 1 29.86 20.19 15.46 < 1 6 3 -1 29.86 7.44 15.53 < 1 -6 -3 0 752.16 594.09 31.29 o 1 6 3 0 752.16 729.76 42.59 o 1 -6 -3 -1 222.11 242.03 37.59 o 1 6 3 1 222.11 243.94 42.21 o 1 -6 -4 1 242.68 287.29 22.17 o 1 6 4 0 9603.01 9759.31 66.14 o 1 -6 -4 0 9603.01 10531.89 65.34 o 1 6 4 1 0.19 15.53 24.81 < 1 -6 -4 -1 0.19 21.79 27.55 < 1 -6 -5 2 599.98 273.02 14.62 o 1 -6 -5 1 119.91 73.73 19.77 o 1 -6 -5 0 772.70 967.93 46.94 o 1 6 5 0 772.70 788.91 48.77 o 1 -6 -5 -1 206.83 98.88 34.23 < 1 6 5 1 206.83 124.14 29.31 o 1 -6 -6 1 311.78 337.74 33.09 o 1 -6 -6 0 26.57 29.08 27.40 < 1 -6 -6 -1 12.06 22.25 41.22 < 1 6 6 1 12.06 7.71 31.64 < 1 7 1 -2 766.68 569.97 17.17 o 1 7 1 -1 1.64 13.97 17.48 < 1 -7 -1 0 2937.64 2923.68 48.51 o 1 7 1 0 2937.64 3068.89 50.60 o 1 7 1 1 58.17 90.98 37.09 < 1 -7 -1 -1 58.17 83.31 26.07 o 1 7 2 -1 408.13 339.19 24.50 o 1 7 2 0 3826.03 4721.66 54.00 o 1 -7 -2 0 3826.03 2861.24 34.80 o 1 7 2 1 0.20 12.67 27.63 < 1 -7 -2 -1 0.20 8.32 24.69 < 1 7 3 -1 48.74 14.04 16.94 < 1 -7 -3 1 48.74 5.99 7.40 < 1 -7 -3 0 5555.92 5546.29 58.92 o 1 7 3 0 5555.92 5989.86 62.09 o 1 -7 -3 -1 24.73 28.28 35.38 < 1 7 3 1 24.73 52.89 40.30 < 1 7 4 -1 2239.36 2326.08 41.03 o 1 -7 -4 1 2239.36 2604.10 44.38 o 1 -7 -4 0 355.55 200.32 36.48 o 1 7 4 0 355.55 212.57 33.13 o 1 -7 -4 -1 274.82 256.99 42.70 o 1 -7 -5 1 394.59 269.05 27.06 o 1 7 5 0 11.39 5.61 21.18 < 1 -7 -5 0 11.39 23.05 29.92 < 1 -7 -6 2 602.94 163.41 18.81 o 1 -7 -6 1 2220.44 2270.02 42.17 o 1 -7 -6 0 128.04 69.53 32.82 < 1 7 6 0 128.04 66.37 36.64 < 1 -7 -7 2 398.04 234.63 23.24 o 1 -7 -7 1 691.18 621.72 40.91 o 1 -7 -7 0 386.31 541.34 45.99 o 1 8 1 -2 1976.13 1541.52 28.28 o 1 8 1 -1 624.79 700.26 32.67 o 1 8 1 0 515.10 403.96 41.22 o 1 8 2 -1 266.97 178.95 26.64 o 1 -8 -2 0 1073.12 1006.29 46.33 o 1 8 2 0 1073.12 1099.63 43.16 o 1 -8 -3 1 517.89 560.12 33.89 o 1 8 3 -1 517.89 544.09 30.61 o 1 -8 -3 0 1365.02 1120.01 45.68 o 1 8 3 0 1365.02 1504.51 53.85 o 1 -8 -4 1 891.09 790.40 37.29 o 1 8 4 -1 891.09 830.47 36.37 o 1 -8 -4 0 252.24 197.99 40.11 o 1 8 4 0 252.24 155.63 39.19 o 1 8 4 1 393.59 3.93 11.33 < 1 8 5 -1 986.77 836.96 44.38 o 1 -8 -5 1 986.77 801.35 43.70 o 1 -8 -5 0 34.04 15.27 28.74 < 1 8 5 0 34.04 17.78 30.34 < 1 -8 -6 1 348.62 347.36 34.61 o 1 8 6 0 654.27 499.06 60.45 o 1 -8 -6 0 654.27 739.98 62.82 o 1 -8 -7 1 3.53 21.87 28.51 < 1 -8 -7 0 648.84 824.40 61.60 o 1 -8 -8 1 580.07 490.74 49.65 o 1 9 1 -2 1602.27 2167.71 38.09 o 1 9 1 -1 33.16 34.84 28.51 < 1 9 1 0 86.08 66.48 35.57 < 1 9 2 -2 170.93 74.65 20.76 o 1 9 2 -1 1760.09 1623.04 46.25 o 1 -9 -2 0 18.33 43.01 33.05 < 1 9 2 0 18.33 24.92 26.03 < 1 9 3 -1 213.74 130.59 34.88 o 1 -9 -3 0 16.71 10.80 13.01 < 1 9 3 0 16.71 5.80 26.98 < 1 -9 -4 1 10.58 23.58 21.07 < 1 9 4 -1 10.58 21.56 25.19 < 1 9 4 0 636.75 635.91 52.28 o 1 -9 -4 0 636.75 628.85 54.34 o 1 -9 -5 1 13.40 9.54 22.48 < 1 9 5 -1 13.40 21.91 29.08 < 1 -9 -5 0 3894.40 5173.05 88.00 o 1 -9 -6 1 5.70 20.65 26.71 < 1 -9 -6 0 438.05 16.18 31.56 < 1 -9 -7 1 24.85 22.17 26.14 < 1 -9 -8 1 1209.13 1345.02 60.49 o 1 10 1 -1 478.08 565.35 49.69 o 1 10 2 -1 34.47 18.51 26.83 < 1 10 3 -1 571.23 580.73 51.52 o 1 10 4 -1 408.84 242.91 37.55 o 1 -10 -4 1 408.84 264.36 36.29 o 1 10 5 -1 7.86 10.76 22.36 < 1 -10 -5 1 7.86 3.24 11.22 < 1 10 5 0 6.63 4.31 13.70 < 1 -10 -6 1 304.09 272.90 44.35 o 1 10 6 -1 304.09 364.80 51.14 o 1 -10 -7 1 19.35 33.24 33.81 < 1 11 2 -1 137.53 77.13 33.01 < 1 11 3 -1 5.22 22.97 31.29 < 1 11 4 -1 498.06 689.34 57.86 o 1 0 0 1 519.14 517.21 12.91 o 2 0 0 -1 519.14 546.95 11.47 o 2 0 0 2 160.94 96.84 27.99 o 2 0 0 -2 160.94 131.06 19.59 o 2 0 0 -3 0.18 13.08 21.60 < 2 0 1 -1 254.58 275.55 16.18 o 2 0 1 1 254.58 293.08 10.29 o 2 0 1 2 11713.05 10714.19 49.34 o 2 0 -1 -2 11713.05 10553.47 49.93 o 2 0 1 -2 11713.05 10950.75 47.73 o 2 0 -1 -3 20.94 24.16 22.16 < 2 0 1 3 20.94 30.42 32.79 < 2 0 1 -3 20.94 23.34 31.07 < 2 0 2 -2 754.81 29.57 26.02 < 2 0 2 2 754.81 8.88 12.63 < 2 0 2 3 903.60 964.45 37.78 o 2 0 2 -3 903.60 943.75 40.40 o 2 0 3 2 83.74 106.65 21.96 o 2 0 3 3 351.29 443.15 30.02 o 2 0 4 3 1030.30 1209.57 34.45 o 2 -1 1 3 557.03 502.97 37.33 o 2 1 -1 -3 557.03 433.87 34.31 o 2 1 1 -3 557.03 479.60 39.05 o 2 1 -1 -1 38.72 51.31 12.26 o 2 -1 -1 1 38.72 49.50 11.78 o 2 1 1 -1 38.72 53.37 12.46 o 2 -1 1 1 38.72 47.45 11.87 o 2 -1 1 -2 2713.22 2761.23 36.73 o 2 -1 -1 -2 2713.22 2610.18 25.32 o 2 -1 -1 -3 20.31 20.30 18.94 < 2 -1 1 -3 20.31 22.72 22.02 < 2 1 2 -3 32.98 66.19 25.91 < 2 -1 2 3 32.98 62.47 26.87 < 2 -1 2 2 762.48 782.38 32.42 o 2 1 2 -2 762.48 846.94 31.86 o 2 1 2 -1 618.54 440.75 19.71 o 2 1 2 2 249.88 189.20 11.05 o 2 -1 2 -3 494.86 667.11 36.25 o 2 -1 3 3 126.82 205.29 31.41 o 2 1 3 -3 126.82 175.97 34.59 o 2 1 3 3 91.86 66.67 19.73 o 2 -1 4 3 384.26 347.49 42.49 o 2 1 4 3 62.17 25.88 14.52 < 2 1 5 3 1111.70 1516.22 42.23 o 2 2 0 -3 3197.27 2919.19 62.50 o 2 -2 0 3 3197.27 3330.20 60.95 o 2 2 0 -2 678.73 703.05 34.85 o 2 -2 0 2 678.73 727.80 30.22 o 2 -2 0 1 19140.44 22240.88 60.22 o 2 2 0 -1 19140.44 22206.54 63.18 o 2 -2 0 -2 185.92 154.46 12.38 o 2 -2 0 -3 2237.30 2825.05 36.48 o 2 2 -1 -3 1377.13 1200.02 45.56 o 2 2 1 -3 1377.13 1276.45 53.51 o 2 -2 -1 3 1377.13 1142.98 64.28 o 2 -2 1 3 1377.13 1300.55 52.69 o 2 -2 -1 2 2698.51 26.08 24.53 < 2 -2 1 1 10211.55 10496.98 51.22 o 2 -2 -1 1 10211.55 10700.46 45.45 o 2 2 1 -1 10211.55 10716.90 42.77 o 2 2 -1 -1 10211.55 10812.53 50.41 o 2 -2 1 -3 734.57 887.06 33.18 o 2 -2 2 3 679.53 636.38 38.23 o 2 2 2 -3 679.54 748.19 48.80 o 2 2 2 -2 248.62 65.72 27.85 < 2 -2 -2 2 248.62 9.64 29.74 < 2 -2 2 2 248.62 5.84 18.66 < 2 2 2 -1 34.77 6.40 14.83 < 2 -2 -2 1 34.77 16.44 16.35 < 2 2 3 -3 113.68 133.01 35.38 o 2 -2 3 3 113.68 159.59 32.48 o 2 2 3 -2 4598.66 4187.88 53.37 o 2 2 3 -1 166.31 219.84 22.02 o 2 2 5 3 1.35 7.39 8.51 < 2 3 1 -3 238.70 232.08 39.36 o 2 3 -1 -3 238.70 189.11 34.11 o 2 -3 -1 3 238.70 188.97 44.57 o 2 -3 1 3 238.70 233.06 39.50 o 2 3 1 -2 872.54 421.47 33.55 o 2 -3 1 2 872.54 970.84 47.42 o 2 3 -1 -2 872.54 882.91 41.61 o 2 -3 -1 2 872.54 409.63 33.97 o 2 -3 -1 1 1166.81 1486.45 30.56 o 2 3 -1 -1 1166.81 1420.53 34.31 o 2 3 1 -1 1166.81 1465.33 31.74 o 2 -3 1 1 1166.81 1336.13 32.48 o 2 -3 -1 -1 3302.21 3539.47 18.35 o 2 -3 1 -3 71.10 112.09 18.55 o 2 -3 2 3 1081.19 1182.90 53.48 o 2 -3 -2 3 1081.19 820.10 79.78 o 2 3 2 -3 1081.19 971.86 60.05 o 2 -3 2 2 375.82 251.67 33.75 o 2 -3 -2 2 375.82 133.01 29.26 o 2 3 2 -2 375.82 170.28 28.90 o 2 3 2 -1 898.54 976.46 29.38 o 2 -3 -2 1 898.54 851.09 31.97 o 2 3 2 1 3888.40 3221.86 24.25 o 2 3 3 -3 177.42 139.07 36.65 o 2 -3 3 3 177.42 116.60 35.80 o 2 -3 -3 2 4542.45 3995.86 76.88 o 2 -3 -3 1 2605.29 2445.68 42.96 o 2 3 3 -1 2605.29 2361.41 38.51 o 2 3 3 1 15.11 6.51 9.11 < 2 3 4 -3 5.78 38.20 41.33 < 2 3 4 -2 2138.99 1718.41 53.85 o 2 4 0 -3 142.65 61.57 49.93 < 2 -4 0 3 142.65 57.96 33.58 < 2 4 0 -2 59.91 23.40 31.80 < 2 -4 0 2 59.91 24.72 25.15 < 2 4 0 -1 804.40 811.67 37.72 o 2 -4 0 1 804.40 935.86 35.10 o 2 -4 1 3 94.06 48.83 34.76 < 2 -4 -1 3 94.06 33.72 39.24 < 2 4 1 -3 94.06 32.96 42.88 < 2 4 -1 -3 94.06 34.59 40.71 < 2 4 -1 -2 4013.80 3414.18 61.35 o 2 4 1 -2 4013.80 3575.13 65.04 o 2 -4 -1 2 4013.80 3739.06 59.40 o 2 4 -1 -1 472.88 484.76 34.56 o 2 -4 -1 1 472.88 577.74 27.43 o 2 4 1 -1 472.88 495.30 31.04 o 2 -4 1 1 472.88 527.67 33.75 o 2 -4 -1 -1 66.17 71.95 14.58 o 2 4 2 -3 407.77 480.25 54.58 o 2 -4 2 3 407.77 466.24 41.86 o 2 -4 -2 2 1539.16 631.39 48.66 o 2 4 2 -2 1539.16 785.26 60.08 o 2 4 2 -1 2375.24 3058.60 43.05 o 2 -4 -2 1 2375.24 2717.93 42.40 o 2 4 2 1 1252.04 1169.68 18.75 o 2 -4 -2 -1 1252.04 1267.20 19.76 o 2 4 3 -3 1526.68 1600.96 64.05 o 2 -4 3 3 1526.67 1941.63 78.94 o 2 4 3 -2 223.16 77.25 28.98 < 2 -4 -3 2 223.16 49.25 37.19 < 2 4 3 -1 4388.70 4846.95 55.65 o 2 -4 -3 1 4388.70 4871.70 56.41 o 2 4 3 1 6853.77 8304.74 37.97 o 2 4 4 -2 2313.66 1645.22 61.68 o 2 -4 -4 2 2313.66 668.09 80.66 o 2 -4 -4 1 6106.80 5213.76 81.28 o 2 4 4 -1 6106.80 6091.90 57.96 o 2 4 4 1 1572.08 1793.48 27.23 o 2 5 -1 -3 400.37 24.61 39.36 < 2 5 1 -2 2243.56 1494.26 57.79 o 2 -5 1 2 2243.56 1405.87 53.76 o 2 -5 -1 2 2243.56 2217.41 53.00 o 2 -5 -1 1 0.97 18.16 22.92 < 2 5 1 -1 0.97 15.08 21.91 < 2 -5 -1 -1 2630.20 3041.51 34.37 o 2 -5 -1 -2 326.18 255.76 10.52 o 2 5 2 -2 162.35 158.78 43.42 o 2 -5 -2 2 162.35 84.74 35.69 < 2 5 2 -1 6170.99 6223.79 65.66 o 2 -5 -2 1 6170.99 5982.89 53.28 o 2 5 2 1 12.29 19.76 16.77 < 2 -5 -2 -1 12.29 1.47 12.07 < 2 -5 -3 3 744.15 8.40 17.28 < 2 -5 -3 2 253.47 95.29 42.94 < 2 5 3 -2 253.47 95.06 36.42 < 2 5 3 -1 193.33 136.84 28.53 o 2 -5 -3 1 193.33 119.76 35.41 o 2 -5 -3 -1 3487.47 4242.21 40.03 o 2 5 3 1 3487.47 4586.77 38.28 o 2 5 4 -2 1728.11 1801.58 63.88 o 2 -5 -4 2 1728.11 1460.62 71.47 o 2 5 4 -1 268.12 273.83 36.23 o 2 -5 -4 1 268.12 290.94 45.19 o 2 5 4 1 2137.39 2604.00 32.87 o 2 5 5 -2 1348.03 1240.70 61.91 o 2 -5 -5 1 1634.11 1336.66 78.32 o 2 5 5 -1 1634.11 1749.34 57.65 o 2 5 5 1 112.91 88.41 17.45 o 2 5 5 2 594.91 461.33 19.62 o 2 5 6 2 2696.57 2854.37 33.15 o 2 -6 0 2 573.02 632.37 44.68 o 2 6 0 -2 573.02 552.17 52.94 o 2 -6 0 1 1278.98 1459.33 57.79 o 2 6 0 -1 1278.98 1451.97 57.68 o 2 -6 -1 2 328.76 140.73 43.92 o 2 6 1 -2 328.76 142.17 51.76 < 2 6 -1 -2 328.76 272.02 48.63 o 2 -6 1 2 328.76 398.63 52.92 o 2 -6 -1 1 1384.52 1596.82 48.46 o 2 6 1 -1 1384.52 1180.09 57.77 o 2 -6 -1 -1 1804.02 1999.26 40.68 o 2 -6 -1 -2 757.81 378.08 17.00 o 2 6 2 -2 93.13 32.22 38.23 < 2 -6 -2 2 93.13 16.97 31.15 < 2 -6 -2 1 181.51 117.31 27.97 o 2 6 2 -1 181.51 125.59 37.47 o 2 -6 -2 -1 372.79 404.81 28.47 o 2 6 3 -2 4608.40 3918.31 87.20 o 2 -6 -3 1 30.13 10.97 27.40 < 2 6 3 -1 30.13 19.54 32.48 < 2 6 3 1 224.13 166.30 24.87 o 2 -6 -3 -1 224.13 195.12 28.30 o 2 6 4 -1 244.89 327.70 39.07 o 2 -6 -4 1 244.89 297.31 45.92 o 2 6 4 1 0.19 12.77 20.13 < 2 -6 -4 -1 0.19 15.70 29.97 < 2 6 5 -1 121.00 91.43 42.32 < 2 -6 -5 1 121.00 39.33 50.07 < 2 6 5 1 208.71 127.46 25.03 o 2 -6 -6 1 314.61 165.68 63.66 < 2 6 6 -1 314.61 234.58 42.91 o 2 6 6 1 12.17 10.91 25.43 < 2 6 6 2 597.24 604.80 28.39 o 2 6 7 2 394.27 415.94 27.54 o 2 -7 -1 1 1.65 14.41 31.24 < 2 7 1 -1 1.65 33.58 37.97 < 2 -7 -1 -1 58.70 68.68 27.68 < 2 -7 -1 -2 1954.51 1259.98 27.26 o 2 -7 -2 1 411.85 329.37 48.32 o 2 7 2 -1 411.85 336.50 48.88 o 2 -7 -2 -1 0.20 28.05 24.98 < 2 -7 -2 -2 2241.05 2427.04 41.44 o 2 7 3 -1 49.19 22.86 36.48 < 2 -7 -3 1 49.19 18.80 36.28 < 2 -7 -3 -1 24.95 10.21 23.71 < 2 7 3 1 24.95 8.60 20.04 < 2 -7 -4 1 2259.72 2154.57 79.39 o 2 7 4 -1 2259.72 2715.42 89.48 o 2 7 4 1 277.32 185.14 36.93 o 2 -7 -4 -1 277.32 191.62 30.70 o 2 7 5 -1 398.18 277.32 47.98 o 2 -7 -5 1 398.18 19.76 33.24 < 2 7 5 1 2687.42 3673.89 57.54 o 2 7 6 -1 2240.63 34.37 39.55 < 2 7 6 1 788.83 1106.62 45.70 o 2 7 7 1 844.41 1158.74 49.42 o 2 8 0 -1 69.35 56.36 50.49 < 2 -8 0 1 69.35 0.51 5.05 < 2 8 1 -1 630.47 521.10 54.55 o 2 -8 -1 -1 9.90 14.04 28.95 < 2 -8 -1 -2 1582.93 2445.20 44.83 o 2 8 2 -1 269.40 119.11 59.15 < 2 -8 -2 -1 484.42 696.54 43.19 o 2 -8 -2 -2 169.53 82.43 25.26 o 2 8 3 -1 522.59 528.40 52.52 o 2 -8 -3 -1 1410.39 1494.59 48.46 o 2 -8 -3 -2 91.94 13.39 24.72 < 2 -8 -4 -1 397.17 344.14 40.88 o 2 8 4 1 397.17 297.51 41.16 o 2 -8 -5 -1 2.77 44.29 50.66 < 2 8 5 1 2.77 23.68 33.77 < 2 -8 -6 1 351.79 0.59 7.87 < 2 8 6 1 141.64 70.23 36.11 < 2 8 7 1 803.09 1390.76 68.56 o 2 8 8 1 72.40 78.35 36.20 < 2 -9 -1 1 33.46 7.19 13.14 < 2 -9 -1 -1 638.30 1003.18 57.54 o 2 -9 -2 1 1776.10 7.53 14.43 < 2 -9 -2 -1 351.16 291.96 41.55 o 2 -9 -3 -1 611.18 701.56 49.62 o 2 -9 -4 -1 0.21 24.05 34.39 < 2 9 4 1 0.21 17.00 30.98 < 2 -9 -5 -1 39.37 32.39 39.95 < 2 9 5 1 39.37 35.86 38.12 < 2 9 6 1 192.13 118.07 42.77 < 2 9 7 1 256.20 371.54 57.17 o 2 9 8 1 336.51 355.98 63.54 o 2 -10 -2 -1 340.14 438.50 52.52 o 2 -10 -3 -1 132.02 123.42 41.58 < 2 -10 -4 -1 352.57 308.36 55.43 o 2 10 5 1 8.64 33.27 35.75 < 2 -10 -5 -1 8.64 36.59 41.10 < 2 10 6 1 1.10 29.69 39.98 < 2