#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180910 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105141.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105141_Fobs loop_ _publ_author_name 'Merlini, Marco' 'Perchiazzi, Natale' 'Hanfland, Michael' 'Bossak, Alexei' _publ_section_title ; Phase transition at high pressure in Cu~2~CO~3~(OH)~2~ related to the reduction of the Jahn--Teller effect ; _journal_coeditor_code PS5017 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 266 _journal_page_last 274 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cod_data_source_file ps5017rosasite_p10sup12.hkl _cod_data_source_block rosasite_p10 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status _jana_refln_twin_domain 0 0 -1 591.28 529.13 13.27 o 1 0 0 1 591.28 529.06 12.01 o 1 0 0 2 33.07 36.02 17.73 < 1 0 0 -2 33.07 147.05 16.86 o 1 0 0 3 1638.62 1385.57 43.77 o 1 0 0 -3 1638.62 1097.52 39.61 o 1 0 0 -4 2934.35 4164.02 86.39 o 1 0 -1 1 274.50 291.36 11.85 o 1 0 -1 -1 274.50 298.70 13.41 o 1 0 1 -1 274.50 292.88 12.17 o 1 0 1 1 274.50 301.62 14.44 o 1 0 -1 2 12059.39 12640.28 59.53 o 1 0 1 2 12059.39 12667.08 61.74 o 1 0 -1 -2 12059.39 12653.46 62.56 o 1 0 1 -2 12059.39 12565.44 54.95 o 1 0 1 3 1914.94 1117.62 49.75 o 1 0 -1 -3 1914.94 1266.26 48.79 o 1 0 1 -3 1914.94 1121.07 43.43 o 1 0 -1 -4 14.59 24.17 38.55 < 1 0 -2 -2 91.65 93.80 25.76 o 1 0 -2 2 91.65 87.11 20.98 o 1 0 -2 3 1185.63 1014.90 40.90 o 1 0 -2 -3 1185.62 1116.98 48.28 o 1 0 -3 -3 822.97 858.60 51.52 o 1 0 -3 3 822.97 857.82 39.47 o 1 1 -1 -4 17.38 30.27 43.89 < 1 -1 -1 3 1134.85 1056.46 35.35 o 1 1 1 -3 1134.85 894.53 41.17 o 1 1 -1 -3 1134.85 1117.07 43.75 o 1 -1 -1 2 2074.41 2252.80 29.65 o 1 1 1 -2 2074.41 2224.67 29.35 o 1 1 -1 -2 2074.41 2149.68 34.82 o 1 1 1 1 2367.14 2142.14 24.38 o 1 1 -1 1 2367.14 2247.60 22.01 o 1 -1 1 -1 2367.14 2211.46 22.79 o 1 -1 -1 -1 2367.14 2190.46 25.26 o 1 -1 -1 -2 3128.90 3225.90 44.49 o 1 1 -1 2 3128.90 3246.51 42.46 o 1 -1 1 -2 3128.90 3336.01 43.36 o 1 1 1 2 3128.90 3299.46 45.04 o 1 -1 1 -3 421.78 326.00 43.59 o 1 1 -1 3 421.78 289.59 37.88 o 1 -1 -1 -3 421.78 333.38 40.14 o 1 1 1 3 421.78 234.48 40.94 o 1 1 -2 -4 230.94 299.73 46.03 o 1 -1 -2 3 24.11 42.16 25.69 < 1 1 -2 -3 24.11 25.21 23.51 < 1 -1 -2 2 728.31 661.41 22.77 o 1 1 -2 -2 728.32 718.57 28.13 o 1 1 2 1 33.11 27.37 16.31 < 1 -1 -2 -1 33.11 33.56 15.80 < 1 -1 -2 -2 533.02 455.20 28.77 o 1 1 -2 2 533.02 533.68 31.83 o 1 1 2 2 533.02 515.88 35.24 o 1 -1 -2 -3 1443.88 1461.01 52.44 o 1 1 2 3 1443.88 1152.82 56.88 o 1 1 -2 3 1443.88 1251.63 49.61 o 1 -1 -3 3 183.50 262.75 29.90 o 1 1 -3 -3 183.50 175.82 35.10 o 1 -1 -3 -2 280.50 337.34 30.41 o 1 -1 -3 -3 110.21 23.16 31.95 < 1 1 -3 3 110.21 62.20 32.46 < 1 -1 -4 3 617.00 490.67 31.79 o 1 -1 -4 -3 175.04 110.04 43.08 < 1 2 0 -3 2352.18 2608.31 44.78 o 1 2 0 -2 763.95 804.64 20.77 o 1 2 0 0 937.78 748.36 9.52 o 1 -2 0 0 937.78 807.19 10.95 o 1 -2 0 -1 8455.11 7646.02 38.83 o 1 2 0 1 8455.11 7681.51 39.88 o 1 2 0 2 229.25 157.88 26.31 o 1 -2 0 -2 229.25 144.10 24.22 o 1 -2 0 -3 2061.71 2529.60 62.68 o 1 2 0 3 2061.71 2325.23 64.91 o 1 2 1 -3 2712.72 3036.69 47.66 o 1 2 -1 -3 2712.72 2908.53 49.68 o 1 -2 -1 3 2712.72 2878.23 42.30 o 1 2 1 -2 89.91 75.19 12.54 o 1 -2 -1 2 89.91 68.64 13.20 o 1 2 -1 -2 89.90 71.28 15.71 o 1 -2 -1 0 42.02 50.35 6.42 o 1 2 1 0 42.02 46.14 6.28 o 1 -2 1 -1 5069.38 5119.18 36.00 o 1 -2 -1 -1 5069.37 5101.06 34.32 o 1 2 1 1 5069.37 4950.79 35.84 o 1 2 -1 1 5069.38 5140.41 35.74 o 1 2 1 2 483.77 461.50 28.08 o 1 2 -1 2 483.77 466.43 32.96 o 1 -2 -1 -2 483.77 457.04 31.58 o 1 -2 1 -2 483.77 518.75 30.57 o 1 -2 -1 -3 1039.58 1270.15 56.88 o 1 2 1 3 1039.58 1240.13 53.16 o 1 -2 1 -3 1039.58 1289.81 55.23 o 1 2 -1 3 1039.58 1136.48 49.04 o 1 2 -2 -3 1123.31 1088.16 47.84 o 1 -2 -2 3 1123.31 954.98 32.41 o 1 -2 -2 2 9.67 15.25 11.87 < 1 -2 -2 0 12163.68 10232.94 32.02 o 1 2 2 0 12163.68 10272.02 40.46 o 1 -2 -2 -1 3653.36 4123.19 34.87 o 1 2 2 1 3653.36 3833.37 36.23 o 1 2 -2 2 72.69 76.53 29.33 < 1 -2 -2 -2 72.69 72.02 25.76 < 1 2 2 2 72.69 83.08 26.43 o 1 -2 -2 -3 233.49 205.93 45.27 o 1 2 2 3 233.49 99.55 39.63 < 1 2 -2 3 233.49 217.85 39.31 o 1 -2 -3 3 649.26 603.29 28.02 o 1 -2 -3 2 4639.21 4653.86 31.44 o 1 2 3 1 684.14 747.37 35.70 o 1 -2 -3 -1 684.14 726.25 24.43 o 1 2 3 2 5569.94 6363.08 68.98 o 1 -2 -3 -2 5569.94 6226.98 62.45 o 1 -2 -3 -3 1620.83 1641.35 58.31 o 1 2 -3 3 1620.83 1752.12 57.66 o 1 -2 -4 3 698.50 511.62 27.85 o 1 -2 -4 -2 387.06 356.11 36.23 o 1 -2 -4 -3 211.39 18.52 34.34 < 1 3 -1 -3 576.09 497.18 31.26 o 1 -3 -1 0 2725.42 2497.92 21.21 o 1 3 1 0 2725.42 2535.33 19.80 o 1 3 1 1 3660.19 3981.00 38.04 o 1 -3 1 -1 3660.19 3901.71 39.08 o 1 -3 -1 -1 3660.19 4033.23 38.07 o 1 3 -1 1 3660.19 3800.60 37.17 o 1 3 -1 2 858.06 924.92 44.09 o 1 3 1 2 858.06 899.22 41.45 o 1 -3 -1 -2 858.06 992.66 39.88 o 1 -3 1 -2 858.06 948.35 36.99 o 1 -3 1 -3 622.55 384.91 45.15 o 1 -3 -1 -3 622.56 523.52 45.18 o 1 3 -2 -3 1662.27 1291.33 41.98 o 1 3 2 0 3025.05 2935.32 24.96 o 1 -3 -2 0 3025.05 3012.17 24.66 o 1 -3 -2 -1 4947.07 5206.47 41.63 o 1 3 2 1 4947.07 5261.26 44.37 o 1 3 -2 2 872.93 1013.86 48.60 o 1 3 2 2 872.93 905.64 41.33 o 1 -3 -2 -2 872.93 917.95 41.47 o 1 3 -2 3 753.83 11.16 24.70 < 1 -3 -3 3 115.65 37.68 14.74 < 1 -3 -3 2 45.05 37.40 7.61 o 1 3 3 0 4047.89 3458.98 44.05 o 1 -3 -3 0 4047.89 3674.41 30.50 o 1 3 3 1 0.54 8.00 19.11 < 1 -3 -3 -1 0.54 4.55 17.60 < 1 -3 -3 -2 382.46 427.62 35.97 o 1 3 3 2 382.46 418.35 39.42 o 1 -3 -4 3 133.42 41.61 17.50 < 1 3 4 1 224.74 285.29 44.74 o 1 -3 -4 -1 224.74 242.90 25.85 o 1 3 4 2 2174.19 2518.33 70.29 o 1 -3 -4 -2 2174.19 2346.94 59.23 o 1 3 4 3 1275.76 2.44 17.90 < 1 4 0 -3 1556.18 585.99 27.74 o 1 4 0 0 9196.29 7792.70 35.93 o 1 -4 0 0 9196.29 7623.25 43.13 o 1 4 0 1 808.58 772.25 29.05 o 1 -4 0 -1 808.58 796.34 29.60 o 1 4 0 2 49.46 37.86 31.47 < 1 -4 0 -2 49.46 32.34 30.57 < 1 4 0 3 247.27 1.08 11.52 < 1 4 -1 -3 733.47 465.87 29.05 o 1 4 1 -1 475.71 425.46 12.88 o 1 4 1 0 203.47 240.62 16.38 o 1 -4 -1 0 203.47 226.31 17.85 o 1 4 -1 1 82.72 91.98 20.79 o 1 4 1 1 82.72 87.80 20.84 o 1 -4 -1 -1 82.72 95.89 24.59 o 1 -4 1 -1 82.72 100.79 22.84 o 1 -4 1 -2 1872.77 2212.68 52.08 o 1 -4 -1 -2 1872.77 2166.82 51.59 o 1 4 1 2 1872.77 2115.43 51.62 o 1 4 -1 2 1872.77 2244.52 53.29 o 1 4 -1 3 557.73 3.24 12.14 < 1 4 1 3 557.73 6.12 12.17 < 1 4 2 -1 3673.74 3939.27 29.05 o 1 -4 -2 1 3673.74 3894.83 23.00 o 1 -4 -2 0 3451.56 3469.37 29.90 o 1 4 2 0 3451.56 3340.56 30.94 o 1 -4 -2 -1 1531.25 1474.38 36.07 o 1 4 2 1 1531.25 1571.88 37.38 o 1 4 2 2 164.99 147.88 32.87 o 1 -4 -2 -2 164.99 163.96 31.97 o 1 4 -2 3 881.56 6.28 12.12 < 1 -4 -3 1 3904.98 3450.88 23.55 o 1 4 3 0 985.98 983.16 26.43 o 1 -4 -3 0 985.98 1018.85 27.28 o 1 -4 -3 -1 7806.93 8304.76 60.66 o 1 4 3 1 7806.93 8462.21 59.69 o 1 -4 -3 -2 2.92 14.35 29.35 < 1 4 3 2 2.92 12.47 31.40 < 1 -4 -4 0 37.80 36.46 19.34 < 1 -4 -4 -1 2021.22 1969.67 44.51 o 1 4 4 1 2021.22 2105.86 47.48 o 1 -4 -4 -2 28.96 47.45 37.75 < 1 4 4 2 28.96 46.30 38.14 < 1 -4 -5 3 508.33 450.53 18.24 o 1 -4 -5 -2 153.46 116.80 38.25 o 1 5 -1 -3 732.35 633.53 26.24 o 1 5 1 -1 11.72 7.25 12.81 < 1 -5 -1 0 865.23 898.49 26.93 o 1 5 1 0 865.23 894.92 24.77 o 1 5 -1 1 3237.23 3261.67 47.87 o 1 5 1 1 3237.23 3298.68 44.21 o 1 -5 -1 -1 3237.23 3351.44 44.30 o 1 5 -1 2 271.33 350.61 42.71 o 1 -5 1 -2 271.33 332.46 43.33 o 1 -5 -1 -2 271.33 305.64 33.51 o 1 5 1 2 271.33 325.50 37.91 o 1 -5 -2 1 6986.59 7487.79 36.46 o 1 5 2 -1 6986.59 7503.11 37.95 o 1 -5 -2 0 5625.20 5626.34 43.08 o 1 5 2 0 5625.20 5811.39 41.82 o 1 5 2 1 0.01 9.36 23.78 < 1 -5 -2 -1 0.01 9.87 21.41 < 1 -5 -2 -2 60.73 29.67 35.33 < 1 5 2 2 60.73 18.08 30.45 < 1 -5 -3 1 495.73 406.69 19.14 o 1 -5 -3 0 1414.52 1471.32 31.77 o 1 5 3 0 1414.52 1604.04 30.50 o 1 -5 -3 -1 4042.18 4399.92 51.41 o 1 5 3 1 4042.18 4410.00 55.59 o 1 -5 -3 -2 339.50 317.28 39.49 o 1 -5 -4 1 177.06 173.89 17.67 o 1 5 4 0 934.19 989.18 42.83 o 1 -5 -4 0 934.19 959.12 28.89 o 1 -5 -4 -1 2482.86 2399.32 50.79 o 1 5 4 1 2482.86 2647.69 52.88 o 1 -5 -5 0 11154.92 10788.86 63.37 o 1 5 5 1 169.03 144.52 45.24 o 1 -5 -5 -1 169.03 103.58 28.94 o 1 5 5 2 585.72 3.57 15.16 < 1 6 0 -1 2056.51 1937.88 27.74 o 1 6 0 0 441.38 560.99 24.27 o 1 -6 0 -1 1378.90 1589.82 45.08 o 1 6 0 1 1378.90 1314.29 40.32 o 1 6 1 -1 1350.22 1278.82 27.49 o 1 6 1 0 554.46 470.93 29.17 o 1 -6 -1 0 554.46 495.32 24.66 o 1 -6 -1 -1 2103.29 2185.36 43.52 o 1 6 1 1 2103.29 2164.98 46.62 o 1 -6 -2 1 331.35 322.02 25.32 o 1 6 2 -1 331.35 295.09 24.45 o 1 -6 -2 0 4756.24 5768.01 49.48 o 1 6 2 0 4756.24 5660.09 47.06 o 1 -6 -2 -1 366.01 434.22 38.07 o 1 6 2 1 366.01 354.80 33.12 o 1 6 2 2 5.93 5.91 11.98 < 1 -6 -3 1 20.02 18.31 19.09 < 1 6 3 -1 20.02 14.61 21.97 < 1 6 3 0 993.76 1155.14 39.68 o 1 -6 -3 0 993.76 1119.19 34.82 o 1 6 3 1 207.18 220.42 33.65 o 1 -6 -3 -1 207.18 213.59 37.63 o 1 6 3 2 3148.74 3.82 11.59 < 1 -6 -4 1 279.84 280.00 24.29 o 1 -6 -4 0 9889.79 10295.39 62.24 o 1 6 4 0 9889.79 10204.88 72.85 o 1 -6 -4 -1 0.82 23.60 27.69 < 1 6 4 1 0.82 25.14 35.31 < 1 -6 -5 2 371.65 323.59 17.96 o 1 -6 -5 1 154.67 89.32 19.55 o 1 6 5 0 680.08 509.85 63.35 o 1 -6 -5 0 680.08 554.20 38.04 o 1 -6 -5 -1 150.82 87.75 34.85 < 1 6 5 1 150.82 119.59 38.64 o 1 -6 -6 0 16.81 21.55 24.43 < 1 6 6 1 30.22 11.20 43.47 < 1 -6 -6 -1 30.22 8.65 26.08 < 1 7 1 -2 527.51 468.77 20.10 o 1 7 1 -1 3.52 8.40 19.83 < 1 -7 -1 0 3216.77 3550.48 55.23 o 1 7 1 0 3216.77 3285.71 41.26 o 1 7 1 1 69.35 111.33 33.38 o 1 -7 -1 -1 69.35 104.93 35.91 < 1 -7 -2 1 426.96 496.14 32.80 o 1 7 2 -1 426.96 434.75 26.77 o 1 -7 -2 0 3355.26 3831.83 56.51 o 1 7 2 0 3355.26 4109.74 51.59 o 1 -7 -2 -1 0.23 22.73 28.75 < 1 7 2 1 0.23 7.20 26.41 < 1 -7 -3 1 105.82 76.02 26.15 < 1 7 3 -1 105.82 60.72 24.66 < 1 -7 -3 0 5088.04 5846.12 64.34 o 1 7 3 0 5088.04 5811.85 57.04 o 1 -7 -3 -1 15.89 14.65 28.31 < 1 7 3 1 15.89 6.49 27.33 < 1 -7 -4 1 2233.86 2723.34 47.04 o 1 7 4 -1 2233.86 2544.36 55.50 o 1 7 4 0 595.19 563.17 44.85 o 1 -7 -4 0 595.19 524.87 37.95 o 1 -7 -4 -1 283.25 242.55 40.32 o 1 -7 -5 2 421.59 316.98 21.23 o 1 -7 -5 1 883.18 740.01 33.70 o 1 -7 -5 0 0.15 13.32 20.98 < 1 7 5 0 0.15 25.97 35.38 < 1 -7 -5 -1 2899.26 8.58 28.11 < 1 -7 -6 2 60.82 42.78 19.11 < 1 -7 -6 1 2136.87 2097.35 42.00 o 1 -7 -6 0 131.95 147.16 29.72 o 1 8 0 -2 265.34 261.23 29.47 o 1 8 0 0 10469.44 10653.89 76.89 o 1 8 1 -2 2115.04 2547.72 41.70 o 1 8 1 -1 687.96 799.30 34.09 o 1 -8 -1 0 872.52 792.08 54.58 o 1 8 1 0 872.52 834.04 40.23 o 1 8 2 -2 2.78 17.67 16.29 < 1 8 2 -1 465.64 561.51 34.82 o 1 8 2 0 1026.61 1323.35 46.60 o 1 -8 -2 0 1026.61 1305.78 51.13 o 1 8 3 -1 464.89 646.14 44.00 o 1 -8 -3 1 464.89 602.48 40.05 o 1 -8 -3 0 1127.87 1186.26 47.57 o 1 8 3 0 1127.87 1225.96 47.15 o 1 8 4 -1 1478.56 1775.15 60.13 o 1 -8 -4 1 1478.56 1649.05 45.84 o 1 -8 -4 0 309.45 257.92 41.47 o 1 8 4 0 309.45 316.16 45.38 o 1 8 4 1 454.55 3.96 13.13 < 1 -8 -5 2 3.98 16.35 17.67 < 1 -8 -5 1 1075.71 969.56 45.29 o 1 8 5 0 23.15 34.89 44.12 < 1 -8 -5 0 23.15 26.06 30.02 < 1 -8 -6 2 70.53 52.79 23.60 < 1 -8 -6 1 300.80 222.84 36.30 o 1 -8 -6 0 620.27 494.07 44.85 o 1 8 6 0 620.27 471.76 79.29 o 1 -8 -7 2 185.73 0.74 10.03 < 1 -8 -7 1 0.79 32.09 29.58 < 1 -8 -7 0 735.46 798.36 54.70 o 1 9 1 -2 33.14 32.48 27.14 < 1 9 1 -1 121.74 94.01 33.10 < 1 9 1 0 71.15 79.10 32.48 < 1 9 2 -2 120.11 52.81 25.21 < 1 9 2 -1 1746.60 2130.50 56.45 o 1 9 2 0 46.19 71.79 31.65 < 1 -9 -2 0 46.19 55.18 35.56 < 1 9 3 -1 313.47 341.50 42.60 o 1 -9 -3 1 313.47 276.32 38.14 o 1 -9 -3 0 19.04 26.89 30.64 < 1 9 3 0 19.04 22.89 34.16 < 1 -9 -4 1 0.84 24.98 31.28 < 1 9 4 -1 0.84 31.10 32.96 < 1 -9 -4 0 508.04 573.57 50.26 o 1 9 4 0 508.04 575.50 51.85 o 1 9 5 -1 16.16 43.27 51.96 < 1 -9 -5 1 16.16 22.17 30.62 < 1 -9 -5 0 3855.88 4877.92 81.91 o 1 9 5 0 3855.88 3.06 37.38 < 1 -9 -6 2 1470.62 7.29 7.34 < 1 -9 -6 1 10.39 11.06 26.98 < 1 -9 -6 0 146.35 22.63 28.75 < 1 -9 -7 1 151.51 81.54 32.34 < 1 10 1 -2 166.07 0.44 22.27 < 1 10 1 -1 289.77 311.72 41.13 o 1 10 2 -1 117.47 101.25 37.84 < 1 -10 -2 0 1154.87 22.50 32.18 < 1 10 3 -1 676.18 696.69 55.99 o 1 10 4 -1 435.06 336.79 51.68 o 1 -10 -4 1 435.06 227.81 41.77 o 1 -10 -5 1 7.50 11.94 29.81 < 1 10 5 -1 7.50 17.41 42.60 < 1 10 5 0 0.08 0.92 15.07 < 1 -10 -6 1 388.05 319.56 47.13 o 1 -10 -7 1 53.22 43.17 34.32 < 1 -10 -8 1 134.37 51.39 34.46 < 1 11 1 -1 0.69 31.56 33.03 < 1 11 2 -1 208.88 129.11 45.57 < 1 11 3 -1 0.10 17.00 37.31 < 1 11 4 -1 625.06 859.91 71.37 o 1 -11 -4 1 625.06 665.23 60.79 o 1 11 5 -1 255.65 344.06 72.98 o 1 -11 -5 1 255.65 199.47 46.95 o 1 0 0 -1 411.39 409.20 8.65 o 2 0 0 1 411.39 423.34 11.12 o 2 0 0 -2 23.01 15.02 14.00 < 2 0 0 2 23.01 32.74 27.39 < 2 0 0 -3 2355.13 2096.08 42.21 o 2 0 1 1 190.99 212.62 8.63 o 2 0 -1 -2 8390.52 9361.98 46.65 o 2 0 1 -2 8390.52 9456.92 50.40 o 2 0 1 2 8390.52 9273.25 42.69 o 2 0 -1 -3 2715.95 2007.60 49.14 o 2 0 1 -3 2715.96 2219.42 40.27 o 2 0 2 2 63.77 49.47 14.80 o 2 0 2 -3 1124.71 1033.51 42.80 o 2 0 2 3 1124.71 878.75 31.97 o 2 0 3 2 123.26 66.64 15.48 o 2 0 3 3 649.95 738.77 33.64 o 2 0 4 3 699.33 812.66 36.90 o 2 1 1 -4 12.10 14.05 29.81 < 2 -1 1 3 1134.85 1177.30 39.19 o 2 1 1 -3 1134.85 1132.92 43.22 o 2 1 -1 -3 1134.85 761.40 43.11 o 2 1 1 -2 1443.31 1516.25 28.97 o 2 -1 -1 2 1443.31 1282.10 51.37 o 2 -1 1 2 1443.31 1566.49 25.80 o 2 1 -1 -2 1443.31 1540.20 32.45 o 2 -1 -1 1 37.54 32.47 13.50 < 2 1 -1 -1 37.54 24.24 13.96 < 2 -1 1 1 37.54 32.28 10.28 o 2 1 1 -1 37.54 30.58 10.52 < 2 -1 1 -2 2176.98 2466.43 31.73 o 2 -1 -1 -2 2176.98 2216.65 24.79 o 2 -1 1 -3 577.46 245.00 24.53 o 2 1 2 -4 160.68 126.35 38.95 o 2 1 2 -3 24.11 22.77 23.62 < 2 -1 2 3 24.11 52.69 31.46 < 2 -1 2 2 506.74 443.57 24.35 o 2 1 2 -2 506.74 436.44 29.88 o 2 1 2 2 370.85 332.65 15.28 o 2 -1 2 -3 1666.06 1127.06 48.11 o 2 1 3 -3 183.50 187.25 36.61 o 2 -1 3 3 183.50 278.93 32.52 o 2 1 3 2 195.16 222.55 14.53 o 2 1 3 3 115.90 23.73 18.10 < 2 -1 4 3 617.00 388.64 36.81 o 2 1 4 3 133.73 90.14 18.32 o 2 1 5 3 3124.62 1911.52 42.32 o 2 2 0 -4 14.30 41.57 42.60 < 2 -2 0 3 1636.57 1836.48 58.39 o 2 2 0 -3 1636.57 1674.64 46.50 o 2 2 0 -2 531.53 562.20 28.23 o 2 -2 0 2 531.53 586.22 33.42 o 2 2 0 -1 18314.49 18392.81 53.98 o 2 -2 0 1 18314.49 18468.98 51.89 o 2 -2 0 -2 159.50 96.92 10.37 o 2 -2 0 -3 1561.62 1988.09 36.26 o 2 2 1 -4 30.69 30.45 38.88 < 2 -2 1 3 1912.66 1986.64 48.02 o 2 -2 -1 3 1912.65 1611.23 71.91 o 2 2 -1 -3 1912.66 2010.72 57.09 o 2 2 1 -3 1912.65 1798.66 54.14 o 2 2 -1 -2 62.55 30.45 20.48 < 2 2 1 -2 62.55 62.26 19.57 o 2 -2 1 2 62.55 57.55 21.44 < 2 -2 -1 2 62.55 55.77 23.65 < 2 2 -1 -1 7064.12 6667.84 45.24 o 2 2 1 -1 7064.12 6892.47 31.97 o 2 -2 -1 1 7064.12 6691.83 38.62 o 2 -2 1 1 7064.12 6929.06 36.04 o 2 -2 1 -3 735.99 1036.64 32.47 o 2 -2 2 3 1184.16 974.46 37.65 o 2 2 2 -3 1184.16 598.57 38.49 o 2 -2 2 2 6.73 15.59 19.84 < 2 -2 -2 2 6.73 37.16 39.70 < 2 2 2 -2 6.73 24.70 22.02 < 2 2 2 -1 75.55 58.70 16.75 o 2 -2 -2 1 75.55 44.12 23.71 < 2 -2 3 3 822.07 273.98 34.63 o 2 2 3 -3 822.07 702.51 39.67 o 2 2 3 -2 3227.81 3257.05 48.11 o 2 2 5 3 509.85 46.01 14.05 o 2 3 -1 -4 42.23 48.11 54.51 < 2 3 -1 -3 420.78 303.79 41.92 o 2 3 1 -3 420.78 305.90 38.13 o 2 -3 -1 3 420.78 277.34 43.59 o 2 -3 1 3 420.78 280.71 35.98 o 2 -3 1 2 287.75 302.38 26.97 o 2 -3 -1 2 287.75 303.08 29.37 o 2 3 1 -2 287.75 289.21 25.98 o 2 3 -1 -2 287.75 271.53 25.14 o 2 3 -1 -1 989.70 867.39 32.76 o 2 3 1 -1 989.70 1194.01 20.63 o 2 -3 1 1 989.70 1079.74 26.90 o 2 -3 -1 1 989.70 1132.23 23.65 o 2 -3 -1 -1 2546.64 2601.28 15.30 o 2 -3 1 -3 735.73 277.92 25.50 o 2 -3 2 3 1440.60 1503.39 48.39 o 2 3 2 -3 1440.60 1437.72 48.97 o 2 -3 -2 3 1440.60 1498.88 71.11 o 2 3 2 -2 173.99 193.64 26.00 o 2 -3 2 2 173.99 169.55 26.42 o 2 -3 -2 2 173.99 131.79 25.61 o 2 3 2 -1 1037.16 1164.14 26.55 o 2 -3 -2 1 1037.16 986.64 26.95 o 2 3 2 1 3442.00 3184.13 18.16 o 2 3 3 -3 109.96 21.29 29.22 < 2 -3 3 3 109.96 59.07 32.41 < 2 -3 -3 2 31.34 17.02 41.17 < 2 3 3 -2 31.34 36.75 24.06 < 2 3 3 -1 2254.19 2090.12 32.28 o 2 -3 -3 1 2254.19 2012.86 49.85 o 2 3 3 1 0.38 7.44 10.59 < 2 3 4 -3 174.63 95.24 34.48 < 2 4 0 -3 2054.52 2337.10 55.44 o 2 -4 0 3 2054.52 1510.66 51.63 o 2 -4 0 2 287.87 254.36 27.32 o 2 4 0 -2 287.87 251.26 34.81 o 2 4 0 -1 577.43 504.07 26.38 o 2 -4 0 1 577.43 656.87 26.11 o 2 4 -1 -3 1035.99 313.74 47.89 o 2 -4 -1 3 1035.99 1189.96 51.06 o 2 4 1 -3 1035.99 729.02 42.32 o 2 -4 1 3 1035.99 198.70 34.63 o 2 4 1 -2 2767.11 2582.43 50.62 o 2 -4 1 2 2767.11 2920.08 45.60 o 2 -4 -1 2 2767.11 2616.60 53.54 o 2 4 -1 -2 2767.11 2845.71 59.27 o 2 4 1 -1 330.98 279.41 25.58 o 2 -4 -1 1 330.98 359.95 20.67 o 2 -4 1 1 330.98 355.57 28.20 o 2 4 -1 -1 330.98 216.03 29.83 o 2 -4 -1 -1 57.56 73.29 10.85 o 2 -4 2 3 232.71 223.89 41.11 o 2 -4 -2 3 232.71 129.11 47.49 < 2 4 2 -3 232.71 204.54 40.84 o 2 -4 2 2 365.24 284.46 37.76 o 2 4 2 -2 365.24 320.81 34.28 o 2 -4 -2 2 365.24 307.57 33.97 o 2 4 2 -1 2556.07 2561.43 36.86 o 2 -4 -2 1 2556.07 2735.38 41.70 o 2 4 2 1 1065.40 1034.04 19.97 o 2 -4 -2 -1 1065.40 1133.44 19.35 o 2 4 3 -3 1615.44 1615.94 56.32 o 2 -4 3 3 1615.44 1685.71 57.05 o 2 4 3 -2 1.42 12.07 20.28 < 2 -4 -3 2 1.42 31.97 46.26 < 2 -4 -3 1 2716.95 2335.67 43.22 o 2 4 3 -1 2716.95 2689.43 37.56 o 2 4 3 1 5431.80 6290.38 33.88 o 2 4 4 -3 210.65 15.68 28.05 < 2 4 4 -2 464.76 386.44 38.66 o 2 -4 -4 2 464.76 198.77 60.55 o 2 -4 -4 1 5387.69 4442.63 82.06 o 2 4 4 -1 5387.69 5514.91 52.00 o 2 4 4 1 1406.30 1538.62 25.23 o 2 4 5 2 106.77 103.43 16.01 o 2 5 1 -3 619.70 572.96 50.73 o 2 5 -1 -3 619.70 671.71 70.78 o 2 5 1 -2 396.89 371.09 35.95 o 2 5 -1 -2 396.89 331.40 45.73 o 2 -5 1 2 396.89 333.71 30.49 o 2 -5 -1 2 396.89 342.65 35.25 o 2 -5 -1 1 8.15 8.21 18.38 < 2 5 1 -1 8.15 9.82 21.66 < 2 -5 1 1 8.15 16.91 21.25 < 2 5 -1 -1 8.15 19.59 30.87 < 2 -5 -1 -1 2252.36 2684.21 27.01 o 2 -5 -1 -2 188.78 176.40 11.51 o 2 -5 2 3 750.90 1.52 16.93 < 2 -5 2 2 1.01 19.09 29.37 < 2 -5 -2 2 1.01 12.55 24.22 < 2 5 2 -2 1.01 15.10 26.29 < 2 5 2 -1 4861.04 4951.26 48.50 o 2 -5 -2 1 4861.04 4460.28 48.99 o 2 5 2 1 0.01 13.45 19.53 < 2 -5 -2 -1 0.01 8.08 16.82 < 2 5 3 -2 367.04 220.39 39.12 o 2 -5 -3 2 367.04 194.45 43.51 o 2 5 3 -1 344.91 301.56 30.45 o 2 -5 -3 1 344.91 255.31 31.20 o 2 -5 -3 -1 2812.41 2921.45 49.60 o 2 5 3 1 2812.41 3413.19 35.47 o 2 5 4 -2 1532.76 1376.53 41.90 o 2 -5 -4 2 1532.76 1029.61 69.40 o 2 -5 -4 1 123.19 76.53 39.67 < 2 5 4 -1 123.19 129.00 25.32 o 2 5 4 1 1727.49 2112.37 33.11 o 2 5 5 -2 673.21 487.47 46.32 o 2 -5 -5 1 1459.30 693.48 72.79 o 2 5 5 -1 1459.30 1347.07 49.78 o 2 5 5 1 117.61 249.08 25.87 o 2 5 5 2 407.53 480.41 19.97 o 2 5 6 2 1680.33 2119.75 37.36 o 2 -6 0 3 245.89 2.88 12.55 < 2 -6 0 2 438.71 387.71 37.21 o 2 6 0 -2 438.71 365.90 42.76 o 2 6 0 -1 1430.85 1572.41 49.30 o 2 -6 0 1 1430.85 1566.51 40.71 o 2 -6 1 3 554.63 2.07 10.04 < 2 6 1 -2 142.54 124.59 35.60 o 2 -6 1 2 142.54 116.89 34.32 o 2 -6 -1 2 142.54 170.37 40.25 o 2 6 -1 -2 142.54 82.83 46.54 < 2 -6 -1 1 939.44 919.57 33.58 o 2 -6 1 1 939.44 880.49 38.68 o 2 6 1 -1 939.44 904.27 40.80 o 2 -6 -1 -1 1463.40 1696.04 30.18 o 2 -6 -1 -2 92.20 143.77 15.57 o 2 -6 2 3 876.86 3.96 11.82 < 2 6 2 -2 48.42 20.85 31.29 < 2 -6 -2 2 48.42 17.70 32.92 < 2 6 2 -1 230.54 170.63 32.67 o 2 -6 -2 1 230.54 165.35 30.38 o 2 6 2 1 254.66 263.25 33.93 o 2 -6 -2 -1 254.66 321.47 26.09 o 2 -6 -3 2 3417.71 22.63 30.18 < 2 6 3 -2 3417.71 3341.77 63.63 o 2 6 3 -1 13.93 44.69 30.76 < 2 -6 -3 1 13.93 11.32 25.10 < 2 6 3 1 144.15 135.03 24.28 o 2 -6 -3 -1 144.15 157.75 25.63 o 2 6 4 -2 225.43 190.33 40.18 o 2 6 4 -1 194.71 186.75 29.04 o 2 -6 -4 1 194.71 161.87 35.91 o 2 6 4 1 0.57 12.15 21.11 < 2 -6 -5 1 107.61 49.36 55.86 < 2 6 5 -1 107.61 85.65 32.87 < 2 6 5 1 104.94 85.05 23.49 o 2 6 5 2 181.73 147.64 21.71 o 2 6 6 1 21.03 16.05 24.00 < 2 6 6 2 459.17 569.04 30.74 o 2 6 7 2 294.89 406.14 31.53 o 2 7 -1 -2 367.02 50.75 41.15 < 2 7 1 -1 2.45 17.94 26.82 < 2 -7 -1 1 2.45 15.92 27.30 < 2 -7 -1 -1 48.25 64.84 25.23 < 2 -7 -1 -2 251.19 363.17 25.72 o 2 7 2 -1 297.07 282.72 34.90 o 2 -7 -2 1 297.07 331.18 36.09 o 2 -7 -2 -1 0.16 14.31 20.83 < 2 -7 -2 -2 1511.94 2013.36 42.62 o 2 -7 -3 1 73.63 40.40 33.22 < 2 7 3 -1 73.63 30.45 33.75 < 2 7 3 1 11.05 15.41 25.52 < 2 -7 -3 -1 11.05 16.14 24.31 < 2 -7 -4 1 1554.25 1567.06 53.26 o 2 7 4 -1 1554.25 1668.21 52.47 o 2 -7 -4 -1 197.07 141.66 46.48 o 2 7 4 1 197.07 209.56 31.24 o 2 7 5 -1 614.49 439.83 36.20 o 2 -7 -5 1 614.49 431.99 66.36 o 2 7 5 1 2017.21 3070.72 47.20 o 2 7 6 -1 1486.77 1701.45 54.40 o 2 7 6 1 689.58 927.59 42.36 o 2 7 6 2 24.18 13.14 17.11 < 2 7 7 1 623.78 908.06 47.47 o 2 8 0 -1 22.87 16.29 46.30 < 2 -8 0 1 22.87 18.10 28.64 < 2 -8 -1 1 478.66 465.74 36.59 o 2 8 1 -1 478.66 428.18 46.59 o 2 -8 -1 -1 3.38 18.08 29.70 < 2 -8 -1 -2 1339.86 2193.70 47.45 o 2 8 2 -1 323.97 279.46 40.73 o 2 -8 -2 1 323.97 16.86 26.11 < 2 -8 -2 -1 345.71 575.80 41.57 o 2 -8 -2 -2 0.13 18.32 22.81 < 2 8 3 -1 323.46 309.82 43.97 o 2 -8 -3 -1 1104.53 1651.19 46.68 o 2 8 3 1 1104.53 1491.30 56.05 o 2 8 4 -1 1028.74 10.57 28.69 < 2 8 4 1 316.26 281.15 38.75 o 2 -8 -4 -1 316.26 284.81 42.40 o 2 8 5 1 2.21 19.64 30.36 < 2 -8 -6 1 209.29 3.90 19.51 < 2 8 6 1 118.89 83.99 29.48 < 2 8 7 1 664.65 872.66 50.64 o 2 -9 -1 -1 435.82 628.97 46.76 o 2 -9 -2 1 1215.23 8.39 12.42 < 2 -9 -2 -1 262.79 323.95 42.23 o 2 -9 -3 1 218.10 6.16 12.59 < 2 9 3 1 396.30 483.27 68.80 o 2 -9 -3 -1 396.30 579.52 44.43 o 2 -9 -4 -1 0.21 6.52 39.41 < 2 9 4 1 0.21 17.70 34.26 < 2 -9 -5 -1 38.90 53.74 59.80 < 2 9 5 1 38.90 16.12 31.02 < 2 9 6 1 174.99 125.23 36.04 o 2 9 7 1 205.67 245.18 41.68 o 2 9 8 1 275.50 337.63 50.44 o 2 -10 -1 -1 996.35 1535.47 68.01 o 2 -10 -2 -1 269.19 372.81 48.15 o 2 -10 -3 -1 130.79 55.02 37.21 < 2 10 4 1 235.12 172.41 62.13 < 2 -10 -4 -1 235.12 267.00 57.95 o 2 -10 -5 -1 0.00 86.22 73.32 < 2 10 5 1 0.00 13.85 37.32 < 2 10 6 1 7.10 20.48 36.92 < 2 -11 -1 -1 324.42 3.41 18.93 < 2