#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180910 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105187.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105187_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; [Ni(MeCN)(H~2~O)~2~(NO~3~)~2~]·(15-crown-5)·MeCN: detailed study of a four-phase sequence that includes an intermediate modulated phase ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 389 _journal_page_last 400 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.430 _cell_angle_gamma 90.000 _cell_length_a 12.1660 _cell_length_b 12.2680 _cell_length_c 16.2010 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file hw5021220K_III_1sup17.hkl _cod_data_source_block 220K_III_1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k06096 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 293.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6231.27 5984.01 105.64 o 2 0 0 25136.45 26003.19 526.11 o 3 0 0 805.14 886.52 16.57 o 4 0 0 1249.05 1046.01 20.71 o 5 0 0 39502.56 43634.15 743.60 o 6 0 0 1864.71 2520.78 43.50 o 7 0 0 7971.78 8527.57 147.06 o 8 0 0 6659.05 6818.74 132.56 o 9 0 0 352.13 389.41 18.64 o 10 0 0 458.39 420.48 20.71 o 11 0 0 963.47 896.88 37.28 o 12 0 0 1147.95 1317.35 64.21 o 13 0 0 869.11 1010.80 86.99 o 14 0 0 17.84 8.29 33.14 o 15 0 0 168.12 16.57 47.64 o 1 1 0 45688.67 45117.21 2498.00 o 2 1 0 1253.56 1352.94 16.80 o 3 1 0 8979.91 8406.32 108.80 o 4 1 0 17088.49 18006.31 210.53 o 5 1 0 1046.18 840.63 11.39 o 6 1 0 11419.24 12309.67 142.80 o 7 1 0 2549.35 2780.58 39.22 o 8 1 0 116.34 114.83 12.43 o 9 1 0 725.26 715.81 18.26 o 10 1 0 122.65 137.72 9.44 o 11 1 0 2265.30 2502.54 61.16 o 12 1 0 1016.13 1086.39 49.41 o 13 1 0 118.59 107.43 26.24 o 14 1 0 164.03 144.92 37.28 o 15 1 0 0.43 36.01 37.74 o 0 2 0 12777.94 12259.42 215.20 o 1 2 0 1070.51 1182.81 16.11 o 2 2 0 3047.43 3349.94 51.78 o 3 2 0 9817.18 9095.35 117.08 o 4 2 0 584.36 799.20 23.82 o 5 2 0 18474.70 19728.27 216.53 o 6 2 0 45.52 19.47 6.21 o 7 2 0 4212.40 4652.10 72.50 o 8 2 0 3350.98 3593.43 67.32 o 9 2 0 794.74 901.01 23.82 o 10 2 0 2314.47 2652.65 50.51 o 11 2 0 7.54 28.31 14.82 o 12 2 0 585.11 623.11 50.75 o 13 2 0 290.49 282.26 38.32 o 14 2 0 10.97 13.24 37.33 o 15 2 0 295.30 337.94 48.27 o 1 3 0 4892.65 5557.53 91.14 o 2 3 0 5122.39 5646.61 113.92 o 3 3 0 8449.29 9124.57 213.34 o 4 3 0 17564.86 17680.23 220.68 o 5 3 0 1150.02 828.61 14.65 o 6 3 0 980.78 1046.78 35.21 o 7 3 0 846.18 955.52 18.87 o 8 3 0 1078.93 1209.55 21.83 o 9 3 0 3059.25 3295.20 55.43 o 10 3 0 460.52 434.63 15.68 o 11 3 0 1676.16 1877.24 56.63 o 12 3 0 57.76 63.52 22.23 o 13 3 0 0.67 -29.55 47.64 o 14 3 0 248.22 152.18 46.25 o 0 4 0 44316.87 44951.07 1478.91 o 1 4 0 2085.36 2512.77 85.96 o 2 4 0 12601.16 13127.79 284.80 o 3 4 0 8226.35 8452.81 181.24 o 4 4 0 689.64 453.32 13.46 o 5 4 0 9373.00 10188.55 170.88 o 6 4 0 875.09 856.03 16.80 o 7 4 0 3209.90 3354.71 56.96 o 8 4 0 3052.30 3217.36 54.13 o 9 4 0 55.93 63.29 8.78 o 10 4 0 2098.36 2493.83 63.70 o 11 4 0 101.59 101.75 21.10 o 12 4 0 112.76 53.04 24.71 o 13 4 0 116.29 98.27 41.43 o 14 4 0 4.34 18.82 40.39 o 1 5 0 12298.83 12349.30 630.71 o 2 5 0 10552.50 13357.37 466.04 o 3 5 0 8146.95 8465.10 292.05 o 4 5 0 6890.08 7603.83 93.21 o 5 5 0 2.25 21.86 7.25 o 6 5 0 3898.59 3942.63 64.39 o 7 5 0 75.58 104.32 9.94 o 8 5 0 11.88 6.21 11.39 o 9 5 0 1178.63 1332.48 33.69 o 10 5 0 257.37 209.75 19.88 o 11 5 0 953.34 1114.41 51.27 o 12 5 0 37.83 23.96 26.57 o 13 5 0 21.18 30.68 28.22 o 14 5 0 319.93 278.94 38.32 o 0 6 0 18852.10 19659.76 749.81 o 1 6 0 139.63 217.51 7.19 o 2 6 0 9567.18 10122.21 279.63 o 3 6 0 522.48 614.65 17.61 o 4 6 0 413.86 393.56 10.91 o 5 6 0 5062.26 5388.14 85.96 o 6 6 0 8.74 12.43 7.96 o 7 6 0 2092.43 1932.87 53.85 o 8 6 0 273.77 251.87 14.65 o 9 6 0 55.29 29.00 10.91 o 10 6 0 1376.80 1706.04 54.41 o 11 6 0 111.44 124.97 20.31 o 12 6 0 231.02 153.47 25.67 o 13 6 0 193.28 132.47 35.97 o 14 6 0 5.27 -8.76 34.11 o 1 7 0 1991.94 2028.36 56.96 o 2 7 0 503.28 655.94 14.11 o 3 7 0 1208.21 1186.75 21.83 o 4 7 0 1461.42 1437.35 25.60 o 5 7 0 10.00 4.83 8.29 o 6 7 0 2646.61 2918.81 40.10 o 7 7 0 415.39 496.29 24.86 o 8 7 0 56.28 37.28 12.38 o 9 7 0 397.11 283.48 19.73 o 10 7 0 40.09 36.29 16.80 o 11 7 0 651.94 711.35 38.26 o 12 7 0 140.74 114.84 29.47 o 13 7 0 5.05 -13.98 37.30 o 0 8 0 2950.20 3373.64 91.13 o 1 8 0 436.43 353.68 12.43 o 2 8 0 15.27 15.02 5.90 o 3 8 0 994.79 913.22 42.46 o 4 8 0 72.19 71.02 8.78 o 5 8 0 4082.13 4560.22 87.05 o 6 8 0 517.07 632.86 22.78 o 7 8 0 247.52 203.06 16.85 o 8 8 0 322.68 271.10 22.89 o 9 8 0 12.96 26.53 15.33 o 10 8 0 485.46 484.47 32.84 o 11 8 0 43.02 39.35 20.90 o 12 8 0 21.17 -13.69 24.46 o 13 8 0 78.79 81.06 101.49 o 1 9 0 866.50 806.60 58.00 o 2 9 0 1224.33 1244.49 27.96 o 3 9 0 43.88 64.81 13.46 o 4 9 0 234.38 139.04 10.91 o 5 9 0 148.16 205.59 41.43 o 6 9 0 483.39 609.58 24.42 o 7 9 0 858.84 896.54 43.50 o 8 9 0 94.54 64.12 16.80 o 9 9 0 131.88 136.15 19.41 o 10 9 0 9.81 -16.80 16.80 o 11 9 0 73.94 74.02 30.34 o 12 9 0 69.58 41.43 31.07 o 0 10 0 6739.25 7127.37 153.28 o 1 10 0 19.78 35.21 6.21 o 2 10 0 121.00 81.82 8.04 o 3 10 0 398.23 638.55 56.96 o 4 10 0 1.35 -4.95 13.46 o 5 10 0 246.58 210.69 25.89 o 6 10 0 62.19 72.92 18.33 o 7 10 0 53.21 26.78 19.44 o 8 10 0 205.52 101.75 20.50 o 9 10 0 0.08 19.47 32.11 o 10 10 0 51.74 78.71 37.28 o 11 10 0 27.67 45.57 31.07 o 1 11 0 532.38 550.97 20.71 o 2 11 0 15.29 2.76 11.12 o 3 11 0 0.19 9.78 29.00 o 4 11 0 144.21 95.63 27.96 o 5 11 0 16.84 1.57 17.61 o 6 11 0 294.25 249.24 24.46 o 7 11 0 155.35 120.21 22.04 o 8 11 0 4.85 3.56 22.22 o 9 11 0 26.36 18.64 35.21 o 10 11 0 0.22 35.21 47.64 o 11 11 0 54.08 29.00 55.93 o 0 12 0 47.25 113.92 35.21 o 1 12 0 3.65 -2.07 24.86 o 2 12 0 7.97 -11.84 19.88 o 3 12 0 492.99 450.85 68.35 o 4 12 0 6.59 37.93 19.44 o 5 12 0 593.57 689.46 85.96 o 6 12 0 0.72 -32.22 32.22 o 7 12 0 3.97 58.00 31.33 o 8 12 0 7.37 60.07 43.50 o 9 12 0 1.55 -45.57 49.71 o 10 12 0 55.37 39.35 49.71 o 1 13 0 1.54 42.98 20.85 o 2 13 0 164.14 96.68 31.07 o 3 13 0 43.36 21.93 30.03 o 4 13 0 258.69 138.01 52.82 o 5 13 0 1.53 9.52 27.07 o 6 13 0 19.75 -20.77 26.83 o 7 13 0 8.03 -2.07 58.00 o 8 13 0 1.49 39.35 60.07 o 0 14 0 26.08 12.43 60.07 o 1 14 0 0.32 6.63 27.57 o 2 14 0 3.07 -19.98 21.83 o 3 14 0 0.77 -2.25 31.36 o 4 14 0 19.52 -7.04 28.32 o 5 14 0 0.82 47.64 62.14 o 6 14 0 0.09 -2.07 45.57 o 7 14 0 6.48 0.00 51.78 o 1 15 0 0.17 41.01 47.45 o 2 15 0 0.15 43.50 51.98 o 3 15 0 0.01 -29.06 46.69 o 4 15 0 3.06 -12.43 58.00 o 5 15 0 0.13 39.35 53.85 o -15 1 1 0.29 -20.01 45.57 o -14 1 1 22.90 37.28 40.39 o -13 1 1 0.90 1.62 26.36 o -12 1 1 25.92 16.57 16.25 o -11 1 1 63.91 61.38 11.44 o -10 1 1 13.40 4.83 5.56 o -9 1 1 727.43 791.81 17.92 o -8 1 1 172.06 162.38 8.43 o -7 1 1 896.49 915.32 18.26 o -6 1 1 4.01 -0.41 3.45 o -5 1 1 598.28 609.71 9.94 o -4 1 1 44.30 34.21 2.93 o -3 1 1 13.05 17.97 2.07 o -2 1 1 5.32 4.14 1.46 o -1 1 1 9.43 10.36 1.46 o 0 1 1 16.14 20.71 1.46 o 1 1 1 2.94 4.14 1.46 o 2 1 1 74.85 78.71 2.93 o 3 1 1 150.84 126.49 4.14 o 4 1 1 490.89 537.75 11.39 o 5 1 1 81.71 74.57 4.39 o 6 1 1 1398.68 1464.49 20.50 o 7 1 1 79.19 75.73 5.86 o 8 1 1 323.23 303.08 12.43 o 9 1 1 0.32 -6.47 6.47 o 10 1 1 1.82 3.01 7.96 o 11 1 1 11.98 16.11 12.94 o 12 1 1 10.98 22.67 17.62 o 13 1 1 26.38 -12.59 26.35 o 14 1 1 0.31 6.53 28.53 o -15 2 1 20.39 20.80 35.68 o -14 2 1 0.68 -2.82 59.03 o -13 2 1 33.41 8.06 19.41 o -12 2 1 7.55 23.47 19.68 o -11 2 1 69.82 46.00 14.82 o -10 2 1 268.29 284.35 13.86 o -9 2 1 26.00 18.27 7.96 o -8 2 1 379.73 418.00 10.66 o -7 2 1 1.87 5.39 6.21 o -6 2 1 944.90 820.79 13.40 o -5 2 1 44.05 50.59 3.71 o -4 2 1 179.46 169.85 3.71 o -3 2 1 175.11 162.76 5.18 o -2 2 1 13.61 19.73 1.46 o -1 2 1 456.27 377.46 5.18 o 0 2 1 177.61 166.80 3.11 o 1 2 1 706.39 662.61 9.44 o 2 2 1 227.82 234.58 5.18 o 3 2 1 134.03 95.46 4.14 o 4 2 1 270.03 275.73 8.29 o 5 2 1 38.29 26.93 3.45 o 6 2 1 145.98 110.13 6.21 o 7 2 1 480.84 501.12 24.86 o 8 2 1 6.62 2.53 6.47 o 9 2 1 27.77 24.86 7.32 o 10 2 1 3.77 3.45 8.43 o 11 2 1 1.20 -13.92 13.92 o 12 2 1 110.03 51.11 23.68 o 13 2 1 2.69 7.22 20.98 o 14 2 1 20.28 -6.02 40.57 o -15 3 1 13.20 -30.34 30.34 o -14 3 1 53.53 104.48 36.27 o -13 3 1 1.90 14.17 21.83 o -12 3 1 5.28 43.20 49.71 o -11 3 1 12.27 16.57 14.82 o -10 3 1 53.25 32.37 7.19 o -9 3 1 78.26 74.25 6.21 o -8 3 1 62.18 53.65 3.93 o -7 3 1 807.05 751.66 17.61 o -6 3 1 179.13 180.07 6.89 o -5 3 1 630.85 606.35 17.61 o -4 3 1 957.54 1023.49 16.57 o -3 3 1 4.09 3.45 2.07 o -2 3 1 3406.82 3329.82 38.79 o -1 3 1 162.84 213.36 4.39 o 0 3 1 1455.63 1206.83 18.26 o 1 3 1 2008.80 1896.98 46.60 o 2 3 1 36.62 29.59 4.14 o 3 3 1 699.97 635.62 9.94 o 4 3 1 519.50 494.37 9.44 o 5 3 1 1.27 4.14 2.93 o 6 3 1 76.37 85.01 6.21 o 7 3 1 41.83 41.71 11.39 o 8 3 1 75.57 60.14 5.86 o 9 3 1 1.73 -6.59 7.19 o 10 3 1 6.47 9.42 7.19 o 11 3 1 40.76 42.46 15.72 o 12 3 1 17.17 17.22 20.18 o 13 3 1 23.15 46.83 25.48 o 14 3 1 4.05 -2.27 37.81 o -14 4 1 7.26 33.33 30.66 o -13 4 1 90.77 97.51 37.28 o -12 4 1 0.14 18.64 24.08 o -11 4 1 36.22 29.69 15.27 o -10 4 1 6.53 3.11 12.23 o -9 4 1 100.61 98.24 7.41 o -8 4 1 16.97 12.43 5.71 o -7 4 1 556.46 586.92 20.71 o -6 4 1 1609.27 1389.04 24.77 o -5 4 1 954.56 1008.76 17.58 o -4 4 1 966.58 1017.10 13.40 o -3 4 1 113.76 112.46 8.29 o -2 4 1 100.24 95.93 3.45 o -1 4 1 1293.97 1083.88 15.33 o 0 4 1 918.36 823.05 40.39 o 1 4 1 461.98 428.77 8.79 o 2 4 1 44.57 53.81 7.25 o 3 4 1 41.38 43.09 5.18 o 4 4 1 433.69 396.55 15.53 o 5 4 1 884.17 820.32 19.68 o 6 4 1 180.05 143.18 11.39 o 7 4 1 461.92 505.07 22.78 o 8 4 1 102.97 114.73 12.38 o 9 4 1 70.26 70.42 11.72 o 10 4 1 12.78 22.54 12.38 o 11 4 1 32.95 7.29 18.64 o 12 4 1 138.02 132.80 26.64 o 13 4 1 0.21 -15.35 70.42 o 14 4 1 26.06 57.86 42.74 o -14 5 1 118.86 80.18 58.00 o -13 5 1 7.70 -31.84 31.84 o -12 5 1 149.69 153.91 23.58 o -11 5 1 43.03 56.06 25.89 o -10 5 1 462.42 455.58 25.67 o -9 5 1 393.59 372.43 15.99 o -8 5 1 28.70 17.95 8.43 o -7 5 1 611.30 497.98 20.71 o -6 5 1 841.10 777.89 17.58 o -5 5 1 164.02 166.75 8.79 o -4 5 1 648.69 684.72 12.94 o -3 5 1 16.23 13.46 5.18 o -2 5 1 3107.95 2972.16 50.75 o -1 5 1 1910.90 1835.17 63.17 o 0 5 1 775.72 852.67 14.43 o 1 5 1 2547.83 2349.43 101.49 o 2 5 1 95.69 77.39 14.50 o 3 5 1 1782.07 1735.43 53.85 o 4 5 1 979.41 853.94 14.43 o 5 5 1 670.71 598.06 27.96 o 6 5 1 1270.42 1346.24 23.35 o 7 5 1 146.04 111.19 12.43 o 8 5 1 499.24 504.08 30.03 o 9 5 1 100.91 97.67 10.91 o 10 5 1 79.81 105.24 27.96 o 11 5 1 217.49 190.42 44.53 o 12 5 1 0.90 18.45 23.82 o 13 5 1 39.37 22.09 38.32 o 14 5 1 0.12 15.51 29.45 o -14 6 1 18.33 -3.60 32.85 o -13 6 1 169.31 182.80 60.07 o -12 6 1 81.72 79.87 27.96 o -11 6 1 377.15 320.84 26.93 o -10 6 1 1018.23 951.48 78.71 o -9 6 1 338.30 339.30 20.71 o -8 6 1 439.43 421.52 19.68 o -7 6 1 73.65 66.04 10.91 o -6 6 1 273.40 217.75 11.44 o -5 6 1 1195.29 1161.95 17.85 o -4 6 1 46.93 57.37 14.50 o -3 6 1 2264.88 2202.85 30.76 o -2 6 1 545.70 575.20 11.88 o -1 6 1 1488.47 1589.60 38.32 o 0 6 1 2175.26 2016.50 68.35 o 1 6 1 379.63 436.51 9.44 o 2 6 1 4967.32 5043.89 127.39 o 3 6 1 46.17 37.40 5.86 o 4 6 1 3460.94 3489.80 51.70 o 5 6 1 123.34 101.09 5.56 o 6 6 1 148.40 178.35 10.36 o 7 6 1 1246.16 1235.34 30.65 o 8 6 1 230.75 193.62 19.68 o 9 6 1 555.87 610.84 40.39 o 10 6 1 214.92 201.78 35.21 o 11 6 1 180.36 188.47 27.97 o 12 6 1 172.60 113.55 25.40 o 13 6 1 2.24 10.60 28.51 o -13 7 1 0.47 7.33 32.95 o -12 7 1 90.96 53.85 26.36 o -11 7 1 221.31 216.76 23.35 o -10 7 1 323.00 264.47 23.35 o -9 7 1 1275.15 1252.84 44.77 o -8 7 1 252.48 205.28 22.78 o -7 7 1 1255.96 1334.07 56.96 o -6 7 1 103.10 123.07 21.75 o -5 7 1 319.87 350.86 10.34 o -4 7 1 2535.13 2682.17 42.30 o -3 7 1 0.69 3.62 5.33 o -2 7 1 4176.96 4284.52 67.32 o -1 7 1 238.44 327.85 12.43 o 0 7 1 1044.41 1191.22 34.18 o 1 7 1 3575.41 3612.07 210.24 o 2 7 1 1.68 0.00 4.97 o 3 7 1 3124.36 3135.73 136.71 o 4 7 1 566.00 483.94 14.91 o 5 7 1 198.45 229.92 9.94 o 6 7 1 518.04 555.18 27.96 o 7 7 1 10.38 18.89 12.38 o 8 7 1 833.58 846.27 31.82 o 9 7 1 345.17 292.70 19.73 o 10 7 1 131.88 130.11 21.39 o 11 7 1 118.62 99.79 21.20 o 12 7 1 8.49 -9.16 22.57 o 13 7 1 31.79 18.75 29.26 o -13 8 1 120.42 174.45 46.88 o -12 8 1 7.62 28.19 29.24 o -11 8 1 38.43 5.57 20.90 o -10 8 1 194.13 189.04 74.57 o -9 8 1 4.30 3.55 14.91 o -8 8 1 310.04 412.41 24.13 o -7 8 1 3.34 3.11 11.72 o -6 8 1 807.64 930.97 39.35 o -5 8 1 1428.36 1469.84 75.60 o -4 8 1 448.00 477.80 16.25 o -3 8 1 1907.58 2025.98 39.26 o -2 8 1 2.24 4.97 8.29 o -1 8 1 1119.14 1182.31 19.96 o 0 8 1 327.55 371.72 41.43 o 1 8 1 391.56 431.71 17.61 o 2 8 1 1568.56 1684.48 35.43 o 3 8 1 74.82 63.71 7.19 o 4 8 1 746.68 735.31 23.44 o 5 8 1 98.27 109.14 29.00 o 6 8 1 37.00 30.09 5.90 o 7 8 1 169.89 118.24 15.33 o 8 8 1 3.22 6.76 16.57 o 9 8 1 211.66 210.88 42.46 o 10 8 1 80.64 109.86 21.39 o 11 8 1 37.01 37.34 33.14 o 12 8 1 70.54 33.97 55.93 o -12 9 1 68.68 82.85 43.50 o -11 9 1 23.25 45.57 26.36 o -10 9 1 77.74 45.27 25.35 o -9 9 1 264.44 327.60 76.64 o -8 9 1 19.75 9.46 26.93 o -7 9 1 454.68 492.51 25.35 o -6 9 1 466.55 493.79 39.35 o -5 9 1 50.82 50.35 9.26 o -4 9 1 900.03 1115.67 85.96 o -3 9 1 49.92 48.84 11.39 o -2 9 1 1920.73 2089.15 64.21 o -1 9 1 185.08 196.53 13.61 o 0 9 1 312.53 335.55 8.29 o 1 9 1 579.39 673.17 20.71 o 2 9 1 18.08 23.60 16.57 o 3 9 1 544.13 568.53 37.28 o 4 9 1 120.96 132.98 11.12 o 5 9 1 248.28 249.44 33.14 o 6 9 1 196.06 232.52 25.89 o 7 9 1 0.65 17.30 12.38 o 8 9 1 76.56 59.01 15.91 o 9 9 1 118.95 113.66 27.96 o 10 9 1 75.75 74.55 58.00 o 11 9 1 115.63 107.31 59.03 o 12 9 1 0.02 6.41 39.35 o -12 10 1 24.66 37.28 43.50 o -11 10 1 89.94 31.07 43.50 o -10 10 1 148.55 98.03 32.18 o -9 10 1 3.65 3.68 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