#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:03:11 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180912 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/53/2105308.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105308_Fobs loop_ _publ_author_name 'St\"oger, Berthold' 'Kautny, Paul' 'Lumpi, Daniel' 'Zobetz, Erich' 'Fr\"ohlich, Johannes' _publ_section_title ; Solvatomorphism of 9,9'-[1,3,4-thiadiazole-2,5-diylbis(2,3-thiophendiyl-4,1-phenylene)]bis[9H-carbazole]: isostructurality, modularity and order--disorder theory ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 667 _journal_page_last 676 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 91.7802(12) _cell_angle_gamma 90 _cell_length_a 15.3042(3) _cell_length_b 10.0019(2) _cell_length_c 47.6862(10) _exptl_crystal_F_000 3208 _reflns_d_resolution_high 0.7683 _cod_data_source_file ry5046hemi_dcmsup7.hkl _cod_data_source_block hemi_dcm #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 410.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 165.57 -3.54 3.54 < 2 0 0 2000.06 1925.03 33.65 o 3 0 0 811.82 814.64 23.02 o 4 0 0 6738.67 6908.52 100.94 o 5 0 0 953.38 1053.72 26.56 o 6 0 0 7253.16 7531.89 93.86 o 7 0 0 3661.19 4133.42 60.21 o 8 0 0 12127.60 13372.50 159.39 o 9 0 0 9062.36 10126.30 127.51 o 10 0 0 23705.30 24058.50 295.75 o 11 0 0 3157.57 2945.11 63.75 o 12 0 0 210.31 198.35 30.11 o 13 0 0 138.44 177.10 31.88 o 14 0 0 20761.70 20807.00 309.92 o 15 0 0 2077.02 1916.18 69.07 o 16 0 0 3751.15 3798.71 102.72 o 17 0 0 11798.20 12481.70 258.56 o 18 0 0 1.12 -15.94 53.13 < 19 0 0 42.01 1.77 56.67 < 1 1 0 975.15 837.66 17.71 o 2 1 0 14486.10 14761.00 157.62 o 3 1 0 28152.60 27446.30 263.87 o 4 1 0 840.47 853.60 15.94 o 5 1 0 11526.00 11132.30 95.63 o 6 1 0 1986.64 1925.03 26.56 o 7 1 0 1402.74 1227.28 23.02 o 8 1 0 7460.27 7020.09 67.30 o 9 1 0 834.50 655.26 19.48 o 10 1 0 0.94 5.31 14.17 < 11 1 0 635.65 653.48 24.79 o 12 1 0 96.34 132.82 21.25 o 13 1 0 7422.49 7347.71 85.01 o 14 1 0 239.47 267.42 26.56 o 15 1 0 1.54 -10.63 26.56 < 16 1 0 1171.61 1112.16 44.27 o 17 1 0 185.53 279.81 35.42 o 18 1 0 938.44 924.44 58.44 o 19 1 0 1665.56 1965.77 85.01 o 0 2 0 1861.83 1951.60 58.44 o 1 2 0 8915.21 8992.93 132.82 o 2 2 0 1303.80 1489.38 24.79 o 3 2 0 28840.50 30258.60 270.96 o 4 2 0 2742.73 2870.73 33.65 o 5 2 0 9219.49 9490.58 88.55 o 6 2 0 502.33 456.91 14.17 o 7 2 0 3405.79 3131.06 37.19 o 8 2 0 395.24 378.98 15.94 o 9 2 0 2871.68 2941.56 37.19 o 10 2 0 3756.04 3719.02 44.27 o 11 2 0 53.35 38.96 17.71 < 12 2 0 660.12 632.23 26.56 o 13 2 0 201.09 143.45 23.02 o 14 2 0 13.47 24.79 24.79 < 15 2 0 13.98 -14.17 26.56 < 16 2 0 1842.49 1928.58 60.21 o 17 2 0 1701.35 1817.01 69.07 o 18 2 0 2547.40 2725.51 92.09 o 19 2 0 1330.20 1455.73 81.46 o 1 3 0 22159.80 21936.90 240.85 o 2 3 0 33700.60 34039.60 297.52 o 3 3 0 3.58 -7.08 10.63 < 4 3 0 670.28 740.26 15.94 o 5 3 0 6793.51 7131.66 65.53 o 6 3 0 1754.91 1701.89 26.56 o 7 3 0 242.79 325.86 14.17 o 8 3 0 11.07 8.85 12.40 < 9 3 0 285.56 228.45 15.94 o 10 3 0 962.69 1113.93 26.56 o 11 3 0 172.30 214.29 21.25 o 12 3 0 5.14 -17.71 21.25 < 13 3 0 425.45 402.01 30.11 o 14 3 0 194.26 159.39 33.65 o 15 3 0 441.50 414.40 40.73 o 16 3 0 318.07 456.91 47.82 o 17 3 0 373.50 366.59 47.82 o 18 3 0 795.39 722.55 58.44 o 19 3 0 3.84 60.21 46.04 < 0 4 0 2122.41 1921.49 54.90 o 1 4 0 12334.20 11886.70 125.74 o 2 4 0 3001.19 3178.87 40.73 o 3 4 0 1770.03 1877.22 28.34 o 4 4 0 22813.60 24317.10 224.91 o 5 4 0 705.14 809.33 19.48 o 6 4 0 463.40 485.24 15.94 o 7 4 0 160.25 260.33 14.17 o 8 4 0 6782.09 6805.80 63.75 o 9 4 0 7506.78 7402.61 88.55 o 10 4 0 357.08 435.66 26.56 o 11 4 0 2321.68 2268.60 53.13 o 12 4 0 347.75 465.76 37.19 o 13 4 0 1398.20 1406.14 54.90 o 14 4 0 304.35 318.77 37.19 o 15 4 0 2512.85 2548.41 70.84 o 16 4 0 372.27 442.74 47.82 o 17 4 0 804.57 988.20 60.21 o 18 4 0 1334.54 1400.83 70.84 o 1 5 0 11781.20 11799.90 127.51 o 2 5 0 26.25 12.40 12.40 < 3 5 0 42.36 42.50 14.17 o 4 5 0 8397.69 8282.78 83.24 o 5 5 0 8371.44 8284.55 86.78 o 6 5 0 423.37 511.81 21.25 o 7 5 0 8544.10 8227.88 88.55 o 8 5 0 297.84 325.86 21.25 o 9 5 0 2.12 19.48 19.48 < 10 5 0 3384.28 3306.38 58.44 o 11 5 0 864.22 828.81 37.19 o 12 5 0 245.74 279.81 30.11 o 13 5 0 5933.04 5780.41 93.86 o 14 5 0 124.06 115.11 30.11 o 15 5 0 496.01 458.68 37.19 o 16 5 0 1531.84 1533.65 63.75 o 17 5 0 838.82 910.27 54.90 o 18 5 0 3285.89 3488.79 99.17 o 0 6 0 32638.50 34289.30 525.97 o 1 6 0 8480.31 7930.36 97.40 o 2 6 0 4372.03 4259.16 54.90 o 3 6 0 1902.67 2079.11 37.19 o 4 6 0 1672.80 1269.78 30.11 o 5 6 0 3.13 -12.40 15.94 < 6 6 0 848.98 821.72 24.79 o 7 6 0 1771.05 1593.86 38.96 o 8 6 0 169.64 162.93 23.02 o 9 6 0 12.30 37.19 23.02 < 10 6 0 199.31 146.99 26.56 o 11 6 0 47.08 30.11 26.56 < 12 6 0 46.41 -5.31 26.56 < 13 6 0 19.18 -15.94 28.34 < 14 6 0 41.15 26.56 31.88 < 15 6 0 1473.29 1445.10 58.44 o 16 6 0 550.84 515.35 46.04 o 17 6 0 3.96 40.73 40.73 < 1 7 0 4820.69 4693.04 72.61 o 2 7 0 814.26 743.80 31.88 o 3 7 0 2016.98 1999.41 42.50 o 4 7 0 1854.13 1755.02 38.96 o 5 7 0 937.71 959.86 31.88 o 6 7 0 3948.92 3821.73 58.44 o 7 7 0 3091.47 3058.45 58.44 o 8 7 0 87.17 95.63 24.79 o 9 7 0 1045.47 1048.41 40.73 o 10 7 0 37.32 46.04 26.56 < 11 7 0 249.11 274.50 31.88 o 12 7 0 1787.44 1758.56 54.90 o 13 7 0 750.27 687.13 40.73 o 14 7 0 770.98 699.53 46.04 o 15 7 0 117.85 95.63 38.96 < 16 7 0 740.20 756.20 53.13 o 0 8 0 46.18 100.94 47.82 < 1 8 0 51.24 37.19 31.88 < 2 8 0 1.37 28.34 31.88 < 3 8 0 3299.68 3193.04 65.53 o 4 8 0 93.13 95.63 24.79 o 5 8 0 41.89 76.15 26.56 < 6 8 0 4011.75 3609.22 67.30 o 7 8 0 1625.01 1491.15 42.50 o 8 8 0 652.23 683.59 35.42 o 9 8 0 3167.41 3051.36 63.75 o 10 8 0 83.38 35.42 28.34 < 11 8 0 1.58 30.11 30.11 < 12 8 0 220.68 180.64 33.65 o 13 8 0 825.51 780.99 44.27 o 14 8 0 696.62 678.28 47.82 o 15 8 0 265.50 313.46 44.27 o 1 9 0 142.58 177.10 35.42 o 2 9 0 7501.83 6696.00 129.28 o 3 9 0 1427.57 1469.90 63.75 o 4 9 0 290.27 290.44 42.50 o 5 9 0 5579.39 5273.92 109.80 o 6 9 0 49.99 15.94 28.34 < 7 9 0 467.61 481.70 37.19 o 8 9 0 4776.50 4870.14 95.63 o 9 9 0 1121.34 1406.14 53.13 o 10 9 0 552.10 543.68 38.96 o 11 9 0 48.96 10.63 30.11 < 12 9 0 0.30 23.02 31.88 < 13 9 0 1347.07 1358.33 58.44 o 14 9 0 4.99 30.11 37.19 < 0 10 0 2663.13 2672.38 100.94 o 1 10 0 417.72 440.97 46.04 o 2 10 0 449.06 449.82 46.04 o 3 10 0 1.02 46.04 40.73 < 4 10 0 505.32 595.04 56.67 o 5 10 0 4953.05 4648.77 120.43 o 6 10 0 144.94 162.93 42.50 o 7 10 0 2787.17 2718.42 85.01 o 8 10 0 613.28 529.52 56.67 o 9 10 0 230.44 175.32 44.27 o 10 10 0 9.62 74.38 37.19 < 11 10 0 281.06 260.33 42.50 o 12 10 0 219.99 317.00 44.27 o 1 11 0 18.08 46.04 46.04 < 2 11 0 124.77 145.22 44.27 o 3 11 0 891.12 841.21 60.21 o 4 11 0 3329.84 2927.40 99.17 o 5 11 0 2138.83 2110.98 92.09 o 6 11 0 1518.10 1563.76 81.46 o 7 11 0 1808.71 1792.21 76.15 o 8 11 0 0.33 24.79 47.82 < 9 11 0 49.19 24.79 47.82 < 10 11 0 270.67 340.02 56.67 o 0 12 0 2210.69 2149.95 152.30 o 1 12 0 889.02 777.45 74.38 o 2 12 0 36.08 -26.56 49.59 < 3 12 0 2146.45 2452.78 99.17 o 4 12 0 99.31 132.82 53.13 < 5 12 0 434.52 552.54 63.75 o 6 12 0 14.71 72.61 51.36 < 7 12 0 162.54 187.72 56.67 o -19 1 1 925.07 878.40 65.53 o -18 1 1 166.48 327.63 46.04 o -17 1 1 447.95 458.68 37.19 o -16 1 1 189.10 196.58 30.11 o -15 1 1 2021.16 2217.24 53.13 o -14 1 1 839.53 912.04 33.65 o -13 1 1 1678.31 1751.48 38.96 o -12 1 1 5909.41 5672.38 69.07 o -11 1 1 4769.20 4774.51 60.21 o -10 1 1 30.84 90.32 14.17 o -9 1 1 1843.59 1786.90 28.34 o -8 1 1 1223.83 1306.97 23.02 o -7 1 1 6103.70 6216.07 60.21 o -6 1 1 3.23 0.00 10.63 < -5 1 1 3124.76 3285.13 35.42 o -4 1 1 3537.09 3116.89 33.65 o -3 1 1 554.12 502.95 12.40 o -2 1 1 5741.88 5426.22 58.44 o -1 1 1 5.95 15.94 7.08 < 1 1 1 8635.62 8341.22 166.47 o 2 1 1 89.97 111.57 7.08 o 3 1 1 16594.70 17219.00 168.24 o 4 1 1 1628.36 1468.13 21.25 o 5 1 1 13596.20 12981.10 113.34 o 6 1 1 2306.87 2236.72 30.11 o 7 1 1 4948.96 4868.37 49.59 o 8 1 1 4470.47 4434.48 47.82 o 9 1 1 4639.34 4758.57 53.13 o 10 1 1 93.27 93.86 14.17 o 11 1 1 3087.82 3014.17 46.04 o 12 1 1 115.30 95.63 19.48 o 13 1 1 1425.47 1544.28 37.19 o 14 1 1 3682.61 3695.99 60.21 o 15 1 1 1112.85 1145.81 40.73 o 16 1 1 554.35 545.46 38.96 o 17 1 1 487.38 602.13 40.73 o 18 1 1 2412.99 2617.48 81.46 o 19 1 1 54.91 111.57 49.59 < -19 2 1 2192.98 2180.05 97.40 o -18 2 1 107.34 184.18 47.82 o -17 2 1 87.82 67.30 38.96 < -16 2 1 50.67 113.34 31.88 o -15 2 1 39.88 70.84 28.34 < -14 2 1 664.02 687.13 31.88 o -13 2 1 1984.28 1951.60 44.27 o -12 2 1 0.30 19.48 19.48 < -11 2 1 8.25 7.08 15.94 < -10 2 1 3058.21 3028.34 38.96 o -9 2 1 948.10 1030.70 23.02 o -8 2 1 218.05 237.31 14.17 o -7 2 1 16235.40 16845.40 143.45 o -6 2 1 2709.17 2698.94 31.88 o -5 2 1 747.68 780.99 17.71 o -4 2 1 21390.10 20939.80 177.10 o -3 2 1 14983.00 14700.70 131.05 o -2 2 1 3107.91 3139.91 40.73 o -1 2 1 407.61 364.82 17.71 o 0 2 1 19032.10 19064.40 274.50 o 1 2 1 19801.20 19284.00 233.77 o 2 2 1 41992.90 43011.30 456.91 o 3 2 1 22061.60 21880.20 191.26 o 4 2 1 20910.50 21526.00 187.72 o 5 2 1 2307.51 2511.22 31.88 o 6 2 1 7653.45 8089.75 76.15 o 7 2 1 5282.94 5328.82 54.90 o 8 2 1 8851.72 8838.86 81.46 o 9 2 1 3295.69 3531.29 42.50 o 10 2 1 1437.64 1613.34 30.11 o 11 2 1 7033.49 6550.78 72.61 o 12 2 1 1905.88 1880.76 38.96 o 13 2 1 775.41 827.04 31.88 o 14 2 1 64.12 -10.63 23.02 < 15 2 1 36.87 67.30 26.56 < 16 2 1 1248.65 1138.73 53.13 o 17 2 1 3176.83 3338.26 92.09 o 18 2 1 10.73 109.80 46.04 < 19 2 1 526.75 607.44 65.53 o -19 3 1 6.33 23.02 46.04 < -18 3 1 25.22 65.53 44.27 < -17 3 1 412.77 378.98 49.59 o -16 3 1 1426.71 1661.16 67.30 o -15 3 1 156.90 230.23 38.96 o -14 3 1 56.14 92.09 33.65 < -13 3 1 1875.52 1840.03 51.36 o -12 3 1 0.39 -17.71 21.25 < -11 3 1 9499.39 8895.53 92.09 o -10 3 1 7.56 21.25 15.94 < -9 3 1 838.75 974.03 21.25 o -8 3 1 819.17 968.72 21.25 o -7 3 1 4928.86 5528.94 53.13 o -6 3 1 302.49 191.26 14.17 o -5 3 1 10810.90 11405.00 97.40 o -4 3 1 55.85 61.98 10.63 o -3 3 1 324.84 263.87 12.40 o -2 3 1 4280.06 4234.37 47.82 o -1 3 1 34572.80 33526.00 363.05 o 0 3 1 2117.30 1971.08 35.42 o 1 3 1 9767.44 8810.53 104.49 o 2 3 1 4343.12 4576.16 51.36 o 3 3 1 1848.24 1948.06 26.56 o 4 3 1 2187.76 2164.11 28.34 o 5 3 1 83.02 129.28 12.40 o 6 3 1 42.11 49.59 12.40 o 7 3 1 1426.37 1457.50 23.02 o 8 3 1 1253.82 1269.78 24.79 o 9 3 1 4962.44 5135.78 54.90 o 10 3 1 3316.06 3258.57 44.27 o 11 3 1 1383.73 1315.82 31.88 o 12 3 1 2417.17 2226.10 46.04 o 13 3 1 97.64 155.84 28.34 o 14 3 1 1398.08 1269.78 53.13 o 15 3 1 775.21 655.26 44.27 o 16 3 1 83.97 104.49 38.96 < 17 3 1 36.07 44.27 42.50 < 18 3 1 303.18 396.70 51.36 o 19 3 1 2360.49 2427.99 92.09 o -18 4 1 355.22 451.60 53.13 o -17 4 1 1412.84 1360.10 67.30 o -16 4 1 550.87 510.04 46.04 o -15 4 1 29.68 -5.31 33.65 < -14 4 1 1107.43 1190.09 53.13 o -13 4 1 9958.90 9400.26 148.76 o -12 4 1 4187.13 4021.85 81.46 o -11 4 1 6928.15 6853.62 100.94 o -10 4 1 1335.71 1252.07 37.19 o -9 4 1 4055.65 4223.74 56.67 o -8 4 1 13993.80 14119.90 118.65 o -7 4 1 4499.63 5318.19 51.36 o -6 4 1 5200.02 4992.34 51.36 o -5 4 1 2286.39 2401.42 33.65 o -4 4 1 166.04 166.47 14.17 o -3 4 1 34792.10 35173.00 299.29 o -2 4 1 814.21 855.37 21.25 o -1 4 1 4200.38 4631.06 58.44 o 0 4 1 5923.35 5801.67 72.61 o 1 4 1 6881.98 7117.49 81.46 o 2 4 1 746.73 750.89 17.71 o 3 4 1 1702.33 1820.55 26.56 o 4 4 1 10984.70 10801.10 102.72 o 5 4 1 25.14 56.67 14.17 o 6 4 1 12825.30 12885.50 116.88 o 7 4 1 15139.70 14971.70 123.97 o 8 4 1 628.31 706.61 19.48 o 9 4 1 390.23 322.32 23.02 o 10 4 1 112.18 85.01 21.25 o 11 4 1 290.47 295.75 28.34 o 12 4 1 3525.47 3373.68 74.38 o 13 4 1 16.49 -3.54 30.11 < 14 4 1 2838.09 2771.55 72.61 o 15 4 1 2080.13 2165.88 67.30 o 16 4 1 282.05 232.00 44.27 o 17 4 1 82.47 77.92 42.50 < 18 4 1 1702.70 1983.48 81.46 o -18 5 1 2544.92 2879.58 86.78 o -17 5 1 1252.21 1209.57 60.21 o -16 5 1 978.98 982.88 54.90 o -15 5 1 15.40 -23.02 31.88 < -14 5 1 49.07 42.50 30.11 < -13 5 1 589.71 543.68 35.42 o -12 5 1 835.32 699.53 37.19 o -11 5 1 10528.20 9687.15 131.05 o -10 5 1 9.28 40.73 23.02 < -9 5 1 3140.28 2883.12 49.59 o -8 5 1 2231.15 2084.42 38.96 o -7 5 1 1024.87 1237.90 28.34 o -6 5 1 2430.16 2583.83 38.96 o -5 5 1 193.94 152.30 15.94 o -4 5 1 9682.15 9561.41 90.32 o -3 5 1 11188.20 10740.90 100.94 o -2 5 1 7120.65 7227.29 79.69 o -1 5 1 6290.95 5867.19 72.61 o 0 5 1 979.28 966.94 26.56 o 1 5 1 2526.42 2629.88 40.73 o 2 5 1 1920.19 1907.32 30.11 o 3 5 1 288.67 311.69 15.94 o 4 5 1 1279.03 1186.54 24.79 o 5 5 1 382.90 402.01 19.48 o 6 5 1 7305.07 7188.33 77.92 o 7 5 1 9211.39 9170.03 95.63 o 8 5 1 66.82 79.69 17.71 o 9 5 1 8496.36 8277.47 102.72 o 10 5 1 8887.66 8582.07 108.03 o 11 5 1 188.89 132.82 26.56 o 12 5 1 7318.18 7069.67 106.26 o 13 5 1 2702.35 2675.92 61.98 o 14 5 1 732.63 786.31 40.73 o 15 5 1 776.58 876.63 44.27 o 16 5 1 2400.60 2569.66 76.15 o 17 5 1 16.57 -35.42 37.19 < 18 5 1 69.94 88.55 40.73 < -17 6 1 1135.16 1122.79 60.21 o -16 6 1 103.29 182.41 40.73 o -15 6 1 628.66 649.94 46.04 o -14 6 1 384.19 435.66 37.19 o -13 6 1 350.02 309.92 33.65 o -12 6 1 229.49 201.89 30.11 o -11 6 1 15.67 30.11 26.56 < -10 6 1 3388.21 3286.90 63.75 o -9 6 1 2884.40 2803.43 56.67 o -8 6 1 8.57 -5.31 21.25 < -7 6 1 238.69 256.79 23.02 o -6 6 1 14.81 15.94 15.94 < -5 6 1 814.17 832.35 24.79 o -4 6 1 3094.58 3235.54 46.04 o -3 6 1 75.36 141.68 15.94 o -2 6 1 2683.72 2980.53 46.04 o -1 6 1 1710.68 1670.02 35.42 o 0 6 1 3432.74 3757.98 60.21 o 1 6 1 54.14 67.30 17.71 o 2 6 1 2419.59 2275.68 35.42 o 3 6 1 2449.88 2628.10 40.73 o 4 6 1 27.94 30.11 17.71 < 5 6 1 270.53 290.44 19.48 o 6 6 1 302.41 363.05 19.48 o 7 6 1 1255.53 1276.86 33.65 o 8 6 1 5607.30 5426.22 77.92 o 9 6 1 69.30 77.92 24.79 o 10 6 1 261.73 203.66 28.34 o 11 6 1 747.62 874.85 38.96 o 12 6 1 451.18 396.70 33.65 o 13 6 1 879.19 842.98 42.50 o 14 6 1 2.75 46.04 30.11 < 15 6 1 367.90 306.38 38.96 o 16 6 1 525.66 547.23 47.82 o 17 6 1 6.70 122.20 40.73 o -16 7 1 130.92 230.23 44.27 o -15 7 1 22.92 53.13 35.42 < -14 7 1 217.41 242.62 37.19 o -13 7 1 36.63 104.49 31.88 o -12 7 1 923.77 887.25 42.50 o -11 7 1 1996.98 2011.81 56.67 o -10 7 1 410.75 364.82 31.88 o -9 7 1 1730.30 1519.48 46.04 o -8 7 1 612.09 680.05 33.65 o -7 7 1 7.59 37.19 23.02 < -6 7 1 5291.60 4707.21 67.30 o -5 7 1 203.80 191.26 23.02 o -4 7 1 3498.73 3403.79 53.13 o -3 7 1 1365.04 1353.01 35.42 o -2 7 1 21.16 -1.77 21.25 < -1 7 1 1764.95 1864.82 44.27 o 0 7 1 11993.40 11768.00 143.45 o 1 7 1 119.73 111.57 21.25 o 2 7 1 405.38 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2891.98 123.97 o -14 0 28 201.04 200.12 63.75 o -13 0 28 416.39 361.28 54.90 o -12 0 28 5853.70 6111.58 131.05 o -11 0 28 1.46 0.00 38.96 < -10 0 28 508.56 432.11 42.50 o -9 0 28 15327.50 14142.90 239.08 o -8 0 28 12736.40 12035.40 189.49 o -7 0 28 1629.03 1577.93 49.59 o -6 0 28 157.06 88.55 24.79 o -5 0 28 36008.60 34489.40 414.40 o -4 0 28 1249.01 1255.61 38.96 o -3 0 28 1679.31 1724.92 42.50 o -2 0 28 17103.90 16629.30 207.20 o -1 0 28 2189.82 2056.08 47.82 o 0 0 28 4748.27 5314.65 86.78 o 1 0 28 82.33 104.49 21.25 o 2 0 28 670.96 722.55 28.34 o 3 0 28 24388.80 25468.20 331.17 o 4 0 28 679.69 779.22 37.19 o 5 0 28 1103.70 979.34 40.73 o 6 0 28 2639.09 2605.08 69.07 o 7 0 28 98.68 161.16 31.88 o 8 0 28 3111.80 2987.61 77.92 o 9 0 28 3850.04 3396.70 86.78 o 10 0 28 14478.50 13988.80 239.08 o 11 0 28 1604.17 1521.25 67.30 o 12 0 28 13346.80 13105.10 232.00 o 13 0 28 2109.56 2022.44 77.92 o 14 0 28 904.82 952.78 70.84 o 15 0 28 239.88 212.51 53.13 o 16 0 28 2370.64 2323.50 111.57 o 17 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1840.41 1854.20 63.75 o 13 2 28 16.24 38.96 35.42 < 14 2 28 10.69 53.13 35.42 < 15 2 28 70.83 19.48 35.42 < 16 2 28 8.31 77.92 38.96 < 17 2 28 282.51 228.45 46.04 o -17 3 28 325.31 331.17 56.67 o -16 3 28 20.12 123.97 46.04 < -15 3 28 637.44 641.09 47.82 o -14 3 28 7.23 1.77 33.65 < -13 3 28 3141.69 2941.56 70.84 o -12 3 28 1.86 12.40 28.34 < -11 3 28 161.83 157.62 30.11 o -10 3 28 18896.70 17670.60 208.97 o -9 3 28 2752.71 2512.99 58.44 o -8 3 28 717.84 687.13 33.65 o -7 3 28 953.18 931.53 30.11 o -6 3 28 225.58 187.72 21.25 o -5 3 28 383.56 347.11 23.02 o -4 3 28 2121.96 2109.21 37.19 o -3 3 28 1532.16 1705.43 35.42 o -2 3 28 16306.90 16177.70 154.07 o -1 3 28 179.30 255.02 17.71 o 0 3 28 6486.70 6814.65 74.38 o 1 3 28 5.02 67.30 15.94 o 2 3 28 1035.02 1096.22 26.56 o 3 3 28 0.05 -42.50 17.71 < 4 3 28 717.23 706.61 30.11 o 5 3 28 5863.89 5775.10 90.32 o 6 3 28 3006.50 3102.72 61.98 o 7 3 28 1048.16 1151.12 42.50 o 8 3 28 4819.62 4627.52 88.55 o 9 3 28 17.63 60.21 30.11 < 10 3 28 266.75 270.96 35.42 o 11 3 28 103.02 85.01 33.65 < 12 3 28 983.91 807.56 47.82 o 13 3 28 29.42 47.82 35.42 < 14 3 28 13.04 21.25 33.65 < 15 3 28 2856.23 2752.07 77.92 o 16 3 28 659.18 660.57 53.13 o -16 4 28 927.87 823.50 61.98 o -15 4 28 145.17 162.93 46.04 o -14 4 28 689.25 664.11 53.13 o -13 4 28 1613.11 1622.20 63.75 o -12 4 28 38.24 106.26 31.88 o -11 4 28 13.09 23.02 26.56 < -10 4 28 25.47 65.53 26.56 < -9 4 28 323.63 478.16 33.65 o -8 4 28 253.16 267.42 28.34 o -7 4 28 560.04 511.81 31.88 o -6 4 28 5326.80 4990.57 67.30 o -5 4 28 371.67 361.28 23.02 o -4 4 28 1546.69 1457.50 33.65 o -3 4 28 1143.43 1094.45 31.88 o -2 4 28 67.26 92.09 19.48 o -1 4 28 2.06 28.34 17.71 < 0 4 28 3587.46 3600.36 53.13 o 1 4 28 5142.70 5440.39 65.53 o 2 4 28 21.95 65.53 19.48 o 3 4 28 3760.57 3757.98 56.67 o 4 4 28 146.54 145.22 23.02 o 5 4 28 918.86 975.80 38.96 o 6 4 28 79.69 58.44 26.56 < 7 4 28 467.29 425.03 31.88 o 8 4 28 6.94 24.79 28.34 < 9 4 28 24.92 -28.34 30.11 < 10 4 28 1007.31 927.98 47.82 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26.56 o 6 3 29 3998.41 3844.75 72.61 o 7 3 29 3262.40 3162.93 65.53 o 8 3 29 43.18 53.13 30.11 < 9 3 29 1431.10 1413.23 53.13 o 10 3 29 2204.44 2199.53 63.75 o 11 3 29 188.12 201.89 35.42 o 12 3 29 906.74 899.65 49.59 o 13 3 29 9.50 19.48 35.42 < 14 3 29 702.77 641.09 46.04 o 15 3 29 163.21 175.32 40.73 o 16 3 29 132.17 88.55 42.50 < -16 4 29 1125.01 1236.13 69.07 o -15 4 29 909.73 954.55 61.98 o -14 4 29 418.58 396.70 49.59 o -13 4 29 814.46 881.94 53.13 o -12 4 29 1571.88 1627.51 56.67 o -11 4 29 1278.32 1214.88 44.27 o -10 4 29 14.13 51.36 28.34 < -9 4 29 452.84 426.80 31.88 o -8 4 29 1865.31 1774.50 47.82 o -7 4 29 1747.14 1716.06 46.04 o -6 4 29 140.15 161.16 24.79 o -5 4 29 0.12 1.77 17.71 < -4 4 29 4301.51 4140.50 56.67 o -3 4 29 1824.54 1655.85 37.19 o -2 4 29 9441.04 9664.13 109.80 o -1 4 29 4831.42 4855.97 60.21 o 0 4 29 989.71 1089.14 30.11 o 1 4 29 5052.87 5307.57 67.30 o 2 4 29 4393.08 4167.07 60.21 o 3 4 29 521.80 573.79 26.56 o 4 4 29 988.52 906.73 35.42 o 5 4 29 308.03 320.54 30.11 o 6 4 29 387.67 432.11 31.88 o 7 4 29 3718.31 3704.85 72.61 o 8 4 29 452.41 423.26 35.42 o 9 4 29 560.66 529.52 38.96 o 10 4 29 2057.16 2077.34 61.98 o 11 4 29 97.66 92.09 37.19 < 12 4 29 657.03 703.07 51.36 o 13 4 29 4213.94 4067.90 92.09 o 14 4 29 7.84 -7.08 35.42 < 15 4 29 801.21 782.76 53.13 o 16 4 29 2630.58 2826.45 90.32 o -16 5 29 2815.42 2877.81 88.55 o -15 5 29 72.91 123.97 40.73 o -14 5 29 19.73 -10.63 35.42 < -13 5 29 2003.43 2153.49 69.07 o -12 5 29 3302.06 3269.19 77.92 o -11 5 29 146.95 131.05 33.65 o -10 5 29 37.79 51.36 31.88 < -9 5 29 1120.35 1062.58 46.04 o -8 5 29 959.46 903.19 44.27 o -7 5 29 424.42 324.09 33.65 o -6 5 29 3534.51 3476.39 63.75 o -5 5 29 0.85 -7.08 21.25 < -4 5 29 865.73 855.37 31.88 o -3 5 29 3319.29 3626.93 56.67 o -2 5 29 277.92 262.10 23.02 o -1 5 29 1105.75 1165.29 35.42 o 0 5 29 2102.96 2254.43 42.50 o 1 5 29 10982.20 10675.30 123.97 o 2 5 29 868.47 974.03 31.88 o 3 5 29 228.79 262.10 24.79 o 4 5 29 2230.81 2153.49 46.04 o 5 5 29 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5 44 1928.72 2123.38 85.01 o -5 5 44 2634.68 2484.66 86.78 o -4 5 44 5587.45 5178.29 113.34 o -3 5 44 59.61 189.49 46.04 o -2 5 44 159.40 157.62 42.50 o -1 5 44 251.67 214.29 38.96 o 0 5 44 197.20 180.64 38.96 o 1 5 44 1296.35 1243.21 56.67 o 2 5 44 757.81 642.86 46.04 o 3 5 44 999.98 1051.95 53.13 o 4 5 44 34.52 44.27 33.65 < 5 5 44 566.57 531.29 44.27 o 6 5 44 15.26 -12.40 35.42 < 7 5 44 547.83 488.79 46.04 o 8 5 44 4.51 8.85 37.19 < 9 5 44 304.05 332.94 44.27 o 10 5 44 242.65 258.56 44.27 o 11 5 44 745.92 726.09 54.90 o -11 6 44 350.03 331.17 61.98 o -10 6 44 0.32 104.49 46.04 < -9 6 44 463.10 541.91 58.44 o -8 6 44 21.32 24.79 46.04 < -7 6 44 822.83 883.71 63.75 o -6 6 44 764.81 802.24 60.21 o -5 6 44 991.61 972.26 61.98 o -4 6 44 1097.23 1009.45 63.75 o -3 6 44 605.20 651.71 61.98 o -2 6 44 1538.06 1423.85 63.75 o -1 6 44 1933.14 2038.38 81.46 o 0 6 44 45.40 23.02 42.50 < 1 6 44 160.46 189.49 40.73 o 2 6 44 3718.26 4080.29 99.17 o 3 6 44 734.76 816.41 51.36 o 4 6 44 773.67 756.20 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50 1395.00 1441.56 95.63 o 4 0 50 66.28 86.78 58.44 < 5 0 50 168.89 134.59 61.98 < 6 0 50 837.01 687.13 79.69 o 7 0 50 726.38 623.38 79.69 o 8 0 50 1162.26 951.01 90.32 o 9 0 50 58.81 106.26 67.30 < 10 0 50 85.87 141.68 67.30 < 11 0 50 1909.51 1988.79 122.20 o -12 1 50 840.09 894.34 72.61 o -11 1 50 651.09 687.13 65.53 o -10 1 50 33.25 60.21 49.59 < -9 1 50 985.92 1124.56 72.61 o -8 1 50 1.38 26.56 46.04 < -7 1 50 5514.00 5066.72 125.74 o -6 1 50 4470.98 3901.43 123.97 o -5 1 50 1477.13 1326.45 74.38 o -4 1 50 12.92 54.90 47.82 < -3 1 50 0.61 40.73 47.82 < -2 1 50 4.59 -5.31 40.73 < -1 1 50 889.13 1020.07 72.61 o 0 1 50 2206.22 2126.92 77.92 o 1 1 50 352.69 357.73 44.27 o 2 1 50 333.29 297.52 42.50 o 3 1 50 137.74 131.05 40.73 o 4 1 50 4993.43 4889.62 111.57 o 5 1 50 2.07 -10.63 40.73 < 6 1 50 25.83 100.94 44.27 < 7 1 50 56.05 88.55 44.27 < 8 1 50 1132.76 981.11 63.75 o 9 1 50 664.35 665.88 58.44 o 10 1 50 569.67 726.09 60.21 o 11 1 50 1430.12 1496.46 77.92 o -11 2 50 1365.64 1583.24 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3 50 3832.50 3618.07 95.63 o 2 3 50 1391.54 1455.73 69.07 o 3 3 50 39.15 -8.85 40.73 < 4 3 50 243.45 295.75 42.50 o 5 3 50 323.45 255.02 42.50 o 6 3 50 1165.13 1090.91 54.90 o 7 3 50 957.31 881.94 51.36 o 8 3 50 209.43 99.17 38.96 < 9 3 50 35.29 3.54 38.96 < 10 3 50 272.63 315.23 49.59 o -10 4 50 954.44 1041.32 69.07 o -9 4 50 359.22 320.54 53.13 o -8 4 50 118.53 170.01 49.59 o -7 4 50 189.13 205.43 44.27 o -6 4 50 380.86 476.39 53.13 o -5 4 50 3286.36 2962.82 92.09 o -4 4 50 66.41 83.24 42.50 < -3 4 50 25.37 61.98 42.50 < -2 4 50 244.58 325.86 49.59 o -1 4 50 251.11 173.55 44.27 o 0 4 50 57.37 44.27 42.50 < 1 4 50 1255.53 1283.95 63.75 o 2 4 50 3.95 100.94 42.50 < 3 4 50 1146.35 951.01 60.21 o 4 4 50 1895.62 1871.90 76.15 o 5 4 50 89.16 70.84 40.73 < 6 4 50 191.68 175.32 38.96 o 7 4 50 1461.14 1379.58 65.53 o 8 4 50 43.41 8.85 38.96 < 9 4 50 98.51 72.61 42.50 < -9 5 50 764.74 780.99 69.07 o -8 5 50 543.89 609.21 61.98 o -7 5 50 78.49 8.85 47.82 < -6 5 50 0.11 35.42 54.90 < -5 5 50 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56 205.47 201.89 51.36 o -6 4 56 393.30 506.49 65.53 o -5 4 56 869.24 919.13 74.38 o -4 4 56 529.22 580.88 60.21 o -3 4 56 142.31 79.69 49.59 < -2 4 56 936.24 1037.78 65.53 o -1 4 56 136.03 198.35 49.59 o 0 4 56 388.63 444.51 54.90 o 1 4 56 108.50 138.13 47.82 < 2 4 56 198.44 217.83 49.59 o 3 4 56 14.48 24.79 49.59 < 4 4 56 6.19 97.40 49.59 < 5 4 56 41.95 67.30 51.36 < -4 5 56 9.26 132.82 58.44 < -3 5 56 904.78 936.84 65.53 o -2 5 56 72.34 -26.56 49.59 < -1 5 56 209.46 235.54 56.67 o 0 5 56 2177.50 2226.10 93.86 o 1 5 56 203.34 260.33 56.67 o 2 5 56 3157.66 3061.99 106.26 o 3 5 56 622.87 665.88 65.53 o -8 1 57 4696.43 4994.11 154.07 o -7 1 57 72.73 42.50 60.21 < -6 1 57 1429.72 1305.20 93.86 o -5 1 57 250.89 233.77 65.53 o -4 1 57 2167.15 2190.68 109.80 o -3 1 57 230.94 175.32 65.53 < -2 1 57 1145.84 1117.48 122.20 o -1 1 57 3111.60 2982.30 116.88 o 0 1 57 2705.80 2847.70 102.72 o 1 1 57 36.87 88.55 53.13 < 2 1 57 247.16 338.25 58.44 o 3 1 57 154.94 201.89 51.36 o 4 1 57 2596.26 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1 61 0.05 51.36 56.67 < -2 2 61 29.67 31.88 60.21 < -1 2 61 299.71 398.47 70.84 o 0 2 61 2100.73 2172.97 100.94 o 1 2 61 959.20 752.66 72.61 o -1 0 62 78.04 256.79 97.40 < 0 0 62 31.62 42.50 113.34 <