#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:03:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180913 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/54/2105451.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105451_Fobs loop_ _publ_author_name 'Zakharov, Boris A.' 'Boldyreva, Elena V.' _publ_section_title ; A high-pressure single-crystal to single-crystal phase transition in DL-alaninium semi-oxalate monohydrate with switching-over hydrogen bonds ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 271 _journal_page_last 280 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.967 _cell_angle_gamma 90.000 _cell_length_a 12.1422 _cell_length_b 6.1377 _cell_length_c 11.2306 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7525 _cod_data_source_file gp5064240sup6.hkl _cod_data_source_block 240 #BEGIN Tags that were not found in dictionaries: _shelx_title 'E 6-230' _shelx_refln_list_code 4 _shelx_f_calc_maximum 103.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 471.96 444.33 11.67 o 0 2 0 10801.68 10485.16 131.34 o 1 2 0 7437.76 7580.06 119.93 o 2 2 0 2519.24 2398.24 85.95 o 1 3 0 139.06 171.46 19.34 o 2 3 0 171.22 166.00 7.99 o 3 3 0 60.98 57.38 6.73 o 0 4 0 1542.65 1445.27 51.70 o 1 4 0 122.64 130.79 5.59 o 3 4 0 272.60 280.12 12.96 o 4 4 0 343.85 346.85 15.76 o 1 5 0 199.15 227.49 9.00 o 2 5 0 101.48 108.36 8.79 o 3 5 0 272.08 261.63 26.53 o 4 5 0 195.64 188.59 19.49 o 0 6 0 30.32 48.98 11.47 o 1 6 0 173.39 170.58 12.06 o 2 6 0 2.41 4.71 5.60 o 3 6 0 141.22 163.88 16.77 o 4 6 0 560.47 541.69 35.03 o 5 6 0 5.69 68.01 31.10 o 1 7 0 3.18 10.45 6.57 o 2 7 0 0.21 6.79 8.68 o 3 7 0 51.00 53.20 11.64 o 4 7 0 4.11 9.81 8.91 o 5 7 0 0.49 16.71 11.84 o -1 1 1 340.67 342.50 5.10 o 0 1 1 1024.85 995.86 15.33 o 1 1 1 13.24 17.26 3.10 o -3 2 1 3817.42 3887.50 136.90 o -2 2 1 1358.20 1422.17 33.73 o -1 2 1 249.91 260.15 4.20 o 0 2 1 23.82 17.98 1.61 o 1 2 1 757.73 693.76 15.41 o 2 2 1 1454.01 1535.14 32.79 o -4 3 1 319.21 326.90 16.05 o -3 3 1 610.68 636.98 15.30 o -2 3 1 1700.13 1796.11 48.92 o 0 3 1 22.72 33.23 8.77 o 1 3 1 117.95 119.86 5.50 o 2 3 1 253.55 242.43 12.11 o 3 3 1 10.36 21.06 11.15 o -4 4 1 147.54 142.52 9.59 o -3 4 1 3660.36 3907.12 64.16 o -2 4 1 618.62 563.61 11.91 o -1 4 1 47.07 46.38 2.94 o 0 4 1 6.68 5.46 1.68 o 1 4 1 74.70 76.01 4.28 o 2 4 1 76.45 92.61 7.51 o 3 4 1 3.02 5.43 3.18 o -5 5 1 25.62 40.12 10.95 o -4 5 1 1.70 8.19 6.95 o -2 5 1 2.74 1.49 2.93 o -1 5 1 24.32 30.80 5.05 o 0 5 1 6.11 3.87 2.76 o 1 5 1 68.31 57.08 5.71 o 2 5 1 146.80 168.19 13.57 o 3 5 1 1.24 9.38 7.16 o 4 5 1 178.52 175.90 17.58 o -5 6 1 36.02 31.92 10.74 o -4 6 1 116.98 134.83 16.11 o -3 6 1 123.24 120.69 14.40 o -2 6 1 192.82 168.65 12.79 o -1 6 1 57.49 71.17 11.57 o 1 6 1 29.14 33.45 7.68 o 2 6 1 76.08 66.22 11.21 o 3 6 1 7.11 14.33 8.40 o 4 6 1 3.29 13.16 12.30 o -5 7 1 5.26 15.97 9.57 o -4 7 1 0.00 4.91 8.91 o -3 7 1 12.32 12.06 9.30 o -1 7 1 7.84 20.33 6.14 o 0 7 1 14.08 12.61 7.39 o 1 7 1 11.87 4.82 6.58 o 2 7 1 1.74 9.28 8.65 o 3 7 1 26.40 14.08 7.36 o 4 7 1 144.34 151.54 32.38 o -2 0 2 1612.87 1613.82 22.83 o -1 0 2 191.52 189.81 5.26 o 0 0 2 182.14 213.14 8.62 o -2 1 2 74.57 78.24 3.19 o -1 1 2 58.55 70.85 1.73 o 0 1 2 4814.69 5043.59 117.14 o -4 2 2 182.99 156.09 13.68 o -3 2 2 20.97 19.00 2.92 o -2 2 2 392.85 385.39 7.47 o -1 2 2 2958.03 2873.86 50.19 o 0 2 2 2276.91 2191.47 44.24 o 1 2 2 133.28 126.86 7.29 o -4 3 2 8.53 11.92 3.60 o -2 3 2 800.48 816.54 12.62 o -1 3 2 224.99 201.38 5.40 o 1 3 2 349.17 333.08 30.07 o 2 3 2 38.90 21.50 6.15 o -5 4 2 1.94 9.16 5.13 o -4 4 2 1.87 2.81 2.40 o -3 4 2 17.39 20.50 2.78 o -2 4 2 114.82 135.46 5.95 o -1 4 2 126.18 132.12 4.91 o 0 4 2 0.00 1.65 3.15 o 1 4 2 186.12 195.86 13.15 o 2 4 2 144.67 166.48 12.91 o 3 4 2 127.25 145.34 14.77 o -5 5 2 24.48 16.59 8.50 o -4 5 2 197.26 194.69 13.29 o -1 5 2 256.05 227.53 10.46 o 0 5 2 51.20 42.52 4.58 o 2 5 2 52.55 40.89 10.54 o 3 5 2 32.84 44.72 9.98 o -6 6 2 278.33 279.11 26.54 o -5 6 2 333.60 359.28 25.49 o -2 6 2 16.47 12.46 5.23 o -1 6 2 198.85 195.19 14.09 o 0 6 2 157.70 132.21 9.83 o 1 6 2 5.87 6.64 5.38 o 2 6 2 0.73 3.30 6.88 o 3 6 2 34.16 38.60 9.45 o -6 7 2 0.54 8.85 12.38 o -5 7 2 30.21 26.24 11.27 o -4 7 2 14.42 31.79 12.19 o -3 7 2 6.05 6.85 7.89 o -2 7 2 5.15 14.18 7.49 o -1 7 2 9.12 27.00 7.57 o 0 7 2 12.99 26.85 6.74 o 1 7 2 115.09 136.24 17.33 o 2 7 2 15.33 6.77 7.23 o 3 7 2 13.66 29.12 11.82 o -4 1 3 1737.05 1682.13 61.11 o -3 1 3 263.30 269.22 10.34 o -2 1 3 261.36 271.26 3.67 o -1 1 3 896.59 913.11 12.90 o 0 1 3 1674.03 1609.06 47.48 o -4 2 3 686.43 668.95 16.00 o -3 2 3 229.00 218.34 7.35 o -2 2 3 116.21 119.54 3.59 o -1 2 3 5.26 1.79 0.69 o 0 2 3 357.13 368.34 7.93 o 1 2 3 371.65 362.67 16.64 o -5 3 3 6.15 4.31 3.62 o -4 3 3 74.46 64.49 4.91 o -3 3 3 350.39 342.62 9.79 o -2 3 3 1542.32 1552.74 26.03 o -1 3 3 193.70 190.76 7.69 o 0 3 3 0.00 3.60 2.52 o 1 3 3 356.78 338.05 22.36 o 2 3 3 998.55 1023.54 41.59 o -6 4 3 16.34 25.74 7.74 o -5 4 3 19.41 17.67 5.04 o -4 4 3 31.21 30.41 6.27 o -3 4 3 12.24 14.71 2.46 o -2 4 3 3.78 6.64 1.74 o -1 4 3 26.90 21.55 2.85 o 0 4 3 28.02 20.70 3.20 o 1 4 3 146.78 142.11 10.90 o 2 4 3 147.96 156.40 14.69 o -6 5 3 19.94 14.75 7.79 o -5 5 3 44.95 51.28 7.78 o -4 5 3 165.27 176.51 12.88 o -2 5 3 217.56 240.90 10.32 o -1 5 3 249.97 254.10 10.88 o 0 5 3 163.23 169.80 9.27 o 1 5 3 14.36 14.08 4.58 o 2 5 3 503.18 546.52 26.68 o 3 5 3 64.58 62.31 25.77 o -6 6 3 123.60 165.28 28.29 o -5 6 3 40.04 57.56 11.02 o -4 6 3 5.09 0.96 8.00 o -3 6 3 15.89 16.70 5.06 o -2 6 3 0.05 7.46 4.41 o -1 6 3 1.55 4.93 3.95 o 1 6 3 0.37 8.35 7.12 o 2 6 3 0.94 12.35 8.16 o 3 6 3 24.31 24.67 13.70 o -6 7 3 0.04 3.40 8.13 o -5 7 3 0.44 8.13 8.80 o -4 7 3 5.32 4.67 8.95 o -3 7 3 18.81 22.91 10.77 o -2 7 3 2.16 6.38 6.24 o -1 7 3 19.10 26.67 6.26 o 0 7 3 29.91 20.35 8.01 o 1 7 3 22.29 18.96 9.43 o 2 7 3 5.70 26.81 11.70 o 3 7 3 15.23 15.99 10.64 o -4 0 4 2548.11 2483.79 110.12 o -3 0 4 1141.79 1200.38 22.49 o -2 0 4 440.83 448.06 13.06 o -1 0 4 123.03 94.91 7.28 o -5 1 4 762.02 656.11 43.13 o -3 1 4 19.14 17.40 1.34 o -2 1 4 3658.01 3874.04 47.97 o -1 1 4 2692.99 2772.98 29.10 o -4 2 4 14.97 14.54 2.42 o -2 2 4 930.33 954.08 18.49 o 0 2 4 549.12 494.46 17.01 o 1 2 4 10.62 8.08 4.04 o -6 3 4 382.29 421.48 23.96 o -5 3 4 361.65 361.19 15.48 o -4 3 4 232.67 211.63 9.63 o -3 3 4 0.46 0.81 1.29 o -2 3 4 1.73 5.72 1.94 o -1 3 4 1137.89 1080.55 21.02 o 0 3 4 1982.45 1963.63 90.85 o 1 3 4 35.16 34.46 6.99 o -6 4 4 68.11 49.64 7.16 o -5 4 4 85.15 88.37 8.83 o -4 4 4 11.87 11.38 2.93 o -3 4 4 3.57 5.65 2.17 o -2 4 4 0.20 2.78 2.32 o -1 4 4 123.43 139.15 6.62 o 0 4 4 7.83 7.75 3.32 o 1 4 4 50.15 43.64 8.26 o 2 4 4 93.67 97.24 15.24 o -6 5 4 165.79 158.86 13.11 o -5 5 4 8.94 11.45 5.24 o -4 5 4 151.72 161.46 9.53 o -3 5 4 192.49 209.71 8.89 o -2 5 4 91.04 95.58 6.22 o 0 5 4 232.34 161.36 28.78 o 1 5 4 107.16 106.38 9.95 o 2 5 4 165.44 130.61 15.70 o -7 6 4 152.02 199.46 27.39 o -6 6 4 28.46 15.14 8.58 o -5 6 4 0.01 1.29 5.67 o -4 6 4 6.54 4.26 4.69 o -3 6 4 0.00 5.57 4.88 o -2 6 4 44.18 54.40 6.42 o 0 6 4 6.90 9.72 6.24 o 1 6 4 0.83 10.07 5.51 o 2 6 4 40.71 45.89 11.24 o -7 7 4 6.65 1.72 17.24 o -6 7 4 45.42 30.18 17.69 o -5 7 4 1.35 8.37 9.77 o -4 7 4 47.18 56.55 13.72 o -3 7 4 0.68 1.60 6.40 o -2 7 4 72.70 75.83 12.84 o -1 7 4 13.01 11.22 6.52 o 0 7 4 52.73 55.45 13.41 o 1 7 4 9.48 6.47 8.03 o 2 7 4 103.21 85.52 17.92 o -5 1 5 116.20 119.39 6.05 o -3 1 5 4348.64 4356.74 52.48 o -2 1 5 53.27 48.53 3.71 o 0 1 5 148.99 160.87 21.78 o -6 2 5 56.16 53.22 7.14 o -5 2 5 3.08 3.11 2.34 o -4 2 5 624.69 685.32 12.28 o -3 2 5 14.28 12.12 1.27 o -2 2 5 210.83 205.14 4.90 o -1 2 5 86.55 82.90 4.20 o 0 2 5 345.24 339.42 17.62 o -6 3 5 124.73 127.77 9.77 o -4 3 5 338.30 334.42 9.56 o -3 3 5 2447.10 2411.52 47.04 o -2 3 5 550.50 550.04 11.32 o -1 3 5 87.88 90.01 5.26 o 0 3 5 46.88 60.48 9.14 o 1 3 5 97.08 115.07 12.52 o -7 4 5 227.31 208.12 18.83 o -5 4 5 51.12 60.19 13.26 o -4 4 5 172.94 166.10 8.34 o -3 4 5 39.60 48.92 4.12 o -2 4 5 201.85 203.95 7.52 o -1 4 5 325.29 329.19 11.26 o 0 4 5 502.98 479.38 22.45 o -7 5 5 153.51 141.84 17.52 o -6 5 5 16.34 22.23 7.01 o -4 5 5 38.84 38.69 5.10 o -3 5 5 1203.85 1178.48 21.31 o -2 5 5 0.59 4.79 3.28 o -1 5 5 142.20 158.51 9.10 o 0 5 5 0.45 7.47 5.53 o 1 5 5 56.00 63.77 10.64 o 2 5 5 9.37 21.06 12.41 o -7 6 5 1.16 11.24 6.64 o -6 6 5 14.03 13.53 6.78 o -5 6 5 0.05 11.78 6.68 o -4 6 5 66.57 58.40 7.27 o -3 6 5 11.60 15.09 4.14 o -2 6 5 37.96 29.54 4.96 o -1 6 5 28.81 27.63 6.96 o 0 6 5 1.68 5.68 6.17 o 1 6 5 22.00 23.90 9.02 o 2 6 5 0.33 1.53 8.45 o -7 7 5 49.72 67.60 17.22 o -6 7 5 31.34 25.75 9.33 o -5 7 5 0.55 5.11 7.03 o -4 7 5 93.33 60.71 15.33 o -3 7 5 40.10 37.48 7.81 o -2 7 5 61.96 56.44 8.52 o -1 7 5 4.61 4.95 7.37 o 0 7 5 0.05 8.73 11.22 o 1 7 5 33.21 63.16 17.34 o 2 7 5 5.14 6.80 19.61 o -6 0 6 145.39 143.59 15.74 o -5 0 6 530.43 522.40 19.86 o -4 0 6 845.15 862.01 20.63 o -3 0 6 2440.86 2255.39 55.26 o -2 0 6 178.57 189.91 10.83 o -1 0 6 25.54 24.10 4.14 o -6 1 6 1884.98 1873.47 43.55 o -5 1 6 1047.67 1155.48 38.47 o -4 1 6 0.47 1.94 0.80 o -3 1 6 228.54 236.14 6.39 o -2 1 6 14.46 13.60 1.27 o -1 1 6 520.15 542.43 11.98 o 0 1 6 66.05 51.79 10.27 o -7 2 6 347.87 350.84 32.43 o -6 2 6 93.10 72.80 11.15 o -5 2 6 1192.17 1306.72 34.87 o -4 2 6 845.46 880.92 14.41 o -3 2 6 10.78 13.52 1.47 o -2 2 6 2.53 2.98 1.27 o -1 2 6 950.68 906.48 18.92 o 0 2 6 24.13 29.95 6.46 o -7 3 6 9.70 5.79 5.21 o -6 3 6 60.88 59.73 7.13 o -5 3 6 575.06 576.15 14.05 o -4 3 6 0.16 2.91 1.76 o -3 3 6 439.31 468.47 10.60 o -2 3 6 310.35 324.65 8.87 o -1 3 6 19.63 12.21 3.14 o 0 3 6 200.98 227.91 17.51 o 1 3 6 8.75 1.23 12.29 o -7 4 6 17.51 11.54 6.00 o -6 4 6 223.81 225.80 11.67 o -5 4 6 46.12 31.43 3.82 o -4 4 6 10.33 25.13 5.78 o -3 4 6 1.16 4.19 2.94 o -2 4 6 3.82 8.60 3.74 o -1 4 6 241.74 231.85 11.45 o 0 4 6 99.49 97.07 12.40 o -7 5 6 8.97 17.89 5.70 o -6 5 6 46.79 50.76 6.34 o -5 5 6 50.79 38.40 5.91 o -4 5 6 16.87 20.97 4.43 o -3 5 6 5.11 4.47 3.48 o 0 5 6 9.94 7.43 5.13 o -7 6 6 12.41 15.01 7.31 o -6 6 6 8.60 16.37 6.37 o -5 6 6 2.43 7.03 5.10 o -4 6 6 69.07 63.69 11.16 o -3 6 6 27.81 23.46 4.65 o -2 6 6 51.41 42.84 6.20 o -1 6 6 93.06 89.55 11.65 o 0 6 6 2.92 7.84 6.73 o 1 6 6 347.51 338.93 32.22 o -7 7 6 14.17 31.73 17.12 o -6 7 6 93.64 92.94 14.09 o -5 7 6 7.34 20.35 9.79 o -4 7 6 0.19 4.99 7.66 o -3 7 6 14.87 23.38 7.18 o -2 7 6 8.20 1.59 7.04 o -1 7 6 32.64 23.15 12.88 o 0 7 6 49.79 11.79 15.10 o 1 7 6 10.85 1.48 10.42 o -7 1 7 370.71 369.42 22.66 o -6 1 7 0.54 1.44 2.44 o -5 1 7 9.80 14.97 1.44 o -4 1 7 5.19 3.48 1.53 o -3 1 7 18.12 13.22 2.04 o -2 1 7 110.95 113.61 4.58 o -1 1 7 61.14 55.90 6.25 o -7 2 7 0.04 2.02 4.59 o -6 2 7 9.22 6.60 2.30 o -5 2 7 144.47 136.88 5.20 o -4 2 7 170.33 175.90 5.48 o -3 2 7 125.56 133.45 4.96 o -2 2 7 247.24 255.50 7.17 o -1 2 7 600.21 608.69 26.08 o 0 2 7 537.55 534.39 41.83 o -8 3 7 252.09 233.66 29.18 o -7 3 7 3.17 16.18 6.97 o -6 3 7 9.62 14.92 3.20 o -5 3 7 0.04 2.22 2.55 o -4 3 7 184.96 188.07 7.94 o -3 3 7 34.84 39.16 3.92 o -2 3 7 8.04 7.58 2.53 o -1 3 7 3.63 10.80 6.75 o -8 4 7 52.52 44.85 10.29 o -7 4 7 208.15 201.14 13.46 o -6 4 7 47.76 56.49 5.90 o -5 4 7 302.68 275.42 11.55 o -4 4 7 298.85 312.65 10.41 o -3 4 7 45.00 40.23 4.28 o -2 4 7 196.46 184.84 11.29 o -1 4 7 72.77 67.42 9.92 o 0 4 7 384.47 415.80 26.75 o -8 5 7 266.08 262.00 18.67 o -7 5 7 60.06 44.14 7.20 o -6 5 7 44.50 27.63 6.35 o -5 5 7 8.47 9.24 4.33 o -4 5 7 38.51 34.35 4.68 o -3 5 7 31.99 31.43 4.20 o -2 5 7 13.80 18.12 4.62 o -1 5 7 26.24 29.64 7.23 o 0 5 7 69.42 86.44 12.32 o -8 6 7 30.37 32.05 23.42 o -7 6 7 11.65 17.69 7.37 o -6 6 7 30.31 39.11 9.10 o -5 6 7 12.62 12.13 6.29 o -4 6 7 0.04 2.89 5.63 o -3 6 7 5.78 13.83 5.13 o -2 6 7 0.29 2.47 4.90 o -1 6 7 14.22 15.62 6.66 o 0 6 7 30.29 42.91 10.25 o -6 7 7 17.97 9.43 9.16 o -4 7 7 4.80 19.71 8.79 o -3 7 7 2.18 14.36 10.09 o -7 0 8 1277.97 1274.98 102.39 o -6 0 8 89.96 92.99 8.31 o -5 0 8 1443.44 1433.16 31.32 o -4 0 8 612.20 595.08 19.91 o -3 0 8 153.04 156.72 11.35 o -2 0 8 5.47 5.39 3.63 o -1 0 8 1288.64 1393.16 76.31 o -8 1 8 17.98 29.23 10.19 o -7 1 8 0.86 4.40 4.05 o -6 1 8 0.10 1.96 2.85 o -5 1 8 26.29 26.58 3.36 o -4 1 8 4.97 6.84 2.14 o -3 1 8 218.57 230.65 8.94 o -2 1 8 648.20 628.58 16.03 o -1 1 8 67.94 74.07 14.73 o -8 2 8 12.62 6.85 6.64 o -7 2 8 750.01 759.48 27.88 o -6 2 8 92.50 78.12 6.55 o -5 2 8 244.51 259.73 10.59 o -4 2 8 490.06 498.05 11.40 o -3 2 8 150.02 148.27 7.81 o -2 2 8 740.54 772.63 21.74 o -1 2 8 13.45 15.69 7.50 o -8 3 8 48.71 44.72 10.46 o -7 3 8 31.87 29.18 6.25 o -6 3 8 208.84 209.17 10.79 o -5 3 8 102.51 97.33 6.33 o -4 3 8 47.11 43.35 5.20 o -3 3 8 68.63 56.70 5.27 o -2 3 8 34.54 25.91 5.17 o -1 3 8 132.45 123.94 19.90 o 0 3 8 60.87 59.82 16.33 o -8 4 8 50.45 55.28 12.53 o -7 4 8 194.58 226.51 14.70 o -6 4 8 102.40 119.11 8.77 o -5 4 8 29.20 34.66 4.98 o -4 4 8 42.08 36.96 4.73 o -3 4 8 66.38 69.24 7.02 o -2 4 8 18.67 26.90 7.07 o -1 4 8 25.26 27.35 10.82 o 0 4 8 214.12 219.98 28.09 o -8 5 8 12.48 8.67 9.59 o -7 5 8 15.51 24.24 9.50 o -5 5 8 31.24 34.28 5.83 o -4 5 8 15.98 9.57 4.36 o -3 5 8 5.17 15.13 6.17 o -2 5 8 5.68 13.38 14.25 o -1 5 8 20.52 2.16 10.29 o 0 5 8 8.34 16.31 17.03 o -8 6 8 127.75 147.63 26.99 o -7 6 8 0.42 12.40 12.40 o -6 6 8 216.11 184.51 23.68 o -5 6 8 5.35 18.24 8.53 o -4 6 8 30.63 38.98 11.67 o -3 6 8 234.53 200.65 20.58 o -2 6 8 30.42 39.41 18.76 o -1 6 8 60.08 42.80 19.29 o 0 6 8 65.88 47.95 21.28 o -8 1 9 33.77 33.21 7.60 o -7 1 9 45.26 59.49 7.83 o -6 1 9 86.79 83.47 6.08 o -4 1 9 204.64 196.50 8.49 o -3 1 9 16.43 10.54 2.74 o -2 1 9 127.56 136.95 11.01 o -7 2 9 289.72 297.66 26.16 o -6 2 9 3.22 8.04 4.10 o -5 2 9 535.37 520.73 17.34 o -4 2 9 26.80 15.31 3.93 o -3 2 9 406.94 406.04 15.87 o -2 2 9 2.44 5.10 4.45 o -1 2 9 5.47 26.40 10.81 o -9 3 9 186.66 174.79 25.88 o -8 3 9 78.10 61.50 12.95 o -7 3 9 11.19 12.80 7.07 o -6 3 9 31.41 33.49 6.41 o -5 3 9 197.39 198.46 14.09 o -4 3 9 133.76 114.96 10.93 o -3 3 9 207.36 189.88 15.27 o -2 3 9 29.44 13.56 8.40 o -1 3 9 100.86 75.95 16.02 o -9 4 9 135.84 138.91 24.10 o -8 4 9 24.63 49.48 12.47 o -7 4 9 15.26 9.48 5.77 o -6 4 9 13.68 18.11 7.63 o -5 4 9 219.48 210.47 15.30 o -4 4 9 44.71 49.95 8.48 o -3 4 9 414.99 442.36 24.10 o -2 4 9 45.79 35.14 12.45 o -1 4 9 17.55 16.29 9.56 o -9 5 9 18.71 27.00 25.31 o -8 5 9 12.84 7.65 9.06 o -7 5 9 10.82 19.86 7.80 o -6 5 9 7.18 15.61 7.96 o -5 5 9 0.02 5.76 5.76 o -4 5 9 228.49 232.54 17.76 o -3 5 9 68.38 73.41 16.12 o -2 5 9 19.29 12.34 11.52 o -1 5 9 37.79 35.72 19.24 o -8 6 9 1.92 1.72 17.21 o -7 6 9 2.68 17.99 28.63 o -6 6 9 0.13 10.51 9.72 o -5 6 9 119.36 130.18 18.54 o -4 6 9 10.04 16.47 9.33 o -3 6 9 79.89 105.36 23.00 o -2 6 9 4.27 16.12 17.17 o -8 0 10 1089.42 1119.43 44.02 o -7 0 10 1.69 4.66 5.17 o -6 0 10 1959.73 1996.05 42.43 o -5 0 10 115.04 101.75 10.01 o -4 0 10 2.35 3.05 4.07 o -3 0 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