#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:03:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180913 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/54/2105452.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105452_Fobs loop_ _publ_author_name 'Zakharov, Boris A.' 'Boldyreva, Elena V.' _publ_section_title ; A high-pressure single-crystal to single-crystal phase transition in DL-alaninium semi-oxalate monohydrate with switching-over hydrogen bonds ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 271 _journal_page_last 280 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.409 _cell_angle_gamma 90.000 _cell_length_a 12.0370 _cell_length_b 6.0534 _cell_length_c 11.2114 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7535 _cod_data_source_file gp5064310sup7.hkl _cod_data_source_block 310 #BEGIN Tags that were not found in dictionaries: _shelx_title 'E 7-313' _shelx_refln_list_code 4 _shelx_f_calc_maximum 100.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 472.27 442.58 10.35 o 1 2 0 7056.80 7301.13 108.24 o 2 2 0 2225.10 2045.67 31.97 o 2 3 0 107.96 111.16 6.68 o 3 3 0 53.51 45.37 5.88 o 0 4 0 1421.11 1431.00 36.16 o 1 4 0 44.45 52.96 3.84 o 2 4 0 553.01 606.01 31.46 o 3 4 0 365.56 382.91 15.49 o 4 4 0 276.39 290.80 14.56 o 1 5 0 172.19 179.53 9.82 o 3 5 0 243.38 208.83 19.66 o 4 5 0 162.80 177.75 18.79 o 0 6 0 86.92 90.71 14.85 o 1 6 0 152.75 140.32 11.13 o 2 6 0 3.70 8.01 5.18 o 3 6 0 141.79 142.90 15.99 o 4 6 0 571.19 563.43 32.42 o 5 6 0 13.83 27.93 15.44 o 1 7 0 4.38 15.27 7.44 o 2 7 0 1.48 7.46 10.02 o 3 7 0 59.50 69.61 13.43 o 4 7 0 8.40 1.43 8.04 o -2 1 1 156.65 123.86 6.18 o -1 1 1 334.52 333.59 5.15 o 0 1 1 957.02 944.38 10.11 o 1 1 1 20.60 25.71 4.25 o -3 2 1 4036.09 4037.25 74.02 o -2 2 1 1451.31 1452.61 31.61 o -1 2 1 392.27 403.63 5.35 o 0 2 1 8.97 5.69 0.90 o 1 2 1 800.92 717.70 16.25 o 2 2 1 1096.56 1180.27 29.58 o -4 3 1 369.19 360.40 17.26 o -3 3 1 638.81 656.22 16.00 o -2 3 1 1765.61 1914.72 39.89 o -1 3 1 116.10 82.53 9.72 o 1 3 1 131.50 136.19 6.09 o 2 3 1 231.65 231.83 12.38 o 3 3 1 7.13 3.14 5.05 o -4 4 1 105.07 108.07 8.54 o -2 4 1 742.03 679.35 14.16 o -1 4 1 41.46 36.73 2.58 o 0 4 1 4.34 1.57 1.79 o 1 4 1 40.00 36.90 3.07 o 2 4 1 84.62 95.72 7.36 o 3 4 1 1.42 3.74 2.96 o -4 5 1 1.24 9.78 6.52 o -3 5 1 54.73 71.63 8.83 o -2 5 1 4.15 2.51 3.92 o -1 5 1 13.09 13.70 3.59 o 0 5 1 1.26 2.41 3.12 o 1 5 1 96.78 77.14 5.70 o 2 5 1 185.54 168.23 12.92 o 3 5 1 0.06 2.89 4.78 o 4 5 1 213.27 215.95 27.23 o -5 6 1 51.52 41.88 12.60 o -4 6 1 53.33 60.50 12.52 o -3 6 1 128.34 143.87 15.97 o -2 6 1 182.72 126.77 17.80 o -1 6 1 32.72 41.79 8.82 o 1 6 1 38.01 36.55 6.40 o 2 6 1 77.59 91.99 14.53 o 3 6 1 8.02 15.49 7.96 o 4 6 1 3.80 20.07 11.46 o -5 7 1 1.26 10.17 8.25 o -4 7 1 1.61 13.21 9.37 o -3 7 1 17.48 22.72 10.46 o -2 7 1 80.77 58.89 19.58 o -1 7 1 8.43 10.73 7.69 o 0 7 1 8.29 14.36 6.41 o 1 7 1 0.60 3.47 7.81 o 3 7 1 11.98 5.03 9.11 o 4 7 1 92.94 118.16 20.57 o -2 0 2 1471.54 1486.17 22.39 o -1 0 2 217.78 219.43 5.79 o 0 0 2 158.64 193.92 8.40 o -3 1 2 310.33 363.94 16.57 o -2 1 2 77.45 83.73 3.35 o -1 1 2 57.97 61.22 1.62 o 0 1 2 4615.86 4721.79 65.27 o -4 2 2 81.51 64.74 7.30 o -3 2 2 4.71 4.44 1.79 o -2 2 2 314.24 315.10 6.69 o -1 2 2 3094.73 3015.70 44.63 o 0 2 2 2403.85 2345.58 35.42 o 1 2 2 161.88 153.21 8.25 o -4 3 2 7.49 6.87 3.34 o -2 3 2 604.66 592.57 11.30 o -1 3 2 210.05 203.69 4.68 o 0 3 2 308.23 347.20 11.49 o 1 3 2 321.38 304.25 26.64 o 2 3 2 26.45 12.72 5.01 o -5 4 2 3.70 6.82 5.32 o -4 4 2 3.66 6.29 3.81 o -3 4 2 8.60 6.90 2.27 o -1 4 2 103.40 110.42 4.71 o 1 4 2 172.95 178.88 12.79 o 2 4 2 102.25 115.59 11.20 o 3 4 2 122.44 141.87 14.85 o -5 5 2 19.57 19.05 7.07 o -4 5 2 185.51 186.48 13.62 o -3 5 2 23.38 13.50 4.19 o -2 5 2 142.27 130.10 8.23 o -1 5 2 228.14 212.37 10.22 o 1 5 2 77.33 70.77 13.47 o 2 5 2 74.36 63.51 9.97 o 3 5 2 24.20 14.74 7.82 o -6 6 2 301.52 308.73 35.43 o -5 6 2 408.08 441.51 28.59 o -2 6 2 18.72 19.64 4.92 o -1 6 2 163.22 180.77 13.57 o 0 6 2 158.33 158.22 11.03 o 1 6 2 7.86 19.31 8.34 o 2 6 2 0.00 5.01 7.33 o 3 6 2 47.39 55.18 10.74 o -5 7 2 41.91 37.03 17.66 o -4 7 2 21.63 24.87 9.59 o -2 7 2 5.73 13.21 8.21 o -1 7 2 11.25 19.84 7.88 o 0 7 2 7.39 21.53 7.13 o 1 7 2 130.27 121.17 16.34 o 2 7 2 16.46 10.92 11.25 o 3 7 2 26.18 6.17 9.76 o -3 1 3 204.21 219.53 7.13 o -2 1 3 198.96 211.56 3.30 o -1 1 3 964.19 974.64 10.73 o 0 1 3 1603.44 1590.81 29.56 o -4 2 3 700.57 701.29 16.95 o -3 2 3 247.65 256.20 8.11 o -2 2 3 134.54 136.29 3.93 o -1 2 3 4.83 1.50 0.69 o 0 2 3 367.90 398.05 8.41 o 1 2 3 453.41 484.67 20.27 o -5 3 3 1.86 3.50 3.07 o -4 3 3 69.00 63.88 4.12 o -3 3 3 313.97 318.07 9.65 o -2 3 3 1455.44 1472.98 26.07 o -1 3 3 173.52 155.36 7.10 o 0 3 3 0.67 1.58 2.66 o 1 3 3 469.88 456.84 26.88 o 2 3 3 1140.76 1186.86 46.26 o -6 4 3 23.26 24.06 6.28 o -5 4 3 10.06 16.52 5.60 o -4 4 3 33.67 38.65 6.22 o -3 4 3 25.78 26.05 3.07 o -2 4 3 4.58 2.19 2.07 o -1 4 3 32.08 21.93 2.97 o 0 4 3 26.44 18.66 2.99 o 1 4 3 132.42 123.89 10.14 o 2 4 3 139.98 165.18 15.94 o -6 5 3 9.43 36.98 20.04 o -5 5 3 46.28 51.43 8.87 o -4 5 3 256.48 261.86 16.11 o -3 5 3 219.33 197.87 9.64 o -2 5 3 185.72 189.68 9.02 o -1 5 3 302.24 286.55 11.35 o 0 5 3 304.08 301.81 27.19 o 1 5 3 7.35 15.30 4.60 o 2 5 3 465.49 490.90 27.03 o 3 5 3 94.23 39.16 28.53 o -6 6 3 162.08 204.14 20.32 o -5 6 3 25.14 37.79 9.53 o -4 6 3 1.42 8.65 5.73 o -3 6 3 31.40 27.19 6.36 o -2 6 3 0.00 7.94 4.44 o 1 6 3 1.57 9.62 7.24 o 2 6 3 0.04 3.38 7.66 o 3 6 3 20.16 8.59 9.84 o -5 7 3 0.39 10.72 10.19 o -4 7 3 9.46 8.00 9.21 o -3 7 3 16.22 14.85 8.95 o -2 7 3 0.43 8.78 6.89 o -1 7 3 30.26 34.81 7.69 o 0 7 3 22.93 17.98 10.99 o 1 7 3 21.34 23.86 9.70 o 2 7 3 4.45 6.25 8.33 o 3 7 3 9.13 12.96 9.84 o -4 0 4 2796.99 2628.73 88.08 o -3 0 4 1120.99 1128.64 22.28 o -2 0 4 468.07 471.97 13.66 o 0 0 4 449.08 447.52 31.82 o -5 1 4 808.96 676.03 44.95 o -4 1 4 940.42 1044.22 15.97 o -3 1 4 8.87 8.65 1.14 o -2 1 4 3648.84 3913.65 33.13 o -1 1 4 2733.76 2716.17 49.48 o 0 1 4 10042.11 10596.43 162.58 o -4 2 4 20.58 21.29 2.75 o -3 2 4 1325.18 1445.81 53.71 o -2 2 4 1110.12 1188.03 22.11 o 0 2 4 414.13 416.01 18.07 o 1 2 4 9.16 0.62 6.18 o -6 3 4 351.87 370.18 23.26 o -5 3 4 374.33 345.07 15.64 o -4 3 4 211.31 182.25 9.28 o -3 3 4 5.44 4.34 1.55 o -2 3 4 5.30 9.39 2.06 o -1 3 4 964.78 915.62 15.99 o 0 3 4 1747.05 1817.66 44.01 o 1 3 4 26.80 16.01 5.11 o -6 4 4 50.88 30.62 6.27 o -5 4 4 97.36 100.37 9.51 o -4 4 4 32.91 27.24 3.77 o -3 4 4 5.57 4.38 2.31 o -2 4 4 0.12 3.45 2.28 o 0 4 4 24.32 18.90 4.09 o 1 4 4 54.58 38.37 7.14 o 2 4 4 48.59 43.59 10.40 o -6 5 4 159.35 158.67 13.25 o -5 5 4 8.70 1.15 5.40 o -4 5 4 140.37 146.61 9.34 o -2 5 4 42.17 48.44 4.60 o -1 5 4 20.30 14.32 3.40 o 1 5 4 86.33 92.71 9.02 o 2 5 4 176.46 151.87 18.04 o -7 6 4 162.47 168.80 21.47 o -6 6 4 21.73 39.94 9.70 o -5 6 4 4.18 12.81 6.58 o -4 6 4 11.78 11.02 5.70 o -3 6 4 0.48 3.53 4.56 o -2 6 4 40.11 47.18 6.43 o -1 6 4 47.62 56.85 6.56 o 0 6 4 1.42 2.90 4.94 o 1 6 4 0.03 3.56 5.70 o 2 6 4 31.42 26.37 10.36 o -6 7 4 51.98 35.40 11.36 o -5 7 4 1.37 8.65 8.71 o -4 7 4 51.54 54.44 14.11 o -3 7 4 2.86 3.55 7.86 o -2 7 4 85.38 109.66 11.95 o -1 7 4 7.26 11.33 8.62 o 0 7 4 84.81 118.37 16.70 o 1 7 4 7.78 12.60 10.28 o 2 7 4 122.99 105.17 19.64 o -5 1 5 155.28 156.59 7.03 o -3 1 5 4617.11 4518.68 41.66 o -2 1 5 66.42 59.08 2.78 o 0 1 5 132.89 161.41 22.56 o -6 2 5 47.94 41.42 6.27 o -5 2 5 9.19 14.75 3.42 o -4 2 5 708.52 755.89 13.19 o -3 2 5 36.09 37.30 2.21 o -2 2 5 133.63 131.65 3.96 o -1 2 5 150.58 142.16 5.60 o 0 2 5 355.96 350.51 18.63 o -6 3 5 138.50 150.28 11.01 o -5 3 5 603.06 580.01 18.82 o -4 3 5 317.46 328.37 9.74 o -3 3 5 2691.68 2654.65 53.82 o -2 3 5 610.92 533.96 21.46 o -1 3 5 146.91 149.27 7.80 o 0 3 5 87.58 103.79 11.85 o 1 3 5 94.24 99.26 12.36 o -7 4 5 215.91 234.71 20.11 o -6 4 5 195.48 220.55 14.83 o -4 4 5 187.13 175.73 8.79 o -3 4 5 47.29 47.84 4.12 o -2 4 5 190.85 184.12 7.21 o -1 4 5 351.74 342.34 12.28 o 0 4 5 559.73 540.88 24.20 o -7 5 5 141.61 120.66 16.88 o -6 5 5 16.52 13.85 5.62 o -4 5 5 23.94 23.08 3.92 o -3 5 5 1245.02 1257.45 23.51 o -2 5 5 0.00 4.13 3.10 o -1 5 5 139.52 165.80 10.20 o 0 5 5 1.75 8.21 6.04 o 1 5 5 52.89 58.74 10.23 o 2 5 5 21.55 34.47 17.60 o -7 6 5 2.95 10.33 8.35 o -6 6 5 17.33 4.79 6.79 o -5 6 5 1.63 9.74 9.50 o -4 6 5 79.68 76.48 9.01 o -3 6 5 4.72 8.57 4.79 o -2 6 5 35.84 27.81 5.17 o -1 6 5 41.79 48.26 7.77 o 0 6 5 6.11 13.83 7.16 o 1 6 5 35.60 37.90 11.35 o 2 6 5 0.22 1.35 7.68 o -6 7 5 57.51 82.70 15.47 o -5 7 5 0.42 13.86 7.74 o -4 7 5 38.89 29.51 13.11 o -3 7 5 45.22 53.42 8.45 o -2 7 5 56.74 36.12 11.68 o -1 7 5 0.07 10.81 10.40 o 0 7 5 12.12 12.77 9.42 o 1 7 5 31.88 17.50 15.91 o -6 0 6 197.27 178.92 17.54 o -5 0 6 474.64 484.87 18.77 o -4 0 6 877.56 897.12 21.48 o -3 0 6 2681.17 2486.66 39.24 o -2 0 6 113.41 119.60 8.86 o -1 0 6 24.46 23.52 4.02 o -6 1 6 1909.35 1833.80 36.91 o -3 1 6 261.94 283.08 7.16 o -2 1 6 19.68 18.24 1.56 o -1 1 6 491.77 496.44 11.64 o 0 1 6 53.53 38.53 9.39 o -7 2 6 395.73 425.71 31.45 o -6 2 6 62.82 64.40 6.95 o -5 2 6 1197.61 1326.64 21.79 o -4 2 6 812.74 863.29 11.38 o -3 2 6 3.73 3.41 1.22 o -2 2 6 0.31 3.01 1.49 o -1 2 6 998.22 984.19 20.67 o 0 2 6 22.03 36.22 7.07 o -7 3 6 0.51 7.03 5.25 o -6 3 6 38.66 38.83 6.30 o -5 3 6 502.32 536.79 13.80 o -4 3 6 7.37 9.76 2.26 o -3 3 6 382.87 414.93 10.18 o -2 3 6 319.77 322.32 10.83 o -1 3 6 5.99 5.32 3.06 o 0 3 6 234.30 284.71 19.84 o -7 4 6 18.14 21.20 6.77 o -6 4 6 204.42 198.66 11.30 o -5 4 6 73.62 66.78 5.25 o -1 4 6 229.68 203.29 18.91 o 0 4 6 149.36 137.18 14.95 o -7 5 6 0.00 5.00 5.34 o -6 5 6 74.47 74.38 8.58 o -5 5 6 77.43 72.29 6.93 o -4 5 6 9.21 22.42 4.90 o -3 5 6 6.62 12.06 3.60 o -1 5 6 0.05 4.02 4.07 o 0 5 6 4.32 6.00 5.48 o -7 6 6 11.98 22.64 6.94 o -6 6 6 20.62 17.84 6.35 o -5 6 6 1.75 9.70 4.86 o -4 6 6 88.79 89.16 10.18 o -3 6 6 34.19 29.08 5.15 o -2 6 6 41.13 46.04 6.96 o -1 6 6 108.71 121.27 13.54 o 0 6 6 3.23 6.24 6.27 o 1 6 6 371.79 371.75 30.35 o -6 7 6 135.60 151.97 16.92 o -5 7 6 14.91 18.38 9.41 o -4 7 6 0.16 7.09 6.78 o -3 7 6 16.35 26.13 7.90 o -2 7 6 3.86 2.01 11.20 o -1 7 6 24.51 46.03 16.95 o 0 7 6 57.32 56.38 14.51 o 1 7 6 5.94 6.99 12.94 o -7 1 7 356.97 323.78 21.87 o -6 1 7 0.05 1.96 2.39 o -5 1 7 3.40 4.69 1.07 o -4 1 7 4.94 2.27 1.58 o -3 1 7 23.95 19.18 2.38 o -2 1 7 113.43 115.30 4.71 o -1 1 7 79.55 77.61 12.76 o -7 2 7 0.44 1.25 3.75 o -6 2 7 10.95 8.45 2.29 o -5 2 7 142.83 139.51 5.33 o -4 2 7 173.46 176.35 5.55 o -3 2 7 96.36 103.08 4.51 o -2 2 7 271.38 276.74 7.85 o -1 2 7 624.91 618.63 25.93 o 0 2 7 759.64 719.15 76.11 o -8 3 7 247.21 246.73 27.10 o -7 3 7 0.88 5.54 4.99 o -6 3 7 15.13 18.52 2.93 o -5 3 7 2.08 4.99 3.01 o -4 3 7 144.74 154.28 7.42 o -3 3 7 48.01 54.92 4.45 o -2 3 7 9.76 11.13 3.13 o -1 3 7 8.22 1.56 6.01 o 0 3 7 0.28 10.86 11.61 o -8 4 7 77.72 81.75 13.06 o -7 4 7 220.99 211.83 13.60 o -6 4 7 49.87 53.90 5.96 o -5 4 7 300.95 279.00 11.97 o -4 4 7 369.19 365.77 11.47 o -3 4 7 38.11 33.37 4.32 o -2 4 7 147.69 133.03 11.13 o -1 4 7 114.20 112.55 12.44 o 0 4 7 504.67 502.90 39.34 o -8 5 7 351.90 331.75 21.22 o -7 5 7 76.37 68.52 9.15 o -6 5 7 55.27 38.50 8.14 o -5 5 7 0.00 2.92 3.93 o -4 5 7 53.97 52.72 4.92 o -3 5 7 52.50 58.21 6.35 o -2 5 7 7.63 12.23 3.90 o -1 5 7 15.73 25.33 8.11 o 0 5 7 56.58 68.99 11.49 o -8 6 7 31.86 53.86 13.57 o -7 6 7 4.83 14.21 7.06 o -6 6 7 23.12 23.19 8.43 o -5 6 7 4.12 10.22 5.68 o -3 6 7 1.14 3.54 5.00 o -2 6 7 0.51 13.82 7.83 o -1 6 7 19.33 22.87 9.47 o 0 6 7 62.81 60.37 11.81 o -5 7 7 12.03 10.43 10.31 o -4 7 7 10.12 21.31 10.55 o -3 7 7 0.94 2.13 15.07 o -7 0 8 1354.85 1319.88 112.81 o -6 0 8 125.01 112.49 9.61 o -5 0 8 1407.13 1350.21 31.88 o -4 0 8 687.70 640.34 21.30 o -3 0 8 232.83 222.81 14.03 o -2 0 8 7.31 5.50 3.12 o -1 0 8 1524.15 1449.87 80.16 o -8 1 8 11.25 15.26 7.65 o -7 1 8 0.31 6.19 4.26 o -6 1 8 0.32 4.08 2.86 o -5 1 8 12.29 9.63 2.65 o -4 1 8 1.48 2.64 2.14 o -3 1 8 257.65 255.86 9.46 o -2 1 8 686.52 679.98 20.32 o -1 1 8 65.41 89.40 15.72 o -8 2 8 6.56 9.52 6.07 o -7 2 8 886.63 869.49 28.80 o -6 2 8 79.64 73.86 6.47 o -5 2 8 246.66 257.18 10.23 o -4 2 8 542.07 567.02 14.14 o -3 2 8 93.88 98.84 6.65 o -2 2 8 747.42 779.83 21.86 o -1 2 8 3.78 1.14 7.94 o -8 3 8 41.42 42.83 10.12 o -7 3 8 22.22 25.25 6.89 o -6 3 8 186.39 177.43 10.08 o -5 3 8 114.07 108.67 7.20 o -4 3 8 32.35 25.03 4.47 o -3 3 8 53.18 38.94 4.76 o -2 3 8 28.38 25.83 5.56 o -1 3 8 154.54 111.47 34.45 o -8 4 8 71.69 59.71 12.60 o -7 4 8 243.11 243.60 17.71 o -6 4 8 76.96 85.45 7.95 o -5 4 8 21.66 30.98 5.30 o -4 4 8 48.58 33.12 5.21 o -3 4 8 46.46 49.67 6.39 o -2 4 8 48.86 38.16 13.66 o -1 4 8 19.94 41.75 11.68 o 0 4 8 234.17 215.51 47.53 o -8 5 8 10.60 7.50 10.63 o -7 5 8 8.55 17.30 8.07 o -5 5 8 30.51 30.66 6.07 o -4 5 8 17.65 24.63 5.71 o -2 5 8 7.67 33.10 14.68 o -1 5 8 32.35 28.37 14.16 o 0 5 8 16.65 1.77 17.69 o -8 6 8 139.18 145.02 27.83 o -7 6 8 0.13 5.75 11.44 o -6 6 8 214.42 219.01 29.46 o -4 6 8 29.70 44.92 12.46 o -3 6 8 270.34 250.34 40.17 o -2 6 8 37.63 30.23 21.07 o -1 6 8 90.76 111.94 27.34 o 0 6 8 56.45 73.37 32.46 o -8 1 9 30.10 31.08 7.24 o -7 1 9 65.38 87.67 8.77 o -6 1 9 113.23 122.75 7.38 o -5 1 9 2.32 7.01 3.91 o -4 1 9 211.91 211.84 8.93 o -3 1 9 7.76 3.47 3.07 o -2 1 9 126.93 144.30 16.55 o -8 2 9 0.72 14.35 11.40 o -7 2 9 275.12 285.22 23.47 o -6 2 9 1.11 1.10 3.73 o -5 2 9 685.41 656.25 19.47 o -4 2 9 40.89 30.41 3.76 o -3 2 9 370.04 400.44 16.30 o -2 2 9 10.87 13.42 5.11 o -1 2 9 13.26 28.82 19.65 o -9 3 9 194.60 183.48 26.74 o -8 3 9 97.68 81.89 14.37 o -7 3 9 10.74 9.49 6.99 o -6 3 9 55.54 66.08 8.70 o -5 3 9 297.38 302.77 17.41 o -4 3 9 119.99 108.95 10.74 o -3 3 9 236.49 214.24 16.32 o -2 3 9 28.72 10.39 10.85 o -1 3 9 113.13 101.28 19.90 o -9 4 9 134.21 164.33 27.21 o -8 4 9 28.10 29.42 9.81 o -7 4 9 9.83 12.65 6.19 o -6 4 9 17.02 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