#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:03:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180913 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/54/2105453.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105453_Fobs loop_ _publ_author_name 'Zakharov, Boris A.' 'Boldyreva, Elena V.' _publ_section_title ; A high-pressure single-crystal to single-crystal phase transition in DL-alaninium semi-oxalate monohydrate with switching-over hydrogen bonds ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 271 _journal_page_last 280 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.608 _cell_angle_gamma 90.000 _cell_length_a 11.9756 _cell_length_b 6.0032 _cell_length_c 11.1991 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7514 _cod_data_source_file gp5064360sup8.hkl _cod_data_source_block 360 #BEGIN Tags that were not found in dictionaries: _shelx_title 'E 8-361' _shelx_refln_list_code 4 _shelx_f_calc_maximum 100.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 431.77 422.78 10.22 o 0 2 0 10199.07 11029.39 102.30 o 1 2 0 6775.74 6958.20 95.51 o 2 2 0 2199.02 1845.00 57.62 o 2 3 0 92.18 87.82 6.40 o 3 3 0 52.18 46.21 6.39 o 0 4 0 1395.19 1373.58 37.27 o 1 4 0 14.66 18.19 2.50 o 2 4 0 509.99 569.08 31.17 o 3 4 0 418.25 416.45 17.40 o 4 4 0 260.37 268.76 15.08 o 1 5 0 162.56 164.93 11.02 o 2 5 0 71.45 116.86 16.57 o 3 5 0 251.44 234.90 26.75 o 4 5 0 168.22 151.24 18.94 o 0 6 0 127.07 105.58 15.89 o 1 6 0 156.33 136.92 11.55 o 2 6 0 5.90 9.14 9.38 o 3 6 0 139.60 152.33 17.19 o 4 6 0 591.90 604.09 43.66 o 5 6 0 7.01 7.66 13.00 o 1 7 0 5.92 10.86 7.64 o 3 7 0 68.79 81.89 13.21 o 4 7 0 8.82 7.25 10.07 o -2 1 1 136.92 123.35 5.93 o -1 1 1 355.44 335.18 5.58 o 0 1 1 943.05 937.68 13.96 o -3 2 1 4154.32 4289.36 59.74 o -2 2 1 1541.33 1523.60 34.28 o -1 2 1 483.81 508.18 6.47 o 0 2 1 3.24 2.06 0.65 o 1 2 1 797.57 759.97 15.34 o 2 2 1 977.41 1013.76 29.49 o -4 3 1 374.20 360.64 18.49 o -3 3 1 638.59 672.93 17.46 o -2 3 1 1849.65 1937.46 34.22 o -1 3 1 120.73 112.04 5.47 o 0 3 1 28.79 23.84 5.22 o 1 3 1 129.17 131.96 6.32 o 2 3 1 258.11 229.21 13.27 o 3 3 1 13.51 14.43 5.73 o -5 4 1 7.16 3.42 5.48 o -4 4 1 83.30 98.69 8.84 o -3 4 1 3656.60 4070.00 115.13 o -2 4 1 849.34 773.36 22.29 o -1 4 1 42.84 36.92 2.91 o 0 4 1 2.53 2.04 1.81 o 1 4 1 30.86 27.41 3.06 o 2 4 1 80.88 83.55 7.17 o 3 4 1 4.28 6.33 3.51 o -5 5 1 7.77 7.86 7.69 o -4 5 1 1.81 1.79 5.70 o -3 5 1 71.11 57.89 7.92 o -1 5 1 8.41 8.53 4.14 o 0 5 1 0.57 2.38 4.03 o 1 5 1 127.07 131.77 9.17 o 2 5 1 231.64 187.93 14.08 o 3 5 1 0.84 6.19 6.34 o 4 5 1 256.34 202.58 34.03 o -5 6 1 46.79 45.10 11.13 o -4 6 1 40.83 37.29 7.92 o -3 6 1 136.12 140.08 17.14 o -2 6 1 197.77 181.27 14.29 o -1 6 1 23.93 30.29 8.94 o 0 6 1 6.90 5.01 5.44 o 1 6 1 53.79 69.17 9.27 o 2 6 1 82.96 86.16 13.26 o 3 6 1 6.99 3.60 6.98 o 4 6 1 1.93 19.62 14.60 o -5 7 1 0.06 13.08 9.08 o -3 7 1 31.99 50.41 11.66 o -2 7 1 108.85 128.93 20.72 o -1 7 1 13.75 14.88 7.02 o 0 7 1 7.74 13.84 7.29 o 1 7 1 0.06 4.46 7.69 o 3 7 1 8.77 16.27 10.21 o 4 7 1 93.93 128.65 21.65 o -2 0 2 1462.45 1458.16 23.88 o -3 1 2 307.59 381.91 18.20 o -1 1 2 50.41 56.02 1.72 o 0 1 2 4494.09 4626.43 40.21 o -4 2 2 46.98 42.40 6.24 o -3 2 2 2.20 0.99 1.58 o -2 2 2 275.19 298.54 7.07 o -1 2 2 3276.26 3153.95 50.75 o 0 2 2 2406.84 2431.55 29.09 o 1 2 2 187.41 165.93 9.20 o -5 3 2 72.57 61.98 12.61 o -4 3 2 6.11 5.93 2.71 o -3 3 2 94.32 112.55 5.62 o -2 3 2 525.99 507.57 11.36 o -1 3 2 233.63 208.23 5.21 o 0 3 2 314.24 364.13 12.71 o 1 3 2 303.13 269.67 30.74 o 2 3 2 21.59 15.85 4.98 o -5 4 2 5.35 6.70 5.57 o -4 4 2 5.51 2.86 3.44 o -3 4 2 10.23 4.85 3.16 o -1 4 2 90.79 94.55 4.74 o 1 4 2 184.79 191.65 13.06 o 2 4 2 85.49 90.43 10.44 o 3 4 2 129.41 146.65 16.47 o -5 5 2 15.36 12.34 7.52 o -4 5 2 194.51 190.07 13.61 o -3 5 2 36.27 16.80 4.69 o -2 5 2 159.65 165.94 9.77 o -1 5 2 229.31 252.94 12.36 o 1 5 2 68.16 59.89 12.89 o 2 5 2 87.28 75.56 10.88 o 3 5 2 28.23 30.71 7.34 o -6 6 2 319.96 346.90 32.19 o -5 6 2 478.33 509.83 32.78 o -4 6 2 39.85 31.65 10.54 o -3 6 2 395.33 398.22 31.68 o -2 6 2 15.91 12.91 6.21 o -1 6 2 149.11 157.89 13.25 o 0 6 2 174.20 156.73 11.89 o 1 6 2 9.61 8.30 5.89 o 2 6 2 0.49 10.16 7.90 o 3 6 2 55.47 50.26 11.47 o -5 7 2 66.01 64.89 13.78 o -4 7 2 19.60 21.80 10.63 o -3 7 2 3.60 3.27 6.98 o -2 7 2 12.13 27.13 9.75 o -1 7 2 12.65 20.91 7.34 o 0 7 2 8.09 17.42 6.66 o 1 7 2 138.72 113.07 15.82 o 2 7 2 14.68 22.52 9.77 o 3 7 2 38.78 47.42 13.23 o -1 1 3 1029.88 1024.02 14.33 o 0 1 3 1542.21 1588.37 31.95 o -4 2 3 716.83 737.70 19.13 o -3 2 3 280.72 290.38 9.41 o -2 2 3 147.45 161.20 4.61 o -1 2 3 3.03 1.19 0.79 o 0 2 3 385.60 396.08 10.85 o -5 3 3 0.01 3.36 3.40 o -4 3 3 91.26 91.63 8.98 o -3 3 3 291.00 299.77 10.11 o -2 3 3 1320.96 1247.71 52.89 o -1 3 3 147.30 125.66 8.96 o 0 3 3 0.42 5.89 2.55 o 1 3 3 505.54 514.66 30.61 o 2 3 3 1344.63 1349.30 54.03 o -6 4 3 32.00 29.38 7.66 o -5 4 3 11.11 19.95 5.24 o -4 4 3 35.69 40.91 6.56 o -3 4 3 33.99 38.15 3.67 o -2 4 3 5.91 4.76 1.99 o -1 4 3 33.84 26.68 3.15 o 0 4 3 23.79 20.67 3.06 o 1 4 3 123.08 112.04 10.19 o 2 4 3 143.22 160.71 17.25 o -6 5 3 2.57 2.54 17.93 o -5 5 3 41.25 43.57 9.39 o -4 5 3 314.05 345.53 19.63 o -3 5 3 262.84 228.80 11.29 o -2 5 3 174.95 184.56 9.72 o -1 5 3 333.27 330.97 13.01 o 1 5 3 7.28 7.10 4.20 o 2 5 3 465.61 495.51 27.94 o 3 5 3 84.48 116.55 32.20 o -6 6 3 183.03 211.59 21.54 o -5 6 3 15.02 31.41 8.45 o -4 6 3 0.48 8.17 7.81 o -3 6 3 31.93 35.00 6.45 o -2 6 3 0.05 8.90 4.09 o -1 6 3 0.98 5.99 4.67 o 0 6 3 0.01 3.68 4.09 o 1 6 3 5.48 9.03 7.25 o 2 6 3 2.01 8.36 6.53 o 3 6 3 19.31 7.14 8.52 o -6 7 3 0.90 2.54 25.38 o -5 7 3 0.26 13.17 8.72 o -4 7 3 11.99 6.75 7.65 o -3 7 3 16.83 13.43 9.10 o -2 7 3 0.23 9.33 5.60 o -1 7 3 39.58 48.09 8.36 o 0 7 3 28.37 27.52 9.47 o 1 7 3 19.23 31.76 11.11 o 2 7 3 5.67 13.44 9.43 o 3 7 3 5.29 23.89 13.84 o -4 0 4 2859.28 2723.88 78.76 o -3 0 4 1048.69 1063.56 24.44 o -2 0 4 497.82 484.14 14.94 o 0 0 4 402.94 390.32 31.68 o -5 1 4 824.42 665.44 47.94 o -4 1 4 926.61 1057.02 17.38 o -2 1 4 3699.51 3911.99 32.28 o -1 1 4 2622.14 2769.82 28.77 o 0 1 4 9594.42 10365.07 173.14 o -5 2 4 1249.08 1412.58 37.73 o -4 2 4 21.18 20.67 2.55 o -3 2 4 1427.88 1411.12 57.41 o -2 2 4 1239.86 1376.91 26.94 o 0 2 4 395.60 351.22 17.75 o 1 2 4 11.06 7.21 5.07 o -6 3 4 339.95 368.75 20.54 o -5 3 4 327.65 317.93 16.15 o -4 3 4 182.53 159.37 9.30 o -3 3 4 7.03 5.78 1.37 o -2 3 4 9.19 13.75 2.38 o -1 3 4 867.44 811.40 25.22 o 0 3 4 1572.91 1702.29 46.09 o 1 3 4 10.22 0.83 3.80 o -6 4 4 49.04 35.06 7.26 o -5 4 4 109.22 110.68 11.25 o -4 4 4 51.57 47.12 5.22 o -3 4 4 4.86 11.17 2.80 o -2 4 4 1.60 2.49 2.26 o -1 4 4 76.38 85.50 5.69 o 0 4 4 31.97 20.63 4.59 o 1 4 4 73.64 58.31 8.88 o 2 4 4 29.27 21.10 10.08 o -7 5 4 44.96 33.28 11.43 o -6 5 4 149.08 180.44 15.34 o -5 5 4 9.51 9.49 4.40 o -4 5 4 133.93 153.15 11.00 o -3 5 4 152.71 177.68 8.78 o -2 5 4 28.70 24.47 3.69 o -1 5 4 6.81 6.18 2.70 o 1 5 4 79.25 91.36 10.03 o 2 5 4 159.51 156.19 18.64 o -7 6 4 196.11 200.30 25.03 o -6 6 4 16.77 10.23 7.74 o -5 6 4 5.14 14.29 6.36 o -4 6 4 17.92 7.98 4.82 o -3 6 4 2.76 9.13 4.84 o -2 6 4 41.80 45.02 6.40 o -1 6 4 49.98 47.24 6.11 o 0 6 4 3.89 3.01 5.11 o 1 6 4 0.03 2.82 5.88 o 2 6 4 38.00 44.66 11.67 o -6 7 4 52.68 30.72 11.99 o -5 7 4 2.11 6.97 10.26 o -4 7 4 42.89 41.29 12.03 o -3 7 4 5.78 7.44 8.15 o -2 7 4 105.44 99.48 16.58 o -1 7 4 5.56 4.02 7.36 o 0 7 4 104.80 125.29 19.27 o 1 7 4 13.62 6.69 8.84 o 2 7 4 145.84 137.86 22.76 o -5 1 5 170.21 172.29 7.99 o -3 1 5 4771.67 4811.49 57.40 o -2 1 5 66.54 63.19 3.45 o 0 1 5 128.87 139.69 23.21 o -6 2 5 36.80 32.17 6.10 o -5 2 5 13.14 15.20 3.00 o -4 2 5 728.03 803.79 14.71 o -3 2 5 42.16 45.41 2.70 o -2 2 5 95.02 103.46 4.12 o -1 2 5 189.95 177.79 6.69 o 0 2 5 341.84 353.04 20.02 o -6 3 5 161.22 173.40 12.55 o -5 3 5 685.80 596.99 28.29 o -4 3 5 340.16 341.44 10.66 o -3 3 5 2830.54 2731.79 57.79 o -2 3 5 657.30 614.59 17.59 o -1 3 5 170.07 176.72 8.42 o 0 3 5 97.24 113.66 14.52 o 1 3 5 106.48 100.91 12.79 o -7 4 5 221.48 233.65 21.51 o -6 4 5 175.95 192.94 14.53 o -4 4 5 196.37 186.91 9.72 o -3 4 5 46.61 56.25 4.74 o -2 4 5 159.51 170.02 7.47 o -1 4 5 353.77 338.17 12.98 o 0 4 5 573.35 576.05 27.03 o 1 4 5 92.70 114.70 15.19 o -7 5 5 146.15 125.27 17.20 o -6 5 5 19.84 15.19 4.91 o -5 5 5 480.22 515.21 21.48 o -4 5 5 14.48 14.14 4.06 o -3 5 5 1307.85 1344.89 28.69 o -2 5 5 0.13 5.92 3.31 o -1 5 5 142.16 183.43 11.45 o 0 5 5 3.00 2.86 4.84 o 1 5 5 62.98 66.36 9.67 o 2 5 5 26.46 23.29 22.87 o -7 6 5 4.49 5.29 7.92 o -6 6 5 22.50 23.71 9.13 o -5 6 5 1.86 3.74 8.89 o -4 6 5 79.35 81.44 16.46 o -3 6 5 2.60 10.94 4.74 o -2 6 5 34.46 27.03 4.74 o -1 6 5 42.72 42.11 11.41 o 0 6 5 7.37 11.08 5.16 o 1 6 5 43.84 36.28 8.76 o 2 6 5 0.02 5.86 7.73 o -6 7 5 81.69 72.15 20.31 o -5 7 5 0.01 9.27 9.82 o -4 7 5 26.10 43.21 14.66 o -3 7 5 49.89 49.09 13.65 o -2 7 5 64.34 45.17 13.91 o -1 7 5 5.41 16.41 9.72 o 0 7 5 23.45 36.47 13.30 o 1 7 5 40.43 27.66 15.90 o -6 0 6 199.05 170.52 19.45 o -5 0 6 422.24 432.94 19.09 o -4 0 6 894.39 925.12 23.56 o -3 0 6 2871.17 2640.60 45.08 o -2 0 6 86.53 88.83 8.01 o -1 0 6 11.55 12.42 3.37 o -6 1 6 1982.87 1860.56 40.28 o -5 1 6 992.75 1104.76 35.25 o -4 1 6 1.52 2.26 0.84 o -3 1 6 290.85 315.53 8.71 o -2 1 6 16.22 17.13 1.57 o -1 1 6 491.72 462.84 12.08 o 0 1 6 34.78 33.97 9.36 o -7 2 6 343.91 410.57 32.82 o -6 2 6 43.10 41.26 6.48 o -5 2 6 1177.28 1282.22 19.00 o -4 2 6 833.04 873.58 12.36 o -2 2 6 2.52 2.71 1.43 o -1 2 6 1014.38 971.71 27.20 o 0 2 6 14.80 24.05 7.57 o -7 3 6 6.55 1.73 5.53 o -6 3 6 39.59 37.93 5.48 o -5 3 6 498.81 501.03 14.41 o -4 3 6 18.23 24.45 3.45 o -3 3 6 365.50 392.81 10.73 o -2 3 6 333.20 321.94 11.15 o -1 3 6 0.45 1.92 2.74 o 0 3 6 288.82 326.50 25.83 o 1 3 6 31.27 26.24 15.34 o -7 4 6 16.68 8.60 5.11 o -6 4 6 159.65 175.94 11.38 o -5 4 6 100.14 95.43 6.70 o -2 4 6 0.04 10.64 3.90 o -1 4 6 210.10 195.20 14.72 o 0 4 6 167.80 158.12 17.21 o -8 5 6 28.18 29.69 11.35 o -6 5 6 92.36 89.21 9.54 o -5 5 6 81.55 81.75 7.74 o -3 5 6 4.21 6.73 3.71 o -2 5 6 0.20 3.60 3.79 o -1 5 6 1.02 5.31 5.13 o 0 5 6 2.65 6.96 6.04 o 1 5 6 11.21 22.48 10.92 o -8 6 6 0.57 13.27 8.56 o -7 6 6 22.57 33.96 9.74 o -6 6 6 27.50 35.27 7.40 o -5 6 6 0.78 6.26 6.18 o -4 6 6 113.02 122.75 15.51 o -3 6 6 34.38 29.09 4.82 o -2 6 6 45.80 39.56 6.56 o -1 6 6 121.61 127.92 14.29 o 0 6 6 5.18 10.47 6.96 o 1 6 6 413.16 420.11 34.61 o -6 7 6 164.74 182.94 28.23 o -5 7 6 21.25 25.81 15.03 o -4 7 6 0.04 16.39 7.86 o -3 7 6 22.06 23.52 11.06 o -2 7 6 1.01 10.19 10.11 o -1 7 6 25.27 30.11 11.80 o 0 7 6 69.24 62.20 18.31 o -7 1 7 332.21 300.22 22.61 o -6 1 7 0.16 4.66 2.71 o -5 1 7 2.55 3.96 1.08 o -4 1 7 3.98 3.78 1.69 o -3 1 7 23.63 21.68 2.70 o -2 1 7 95.60 105.39 4.87 o -1 1 7 105.36 109.04 10.47 o -7 2 7 1.36 8.16 4.93 o -6 2 7 9.51 8.95 2.44 o -5 2 7 143.71 141.03 5.79 o -4 2 7 167.06 171.86 5.87 o -3 2 7 79.49 82.77 4.01 o -2 2 7 246.16 283.14 8.54 o -1 2 7 632.39 638.25 46.60 o 0 2 7 802.98 853.30 77.45 o -8 3 7 298.05 266.86 27.22 o -7 3 7 0.99 6.44 5.05 o -6 3 7 22.31 20.31 2.85 o -5 3 7 3.74 7.91 2.28 o -4 3 7 135.71 145.06 7.69 o -3 3 7 63.24 61.48 4.57 o -2 3 7 12.12 13.67 2.98 o -1 3 7 12.69 1.86 5.09 o 0 3 7 1.55 1.51 6.40 o -8 4 7 71.99 83.51 14.31 o -7 4 7 225.25 212.71 14.85 o -6 4 7 50.55 46.14 5.32 o -5 4 7 296.74 290.73 12.92 o -4 4 7 418.23 401.75 14.75 o -3 4 7 39.37 42.53 5.08 o -2 4 7 117.99 109.04 9.53 o -1 4 7 125.47 124.21 14.46 o 0 4 7 532.16 580.48 35.04 o -8 5 7 407.58 385.25 27.79 o -7 5 7 75.86 83.75 10.38 o -6 5 7 60.30 47.48 7.38 o -5 5 7 0.16 6.52 4.64 o -4 5 7 60.65 58.45 5.12 o -3 5 7 60.89 67.14 6.68 o -2 5 7 6.08 6.51 4.01 o -1 5 7 12.64 19.50 6.74 o 0 5 7 51.39 61.46 10.06 o -8 6 7 40.40 46.34 12.67 o -7 6 7 3.03 15.61 7.13 o -6 6 7 14.01 27.80 7.53 o -5 6 7 1.62 2.65 5.39 o -4 6 7 8.48 12.65 5.63 o -3 6 7 0.41 12.21 5.90 o -2 6 7 1.46 12.26 6.67 o -1 6 7 22.66 37.83 8.69 o 0 6 7 80.41 61.81 18.38 o -5 7 7 16.01 9.84 13.53 o -4 7 7 13.70 23.79 12.91 o -7 0 8 1433.16 1343.65 127.54 o -6 0 8 113.96 117.79 10.52 o -5 0 8 1317.14 1331.20 33.31 o -4 0 8 794.94 705.72 23.95 o -3 0 8 283.17 270.39 16.66 o -2 0 8 14.10 10.50 4.12 o -1 0 8 1490.09 1254.29 79.10 o -8 1 8 10.06 36.80 12.84 o -7 1 8 3.81 8.06 4.09 o -6 1 8 5.97 6.27 2.75 o -5 1 8 13.47 11.77 3.30 o -4 1 8 0.60 1.37 1.76 o -3 1 8 254.12 263.68 10.25 o -2 1 8 678.41 688.16 21.86 o -1 1 8 70.15 67.57 17.81 o -8 2 8 1.79 1.11 6.33 o -7 2 8 980.10 966.67 32.76 o -6 2 8 74.96 70.82 7.05 o -5 2 8 224.74 222.56 10.08 o -4 2 8 596.77 603.21 15.76 o -3 2 8 78.72 71.83 5.99 o -1 2 8 0.42 1.72 5.92 o -8 3 8 31.13 25.85 9.41 o -7 3 8 18.82 13.95 10.35 o -6 3 8 175.07 179.11 13.30 o -5 3 8 110.15 111.02 8.20 o -4 3 8 26.57 19.38 3.88 o -3 3 8 49.24 40.28 5.31 o -2 3 8 24.92 24.24 5.90 o -1 3 8 152.08 153.58 23.48 o 0 3 8 41.23 36.57 18.09 o -8 4 8 79.18 70.16 13.91 o -7 4 8 248.83 255.80 19.01 o -6 4 8 65.90 63.72 6.64 o -5 4 8 27.16 44.05 6.36 o -4 4 8 73.44 51.49 6.62 o -3 4 8 40.36 42.31 6.01 o -1 4 8 2.59 1.54 10.79 o 0 4 8 292.18 298.22 75.19 o -8 5 8 12.40 1.63 11.42 o -7 5 8 11.24 4.91 8.26 o -5 5 8 32.08 23.95 6.06 o -4 5 8 23.61 19.93 6.18 o -2 5 8 5.45 17.45 15.44 o -1 5 8 34.67 22.44 12.97 o 0 5 8 25.50 14.20 18.67 o -8 6 8 130.86 146.65 29.79 o -7 6 8 0.00 13.55 10.39 o -6 6 8 228.84 214.97 27.99 o -5 6 8 1.41 14.62 8.23 o -2 6 8 51.50 25.07 12.41 o -1 6 8 149.71 172.26 29.96 o 0 6 8 77.40 101.98 32.62 o -8 1 9 27.10 19.90 7.28 o -6 1 9 124.03 131.35 8.05 o -5 1 9 5.60 6.08 3.26 o -4 1 9 222.88 211.83 9.53 o -3 1 9 6.04 2.78 3.27 o -2 1 9 114.92 123.02 14.59 o -8 2 9 1.13 9.90 6.88 o -7 2 9 258.96 255.07 23.39 o -6 2 9 3.58 6.40 3.90 o -5 2 9 755.56 754.79 22.35 o -4 2 9 53.75 46.55 4.94 o -3 2 9 372.45 363.77 16.71 o -2 2 9 18.20 13.98 4.79 o -1 2 9 14.44 8.06 11.28 o -9 3 9 213.10 186.26 27.98 o -8 3 9 106.16 81.26 14.75 o -7 3 9 7.54 11.46 6.64 o -6 3 9 59.44 53.53 7.95 o -5 3 9 326.44 335.66 19.81 o -4 3 9 104.55 84.34 10.19 o -3 3 9 237.00 224.31 18.28 o -2 3 9 19.65 24.52 10.90 o -1 3 9 112.71 101.24 35.73 o -8 4 9 23.12 39.55 11.98 o -7 4 9 7.62 12.32 5.97 o -6 4 9 23.27 20.17 9.34 o -5 4 9 292.79 272.56 18.98 o -4 4 9 73.62 89.82 11.75 o -3 4 9 457.09 483.37 27.92 o -2 4 9 39.16 42.69 18.11 o -1 4 9 36.28 50.83 23.32 o -9 5 9 34.89 41.90 19.15 o -8 5 9 19.99 19.21 12.43 o -7 5 9 4.48 7.06 7.34 o -6 5 9 1.10 10.45 7.39 o -5 5 9 1.09 14.34 5.99 o -4 5 9 309.33 317.27 23.77 o -3 5 9 26.76 19.30 15.27 o -2 5 9 11.17 2.31 16.23 o -1 5 9 68.78 76.63 21.29 o -8 6 9 0.11 2.23 22.34 o -7 6 9 0.34 7.43 16.73 o -6 6 9 2.77 14.23 20.31 o -5 6 9 130.31 102.63 20.26 o -4 6 9 4.76 1.90 12.98 o -3 6 9 81.64 143.10 54.06 o -8 0 10 1425.56 1406.61 54.38 o -7 0 10 12.34 10.22 5.42 o -6 0 10 2318.05 2332.84 50.70 o -5 0 10 83.09 95.95 10.30 o -4 0 10 14.53 10.78 4.25 o -3 0 10 45.22 47.22 8.55 o -2 0 10 95.13 67.40 13.90 o -9 1 10 142.78 120.78 20.76 o -8 1 10 2.56 4.33 3.95 o -7 1 10 1781.20 1807.22 45.10 o -6 1 10 635.49 634.54 18.53 o -5 1 10 97.42 89.28 6.88 o -4 1 10 488.38 475.97 15.26 o -3 1 10 65.93 66.37 7.58 o -9 2 10 285.78 270.86 27.82 o -8 2 10 150.49 159.34 14.29 o -7 2 10 305.89 307.83 17.07 o -6 2 10 495.65 498.41 20.05 o -5 2 10 22.21 29.51 5.09 o -4 2 10 2.66 3.55 4.30 o -3 2 10 103.62 122.02 11.70 o -2 2 10 19.32 16.29 10.27 o -9 3 10 38.05 37.89 14.53 o -8 3 10 55.95 35.37 8.92 o -7 3 10 486.44 484.53 25.70 o -6 3 10 35.90 40.48 8.11 o -5 3 10 84.04 79.53 10.65 o -4 3 10 416.11 395.02 22.53 o -3 3 10 4.36 4.31 5.71 o -2 3 10 2.49 1.99 11.51 o -9 4 10 33.26 29.08 12.44 o -8 4 10 43.54 51.21 12.61 o -7 4 10 0.78 2.95 5.51 o -6 4 10 81.81 86.92 11.78 o -5 4 10 0.18 10.75 6.02 o -4 4 10 22.26 22.64 7.07 o -3 4 10 17.32 2.03 14.07 o -2 4 10 31.51 40.52 16.61 o -9 5 10 8.51 18.88 17.97 o -8 5 10 11.06 15.49 12.57 o -7 5 10 0.24 9.96 8.48 o -6 5 10 125.17 131.13 14.74 o -4 5 10 3.29 8.87 7.33 o -3 5 10 397.10 458.67 50.44 o -2 5 10 0.01 1.41 11.36 o -9 1 11 0.43 2.45 5.36 o -8 1 11 0.84 2.25 4.69 o -7 1 11 148.09 167.92 11.09 o -6 1 11 156.74 168.65 11.08 o -5 1 11 3.28 6.24 4.07 o -4 1 11 28.73 28.98 4.75 o -3 1 11 0.08 7.17 6.75 o -9 2 11 39.78 28.03 11.15 o -8 2 11 5.47 2.82 6.84 o -7 2 11 0.08 5.31 4.87 o -6 2 11 13.06 5.47 5.41 o -5 2 11 1.42 6.37 4.35 o -4 2 11 36.22 31.16 6.41 o -3 2 11 3.67 3.96 6.75 o -2 2 11 6.16 10.34 22.72 o -10 3 11 370.61 348.37 75.88 o -9 3 11 60.54 66.41 14.07 o -8 3 11 85.39 89.75 11.99 o -7 3 11 0.45 9.28 6.19 o -6 3 11 2.10 13.22 7.75 o -5 3 11 64.84 73.87 10.98 o -4 3 11 46.37 32.52 8.97 o -3 3 11 30.08 51.20 16.51 o -2 3 11 2.01 11.06 16.14 o -9 4 11 39.35 38.85 13.60 o -8 4 11 143.94 138.59 16.32 o -7 4 11 12.67 8.72 6.22 o -6 4 11 72.73 62.76 9.69 o -5 4 11 27.46 21.59 10.69 o -4 4 11 2.66 6.95 8.90 o -3 4 11 21.71 24.04 10.73 o -2 4 11 2.05 7.31 13.33 o -8 5 11 16.90 16.92 21.78 o -7 5 11 9.18 39.74 29.13 o -6 5 11 25.36 51.10 27.07 o -5 5 11 10.91 29.02 20.11 o -9 0 12 6.71 11.85 10.73 o -8 0 12 111.33 104.64 12.71 o -7 0 12 30.74 31.54 5.91 o -6 0 12 44.98 53.88 11.25 o -5 0 12 599.63 651.57 30.45 o -4 0 12 184.28 185.41 21.70 o -10 1 12 0.09 28.06 17.13 o -9 1 12 24.50 15.74 6.85 o -8 1 12 85.54 80.03 10.22 o -7 1 12 416.22 443.09 21.92 o -6 1 12 17.58 9.53 5.36 o -5 1 12 36.93 44.10 7.72 o -4 1 12 381.42 407.57 22.08 o -3 1 12 352.51 281.82 71.24 o -10 2 12 11.23 23.47 17.30 o -9 2 12 27.32 38.65 13.12 o -8 2 12 21.95 18.59 7.81 o -7 2 12 2.46 3.57 5.49 o -6 2 12 4.84 9.29 5.23 o -5 2 12 12.25 10.56 5.82 o -4 2 12 8.02 13.03 7.30 o -3 2 12 2.26 32.41 21.84 o -10 3 12 0.07 23.28 14.38 o -9 3 12 3.31 5.69 7.51 o -8 3 12 7.41 6.16 6.09 o -7 3 12 17.14 18.30 5.96 o -6 3 12 9.49 11.64 6.61 o -5 3 12 19.53 18.72 7.38 o -4 3 12 0.02 6.14 9.68 o -3 3 12 7.90 4.88 9.95 o -8 4 12 7.06 19.66 19.68 o -7 4 12 6.27 2.80 9.69 o -6 4 12 10.61 4.95 9.75 o -5 4 12 26.77 23.10 15.13 o -10 1 13 5.91 2.01 10.92 o -9 1 13 31.96 46.53 8.98 o -8 1 13 7.07 7.37 5.34 o -7 1 13 0.78 7.42 5.79 o -6 1 13 29.71 23.11 7.26 o -5 1 13 0.00 9.14 5.51 o -4 1 13 48.25 60.07 19.68 o -10 2 13 3.72 10.73 16.06 o -9 2 13 36.80 49.20 10.46 o -8 2 13 1.42 13.55 6.33 o -7 2 13 19.99 20.35 7.77 o -6 2 13 15.43 14.54 9.66 o -5 2 13 76.31 80.86 12.88 o -4 2 13 185.82 175.99 31.54 o -9 3 13 0.41 8.39 12.05 o -8 3 13 28.93 4.88 9.84 o -7 3 13 20.55 22.62 14.89 o -6 3 13 26.38 27.24 16.60 o -5 3 13 147.57 70.13 26.95 o -10 0 14 15.53 1.13 11.32 o -9 0 14 53.27 40.84 13.74 o -8 0 14 317.37 319.79 39.29 o -7 0 14 923.14 976.24 68.96 o -6 0 14 33.05 52.47 16.19 o -5 0 14 249.67 263.41 36.18 o -10 1 14 6.71 20.15 27.65 o -9 1 14 0.56 9.60 8.14 o -8 1 14 234.11 253.51 22.18 o -7 1 14 74.00 94.47 10.99 o -6 1 14 67.54 68.09 11.43 o -5 1 14 14.99 17.45 10.75 o -9 2 14 26.11 57.45 19.73 o -8 2 14 159.53 215.55 50.54 o -7 2 14 253.61 223.65 48.44 o -6 2 14 368.66 415.04 67.86 o