#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/54/2105454.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105454_Fobs loop_ _publ_author_name 'Zakharov, Boris A.' 'Boldyreva, Elena V.' _publ_section_title ; A high-pressure single-crystal to single-crystal phase transition in DL-alaninium semi-oxalate monohydrate with switching-over hydrogen bonds ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 271 _journal_page_last 280 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.795 _cell_angle_gamma 90.000 _cell_length_a 11.9049 _cell_length_b 5.9492 _cell_length_c 11.1846 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7555 _[local]_cod_data_source_file gp5064430sup9.hkl _[local]_cod_data_source_block 430 #BEGIN Tags that were not found in dictionaries: _shelx_title 'E 9-433' _shelx_refln_list_code 4 _shelx_f_calc_maximum 100.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 432.50 403.40 9.42 o 0 2 0 9999.61 10778.60 125.74 o 1 2 0 6555.58 6761.82 107.80 o 2 2 0 1958.31 1744.50 52.65 o 1 3 0 92.19 88.92 4.86 o 2 3 0 85.03 82.95 6.65 o 3 3 0 51.17 45.29 6.09 o 0 4 0 1300.63 1293.94 33.98 o 1 4 0 1.07 3.01 1.99 o 2 4 0 473.16 505.36 36.97 o 3 4 0 460.12 477.54 18.09 o 4 4 0 217.62 233.20 14.01 o 1 5 0 150.50 158.09 10.90 o 2 5 0 59.07 50.50 18.48 o 3 5 0 238.36 207.24 21.13 o 4 5 0 149.65 147.07 18.97 o 0 6 0 182.48 168.95 20.29 o 1 6 0 143.65 134.80 11.20 o 3 6 0 132.51 169.85 18.49 o 4 6 0 632.69 626.67 36.01 o 5 6 0 8.23 1.43 10.05 o 1 7 0 5.53 16.22 7.64 o 3 7 0 84.19 71.56 13.60 o 4 7 0 9.86 23.69 10.65 o -2 1 1 144.98 120.85 5.73 o -1 1 1 335.33 340.25 6.07 o 0 1 1 944.87 918.50 17.72 o -3 2 1 4342.77 4485.15 90.76 o -2 2 1 1641.08 1618.81 32.82 o -1 2 1 600.77 621.26 7.00 o 0 2 1 4.83 1.59 0.93 o 1 2 1 851.76 778.02 15.27 o 2 2 1 838.09 855.31 26.36 o -4 3 1 367.79 387.80 18.89 o -3 3 1 684.14 676.02 17.09 o -2 3 1 1819.99 1931.24 30.12 o -1 3 1 109.04 120.99 4.48 o 0 3 1 44.05 54.91 4.08 o 1 3 1 134.96 130.09 6.19 o 2 3 1 238.59 232.68 12.97 o 3 3 1 6.22 6.92 4.61 o -5 4 1 8.46 3.34 5.93 o -4 4 1 72.19 86.51 8.24 o -3 4 1 3721.74 4112.93 93.09 o -2 4 1 934.39 862.74 28.02 o -1 4 1 37.24 28.54 2.51 o 0 4 1 0.44 1.42 2.33 o 1 4 1 28.24 29.60 3.52 o 2 4 1 78.95 82.23 7.22 o 3 4 1 4.64 5.12 3.39 o -5 5 1 6.13 15.27 9.48 o -4 5 1 4.20 7.10 6.81 o -3 5 1 87.91 86.43 9.87 o -1 5 1 3.39 5.84 4.21 o 0 5 1 0.21 5.17 3.51 o 2 5 1 249.93 238.27 15.89 o 3 5 1 3.43 14.89 8.58 o 4 5 1 271.29 244.09 29.75 o -5 6 1 48.71 60.55 17.00 o -4 6 1 25.11 45.17 13.53 o -2 6 1 187.21 177.26 14.11 o 0 6 1 4.07 9.99 5.24 o 2 6 1 81.45 101.63 17.05 o 3 6 1 6.87 7.12 8.19 o -5 7 1 0.02 18.88 13.05 o -4 7 1 7.57 16.37 13.58 o -3 7 1 41.96 45.52 11.49 o -2 7 1 109.47 109.01 19.74 o -1 7 1 12.75 11.33 6.88 o 1 7 1 2.11 6.84 10.12 o 3 7 1 5.16 10.93 9.15 o 4 7 1 70.69 118.34 21.96 o -2 0 2 1385.12 1368.65 38.33 o -3 1 2 301.66 385.21 17.85 o -1 1 2 41.24 49.44 1.59 o 0 1 2 4344.34 4409.73 43.66 o -4 2 2 21.50 14.60 3.63 o -3 2 2 1.70 1.25 1.78 o -2 2 2 265.76 276.87 6.68 o -1 2 2 3424.55 3299.64 59.22 o 0 2 2 2456.50 2476.69 38.06 o 1 2 2 214.20 199.66 9.87 o -5 3 2 67.89 63.68 12.80 o -4 3 2 3.32 7.00 2.82 o -3 3 2 98.05 112.90 7.08 o -2 3 2 479.82 443.73 10.44 o -1 3 2 244.20 222.86 6.33 o 0 3 2 344.18 392.49 20.83 o 1 3 2 258.31 228.77 21.42 o 2 3 2 25.37 13.06 5.64 o -5 4 2 19.69 25.95 7.00 o -4 4 2 17.00 16.68 4.86 o -3 4 2 16.58 14.33 3.31 o -2 4 2 105.42 126.47 6.48 o -1 4 2 75.31 86.88 4.68 o 0 4 2 8.62 18.05 5.37 o 2 4 2 67.46 78.24 9.81 o 3 4 2 131.00 137.17 15.06 o -5 5 2 13.11 7.27 5.87 o -4 5 2 177.43 190.38 13.20 o -3 5 2 47.34 28.45 6.13 o -2 5 2 159.48 143.80 8.50 o -1 5 2 209.81 233.22 11.35 o 0 5 2 54.75 56.80 5.59 o 1 5 2 77.46 61.46 16.34 o 2 5 2 76.17 72.73 10.77 o 3 5 2 13.70 26.25 11.75 o -6 6 2 360.55 353.07 32.43 o -5 6 2 551.43 525.38 33.10 o -4 6 2 14.78 16.52 9.89 o -3 6 2 407.06 401.25 30.88 o -2 6 2 13.89 10.76 5.33 o -1 6 2 120.23 118.09 11.18 o 0 6 2 164.28 164.65 11.81 o 1 6 2 12.50 5.79 6.26 o 2 6 2 3.30 12.32 6.98 o 3 6 2 71.07 82.09 13.67 o -5 7 2 69.92 49.94 13.28 o -4 7 2 28.09 14.42 10.93 o -3 7 2 1.80 8.41 8.88 o -2 7 2 12.59 16.71 9.16 o -1 7 2 17.57 27.57 7.76 o 0 7 2 7.91 12.46 6.09 o 1 7 2 145.16 131.62 25.32 o 2 7 2 10.67 21.77 12.46 o 3 7 2 56.02 60.98 16.40 o -1 1 3 1061.70 1067.01 15.71 o 0 1 3 1572.09 1557.87 30.96 o -4 2 3 694.35 752.92 19.25 o -3 2 3 301.67 315.56 9.64 o -2 2 3 192.27 199.62 5.02 o -1 2 3 3.96 1.72 0.81 o 0 2 3 381.21 382.48 11.38 o -5 3 3 0.00 3.09 3.31 o -4 3 3 76.14 50.48 11.65 o -3 3 3 266.92 286.84 9.67 o -2 3 3 1310.54 1208.25 45.94 o -1 3 3 130.26 116.84 8.34 o 0 3 3 4.22 10.86 2.91 o 1 3 3 580.72 596.98 32.06 o 2 3 3 1519.39 1595.29 186.28 o -6 4 3 38.36 36.77 9.02 o -5 4 3 7.60 10.65 4.53 o -4 4 3 32.16 34.71 5.92 o -3 4 3 41.14 48.78 4.54 o -2 4 3 8.75 9.02 2.29 o -1 4 3 44.66 40.69 3.84 o 0 4 3 18.48 15.58 3.00 o 1 4 3 113.06 108.88 10.29 o 2 4 3 117.57 138.53 15.16 o -6 5 3 0.81 7.29 9.46 o -5 5 3 45.99 44.02 6.72 o -4 5 3 388.95 406.92 20.89 o -3 5 3 303.87 283.93 12.30 o -2 5 3 169.32 177.53 9.41 o -1 5 3 379.52 369.54 13.55 o 1 5 3 5.53 2.53 4.22 o 2 5 3 478.01 503.06 27.62 o 3 5 3 101.58 205.98 95.07 o -6 6 3 200.17 252.01 23.36 o -5 6 3 15.84 22.72 7.66 o -4 6 3 0.28 5.91 7.82 o -3 6 3 31.35 24.34 6.29 o -2 6 3 0.14 9.53 5.06 o -1 6 3 1.22 2.86 4.70 o 0 6 3 0.23 3.72 4.78 o 1 6 3 6.93 4.25 7.32 o 3 6 3 13.65 1.96 7.52 o -5 7 3 1.11 6.94 8.72 o -4 7 3 14.44 24.43 12.71 o -3 7 3 16.38 12.59 11.37 o -2 7 3 0.37 5.57 7.77 o -1 7 3 46.86 42.42 10.74 o 0 7 3 27.75 25.63 10.34 o 1 7 3 12.38 17.25 10.25 o 2 7 3 7.08 11.45 11.00 o -4 0 4 2820.93 2619.70 55.67 o -3 0 4 958.54 1016.66 22.19 o -2 0 4 495.68 474.13 14.35 o -1 0 4 250.47 212.73 11.84 o 0 0 4 323.88 338.33 28.90 o -5 1 4 807.16 672.13 47.87 o -4 1 4 980.64 1042.30 16.89 o -3 1 4 3.40 4.33 0.96 o -2 1 4 3715.54 3896.72 35.93 o -1 1 4 2702.89 2744.56 59.93 o 0 1 4 9686.43 10129.90 167.54 o -5 2 4 1191.10 1335.54 48.70 o -4 2 4 24.09 22.18 2.63 o -3 2 4 1467.25 1390.67 49.78 o 0 2 4 313.49 289.22 15.81 o 1 2 4 17.65 14.91 4.87 o -6 3 4 367.17 373.18 20.19 o -5 3 4 308.40 298.92 15.26 o -4 3 4 155.49 152.89 9.07 o -3 3 4 5.93 5.57 1.47 o -2 3 4 14.73 18.70 2.95 o -1 3 4 790.65 702.20 20.75 o 0 3 4 1475.53 1604.59 43.57 o 1 3 4 11.79 5.67 4.42 o -5 4 4 122.74 127.38 11.03 o -4 4 4 74.02 71.94 6.68 o -3 4 4 3.36 2.01 2.21 o -2 4 4 2.44 3.40 2.45 o -1 4 4 51.93 69.14 5.10 o 0 4 4 56.78 34.70 6.45 o 1 4 4 60.52 39.41 6.74 o -7 5 4 60.80 57.15 17.52 o -6 5 4 159.11 164.52 22.08 o -5 5 4 9.62 5.52 4.93 o -4 5 4 133.90 153.50 10.59 o -3 5 4 150.63 174.47 8.82 o -2 5 4 12.18 16.09 3.53 o -1 5 4 0.74 5.90 3.08 o 0 5 4 310.95 334.95 17.98 o 1 5 4 70.63 75.32 9.30 o 2 5 4 163.57 147.00 18.50 o -7 6 4 217.09 204.15 24.73 o -6 6 4 15.56 22.34 8.61 o -5 6 4 11.37 11.58 7.56 o -4 6 4 21.48 29.32 8.82 o -3 6 4 4.89 13.14 5.39 o -2 6 4 31.70 26.39 4.89 o -1 6 4 54.72 51.84 6.47 o 0 6 4 1.10 7.46 5.33 o 1 6 4 1.92 19.59 10.55 o 2 6 4 41.23 24.13 12.34 o -6 7 4 50.42 11.70 21.87 o -5 7 4 2.94 25.87 11.58 o -4 7 4 42.70 38.05 12.39 o -3 7 4 8.06 22.15 10.36 o -2 7 4 118.55 108.38 14.77 o -1 7 4 3.27 16.79 9.59 o 0 7 4 125.03 123.97 17.02 o 2 7 4 166.78 146.53 23.63 o -5 1 5 179.89 181.91 8.02 o -3 1 5 4956.77 5028.19 63.48 o -2 1 5 63.26 60.61 3.51 o 0 1 5 126.63 122.22 21.15 o -6 2 5 43.08 38.60 6.49 o -5 2 5 20.35 29.44 4.46 o -4 2 5 732.53 805.42 14.46 o -3 2 5 44.66 52.80 2.79 o -2 2 5 66.95 64.83 3.19 o -1 2 5 213.68 212.71 7.11 o 0 2 5 330.12 333.15 19.07 o -6 3 5 140.07 166.40 12.17 o -5 3 5 752.33 679.77 23.22 o -4 3 5 338.37 363.93 10.82 o -3 3 5 2972.76 2902.06 70.59 o -2 3 5 739.35 668.27 17.80 o -1 3 5 208.27 231.69 10.28 o 0 3 5 125.42 129.62 13.44 o 1 3 5 103.74 91.68 12.40 o -7 4 5 236.89 225.22 20.89 o -6 4 5 181.14 196.86 14.59 o -4 4 5 180.64 171.85 9.28 o -3 4 5 40.71 47.75 4.24 o -2 4 5 139.60 145.99 6.85 o -1 4 5 337.85 289.68 33.66 o 0 4 5 644.06 600.63 27.11 o 1 4 5 112.19 121.03 14.77 o -7 5 5 145.66 128.91 18.36 o -6 5 5 16.33 11.50 5.38 o -5 5 5 468.43 499.59 20.88 o -4 5 5 14.79 17.02 3.95 o -3 5 5 1324.30 1343.27 25.33 o -2 5 5 1.09 4.03 2.93 o -1 5 5 160.21 184.02 11.24 o 0 5 5 4.36 9.58 5.51 o 1 5 5 67.06 66.38 9.51 o 2 5 5 45.41 51.21 13.72 o -7 6 5 5.98 5.96 7.33 o -6 6 5 27.13 13.42 7.44 o -5 6 5 1.56 1.61 7.91 o -4 6 5 87.15 95.75 11.51 o -2 6 5 23.92 23.74 4.63 o -1 6 5 42.10 28.75 10.38 o 0 6 5 13.80 16.30 6.98 o 1 6 5 45.11 51.35 10.89 o 2 6 5 0.02 6.04 12.67 o -6 7 5 91.66 143.80 43.02 o -5 7 5 0.05 12.73 9.54 o -4 7 5 10.69 1.65 9.50 o -3 7 5 50.59 38.53 9.59 o -2 7 5 62.64 36.58 11.31 o -1 7 5 10.94 9.91 8.50 o 0 7 5 41.93 49.32 13.67 o 1 7 5 42.39 37.16 13.63 o -6 0 6 162.39 156.44 18.20 o -5 0 6 374.72 376.90 17.45 o -4 0 6 936.89 949.73 24.34 o -3 0 6 3120.48 2822.07 44.42 o -2 0 6 63.87 61.84 6.79 o -1 0 6 11.61 15.46 3.17 o -6 1 6 2033.43 1884.99 56.39 o -5 1 6 1044.99 1157.47 27.81 o -4 1 6 0.29 1.37 0.92 o -3 1 6 344.46 366.97 9.13 o -2 1 6 17.12 16.81 1.61 o -1 1 6 430.08 444.61 11.47 o 0 1 6 20.48 21.28 8.08 o -7 2 6 354.00 393.53 31.68 o -5 2 6 1128.03 1225.16 18.14 o -4 2 6 881.08 883.95 13.08 o -3 2 6 0.22 2.19 1.26 o -2 2 6 5.40 6.41 1.38 o -1 2 6 1026.72 1011.01 37.73 o 0 2 6 21.22 32.12 8.52 o -7 3 6 7.32 1.16 6.47 o -6 3 6 32.60 30.66 6.83 o -5 3 6 467.90 482.85 13.81 o -4 3 6 26.11 33.66 12.02 o -3 3 6 362.62 369.87 10.14 o -2 3 6 296.36 298.97 10.40 o -1 3 6 0.00 4.18 2.99 o 0 3 6 333.87 360.86 24.04 o -7 4 6 8.97 9.58 5.17 o -6 4 6 149.04 144.18 10.27 o -5 4 6 135.84 131.41 8.27 o -4 4 6 0.11 4.77 3.74 o -2 4 6 0.75 8.51 4.39 o -1 4 6 213.65 213.39 13.38 o 0 4 6 203.00 191.13 18.90 o -8 5 6 24.17 61.47 21.27 o -7 5 6 6.08 6.30 5.22 o -6 5 6 112.19 116.71 10.44 o -5 5 6 101.13 107.43 8.57 o -4 5 6 2.01 5.02 4.10 o -3 5 6 1.24 4.90 3.61 o -2 5 6 0.01 2.08 3.66 o -1 5 6 3.06 9.32 6.06 o 0 5 6 0.00 6.76 6.23 o 1 5 6 19.91 11.47 12.00 o -7 6 6 28.56 36.83 8.92 o -6 6 6 36.17 33.62 7.32 o -5 6 6 0.00 6.74 6.36 o -4 6 6 137.01 143.51 12.85 o -3 6 6 34.14 29.79 4.92 o -2 6 6 36.89 26.64 5.73 o -1 6 6 148.21 140.45 15.08 o 0 6 6 8.42 12.30 7.04 o 1 6 6 424.86 382.85 33.09 o -5 7 6 30.64 34.53 12.26 o -4 7 6 0.00 10.23 9.81 o -3 7 6 26.72 25.35 8.49 o -2 7 6 0.28 8.88 10.22 o -1 7 6 18.18 20.14 12.95 o 0 7 6 80.10 85.38 21.40 o -7 1 7 308.78 290.59 22.08 o -6 1 7 2.39 7.92 3.45 o -5 1 7 0.06 2.36 1.13 o -4 1 7 1.58 2.17 1.87 o -3 1 7 18.68 17.07 2.13 o -2 1 7 78.31 91.13 4.58 o -1 1 7 127.86 126.06 21.03 o -7 2 7 3.82 10.17 4.91 o -6 2 7 5.50 3.62 1.96 o -5 2 7 133.49 128.76 5.46 o -4 2 7 162.29 168.33 5.58 o -3 2 7 63.38 61.90 3.36 o -2 2 7 254.58 276.95 8.26 o -1 2 7 639.73 639.78 40.39 o 0 2 7 956.43 963.39 107.56 o -8 3 7 325.12 290.55 23.45 o -7 3 7 7.20 4.63 5.37 o -6 3 7 21.69 18.42 2.91 o -5 3 7 3.95 2.79 2.94 o -4 3 7 124.64 131.64 7.73 o -3 3 7 81.92 81.23 5.25 o -2 3 7 12.19 11.74 3.02 o -1 3 7 16.12 5.25 5.00 o 0 3 7 5.81 3.06 7.77 o -8 4 7 78.99 93.01 15.49 o -7 4 7 225.80 232.46 14.94 o -6 4 7 43.24 40.26 5.54 o -5 4 7 308.66 287.46 12.63 o -4 4 7 471.39 444.11 13.19 o -3 4 7 31.61 24.87 4.37 o -2 4 7 106.07 92.44 7.55 o -1 4 7 132.57 134.56 15.39 o 0 4 7 579.58 612.24 35.13 o -8 5 7 468.17 481.95 34.72 o -7 5 7 81.51 68.30 9.10 o -6 5 7 56.74 53.47 7.49 o -5 5 7 1.50 6.20 4.75 o -4 5 7 75.77 66.58 6.39 o -3 5 7 56.86 59.71 6.82 o -2 5 7 2.99 8.06 3.93 o -1 5 7 9.91 16.87 6.56 o 0 5 7 51.07 67.64 12.36 o -8 6 7 32.93 39.31 11.76 o -7 6 7 1.53 11.18 6.52 o -6 6 7 15.85 29.74 7.89 o -5 6 7 1.18 6.83 5.23 o -4 6 7 13.56 23.30 8.68 o -3 6 7 0.39 11.90 6.24 o -2 6 7 1.08 14.51 8.06 o -1 6 7 24.68 21.14 7.54 o 0 6 7 106.98 139.15 25.90 o -7 0 8 1464.57 1527.16 61.22 o -6 0 8 126.75 117.13 10.02 o -5 0 8 1270.33 1274.84 31.70 o -4 0 8 825.81 732.27 23.79 o -3 0 8 317.25 311.12 17.65 o -2 0 8 7.27 6.58 3.42 o -8 1 8 12.75 29.29 19.36 o -7 1 8 1.14 6.79 4.52 o -6 1 8 8.66 5.96 2.70 o -5 1 8 15.21 14.67 3.07 o -4 1 8 0.09 1.92 1.88 o -3 1 8 266.36 269.86 10.21 o -2 1 8 689.66 671.35 20.97 o -1 1 8 79.15 84.20 16.95 o -8 2 8 0.05 11.74 7.26 o -7 2 8 994.74 1038.63 32.96 o -6 2 8 72.10 70.14 6.59 o -5 2 8 212.92 216.96 9.93 o -4 2 8 626.52 659.15 15.96 o -3 2 8 65.37 67.52 5.68 o -2 2 8 698.12 775.09 29.84 o -1 2 8 0.28 1.33 9.31 o -8 3 8 37.89 38.59 12.95 o -7 3 8 22.55 15.66 5.22 o -6 3 8 165.04 155.00 12.04 o -5 3 8 122.19 119.24 8.12 o -4 3 8 17.95 14.26 3.82 o -3 3 8 39.31 31.52 5.44 o -2 3 8 22.60 18.38 4.53 o -1 3 8 166.17 164.35 23.37 o -8 4 8 88.97 73.64 13.98 o -7 4 8 262.93 270.10 22.50 o -6 4 8 41.90 33.51 6.13 o -5 4 8 29.25 40.71 6.15 o -4 4 8 75.75 67.66 7.63 o -3 4 8 38.66 44.22 9.21 o -1 4 8 3.45 10.38 8.13 o 0 4 8 331.40 325.55 115.22 o -8 5 8 5.48 1.73 11.27 o -7 5 8 12.43 18.50 9.54 o -6 5 8 0.70 8.98 5.82 o -5 5 8 30.85 20.16 6.55 o -4 5 8 28.32 28.66 5.95 o -3 5 8 6.78 16.89 6.92 o -2 5 8 5.65 1.56 11.02 o 0 5 8 42.98 67.64 26.03 o -8 6 8 118.58 102.80 35.03 o -7 6 8 0.04 18.04 16.55 o -6 6 8 232.66 243.00 29.59 o -5 6 8 0.06 6.22 8.26 o -4 6 8 21.80 49.31 19.91 o -3 6 8 413.70 429.66 44.17 o -2 6 8 60.14 35.19 25.62 o -1 6 8 183.45 156.66 27.16 o 0 6 8 83.67 148.40 39.62 o -8 1 9 29.50 19.08 6.34 o -6 1 9 140.60 138.56 8.05 o -5 1 9 6.37 11.41 3.39 o -4 1 9 224.81 206.02 9.06 o -3 1 9 5.16 5.27 3.12 o -2 1 9 135.05 152.90 12.88 o -8 2 9 0.45 9.66 9.10 o -7 2 9 254.56 253.17 23.24 o -6 2 9 1.04 2.35 4.48 o -5 2 9 872.11 851.67 23.17 o -4 2 9 75.48 73.52 6.09 o -3 2 9 352.00 351.59 15.86 o -2 2 9 28.90 16.55 6.42 o -1 2 9 14.38 25.11 12.79 o -9 3 9 227.55 192.03 28.47 o -8 3 9 135.89 99.79 15.70 o -7 3 9 7.05 21.23 7.72 o -6 3 9 70.35 93.16 10.79 o -5 3 9 376.56 376.05 20.40 o -4 3 9 94.15 84.42 10.62 o -3 3 9 243.55 205.64 16.90 o -2 3 9 17.71 5.98 9.86 o -1 3 9 120.05 98.99 19.85 o -9 4 9 169.30 209.97 31.14 o -8 4 9 27.75 42.29 12.33 o -7 4 9 3.90 13.39 6.94 o -6 4 9 20.06 12.95 6.60 o -5 4 9 314.29 296.50 19.12 o -4 4 9 97.22 115.25 12.50 o -3 4 9 493.37 530.05 28.64 o -2 4 9 38.87 52.39 16.18 o -1 4 9 37.32 36.01 14.65 o -9 5 9 31.34 52.94 18.51 o -8 5 9 18.31 19.88 10.18 o -7 5 9 1.91 11.73 9.78 o -6 5 9 1.10 5.66 5.75 o -5 5 9 0.23 6.70 6.50 o -4 5 9 333.75 357.27 24.94 o -3 5 9 15.73 34.77 15.72 o -2 5 9 7.16 1.70 11.81 o -7 6 9 0.56 2.34 23.38 o -6 6 9 4.43 12.29 20.83 o -5 6 9 135.91 137.10 22.75 o -4 6 9 4.09 12.53 16.91 o -3 6 9 85.55 82.21 23.79 o -8 0 10 1580.79 1501.03 54.51 o -7 0 10 7.76 10.27 5.57 o -6 0 10 2510.50 2482.50 50.82 o -5 0 10 101.96 114.95 11.59 o -4 0 10 16.50 6.86 4.86 o -3 0 10 38.62 30.95 7.55 o -2 0 10 126.86 76.77 36.94 o -9 1 10 136.67 127.72 22.90 o -8 1 10 0.02 6.67 3.98 o -7 1 10 1774.75 1769.21 59.90 o -6 1 10 623.07 611.98 17.78 o -5 1 10 58.22 52.78 5.12 o -4 1 10 509.01 513.09 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