#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:03:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180913 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/54/2105455.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105455_Fobs loop_ _publ_author_name 'Zakharov, Boris A.' 'Boldyreva, Elena V.' _publ_section_title ; A high-pressure single-crystal to single-crystal phase transition in DL-alaninium semi-oxalate monohydrate with switching-over hydrogen bonds ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 271 _journal_page_last 280 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.977 _cell_angle_gamma 90.000 _cell_length_a 11.8071 _cell_length_b 5.8748 _cell_length_c 11.1638 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7555 _cod_data_source_file gp5064540sup10.hkl _cod_data_source_block 540 #BEGIN Tags that were not found in dictionaries: _shelx_title 'E 10-535' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 404.42 367.10 9.07 o 0 2 0 9498.89 9380.76 357.84 o 1 2 0 6219.42 6329.82 91.85 o 2 2 0 1704.84 1534.39 54.46 o 1 3 0 78.83 76.41 4.60 o 2 3 0 80.00 82.53 6.49 o 3 3 0 56.41 49.00 6.59 o 0 4 0 1124.48 1127.34 32.88 o 1 4 0 8.44 6.42 2.06 o 2 4 0 400.54 411.58 43.23 o 3 4 0 507.51 529.44 18.85 o 4 4 0 204.83 193.94 12.70 o 2 5 0 25.92 10.23 5.92 o 3 5 0 256.50 243.68 22.72 o 4 5 0 109.87 121.72 16.84 o 0 6 0 283.72 249.18 24.65 o 1 6 0 107.57 100.00 10.20 o 2 6 0 14.22 12.03 9.67 o 3 6 0 105.32 135.27 16.49 o 4 6 0 662.22 634.64 35.69 o 1 7 0 6.18 27.86 11.72 o 2 7 0 0.85 10.61 9.15 o 3 7 0 73.65 59.88 19.95 o 4 7 0 5.15 14.67 12.58 o -2 1 1 130.94 118.11 7.25 o -1 1 1 340.22 346.51 6.21 o 0 1 1 983.39 931.39 11.83 o 1 1 1 31.59 30.11 6.56 o -3 2 1 4694.09 4871.14 63.50 o -2 2 1 1772.16 1785.40 29.94 o -1 2 1 774.49 791.94 9.98 o 0 2 1 1.78 0.44 0.53 o 1 2 1 875.45 804.97 15.20 o 2 2 1 659.67 680.68 23.33 o -3 3 1 684.13 693.75 16.05 o -2 3 1 1774.32 1877.97 28.52 o -1 3 1 106.68 118.32 4.48 o 0 3 1 68.29 78.15 5.04 o 1 3 1 124.79 128.16 6.17 o 2 3 1 255.49 221.25 12.45 o 3 3 1 0.24 1.65 5.28 o -4 4 1 70.06 66.57 7.12 o -3 4 1 3790.24 4177.15 69.57 o -2 4 1 1057.48 1009.94 26.52 o -1 4 1 31.94 27.86 2.63 o 0 4 1 2.02 6.28 2.25 o 1 4 1 18.80 24.20 3.28 o 2 4 1 61.53 76.54 6.84 o 3 4 1 8.65 9.94 4.25 o -5 5 1 8.95 14.44 12.22 o -4 5 1 15.52 13.45 7.92 o -3 5 1 103.55 95.21 10.53 o -2 5 1 0.00 1.44 4.64 o 1 5 1 137.41 106.91 8.55 o 2 5 1 287.31 251.01 19.17 o 3 5 1 0.34 5.79 7.30 o 4 5 1 231.47 216.13 27.41 o -5 6 1 38.46 50.84 12.74 o -4 6 1 18.98 14.63 7.54 o -3 6 1 128.81 138.79 17.13 o -2 6 1 169.27 144.03 12.54 o -1 6 1 16.71 18.68 6.80 o 0 6 1 0.73 8.39 5.21 o 1 6 1 85.06 104.34 11.46 o 2 6 1 94.21 93.81 13.95 o 3 6 1 9.37 10.67 7.92 o 4 6 1 0.09 22.10 15.08 o -4 7 1 7.76 2.28 9.85 o -3 7 1 66.85 68.90 11.95 o -2 7 1 106.61 115.21 19.48 o -1 7 1 22.92 24.67 7.07 o 0 7 1 0.05 4.10 7.03 o 1 7 1 6.16 16.30 10.39 o 2 7 1 0.65 8.18 10.18 o 3 7 1 0.05 6.03 9.63 o -2 0 2 1322.53 1311.21 82.79 o -1 0 2 291.59 283.52 6.17 o -2 1 2 75.59 79.05 3.37 o -1 1 2 38.49 40.71 1.55 o 0 1 2 3980.20 4092.64 127.58 o -4 2 2 11.07 6.68 3.77 o -3 2 2 0.45 2.46 1.71 o -2 2 2 230.63 241.61 6.12 o -1 2 2 3537.15 3422.19 55.70 o 0 2 2 2424.10 2470.71 38.08 o 1 2 2 230.81 236.00 10.52 o -4 3 2 0.32 1.60 2.23 o -3 3 2 86.49 113.31 12.96 o -2 3 2 356.07 358.18 9.24 o -1 3 2 283.66 263.57 7.92 o 0 3 2 404.16 420.53 19.94 o 1 3 2 218.33 200.47 19.38 o 2 3 2 19.00 6.05 4.05 o -5 4 2 46.40 36.91 10.09 o -4 4 2 35.22 43.19 6.83 o -3 4 2 14.44 12.80 2.99 o -2 4 2 85.60 98.48 4.92 o -1 4 2 48.51 50.16 3.51 o 0 4 2 18.39 18.31 3.11 o 2 4 2 37.72 39.38 10.40 o 3 4 2 116.05 106.49 18.06 o -5 5 2 9.95 10.05 8.53 o -4 5 2 190.02 218.43 13.96 o -3 5 2 51.74 47.35 6.25 o -1 5 2 188.36 166.81 9.24 o 0 5 2 39.95 31.45 5.76 o 1 5 2 93.63 80.61 15.17 o 2 5 2 56.78 55.29 9.96 o 3 5 2 9.32 18.39 10.17 o -6 6 2 395.60 455.00 63.62 o -5 6 2 613.97 619.54 35.23 o -4 6 2 3.43 11.31 8.21 o -3 6 2 394.03 359.67 29.67 o -2 6 2 17.43 21.66 6.92 o -1 6 2 73.66 66.14 8.23 o 0 6 2 170.00 157.88 11.67 o 1 6 2 16.94 26.87 8.84 o 2 6 2 12.53 8.26 6.79 o 3 6 2 85.04 72.81 14.12 o -4 7 2 39.42 29.62 10.69 o -3 7 2 0.56 1.85 10.33 o -2 7 2 9.12 12.47 7.41 o -1 7 2 10.82 18.36 8.16 o 0 7 2 8.33 6.91 7.17 o 1 7 2 99.87 97.24 16.25 o 2 7 2 14.18 9.35 9.13 o 3 7 2 81.86 86.57 25.02 o -3 1 3 174.90 178.72 6.66 o -2 1 3 103.87 115.55 2.59 o -1 1 3 1153.89 1114.21 13.02 o 0 1 3 1591.97 1552.31 48.32 o -3 2 3 322.75 341.93 9.87 o -2 2 3 269.39 264.98 5.62 o -1 2 3 4.49 2.23 0.91 o 0 2 3 367.91 366.60 13.24 o -5 3 3 0.19 2.49 3.49 o -4 3 3 63.71 51.03 9.22 o -3 3 3 224.04 253.73 8.98 o -2 3 3 1265.12 1101.81 38.26 o -1 3 3 131.96 108.26 9.42 o 0 3 3 11.23 13.39 3.16 o 1 3 3 676.43 713.02 28.80 o -6 4 3 70.86 99.05 14.67 o -5 4 3 6.40 12.99 4.54 o -4 4 3 28.37 31.77 5.76 o -3 4 3 84.90 79.99 5.45 o -2 4 3 15.37 20.90 2.73 o -1 4 3 62.10 52.62 4.34 o 0 4 3 23.67 24.05 3.66 o 1 4 3 93.37 92.70 9.03 o 2 4 3 110.42 112.53 13.40 o -6 5 3 0.38 5.45 6.43 o -5 5 3 36.21 33.77 6.41 o -4 5 3 493.84 475.87 22.20 o -3 5 3 339.22 303.97 13.26 o -2 5 3 145.07 159.06 8.90 o -1 5 3 427.00 395.95 13.80 o 0 5 3 604.09 580.42 19.05 o 1 5 3 3.97 9.72 4.96 o 2 5 3 408.52 442.03 25.34 o 3 5 3 130.86 154.17 23.44 o -6 6 3 215.70 271.09 24.18 o -5 6 3 9.86 30.80 9.36 o -4 6 3 0.66 1.96 6.52 o -3 6 3 24.26 41.52 7.61 o -1 6 3 9.85 12.34 5.31 o 0 6 3 1.03 5.60 5.67 o 1 6 3 9.81 19.38 7.47 o 2 6 3 7.44 14.68 8.12 o 3 6 3 6.04 9.79 9.32 o -5 7 3 9.55 2.37 16.51 o -4 7 3 17.13 28.41 11.82 o -3 7 3 21.82 34.70 13.72 o -2 7 3 0.02 15.60 8.17 o -1 7 3 61.09 80.85 12.26 o 0 7 3 35.51 48.53 12.34 o 1 7 3 9.95 11.89 8.62 o 2 7 3 0.89 2.83 9.90 o -4 0 4 2529.65 2519.43 60.47 o -3 0 4 826.73 929.15 26.87 o -2 0 4 469.97 480.76 14.14 o -1 0 4 332.68 284.30 13.32 o -5 1 4 847.94 734.79 49.41 o -4 1 4 966.26 1018.27 31.93 o -3 1 4 5.82 3.96 0.87 o -2 1 4 3726.11 3917.81 50.32 o -1 1 4 2804.03 2798.00 33.06 o 0 1 4 9613.77 9832.80 161.54 o -5 2 4 1162.75 1348.83 35.50 o -4 2 4 21.64 20.74 2.47 o -3 2 4 1451.91 1360.52 34.95 o -1 2 4 0.12 1.06 2.78 o 0 2 4 245.69 234.76 13.91 o 1 2 4 22.54 20.53 5.68 o -6 3 4 415.50 382.33 29.15 o -5 3 4 249.78 263.54 14.37 o -4 3 4 144.61 138.45 8.51 o -3 3 4 6.57 5.18 1.40 o -2 3 4 22.86 26.11 3.60 o -1 3 4 627.01 563.54 18.17 o 0 3 4 1309.91 1329.42 39.03 o 1 3 4 11.22 10.85 5.23 o -6 4 4 29.59 41.98 8.89 o -5 4 4 129.09 142.68 11.86 o -4 4 4 108.34 90.84 11.44 o -3 4 4 4.36 6.16 2.90 o -2 4 4 8.22 4.18 2.42 o -1 4 4 34.69 41.84 3.92 o 0 4 4 72.22 55.71 10.41 o 1 4 4 61.25 53.76 7.90 o 2 4 4 15.23 33.45 23.42 o -6 5 4 123.24 119.35 17.38 o -5 5 4 4.64 4.05 5.14 o -4 5 4 161.95 185.73 11.55 o -3 5 4 151.05 180.71 9.35 o -2 5 4 3.57 10.04 3.29 o -1 5 4 8.02 10.75 3.37 o 0 5 4 342.18 354.68 18.28 o 1 5 4 51.83 62.14 7.99 o 2 5 4 135.76 120.98 17.04 o -7 6 4 222.25 226.31 25.53 o -6 6 4 4.91 8.66 8.84 o -5 6 4 19.40 29.99 8.28 o -4 6 4 21.19 23.91 9.04 o -3 6 4 6.01 14.00 5.40 o -2 6 4 33.11 21.97 5.03 o -1 6 4 52.86 55.43 6.39 o 0 6 4 0.77 10.19 8.52 o 1 6 4 4.18 6.44 7.27 o 2 6 4 42.83 49.69 13.80 o -5 7 4 0.71 19.87 12.77 o -4 7 4 35.80 28.62 16.28 o -3 7 4 8.25 18.57 10.66 o -2 7 4 139.45 107.63 19.11 o -1 7 4 0.16 14.92 9.42 o 0 7 4 153.96 167.77 19.99 o -5 1 5 200.24 199.51 8.77 o -4 1 5 36.92 41.92 7.12 o -3 1 5 5239.07 5350.25 49.20 o -2 1 5 55.44 52.04 3.99 o 0 1 5 98.49 89.85 17.74 o -6 2 5 39.74 38.07 6.48 o -5 2 5 36.62 42.98 4.88 o -4 2 5 726.52 797.66 14.10 o -3 2 5 49.31 54.86 2.75 o -2 2 5 37.40 36.43 2.44 o -1 2 5 259.72 254.77 7.64 o 0 2 5 308.08 283.09 17.41 o -6 3 5 150.30 164.32 13.75 o -4 3 5 371.23 396.46 11.10 o -3 3 5 3268.92 2997.02 91.41 o -2 3 5 856.10 855.87 15.52 o -1 3 5 236.53 265.31 10.72 o 0 3 5 171.10 187.58 15.73 o 1 3 5 104.72 97.46 12.26 o -7 4 5 230.14 229.96 20.94 o -6 4 5 175.20 191.97 14.27 o -4 4 5 173.42 155.69 8.49 o -3 4 5 34.17 33.24 3.88 o -2 4 5 121.36 125.44 6.25 o 0 4 5 676.96 659.11 28.03 o 1 4 5 155.22 163.58 17.34 o -7 5 5 126.48 113.09 16.30 o -6 5 5 20.04 11.58 5.38 o -5 5 5 479.46 519.18 21.04 o -4 5 5 14.39 10.82 3.85 o -3 5 5 1348.41 1327.49 24.68 o -2 5 5 0.02 5.87 3.25 o -1 5 5 168.94 198.48 11.39 o 0 5 5 12.96 22.61 7.15 o 1 5 5 54.07 56.01 10.50 o 2 5 5 53.73 75.24 16.81 o -7 6 5 5.90 12.82 10.18 o -6 6 5 30.00 20.46 8.60 o -5 6 5 5.33 9.83 7.42 o -4 6 5 75.73 92.86 11.34 o -3 6 5 0.12 7.90 5.21 o -2 6 5 16.78 13.95 4.74 o -1 6 5 46.68 60.06 12.43 o 0 6 5 7.39 12.94 5.92 o 1 6 5 34.24 43.83 9.75 o 2 6 5 3.85 9.88 12.41 o -5 7 5 0.64 6.98 10.59 o -4 7 5 0.88 24.64 17.01 o -3 7 5 49.46 66.93 14.12 o -1 7 5 22.12 27.13 9.45 o 0 7 5 76.88 35.49 14.63 o -6 0 6 131.37 119.89 18.00 o -5 0 6 284.50 305.85 15.34 o -4 0 6 1021.40 1022.91 23.49 o -3 0 6 3243.04 3001.34 44.31 o -2 0 6 26.70 25.25 3.95 o -1 0 6 9.41 10.51 3.18 o -6 1 6 2044.97 1929.01 44.41 o -5 1 6 1059.60 1210.00 28.01 o -4 1 6 0.67 1.40 0.97 o -3 1 6 423.77 435.05 9.67 o -2 1 6 12.06 11.97 1.26 o -1 1 6 410.12 426.19 10.99 o 0 1 6 5.40 2.81 6.43 o -7 2 6 328.44 367.76 32.03 o -6 2 6 12.38 17.52 5.40 o -5 2 6 1037.71 1117.08 17.01 o -4 2 6 882.36 875.73 12.20 o -3 2 6 0.98 3.04 1.35 o -2 2 6 12.19 14.29 1.67 o -1 2 6 1002.61 957.77 93.00 o 0 2 6 29.75 46.00 9.59 o -7 3 6 21.01 13.89 5.33 o -6 3 6 29.59 25.65 5.73 o -5 3 6 423.12 430.85 13.85 o -4 3 6 37.62 41.15 5.26 o -3 3 6 314.76 349.81 10.12 o -2 3 6 271.02 290.01 10.04 o -1 3 6 3.91 6.47 3.08 o 0 3 6 402.97 442.75 25.67 o -7 4 6 6.33 6.04 6.66 o -6 4 6 112.24 119.33 9.07 o -5 4 6 181.03 183.63 9.68 o -4 4 6 0.03 2.23 3.42 o -3 4 6 5.01 4.18 3.30 o -1 4 6 195.72 206.84 14.39 o 0 4 6 244.19 189.23 18.94 o 1 4 6 90.38 156.66 90.07 o -7 5 6 16.36 15.92 5.50 o -6 5 6 177.44 169.29 12.51 o -5 5 6 99.64 120.29 8.92 o -4 5 6 0.87 6.92 4.09 o -3 5 6 0.01 5.35 3.31 o -2 5 6 1.31 8.46 4.15 o -1 5 6 21.03 19.46 6.41 o 0 5 6 1.02 9.40 6.33 o 1 5 6 35.55 42.75 15.42 o -7 6 6 40.03 50.69 10.52 o -6 6 6 52.80 45.58 9.29 o -5 6 6 0.50 7.38 6.27 o -4 6 6 172.30 191.59 14.55 o -3 6 6 38.87 33.92 5.84 o -2 6 6 27.59 17.38 5.42 o -1 6 6 158.38 168.43 16.02 o 0 6 6 10.10 9.99 6.35 o 1 6 6 425.61 381.33 32.74 o -4 7 6 0.46 16.20 12.09 o -3 7 6 25.54 22.12 9.78 o -2 7 6 0.91 1.81 10.43 o -1 7 6 12.50 12.82 11.38 o -7 1 7 295.04 250.64 19.81 o -6 1 7 6.63 10.69 3.34 o -5 1 7 0.77 1.61 1.14 o -4 1 7 0.12 1.85 1.60 o -3 1 7 15.15 13.65 2.07 o -2 1 7 57.50 69.03 3.96 o -1 1 7 147.80 144.55 15.97 o -7 2 7 1.07 6.41 4.61 o -6 2 7 5.06 3.95 2.12 o -5 2 7 117.51 119.56 5.22 o -4 2 7 154.72 157.42 5.40 o -3 2 7 40.99 42.92 2.91 o -2 2 7 236.07 273.22 7.99 o -1 2 7 638.64 678.66 34.70 o 0 2 7 1211.37 1100.91 135.31 o -8 3 7 337.84 264.69 29.02 o -7 3 7 13.83 10.21 5.13 o -6 3 7 25.48 26.72 4.09 o -5 3 7 5.06 5.55 2.87 o -4 3 7 105.27 101.92 7.56 o -3 3 7 107.81 108.82 6.29 o -2 3 7 8.17 7.44 2.90 o -1 3 7 16.20 3.97 6.72 o 0 3 7 10.71 4.56 6.96 o -8 4 7 91.56 85.93 14.91 o -7 4 7 203.75 235.03 15.13 o -6 4 7 28.56 25.79 4.45 o -5 4 7 310.12 300.01 12.60 o -4 4 7 517.60 510.90 16.09 o -3 4 7 33.39 31.24 4.87 o -2 4 7 66.76 52.12 6.17 o -1 4 7 136.22 139.69 13.56 o 0 4 7 666.44 665.16 35.92 o -8 5 7 525.63 513.06 30.37 o -7 5 7 91.96 85.84 11.34 o -6 5 7 51.39 41.32 7.04 o -5 5 7 7.62 11.05 4.73 o -4 5 7 94.79 78.29 9.16 o -3 5 7 58.61 72.97 6.99 o -2 5 7 1.41 4.95 4.16 o -1 5 7 4.09 8.94 6.26 o 0 5 7 48.23 53.93 11.09 o -8 6 7 34.16 58.03 17.07 o -7 6 7 1.01 7.28 6.58 o -6 6 7 14.33 30.28 8.89 o -5 6 7 0.17 11.86 6.99 o -4 6 7 15.81 14.37 6.09 o -2 6 7 16.25 16.25 8.00 o -1 6 7 38.54 52.78 11.44 o 0 6 7 158.09 188.60 32.16 o -7 0 8 1721.32 1760.86 64.20 o -6 0 8 142.09 142.04 11.18 o -5 0 8 1204.97 1219.57 30.42 o -4 0 8 868.17 819.77 24.58 o -3 0 8 358.97 371.47 18.52 o -2 0 8 1.67 2.93 3.95 o -8 1 8 11.26 20.54 8.96 o -7 1 8 1.24 9.01 5.80 o -6 1 8 24.57 18.97 3.56 o -5 1 8 17.39 15.19 3.04 o -4 1 8 6.63 6.69 2.43 o -3 1 8 260.81 275.91 9.99 o -2 1 8 652.11 625.47 19.86 o -1 1 8 72.01 67.80 15.04 o -8 2 8 0.00 5.36 7.38 o -7 2 8 1056.36 1066.38 35.39 o -6 2 8 81.83 83.84 7.99 o -5 2 8 174.49 188.90 9.04 o -4 2 8 657.79 715.54 16.21 o -3 2 8 53.75 50.13 5.15 o -2 2 8 703.74 764.05 28.95 o -1 2 8 0.57 1.86 13.08 o -8 3 8 21.94 11.25 7.55 o -7 3 8 25.14 14.55 9.45 o -6 3 8 151.83 141.52 13.59 o -5 3 8 125.71 124.87 10.18 o -4 3 8 5.47 4.67 4.23 o -3 3 8 32.20 23.82 4.93 o -2 3 8 19.54 17.85 5.21 o -1 3 8 161.42 158.35 29.76 o -8 4 8 102.67 84.40 20.48 o -7 4 8 265.65 297.60 24.03 o -6 4 8 27.13 17.36 6.01 o -4 4 8 75.12 81.49 8.55 o -3 4 8 45.68 54.12 7.37 o -1 4 8 0.74 1.24 8.71 o 0 4 8 343.45 406.24 57.36 o -8 5 8 5.44 15.75 15.24 o -7 5 8 8.45 13.06 8.53 o -6 5 8 4.72 8.34 6.42 o -5 5 8 37.52 32.02 8.09 o -4 5 8 44.41 44.99 7.96 o -3 5 8 1.44 9.37 6.59 o -2 5 8 5.60 7.34 10.05 o -1 5 8 71.46 65.73 16.68 o 0 5 8 30.39 68.32 27.63 o -8 6 8 106.52 86.54 31.05 o -7 6 8 0.42 1.94 13.17 o -6 6 8 219.48 153.53 26.43 o -5 6 8 2.50 12.45 6.83 o -4 6 8 24.94 26.65 10.80 o -3 6 8 499.16 511.89 47.44 o -2 6 8 60.47 74.66 19.69 o -1 6 8 245.37 262.81 35.90 o 0 6 8 107.17 158.97 41.18 o -8 1 9 30.99 23.56 7.94 o -6 1 9 138.62 147.76 7.90 o -4 1 9 212.83 201.73 8.85 o -3 1 9 4.79 2.54 3.10 o -2 1 9 143.02 167.22 13.69 o -8 2 9 1.83 4.37 7.10 o -7 2 9 244.51 282.53 22.58 o -6 2 9 0.39 5.50 4.03 o -5 2 9 983.18 956.88 24.07 o -4 2 9 112.67 109.32 7.91 o -3 2 9 339.09 355.76 15.80 o -1 2 9 25.16 18.15 11.02 o -9 3 9 184.91 166.68 25.94 o -8 3 9 181.23 148.72 23.51 o -7 3 9 4.12 7.62 6.61 o -6 3 9 82.79 92.77 10.77 o -5 3 9 428.83 396.00 20.40 o -4 3 9 80.67 67.76 7.65 o -3 3 9 221.09 190.13 15.90 o -2 3 9 17.68 25.93 14.98 o -1 3 9 139.98 126.06 21.89 o -9 4 9 214.14 269.46 33.68 o -8 4 9 32.14 38.37 11.49 o -7 4 9 7.03 16.04 7.80 o -6 4 9 18.62 11.03 6.32 o -5 4 9 326.34 323.54 19.53 o -4 4 9 114.88 144.60 13.35 o -3 4 9 510.43 496.12 26.71 o -2 4 9 46.41 55.26 17.21 o -1 4 9 55.19 52.11 19.39 o -9 5 9 19.93 24.40 37.20 o -8 5 9 26.97 15.60 11.90 o -7 5 9 0.16 1.88 8.17 o -6 5 9 1.03 7.60 7.27 o -5 5 9 0.67 17.23 7.47 o -4 5 9 352.30 351.18 23.87 o -3 5 9 9.83 22.98 14.60 o -2 5 9 4.09 2.42 11.71 o -1 5 9 114.45 125.27 25.12 o -7 6 9 0.00 11.73 20.73 o -6 6 9 0.02 1.77 17.66 o -5 6 9 138.97 155.97 42.04 o -8 0 10 1816.58 1800.57 71.26 o -7 0 10 0.48 7.42 4.65 o -6 0 10 2723.18 2716.83 52.01 o -5 0 10 135.21 128.85 11.57 o -4 0 10 17.05 13.84 5.09 o -3 0 10 31.12 25.19 6.81 o -2 0 10 102.43 81.84 34.79 o -9 1 10 111.79 126.49 22.63 o -8 1 10 4.33 9.31 4.91 o -7 1 10 1722.38 1715.35 31.71 o -6 1 10 580.85 571.96 16.77 o -5 1 10 16.61 13.84 3.30 o -4 1 10 601.81 561.38 15.81 o -3 1 10 66.32 78.10 8.39 o -9 2 10 309.79 299.24 27.18 o -8 2 10 224.11 229.86 15.99 o -7 2 10 329.10 362.36 19.75 o -6 2 10 586.04 594.18 22.50 o -5 2 10 52.79 61.28 8.06 o -4 2 10 4.27 6.65 4.84 o -3 2 10 145.96 165.87 13.38 o -2 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