#------------------------------------------------------------------------------
#$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $
#$Revision: 88054 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/54/2105468.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2105468_Fobs
loop_
_publ_author_name
'Reibenspies, Joseph'
'Bhuvanesh, Nattamai'
_publ_section_title
;
 Absolute structure of <i>R</i>-({-})-2-methylpiperazine and
 <i>S</i>-(+)-2-methylpiperazine
;
_journal_coeditor_code           RY5050
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              288
_journal_page_last               293
_journal_volume                  69
_journal_year                    2013
_cell_angle_alpha                90.000
_cell_angle_beta                 107.018
_cell_angle_gamma                90.000
_cell_length_a                   6.0262
_cell_length_b                   11.5550
_cell_length_c                   7.1392
_exptl_crystal_F_000             261.00
_reflns_d_resolution_high        0.8600
_[local]_cod_data_source_file    ry5050smpipbrsup5.hkl
_[local]_cod_data_source_block   smpipbr
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' smpipbr in P2(1)'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            150.80
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 -13 0 714.84 719.14 18.85 o
0 -12 0 881.35 896.68 28.83 o
1 -12 0 109.99 107.01 4.43 o
2 -12 0 524.72 516.07 17.12 o
1 -11 0 298.99 294.09 9.05 o
2 -11 0 986.20 982.37 31.96 o
3 -11 0 992.61 976.40 44.80 o
0 -10 0 2513.95 2537.24 117.27 o
1 -10 0 108.21 101.12 4.51 o
2 -10 0 71.27 78.63 5.20 o
3 -10 0 35.95 40.95 5.63 o
1 -9 0 3003.97 2999.76 76.03 o
2 -9 0 501.38 500.06 14.74 o
3 -9 0 444.39 471.63 18.57 o
4 -9 0 662.34 689.57 38.44 o
0 -8 0 57.45 57.91 2.61 o
1 -8 0 1210.28 1192.21 19.03 o
2 -8 0 844.12 850.88 18.25 o
3 -8 0 762.09 805.81 53.74 o
4 -8 0 1148.51 1171.20 40.33 o
5 -8 0 12.78 13.06 4.20 o
1 -7 0 2875.45 2948.92 39.51 o
2 -7 0 802.70 805.67 12.62 o
3 -7 0 884.20 871.39 22.22 o
4 -7 0 649.71 616.78 24.35 o
5 -7 0 213.15 203.48 12.70 o
0 -6 0 8395.17 8950.82 189.41 o
1 -6 0 761.93 774.64 12.81 o
2 -6 0 1176.71 1109.46 15.64 o
3 -6 0 242.41 227.48 6.32 o
4 -6 0 160.43 159.34 8.42 o
5 -6 0 2452.44 2328.40 120.94 o
1 -5 0 166.73 151.47 2.78 o
2 -5 0 2996.26 2904.40 45.37 o
3 -5 0 3365.88 3220.22 57.57 o
4 -5 0 115.67 111.12 6.11 o
5 -5 0 395.11 377.13 22.59 o
6 -5 0 94.09 100.19 8.10 o
0 -4 0 6304.37 6538.33 116.35 o
1 -4 0 1230.32 1146.90 15.74 o
2 -4 0 1902.37 1886.18 23.95 o
3 -4 0 1136.38 1124.36 21.16 o
4 -4 0 1511.82 1566.75 40.31 o
5 -4 0 1699.35 1628.93 86.39 o
6 -4 0 79.28 88.57 8.44 o
1 -3 0 8654.69 8296.82 106.81 o
2 -3 0 765.19 758.97 9.12 o
3 -3 0 295.53 317.64 6.16 o
4 -3 0 1859.42 1836.46 59.53 o
5 -3 0 77.46 83.04 9.59 o
6 -3 0 1971.95 2068.53 102.63 o
0 -2 0 5225.23 4432.28 107.42 o
1 -2 0 2662.66 2706.26 42.65 o
2 -2 0 3872.01 3881.86 43.82 o
3 -2 0 2066.99 2117.66 31.80 o
4 -2 0 2525.36 2513.37 45.20 o
5 -2 0 516.76 507.84 17.27 o
6 -2 0 178.52 191.96 14.92 o
1 -1 0 1300.91 1345.29 17.94 o
2 -1 0 5424.69 5356.85 61.68 o
3 -1 0 1801.37 1796.95 24.79 o
4 -1 0 501.21 518.39 8.77 o
5 -1 0 479.69 508.48 14.30 o
6 -1 0 523.71 470.97 24.92 o
1 0 0 105.04 82.44 1.36 o
2 0 0 2450.70 2492.53 30.06 o
3 0 0 37.17 46.14 1.63 o
4 0 0 34.47 42.95 2.14 o
5 0 0 5040.48 5012.32 125.64 o
6 0 0 536.09 544.92 35.68 o
1 1 0 1164.07 1215.85 19.41 o
2 1 0 5427.71 5430.44 63.50 o
3 1 0 1872.46 1864.12 22.56 o
4 1 0 438.17 443.78 9.49 o
5 1 0 479.96 481.39 13.83 o
6 1 0 527.05 519.91 32.21 o
0 2 0 5179.99 4415.03 102.59 o
1 2 0 2792.31 2840.15 39.16 o
2 2 0 3809.38 3820.36 47.90 o
3 2 0 2039.25 2098.90 32.53 o
4 2 0 2580.18 2596.25 47.34 o
5 2 0 518.62 525.47 21.42 o
6 2 0 170.22 180.20 9.89 o
1 3 0 8678.16 8284.48 106.98 o
2 3 0 767.47 756.56 9.05 o
3 3 0 301.33 321.06 6.18 o
4 3 0 1843.69 1887.10 39.93 o
5 3 0 74.75 78.71 6.73 o
6 3 0 1979.11 1927.09 89.88 o
0 4 0 6247.28 6491.03 111.76 o
1 4 0 1214.09 1094.75 17.37 o
2 4 0 1945.59 1906.78 24.89 o
3 4 0 1161.33 1132.50 17.88 o
4 4 0 1496.70 1540.04 40.20 o
5 4 0 1690.51 1648.65 86.03 o
6 4 0 82.71 78.76 11.60 o
1 5 0 158.53 144.93 2.83 o
2 5 0 2942.41 2723.52 43.86 o
3 5 0 3360.81 3161.86 58.88 o
4 5 0 126.12 124.78 5.03 o
5 5 0 371.35 361.49 17.02 o
6 5 0 92.83 93.62 6.87 o
0 6 0 8305.95 8805.22 180.50 o
1 6 0 801.50 810.73 12.76 o
2 6 0 1219.02 1157.11 17.81 o
3 6 0 245.35 234.45 6.13 o
4 6 0 178.54 171.05 8.99 o
5 6 0 2442.13 2341.96 117.80 o
1 7 0 2840.23 2901.89 38.96 o
2 7 0 803.77 798.02 14.07 o
3 7 0 895.89 887.36 21.50 o
4 7 0 674.30 638.48 20.68 o
5 7 0 192.69 172.69 10.06 o
0 8 0 48.42 57.98 2.71 o
1 8 0 1156.35 1158.82 18.14 o
2 8 0 874.64 860.10 17.25 o
3 8 0 760.75 793.36 20.45 o
4 8 0 1130.14 1129.97 44.29 o
5 8 0 10.39 12.04 3.44 o
1 9 0 2985.96 2984.48 54.18 o
2 9 0 535.33 551.91 14.46 o
3 9 0 476.97 506.20 15.62 o
4 9 0 693.55 709.86 25.96 o
0 10 0 2462.42 2525.36 86.78 o
1 10 0 93.82 88.36 4.97 o
2 10 0 68.03 71.54 4.61 o
3 10 0 47.98 49.78 3.46 o
4 10 0 95.63 98.04 7.81 o
1 11 0 310.78 308.60 10.09 o
2 11 0 998.35 989.18 28.56 o
3 11 0 998.21 950.63 33.74 o
0 12 0 898.62 883.34 31.50 o
1 12 0 108.34 112.12 4.99 o
2 12 0 509.20 509.50 18.77 o
3 12 0 166.64 167.37 10.03 o
1 13 0 726.83 720.19 20.75 o
-1 -13 1 379.06 356.86 20.78 o
0 -13 1 175.95 157.44 6.26 o
1 -13 1 22.92 17.19 3.93 o
-3 -12 1 1.86 2.90 3.30 o
-2 -12 1 536.83 516.32 17.01 o
-1 -12 1 300.28 299.95 8.84 o
0 -12 1 513.26 520.31 14.53 o
1 -12 1 365.76 365.03 10.31 o
2 -12 1 42.98 38.23 2.90 o
-3 -11 1 175.91 168.69 10.86 o
-2 -11 1 724.43 732.20 24.36 o
-1 -11 1 617.17 621.78 16.98 o
0 -11 1 575.17 577.14 13.84 o
1 -11 1 1355.40 1428.54 35.91 o
2 -11 1 112.41 123.33 4.90 o
3 -11 1 34.09 25.36 3.77 o
-4 -10 1 792.14 791.12 27.20 o
-3 -10 1 14.98 14.07 4.76 o
-2 -10 1 1044.16 1048.34 24.92 o
-1 -10 1 183.37 180.42 6.34 o
0 -10 1 130.36 131.37 4.25 o
1 -10 1 521.92 564.17 14.74 o
2 -10 1 111.73 113.46 5.03 o
3 -10 1 1315.20 1381.29 72.50 o
4 -10 1 117.42 118.85 8.07 o
-5 -9 1 582.77 539.81 30.60 o
-4 -9 1 365.25 353.63 14.30 o
-3 -9 1 3069.44 3011.95 81.57 o
-2 -9 1 367.14 374.72 11.32 o
-1 -9 1 919.36 959.77 20.98 o
0 -9 1 330.42 351.49 7.82 o
1 -9 1 814.66 860.41 16.74 o
2 -9 1 2398.44 2465.58 61.56 o
3 -9 1 350.75 347.06 19.47 o
4 -9 1 1196.33 1225.06 57.64 o
-5 -8 1 779.80 777.05 40.29 o
-4 -8 1 88.32 86.00 5.13 o
-3 -8 1 15.60 19.88 2.80 o
-2 -8 1 102.95 104.93 5.48 o
-1 -8 1 2531.63 2566.23 38.15 o
0 -8 1 1730.65 1712.91 26.29 o
1 -8 1 55.51 61.19 2.49 o
2 -8 1 441.47 465.37 10.47 o
3 -8 1 83.41 81.19 4.78 o
4 -8 1 723.75 692.42 25.24 o
5 -8 1 905.84 851.90 46.29 o
-5 -7 1 422.13 382.93 22.35 o
-4 -7 1 249.77 242.46 9.25 o
-3 -7 1 3103.20 3057.15 59.43 o
-2 -7 1 485.98 494.82 7.66 o
-1 -7 1 995.83 980.60 13.64 o
0 -7 1 700.56 661.42 10.00 o
1 -7 1 846.15 839.84 14.33 o
2 -7 1 2247.97 2192.10 44.50 o
3 -7 1 747.93 727.55 17.86 o
4 -7 1 792.86 778.41 28.78 o
5 -7 1 161.63 168.34 11.62 o
-6 -6 1 152.41 141.08 9.92 o
-5 -6 1 292.84 282.14 17.52 o
-4 -6 1 2618.97 2576.60 64.12 o
-3 -6 1 31.44 38.09 2.44 o
-2 -6 1 3855.57 3778.85 70.49 o
-1 -6 1 1189.43 1199.56 17.92 o
0 -6 1 248.77 257.37 4.97 o
1 -6 1 3140.46 3138.12 51.18 o
2 -6 1 113.36 110.95 3.15 o
3 -6 1 3775.96 3640.35 80.27 o
4 -6 1 777.43 786.45 28.26 o
5 -6 1 272.85 259.98 16.99 o
-6 -5 1 298.98 284.70 16.76 o
-5 -5 1 873.40 859.84 32.94 o
-4 -5 1 1054.65 1033.43 21.67 o
-3 -5 1 132.22 130.07 3.05 o
-2 -5 1 1749.82 1687.90 26.41 o
-1 -5 1 1385.31 1307.27 23.20 o
0 -5 1 1095.12 1009.17 14.90 o
1 -5 1 5085.46 4945.82 68.53 o
2 -5 1 271.88 277.39 5.75 o
3 -5 1 310.33 309.59 7.28 o
4 -5 1 622.39 633.25 33.77 o
5 -5 1 245.08 229.11 16.16 o
-6 -4 1 956.42 956.38 50.96 o
-5 -4 1 830.74 854.35 32.46 o
-4 -4 1 1603.78 1599.94 31.68 o
-3 -4 1 45.73 50.06 1.83 o
-2 -4 1 2366.73 2345.28 33.29 o
-1 -4 1 2980.84 2918.32 40.90 o
0 -4 1 4993.66 4688.25 57.88 o
1 -4 1 2412.22 2376.20 31.95 o
2 -4 1 567.65 584.56 8.74 o
3 -4 1 2357.20 2344.03 42.07 o
4 -4 1 641.11 637.04 23.41 o
5 -4 1 958.48 934.51 52.19 o
6 -4 1 132.23 134.50 9.79 o
-6 -3 1 43.02 54.89 7.85 o
-5 -3 1 689.03 703.10 19.91 o
-4 -3 1 567.30 586.08 10.12 o
-3 -3 1 7432.31 7459.66 105.08 o
-2 -3 1 617.91 622.63 9.11 o
-1 -3 1 2376.97 2334.26 29.55 o
0 -3 1 470.17 474.69 6.98 o
1 -3 1 1066.58 1054.47 13.36 o
2 -3 1 7599.24 7435.04 93.83 o
3 -3 1 1019.81 1043.52 21.17 o
4 -3 1 1669.60 1617.51 47.84 o
5 -3 1 59.16 81.10 9.22 o
6 -3 1 134.56 125.39 10.52 o
-6 -2 1 1938.41 1888.70 72.39 o
-5 -2 1 1506.58 1530.14 30.27 o
-4 -2 1 1127.17 1119.58 16.32 o
-3 -2 1 4.08 7.12 0.91 o
-2 -2 1 1920.09 1973.05 25.44 o
-1 -2 1 6992.07 6602.37 93.13 o
0 -2 1 7599.93 6272.53 100.31 o
1 -2 1 626.56 651.09 8.11 o
2 -2 1 1083.83 1106.11 13.82 o
3 -2 1 1463.19 1471.10 25.80 o
4 -2 1 1393.31 1376.39 32.94 o
5 -2 1 2084.45 2097.98 107.14 o
6 -2 1 47.54 52.17 7.57 o
-6 -1 1 213.44 228.19 19.08 o
-5 -1 1 370.69 369.70 8.38 o
-4 -1 1 1673.49 1714.50 24.72 o
-3 -1 1 1831.61 1823.46 25.33 o
-2 -1 1 4468.90 4569.21 61.21 o
0 -1 1 402.10 448.22 11.90 o
1 -1 1 5057.33 5145.79 68.90 o
2 -1 1 1658.58 1665.65 19.07 o
3 -1 1 950.66 953.16 19.56 o
4 -1 1 855.42 837.34 18.83 o
5 -1 1 660.21 627.36 49.68 o
6 -1 1 950.68 928.27 50.37 o
-6 0 1 19.39 21.04 4.03 o
-5 0 1 102.05 108.74 3.97 o
-4 0 1 7036.56 6889.52 103.86 o
-3 0 1 78.64 80.86 1.72 o
-2 0 1 15321.13 13022.57 203.74 o
-1 0 1 12.51 11.88 0.72 o
0 0 1 11.69 12.44 0.68 o
1 0 1 6086.66 5894.48 75.75 o
2 0 1 1259.84 1352.07 16.59 o
3 0 1 11391.74 11539.75 196.86 o
4 0 1 639.21 627.67 14.86 o
5 0 1 155.83 153.13 11.19 o
-6 1 1 215.39 215.30 10.98 o
-5 1 1 358.57 377.04 8.93 o
-4 1 1 1652.90 1636.08 22.46 o
-3 1 1 1828.77 1812.53 25.90 o
-2 1 1 4463.42 4546.41 58.14 o
-1 1 1 122.84 140.95 2.79 o
0 1 1 447.98 451.57 12.40 o
1 1 1 5122.02 5242.94 66.62 o
2 1 1 1570.13 1566.09 18.86 o
3 1 1 952.01 966.56 17.28 o
4 1 1 839.86 825.73 17.49 o
5 1 1 659.34 631.48 30.25 o
6 1 1 979.65 917.34 54.26 o
-6 2 1 1921.85 1913.91 71.40 o
-5 2 1 1535.17 1579.94 32.67 o
-4 2 1 1123.69 1119.34 15.36 o
-3 2 1 4.59 10.03 1.40 o
-2 2 1 1907.50 1987.43 28.28 o
-1 2 1 7107.15 6647.29 81.50 o
0 2 1 7517.06 6398.66 102.31 o
1 2 1 574.61 600.25 8.83 o
2 2 1 1174.76 1189.86 14.40 o
3 2 1 1449.65 1476.86 26.59 o
4 2 1 1398.05 1380.94 29.78 o
5 2 1 2076.16 2020.17 77.13 o
6 2 1 42.73 50.61 9.52 o
-6 3 1 45.34 51.31 8.25 o
-5 3 1 695.47 718.17 19.22 o
-4 3 1 565.06 578.88 9.36 o
-3 3 1 7441.44 7469.34 104.29 o
-2 3 1 614.53 638.99 10.19 o
-1 3 1 2358.24 2366.14 28.90 o
0 3 1 499.38 476.39 8.20 o
1 3 1 1108.12 1088.01 13.19 o
2 3 1 7552.66 7522.20 88.53 o
3 3 1 1010.32 1023.34 17.70 o
4 3 1 1704.51 1687.91 42.35 o
5 3 1 46.68 60.51 5.99 o
6 3 1 135.06 131.08 12.98 o
-6 4 1 963.07 951.99 37.26 o
-5 4 1 828.76 839.06 22.82 o
-4 4 1 1591.63 1581.94 28.02 o
-3 4 1 44.84 47.23 1.71 o
-2 4 1 2396.28 2396.74 32.76 o
-1 4 1 2998.97 2997.77 38.97 o
0 4 1 5017.36 4730.25 73.59 o
1 4 1 2418.97 2364.89 35.71 o
2 4 1 579.86 599.64 8.62 o
3 4 1 2331.46 2263.63 43.03 o
4 4 1 627.76 622.37 17.25 o
5 4 1 992.45 981.73 67.62 o
6 4 1 126.29 116.67 11.32 o
-6 5 1 300.22 270.18 16.99 o
-5 5 1 883.26 858.04 21.08 o
-4 5 1 1043.95 1007.68 24.01 o
-3 5 1 131.06 131.68 2.95 o
-2 5 1 1720.64 1688.50 23.68 o
-1 5 1 1349.28 1204.90 24.98 o
0 5 1 1133.94 1061.34 14.34 o
1 5 1 4956.47 4957.73 75.55 o
2 5 1 269.55 259.68 5.94 o
3 5 1 333.31 325.72 7.79 o
4 5 1 615.46 567.55 28.66 o
5 5 1 247.27 242.30 12.26 o
-6 6 1 164.68 152.33 8.36 o
-5 6 1 304.57 281.69 13.76 o
-4 6 1 2622.06 2453.60 71.54 o
-3 6 1 29.80 33.46 2.16 o
-2 6 1 3858.20 3623.74 55.72 o
-1 6 1 1231.74 1207.32 16.66 o
0 6 1 311.62 326.68 4.97 o
1 6 1 3176.21 3185.98 52.51 o
2 6 1 119.30 119.45 3.71 o
3 6 1 3721.65 3577.22 74.82 o
4 6 1 825.75 757.37 33.97 o
5 6 1 287.00 270.17 12.87 o
-5 7 1 425.23 387.15 13.46 o
-4 7 1 248.84 246.69 7.02 o
-3 7 1 3068.91 2919.00 77.60 o
-2 7 1 487.05 466.28 8.86 o
-1 7 1 1004.56 958.58 13.64 o
0 7 1 734.19 695.26 10.23 o
1 7 1 837.97 857.02 14.10 o
2 7 1 2273.79 2285.55 36.19 o
3 7 1 729.90 716.30 17.34 o
4 7 1 756.18 799.34 31.59 o
5 7 1 162.15 174.44 9.07 o
-5 8 1 758.37 740.13 27.76 o
-4 8 1 82.66 86.69 4.70 o
-3 8 1 14.51 17.44 2.82 o
-2 8 1 95.70 103.43 3.97 o
-1 8 1 2456.91 2474.22 40.73 o
0 8 1 1776.09 1755.92 26.22 o
1 8 1 55.86 61.41 2.49 o
2 8 1 428.11 450.53 10.38 o
3 8 1 72.31 78.44 5.35 o
4 8 1 692.06 693.77 27.49 o
5 8 1 931.88 912.56 46.19 o
-5 9 1 624.37 613.21 29.46 o
-4 9 1 386.30 376.79 12.07 o
-3 9 1 2991.13 2960.41 64.60 o
-2 9 1 397.91 423.04 9.21 o
-1 9 1 974.66 1028.49 20.50 o
0 9 1 381.37 398.95 8.46 o
1 9 1 847.74 861.90 17.92 o
2 9 1 2368.89 2355.87 52.58 o
3 9 1 343.47 324.80 11.65 o
4 9 1 1224.63 1244.68 37.13 o
-4 10 1 754.07 753.31 27.52 o
-3 10 1 13.05 14.64 2.86 o
-2 10 1 1009.87 1049.56 21.46 o
-1 10 1 187.77 189.09 5.04 o
0 10 1 162.28 164.32 4.82 o
1 10 1 477.42 498.38 13.74 o
2 10 1 105.40 105.52 5.30 o
3 10 1 1279.34 1320.06 48.09 o
4 10 1 109.03 109.58 8.13 o
-4 11 1 329.50 315.02 16.88 o
-3 11 1 193.07 192.24 6.91 o
-2 11 1 739.48 746.38 21.89 o
-1 11 1 610.12 627.43 14.34 o
0 11 1 577.83 584.78 14.93 o
1 11 1 1361.48 1336.70 39.38 o
2 11 1 120.87 124.44 5.34 o
3 11 1 33.58 31.83 2.95 o
-3 12 1 1.97 2.88 2.14 o
-2 12 1 534.18 501.85 15.18 o
-1 12 1 297.71 302.32 8.42 o
0 12 1 508.73 522.22 15.71 o
1 12 1 359.21 361.56 11.45 o
2 12 1 44.76 42.42 5.34 o
-1 13 1 390.47 389.84 13.83 o
0 13 1 177.89 161.69 5.74 o
1 13 1 25.45 24.39 2.58 o
-2 -12 2 274.87 260.68 9.31 o
-1 -12 2 821.79 819.62 21.37 o
0 -12 2 84.83 81.17 5.24 o
1 -12 2 665.82 663.91 21.36 o
-3 -11 2 934.44 940.27 43.31 o
-2 -11 2 188.52 190.44 7.76 o
-1 -11 2 272.12 272.97 8.38 o
0 -11 2 179.48 175.18 6.14 o
1 -11 2 501.28 498.78 13.77 o
2 -11 2 905.90 867.05 24.06 o
-4 -10 2 75.81 74.98 4.99 o
-3 -10 2 24.42 24.47 3.47 o
-2 -10 2 135.49 131.49 4.13 o
-1 -10 2 1994.93 2098.17 38.83 o
0 -10 2 57.05 62.59 2.51 o
1 -10 2 476.63 505.04 10.34 o
2 -10 2 100.08 106.96 4.93 o
3 -10 2 133.98 138.96 10.72 o
-5 -9 2 1191.46 1173.73 60.95 o
-4 -9 2 329.51 328.29 13.76 o
-3 -9 2 383.05 386.45 9.22 o
-2 -9 2 1169.98 1182.26 22.49 o
-1 -9 2 397.00 409.53 7.89 o
0 -9 2 3294.74 3416.95 51.95 o
1 -9 2 447.82 458.30 8.58 o
2 -9 2 707.09 731.09 16.08 o
3 -9 2 239.31 248.98 9.99 o
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