#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/54/2105479.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105479_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Taouss, Christina' 'Teschmit, Nicole' 'Thomas, Lena' _publ_section_title ; Methylthioureas and their morpholine and dioxane adducts; hydrogen-bonding patterns ; _journal_coeditor_code GP5065 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 405 _journal_page_last 413 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.182 _cell_angle_beta 73.785 _cell_angle_gamma 81.448 _cell_length_a 7.6615 _cell_length_b 7.6945 _cell_length_c 8.0283 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.7101 _[local]_cod_data_source_file gp5065birkesup2.hkl _[local]_cod_data_source_block birke #BEGIN Tags that were not found in dictionaries: _shelx_title ' Birke in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 16.07 16.98 0.32 o 2 0 0 4603.07 4593.41 23.41 o 3 0 0 416.53 432.21 3.45 o 4 0 0 2.80 4.53 0.48 o 5 0 0 57.25 61.99 1.52 o 6 0 0 293.44 307.48 4.27 o 7 0 0 32.85 29.93 2.08 o 8 0 0 525.94 534.72 8.91 o 9 0 0 15.59 15.56 1.72 o 10 0 0 170.23 170.92 9.50 o -10 1 0 26.32 32.78 4.39 o -9 1 0 156.64 167.19 6.24 o -8 1 0 46.53 44.92 2.59 o -7 1 0 94.58 97.67 2.66 o -6 1 0 149.93 148.93 3.23 o -5 1 0 165.25 156.08 1.38 o -4 1 0 375.43 394.24 2.42 o -3 1 0 74.46 71.50 0.86 o -2 1 0 374.74 393.85 2.02 o -1 1 0 36.58 34.82 0.39 o 0 1 0 104.85 118.54 0.86 o 1 1 0 151.21 174.73 0.97 o 2 1 0 296.47 332.63 1.47 o 3 1 0 2101.11 2137.74 11.84 o 4 1 0 1199.18 1219.73 8.68 o 5 1 0 68.28 76.05 1.60 o 6 1 0 95.89 93.82 2.16 o 7 1 0 41.36 38.27 1.68 o 8 1 0 19.03 17.41 1.30 o 9 1 0 59.47 59.01 3.21 o -9 2 0 124.52 126.76 6.33 o -8 2 0 34.21 30.98 2.59 o -7 2 0 6.44 5.52 0.93 o -6 2 0 88.01 85.67 2.32 o -5 2 0 601.46 621.17 5.08 o -4 2 0 208.22 210.57 2.17 o -3 2 0 1337.65 1341.53 7.06 o -2 2 0 636.38 641.58 3.41 o -1 2 0 3289.80 3355.39 12.47 o 0 2 0 0.20 0.57 0.20 o 1 2 0 3782.31 3747.64 11.26 o 2 2 0 348.72 335.52 2.69 o 3 2 0 1.36 0.36 0.16 o 4 2 0 297.69 313.39 2.02 o 5 2 0 465.72 433.10 3.99 o 6 2 0 0.49 -0.17 0.47 o 7 2 0 611.81 619.67 9.48 o 8 2 0 1.97 2.01 0.77 o 9 2 0 61.74 66.25 3.83 o 10 2 0 0.87 -1.22 7.81 o -9 3 0 38.09 39.73 3.17 o -8 3 0 127.43 131.39 4.29 o -7 3 0 3.64 2.77 0.79 o -6 3 0 12.20 12.04 0.76 o -5 3 0 6.64 6.94 0.71 o -4 3 0 53.10 55.47 1.18 o -3 3 0 0.70 2.57 0.37 o -2 3 0 1129.31 1157.99 6.03 o -1 3 0 884.44 855.76 4.82 o 0 3 0 58.23 59.38 0.93 o 1 3 0 1050.50 1052.63 4.82 o 2 3 0 2.07 2.45 0.29 o 3 3 0 8.42 10.89 0.45 o 4 3 0 39.32 44.99 0.88 o 5 3 0 13.40 11.38 0.40 o 6 3 0 91.21 87.60 2.60 o 7 3 0 173.83 173.31 3.67 o 8 3 0 121.31 122.82 3.66 o 9 3 0 58.46 62.20 3.48 o 10 3 0 65.67 67.30 5.84 o -9 4 0 14.93 12.36 4.37 o -8 4 0 149.79 150.61 7.57 o -7 4 0 3.56 3.79 1.13 o -6 4 0 333.11 330.60 4.19 o -5 4 0 2.56 2.20 0.54 o -4 4 0 289.59 290.16 3.47 o -3 4 0 0.46 0.91 0.40 o -2 4 0 8.64 14.97 0.54 o -1 4 0 31.13 27.12 0.86 o 0 4 0 10.70 19.35 0.68 o 1 4 0 0.50 0.39 0.25 o 2 4 0 413.43 390.47 2.58 o 3 4 0 379.80 379.93 2.88 o 4 4 0 274.09 251.43 2.18 o 5 4 0 151.53 161.60 2.36 o 6 4 0 0.36 0.68 0.70 o 7 4 0 45.90 43.87 2.02 o 8 4 0 39.97 38.49 2.04 o 9 4 0 30.95 29.63 2.50 o -8 5 0 0.44 -0.65 1.20 o -7 5 0 11.93 9.97 1.53 o -6 5 0 480.64 478.45 8.12 o -5 5 0 67.04 69.54 2.20 o -4 5 0 811.86 803.53 7.00 o -3 5 0 74.26 89.72 1.77 o -2 5 0 252.45 241.90 2.55 o -1 5 0 111.13 117.15 2.64 o 0 5 0 67.00 62.32 1.32 o 1 5 0 21.38 21.51 0.80 o 2 5 0 81.19 74.41 1.20 o 3 5 0 31.10 30.19 1.12 o 4 5 0 259.41 253.90 3.39 o 5 5 0 99.33 99.13 2.15 o 6 5 0 391.15 390.82 5.98 o 7 5 0 62.82 63.73 2.54 o 8 5 0 116.57 116.22 5.20 o 9 5 0 1.18 2.10 1.65 o -7 6 0 125.27 128.64 5.11 o -6 6 0 6.97 6.78 1.25 o -5 6 0 20.57 22.11 1.40 o -4 6 0 28.66 30.57 1.50 o -3 6 0 352.58 330.39 4.43 o -2 6 0 209.38 210.33 3.31 o -1 6 0 682.59 653.45 6.06 o 0 6 0 351.74 341.41 3.98 o 1 6 0 61.07 51.92 1.45 o 2 6 0 16.88 18.62 0.99 o 3 6 0 7.19 6.92 0.74 o 4 6 0 2.08 2.34 0.53 o 5 6 0 115.95 110.99 2.48 o 6 6 0 34.13 34.19 2.58 o 7 6 0 298.66 296.77 5.70 o 8 6 0 80.68 79.90 3.66 o 9 6 0 217.91 208.69 14.17 o -7 7 0 214.60 245.92 16.06 o -6 7 0 1.72 2.60 1.27 o -5 7 0 453.97 448.23 6.69 o -4 7 0 2.90 2.17 0.79 o -3 7 0 143.68 139.64 3.18 o -2 7 0 3.03 5.97 0.81 o -1 7 0 2.69 3.46 0.59 o 0 7 0 46.33 44.73 1.52 o 1 7 0 291.11 297.40 4.29 o 2 7 0 41.52 43.61 1.67 o 3 7 0 502.12 501.07 5.68 o 4 7 0 19.76 18.93 1.12 o 5 7 0 73.30 74.16 2.11 o 6 7 0 0.02 0.30 0.92 o 7 7 0 5.94 4.69 1.16 o 8 7 0 1.21 -0.86 3.23 o -5 8 0 213.52 221.85 4.90 o -4 8 0 138.45 140.68 3.60 o -3 8 0 161.35 175.64 3.86 o -2 8 0 284.79 277.97 4.76 o -1 8 0 72.42 73.47 2.66 o 0 8 0 39.27 39.61 1.67 o 1 8 0 0.63 0.47 0.61 o 2 8 0 86.26 80.20 2.31 o 3 8 0 14.86 13.94 1.12 o 4 8 0 307.56 303.86 5.03 o 5 8 0 27.14 29.32 1.55 o 6 8 0 294.05 287.98 6.36 o 7 8 0 60.44 67.72 4.28 o -4 9 0 0.35 -0.50 1.05 o -3 9 0 20.20 24.03 1.72 o -2 9 0 121.59 126.40 3.68 o -1 9 0 2.46 2.18 0.92 o 0 9 0 70.67 79.02 3.19 o 1 9 0 2.26 2.66 0.95 o 2 9 0 24.42 25.21 1.55 o 3 9 0 0.66 0.18 0.77 o 4 9 0 0.01 -0.13 0.73 o 5 9 0 27.19 26.69 1.54 o 6 9 0 32.23 30.06 7.33 o -2 10 0 4.25 2.35 2.89 o -1 10 0 0.75 3.32 2.20 o 0 10 0 38.38 34.78 2.35 o 1 10 0 153.77 157.22 4.04 o 2 10 0 130.21 140.57 4.31 o 3 10 0 133.72 119.30 4.85 o 4 10 0 5.29 7.80 1.66 o -2 -10 1 1.15 5.46 2.37 o -1 -10 1 8.99 9.17 2.08 o 0 -10 1 107.33 113.66 6.13 o 1 -10 1 38.02 33.89 5.81 o -5 -9 1 1.26 2.08 1.28 o -4 -9 1 2.87 3.27 0.91 o -3 -9 1 32.76 33.35 1.79 o -2 -9 1 51.47 53.78 2.25 o -1 -9 1 5.68 5.42 1.04 o 0 -9 1 30.53 30.35 2.10 o 1 -9 1 10.77 10.55 1.22 o 2 -9 1 10.15 12.96 1.27 o 3 -9 1 63.99 66.15 2.79 o 4 -9 1 76.71 79.31 4.58 o -6 -8 1 9.85 11.36 1.63 o -5 -8 1 13.98 13.35 1.14 o -4 -8 1 1.75 1.55 0.66 o -3 -8 1 251.35 255.48 4.36 o -2 -8 1 5.53 5.67 0.76 o -1 -8 1 218.79 213.55 3.81 o 0 -8 1 41.73 42.24 1.94 o 1 -8 1 278.21 286.62 4.81 o 2 -8 1 41.32 38.90 1.81 o 3 -8 1 30.43 29.89 1.51 o 4 -8 1 11.49 10.35 1.33 o 5 -8 1 150.62 155.99 3.92 o -7 -7 1 95.38 93.74 4.03 o -6 -7 1 43.71 44.58 2.67 o -5 -7 1 91.76 89.42 2.38 o -4 -7 1 4.55 4.65 0.74 o -3 -7 1 31.80 29.38 1.31 o -2 -7 1 165.01 162.87 2.69 o -1 -7 1 0.03 0.62 0.55 o 0 -7 1 327.09 328.14 4.10 o 1 -7 1 159.43 151.29 2.85 o 2 -7 1 82.39 86.05 2.44 o 3 -7 1 124.42 124.85 2.92 o 4 -7 1 81.73 82.15 2.59 o 5 -7 1 100.40 107.60 3.22 o 6 -7 1 21.31 24.85 2.16 o -8 -6 1 0.44 -0.47 1.23 o -7 -6 1 29.82 29.35 2.01 o -6 -6 1 91.33 91.70 3.28 o -5 -6 1 2.41 3.08 0.57 o -4 -6 1 565.64 558.76 5.18 o -3 -6 1 13.13 11.32 0.83 o -2 -6 1 484.42 472.42 5.05 o -1 -6 1 21.22 19.78 0.96 o 0 -6 1 0.35 0.70 0.43 o 1 -6 1 9.52 8.00 0.66 o 2 -6 1 122.37 122.35 2.48 o 3 -6 1 0.00 0.45 0.60 o 4 -6 1 486.62 483.79 5.79 o 5 -6 1 57.48 54.48 2.14 o 6 -6 1 315.67 311.56 5.33 o 7 -6 1 21.55 18.63 1.90 o -9 -5 1 59.16 61.66 9.32 o -8 -5 1 127.70 127.65 4.73 o -7 -5 1 14.21 16.15 1.48 o -6 -5 1 29.12 26.10 1.61 o -5 -5 1 141.45 137.80 2.42 o -4 -5 1 148.43 147.57 2.36 o -3 -5 1 377.49 383.25 3.53 o -2 -5 1 75.00 74.41 1.64 o -1 -5 1 1139.22 1143.59 6.87 o 0 -5 1 36.28 38.05 1.17 o 1 -5 1 582.80 603.52 5.20 o 2 -5 1 177.53 165.34 2.50 o 3 -5 1 32.39 31.42 1.37 o 4 -5 1 0.03 -0.60 0.60 o 5 -5 1 102.48 95.57 2.34 o 6 -5 1 22.06 22.39 1.37 o 7 -5 1 85.66 80.52 3.87 o 8 -5 1 66.80 70.83 3.53 o -9 -4 1 56.20 58.33 3.89 o -8 -4 1 1.96 2.50 1.03 o -7 -4 1 414.26 415.60 8.08 o -6 -4 1 23.62 24.42 1.48 o -5 -4 1 404.34 390.19 4.60 o -4 -4 1 6.18 5.31 0.53 o -3 -4 1 53.46 47.99 0.90 o -2 -4 1 15.27 12.89 0.49 o -1 -4 1 971.93 974.72 5.53 o 0 -4 1 69.12 68.06 1.38 o 1 -4 1 960.00 949.37 6.56 o 2 -4 1 50.17 49.42 1.51 o 3 -4 1 472.87 459.36 4.42 o 4 -4 1 38.37 41.67 1.23 o 5 -4 1 209.14 204.08 2.98 o 6 -4 1 74.37 77.77 2.04 o 7 -4 1 24.47 25.16 2.16 o 8 -4 1 22.07 19.79 2.00 o 9 -4 1 72.96 76.07 9.44 o -9 -3 1 10.91 10.91 1.58 o -8 -3 1 15.31 11.26 1.46 o -7 -3 1 1.75 1.71 0.77 o -6 -3 1 57.18 51.78 1.80 o -5 -3 1 255.38 261.30 2.63 o -4 -3 1 736.31 749.78 4.95 o -3 -3 1 1396.55 1379.22 6.61 o -2 -3 1 682.64 720.29 3.88 o -1 -3 1 50.47 53.32 1.06 o 0 -3 1 695.26 675.38 4.54 o 1 -3 1 532.30 533.74 4.33 o 2 -3 1 46.66 30.58 0.96 o 3 -3 1 909.04 922.68 6.28 o 4 -3 1 151.49 136.77 2.03 o 5 -3 1 320.49 321.72 4.05 o 6 -3 1 78.49 80.07 1.76 o 7 -3 1 9.72 10.75 1.29 o 8 -3 1 36.80 35.99 2.12 o 9 -3 1 1.71 2.45 1.25 o -9 -2 1 6.26 4.08 1.14 o -8 -2 1 119.68 118.08 3.85 o -7 -2 1 33.94 30.29 1.71 o -6 -2 1 0.07 0.39 0.53 o -5 -2 1 52.06 57.67 0.89 o -4 -2 1 98.85 99.31 1.18 o -3 -2 1 236.55 241.31 1.75 o -2 -2 1 820.89 840.28 4.10 o -1 -2 1 5.89 7.27 0.34 o 0 -2 1 7311.06 7105.11 41.23 o 1 -2 1 183.13 181.96 1.78 o 2 -2 1 371.77 374.87 2.75 o 3 -2 1 184.52 190.91 1.84 o 4 -2 1 285.73 284.25 2.66 o 5 -2 1 115.57 128.06 1.81 o 6 -2 1 533.21 556.08 4.69 o 7 -2 1 7.09 6.93 0.99 o 8 -2 1 268.14 270.26 5.57 o 9 -2 1 1.56 -0.89 1.24 o 10 -2 1 3.51 6.41 2.92 o -9 -1 1 35.63 40.48 3.79 o -8 -1 1 132.10 140.41 4.19 o -7 -1 1 0.04 -0.59 0.66 o -6 -1 1 188.09 187.46 3.22 o -5 -1 1 0.07 0.26 0.18 o -4 -1 1 279.94 286.99 2.04 o -3 -1 1 0.35 0.82 0.19 o -2 -1 1 1.56 1.69 0.20 o -1 -1 1 877.49 859.44 3.05 o 0 -1 1 1484.21 1589.69 5.45 o 1 -1 1 1705.45 1636.83 6.14 o 2 -1 1 1671.08 1714.73 6.41 o 3 -1 1 196.30 178.41 1.42 o 4 -1 1 1806.61 1841.93 8.31 o 5 -1 1 7.73 8.83 0.35 o 6 -1 1 12.04 11.13 0.83 o 7 -1 1 61.11 54.52 1.73 o 8 -1 1 260.37 255.42 5.79 o 9 -1 1 19.35 22.84 2.54 o 10 -1 1 165.70 179.49 9.77 o -10 0 1 7.07 7.56 3.36 o -9 0 1 6.46 5.16 1.60 o -8 0 1 15.43 11.94 1.57 o -7 0 1 213.16 211.86 4.96 o -6 0 1 0.41 0.34 0.46 o -5 0 1 1253.48 1209.85 7.95 o -4 0 1 386.37 387.45 2.38 o -3 0 1 800.21 765.90 3.85 o -2 0 1 485.06 483.71 2.54 o -1 0 1 166.11 179.36 1.02 o 0 0 1 16.95 16.43 0.47 o 1 0 1 80.99 91.87 0.57 o 2 0 1 1114.74 1126.04 3.67 o 3 0 1 1305.43 1278.35 6.54 o 4 0 1 685.96 775.68 5.77 o 5 0 1 630.44 605.23 5.33 o 6 0 1 4.51 8.10 0.71 o 7 0 1 297.84 314.76 4.02 o 8 0 1 0.02 -0.17 0.78 o 9 0 1 14.77 13.75 1.50 o 10 0 1 2.69 -0.27 1.31 o -9 1 1 110.54 111.00 6.00 o -8 1 1 2.28 2.05 1.10 o -7 1 1 5.70 4.78 0.82 o -6 1 1 63.04 67.55 2.34 o -5 1 1 221.82 218.22 1.78 o -4 1 1 146.74 152.29 1.44 o -3 1 1 80.11 63.87 0.84 o -2 1 1 1022.77 1041.81 4.53 o -1 1 1 1645.90 1695.77 5.96 o 0 1 1 1328.61 1269.84 4.75 o 1 1 1 1984.70 2025.94 8.44 o 2 1 1 3226.69 3133.36 12.67 o 3 1 1 65.35 77.19 0.65 o 4 1 1 221.91 213.54 2.39 o 5 1 1 98.28 87.88 1.74 o 6 1 1 102.48 100.83 1.86 o 7 1 1 474.61 464.45 5.09 o 8 1 1 24.91 21.71 1.24 o 9 1 1 140.01 133.91 5.18 o 10 1 1 11.47 15.90 2.22 o -9 2 1 198.87 188.99 7.93 o -8 2 1 533.51 527.52 10.41 o -7 2 1 195.56 201.49 4.31 o -6 2 1 792.21 792.28 8.27 o -5 2 1 28.46 26.87 0.80 o -4 2 1 212.17 206.85 2.30 o -3 2 1 109.34 117.14 1.54 o -2 2 1 313.39 310.21 2.21 o -1 2 1 1503.62 1504.80 5.84 o 0 2 1 723.08 751.22 3.34 o 1 2 1 179.08 206.29 1.27 o 2 2 1 3852.75 3820.43 17.35 o 3 2 1 818.31 808.63 3.56 o 4 2 1 957.68 912.74 3.90 o 5 2 1 152.03 172.44 2.52 o 6 2 1 12.71 13.03 0.73 o 7 2 1 164.87 147.96 3.05 o 8 2 1 176.68 178.46 3.96 o 9 2 1 124.44 131.01 5.72 o 10 2 1 346.33 366.95 18.73 o -9 3 1 1.68 0.90 1.43 o -8 3 1 13.19 16.23 1.86 o -7 3 1 94.80 99.73 3.44 o -6 3 1 865.62 871.00 8.91 o -5 3 1 122.27 126.89 2.13 o -4 3 1 1293.18 1264.62 7.27 o -3 3 1 36.20 36.62 0.86 o -2 3 1 240.34 225.97 2.06 o -1 3 1 6.59 6.97 0.39 o 0 3 1 11.19 13.22 0.49 o 1 3 1 780.02 797.00 4.02 o 2 3 1 461.92 420.12 2.77 o 3 3 1 206.98 210.41 1.76 o 4 3 1 121.37 115.34 1.38 o 5 3 1 215.65 224.08 1.73 o 6 3 1 246.70 249.77 3.78 o 7 3 1 49.40 46.43 2.23 o 8 3 1 72.80 71.82 2.77 o 9 3 1 0.18 0.29 1.10 o 10 3 1 74.10 80.83 4.57 o -8 4 1 141.38 141.10 5.78 o -7 4 1 193.93 193.77 6.27 o -6 4 1 10.25 9.34 1.04 o -5 4 1 139.36 141.08 2.60 o -4 4 1 147.78 150.50 2.34 o -3 4 1 332.97 328.63 3.12 o -2 4 1 841.41 880.17 5.62 o -1 4 1 1271.54 1270.49 8.19 o 0 4 1 1201.25 1219.17 6.76 o 1 4 1 136.22 141.97 1.56 o 2 4 1 27.41 23.07 0.54 o 3 4 1 51.75 49.82 0.81 o 4 4 1 41.97 39.89 0.99 o 5 4 1 53.77 55.45 1.50 o 6 4 1 296.19 288.17 4.97 o 7 4 1 147.13 145.99 4.56 o 8 4 1 211.25 201.38 6.40 o 9 4 1 159.53 158.15 6.81 o 10 4 1 17.86 14.06 5.11 o -8 5 1 0.45 0.50 1.82 o -7 5 1 250.63 256.19 7.74 o -6 5 1 2.39 2.09 0.94 o -5 5 1 266.36 270.40 3.80 o -4 5 1 8.88 7.90 0.72 o -3 5 1 1.01 0.36 0.49 o -2 5 1 87.78 86.80 1.67 o -1 5 1 135.88 125.18 2.09 o 0 5 1 48.08 53.14 1.27 o 1 5 1 501.15 482.02 4.55 o 2 5 1 179.78 191.78 1.98 o 3 5 1 402.69 388.28 3.66 o 4 5 1 6.35 5.79 0.49 o 5 5 1 35.07 34.23 1.38 o 6 5 1 13.75 14.50 1.57 o 7 5 1 91.29 86.03 3.12 o 8 5 1 25.93 26.47 2.54 o 9 5 1 108.92 123.06 5.47 o -7 6 1 31.02 29.15 2.79 o -6 6 1 22.98 23.21 1.95 o -5 6 1 420.54 422.19 5.53 o -4 6 1 5.68 4.29 0.68 o -3 6 1 315.99 322.79 3.99 o -2 6 1 43.41 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73.08 2.34 o 5 4 9 7.87 8.14 0.94 o 6 4 9 350.55 346.69 5.22 o 7 4 9 13.08 11.94 1.10 o 8 4 9 124.46 113.66 9.15 o -2 5 9 0.11 1.11 1.15 o -1 5 9 74.94 82.45 3.47 o 0 5 9 8.02 5.80 1.06 o 1 5 9 272.32 274.62 5.78 o 2 5 9 61.26 59.04 2.51 o 3 5 9 234.07 243.76 4.51 o 4 5 9 8.65 9.11 1.06 o 5 5 9 112.55 109.13 3.08 o 6 5 9 5.54 5.35 1.16 o 7 5 9 14.87 11.78 1.67 o 8 5 9 0.40 -0.41 2.91 o -1 6 9 146.18 149.33 9.62 o 0 6 9 2.57 1.07 1.21 o 1 6 9 7.57 7.58 1.38 o 2 6 9 51.12 49.71 2.48 o 3 6 9 174.14 175.50 4.34 o 4 6 9 0.11 0.36 0.89 o 5 6 9 502.40 515.49 7.39 o 6 6 9 13.33 12.04 1.32 o 7 6 9 228.27 216.92 10.98 o 1 7 9 50.01 44.90 8.03 o 2 7 9 73.15 71.67 3.07 o 3 7 9 28.45 29.61 1.76 o 4 7 9 2.26 0.08 0.94 o 5 7 9 31.73 33.21 1.96 o 6 7 9 13.59 14.54 2.18 o 2 8 9 103.58 95.65 9.75 o 3 8 9 1.35 2.22 4.29 o 4 8 9 194.41 194.32 13.76 o 0 -2 10 1.30 3.94 1.43 o 1 -2 10 11.32 10.53 2.31 o 2 -2 10 142.22 137.18 5.94 o 3 -2 10 26.38 23.13 3.03 o 4 -2 10 209.79 237.99 16.58 o -1 -1 10 48.00 45.79 3.53 o 0 -1 10 4.64 5.80 0.97 o 1 -1 10 3.66 1.31 0.93 o 2 -1 10 3.15 2.03 0.95 o 3 -1 10 13.27 14.56 1.68 o 4 -1 10 3.73 5.89 2.02 o 5 -1 10 186.43 183.38 6.25 o 6 -1 10 10.29 10.45 1.87 o -1 0 10 55.64 56.11 2.94 o 0 0 10 8.91 9.94 1.19 o 1 0 10 284.80 295.06 5.94 o 2 0 10 8.17 6.85 1.13 o 3 0 10 174.63 178.93 4.55 o 4 0 10 3.01 0.99 1.01 o 5 0 10 7.41 9.59 1.70 o 6 0 10 2.76 2.71 1.10 o -1 1 10 26.89 26.34 2.55 o 0 1 10 34.20 32.56 2.08 o 1 1 10 8.11 7.93 1.11 o 2 1 10 246.76 247.03 5.38 o 3 1 10 49.69 51.06 2.46 o 4 1 10 292.32 290.95 6.23 o 5 1 10 19.72 21.46 1.75 o 6 1 10 122.59 118.14 3.71 o 7 1 10 7.61 2.42 1.33 o -1 2 10 3.58 2.10 1.19 o 0 2 10 75.64 78.36 3.16 o 1 2 10 63.00 67.27 2.59 o 2 2 10 62.82 61.29 2.53 o 3 2 10 1.92 1.51 0.88 o 4 2 10 49.56 49.72 2.41 o 5 2 10 5.47 3.84 0.85 o 6 2 10 219.06 212.76 4.69 o 7 2 10 4.98 1.71 0.82 o -1 3 10 57.01 50.89 3.05 o 0 3 10 81.27 80.37 3.21 o 1 3 10 152.76 154.22 4.17 o 2 3 10 124.08 124.36 3.78 o 3 3 10 120.61 131.08 3.89 o 4 3 10 0.55 -0.88 0.89 o 5 3 10 106.16 103.77 3.06 o 6 3 10 12.62 10.61 1.07 o 7 3 10 1.36 -0.65 1.41 o 0 4 10 1.79 2.77 1.10 o 1 4 10 78.84 87.91 3.17 o 2 4 10 51.86 52.32 2.32 o 3 4 10 185.76 188.86 4.44 o 4 4 10 19.00 20.06 1.67 o 5 4 10 241.66 242.44 4.36 o 6 4 10 1.93 1.38 1.15 o 7 4 10 27.59 30.04 2.95 o 0 5 10 31.05 26.90 5.60 o 1 5 10 47.23 46.62 3.19 o 2 5 10 1.63 1.36 0.91 o 3 5 10 7.73 6.18 1.12 o 4 5 10 10.55 8.90 1.16 o 5 5 10 101.76 98.59 3.08 o 6 5 10 0.13 -0.82 0.82 o 1 6 10 34.59 50.52 7.29 o 2 6 10 101.11 101.78 6.01 o 3 6 10 8.98 12.11 3.24 o 4 6 10 47.34 45.97 3.21 o 5 6 10 3.51 5.70 1.53 o 3 0 11 32.47 29.64 5.62 o 3 1 11 0.08 2.03 2.25 o 3 3 11 1.76 8.63 4.83 o 4 3 11 32.78 38.32 7.38 o 5 3 11 84.30 95.28 10.83 o 3 4 11 1.44 0.70 2.94 o 4 4 11 0.36 2.07 3.02 o