data_2105779 _cell_angle_alpha 104.906 _cell_angle_beta 106.449 _cell_angle_gamma 95.863 _cell_length_a 11.0030 _cell_length_b 12.7689 _cell_length_c 14.9201 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file bi5028IIsup5.hkl _[local]_cod_data_source_block II _shelx_refln_list_code 4 _shelx_f_calc_maximum 671.34 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3247.28 2524.69 61.68 o 3 0 0 2209.66 2015.29 50.43 o 4 0 0 535.61 489.69 30.04 o 5 0 0 11278.34 11360.61 230.63 o 6 0 0 35837.04 35384.16 663.37 o 7 0 0 2456.09 2537.40 83.14 o 8 0 0 303.05 254.30 48.55 o 9 0 0 59.62 14.59 48.84 o 10 0 0 0.72 -19.41 55.32 o 11 0 0 1028.60 739.35 77.97 o 12 0 0 164.55 165.25 78.08 o 13 0 0 19.95 -16.51 77.84 o -13 1 0 0.47 -135.62 135.62 o -12 1 0 26.53 -25.92 76.50 o -11 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53.43 o -5 6 0 222.60 226.40 46.50 o -4 6 0 15151.60 14618.08 381.78 o -3 6 0 13639.66 12802.57 291.61 o -2 6 0 587.49 657.59 47.85 o -1 6 0 114.02 210.50 31.22 o 0 6 0 16.65 123.80 31.47 o 1 6 0 1150.68 1727.66 68.03 o 2 6 0 574.83 756.11 57.66 o 3 6 0 25.29 166.13 35.31 o 4 6 0 16105.33 16465.03 343.19 o 5 6 0 1171.40 1233.67 64.29 o 6 6 0 413.23 301.49 49.95 o 7 6 0 2994.72 3041.99 112.94 o 8 6 0 268.18 281.92 61.25 o 9 6 0 0.41 32.25 62.83 o 10 6 0 1140.93 1187.92 91.36 o 11 6 0 305.73 297.25 110.84 o -13 7 0 4.16 58.90 173.56 o -12 7 0 8.12 -14.35 86.11 o -11 7 0 144.80 149.82 86.07 o -10 7 0 2571.77 2604.61 117.92 o -9 7 0 1221.57 1042.25 81.02 o -8 7 0 549.33 501.34 69.40 o -7 7 0 15.85 31.57 43.43 o -6 7 0 3770.05 3880.54 168.07 o -5 7 0 5236.22 5255.43 408.81 o -4 7 0 16988.45 17075.22 377.88 o -3 7 0 2.12 86.71 28.87 o -2 7 0 9533.27 9784.89 275.96 o -1 7 0 476.80 460.52 53.15 o 0 7 0 104.53 175.30 34.26 o 1 7 0 12196.34 12303.20 302.36 o 2 7 0 10828.83 9576.05 285.67 o 3 7 0 3414.13 4188.67 143.60 o 4 7 0 37306.07 40243.05 710.35 o 5 7 0 682.83 725.26 91.36 o 6 7 0 1892.49 2139.89 96.41 o 7 7 0 5005.35 5710.49 176.64 o 8 7 0 96.35 169.36 71.83 o 9 7 0 4.64 51.84 75.23 o 10 7 0 56.00 -74.23 78.73 o -12 8 0 16.80 43.96 118.51 o -11 8 0 0.29 -87.25 87.25 o -10 8 0 311.03 466.11 149.28 o -9 8 0 355.93 308.05 73.68 o -8 8 0 22.42 33.12 59.26 o -7 8 0 277.41 395.27 66.37 o -6 8 0 803.33 787.86 85.78 o -5 8 0 16373.93 17668.14 571.58 o -4 8 0 10461.67 10529.27 253.24 o -3 8 0 44.33 99.49 32.40 o -2 8 0 6123.29 6316.01 200.44 o -1 8 0 255.37 167.28 89.92 o 0 8 0 75.82 26.98 38.86 o 1 8 0 62698.35 66884.72 1415.72 o 2 8 0 13396.36 12607.63 320.48 o 3 8 0 114.36 45.84 65.03 o 4 8 0 165.05 115.17 59.35 o 5 8 0 433.02 484.43 67.57 o 6 8 0 2215.84 2026.73 99.52 o 7 8 0 9750.05 10023.93 253.98 o 8 8 0 106.28 128.64 68.69 o 9 8 0 746.38 721.09 100.84 o 10 8 0 586.80 1051.95 196.35 o -12 9 0 0.21 -50.42 116.61 o -11 9 0 109.81 89.12 87.90 o -10 9 0 346.07 57.33 80.16 o -9 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