#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:45:48 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181878 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/59/2105937.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2105937 _cell_angle_alpha 90.000 _cell_angle_beta 109.413 _cell_angle_gamma 90.000 _cell_length_a 11.3416 _cell_length_b 9.0552 _cell_length_c 11.8030 _exptl_crystal_F_000 536.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file dk5007Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'I in P 21/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1973.64 1763.98 88.46 o 4 0 0 3141.88 3116.67 127.02 o 6 0 0 1145.39 1250.27 46.01 o 8 0 0 10.95 9.83 2.37 o 10 0 0 376.69 376.90 12.48 o 12 0 0 0.23 -1.19 3.57 o 1 1 0 275.02 179.08 30.58 o 3 1 0 1065.70 977.87 23.82 o 4 1 0 547.53 557.37 15.86 o 5 1 0 80.73 97.08 2.84 o 6 1 0 66.90 63.97 2.45 o 7 1 0 131.94 128.65 3.31 o 8 1 0 1.73 2.97 0.94 o 9 1 0 41.40 38.94 1.94 o 10 1 0 15.91 13.43 1.46 o 11 1 0 11.92 10.81 2.42 o 12 1 0 90.63 86.54 5.04 o 1 2 0 2212.32 2101.73 41.04 o 2 2 0 1291.25 1143.77 17.56 o 3 2 0 365.70 376.91 7.28 o 4 2 0 41.56 61.64 2.19 o 6 2 0 60.35 71.03 1.97 o 7 2 0 63.97 61.65 1.98 o 8 2 0 151.48 160.51 4.17 o 9 2 0 1.00 -0.35 0.92 o 10 2 0 227.26 209.18 5.26 o 11 2 0 4.02 4.90 3.02 o 12 2 0 21.05 18.54 1.71 o 1 3 0 89.41 78.40 1.21 o 2 3 0 179.96 191.22 2.96 o 3 3 0 467.47 525.34 8.21 o 4 3 0 93.32 91.36 1.84 o 5 3 0 105.43 121.54 2.59 o 6 3 0 7.18 9.37 1.09 o 7 3 0 0.34 18.44 10.21 o 8 3 0 2.46 2.11 0.66 o 9 3 0 29.11 31.61 1.29 o 10 3 0 6.58 9.75 1.18 o 11 3 0 15.54 10.06 1.47 o 12 3 0 1.96 -1.89 1.89 o 0 4 0 21.60 17.00 0.73 o 1 4 0 232.66 167.55 2.95 o 2 4 0 303.14 293.12 4.29 o 3 4 0 893.07 870.71 12.23 o 4 4 0 157.88 184.42 3.43 o 5 4 0 1177.23 1259.86 22.23 o 6 4 0 7.14 7.70 0.74 o 7 4 0 374.14 371.80 8.55 o 8 4 0 0.92 1.28 1.05 o 9 4 0 13.76 17.62 1.41 o 10 4 0 99.72 87.96 2.84 o 11 4 0 131.03 138.57 8.04 o 1 5 0 1510.78 1529.24 20.56 o 2 5 0 12.55 8.79 0.51 o 3 5 0 240.03 276.37 4.22 o 4 5 0 67.04 65.72 1.83 o 5 5 0 163.34 151.94 3.11 o 6 5 0 51.95 41.48 1.42 o 7 5 0 10.50 13.96 0.98 o 8 5 0 3.97 3.00 0.90 o 9 5 0 86.17 89.24 2.67 o 10 5 0 24.50 26.25 4.09 o 11 5 0 106.13 115.56 4.77 o 0 6 0 21.73 26.82 1.11 o 1 6 0 415.61 418.25 5.69 o 2 6 0 32.50 39.30 1.10 o 3 6 0 37.29 30.48 0.88 o 4 6 0 66.57 71.22 1.92 o 5 6 0 1198.65 1195.28 26.72 o 6 6 0 509.78 522.87 9.62 o 7 6 0 2.97 2.74 1.00 o 8 6 0 100.05 100.75 2.63 o 9 6 0 92.84 90.42 3.48 o 10 6 0 61.76 63.65 7.77 o 1 7 0 2.93 6.97 0.70 o 2 7 0 48.96 50.79 1.39 o 3 7 0 304.45 311.48 4.76 o 4 7 0 340.99 352.56 5.92 o 5 7 0 4.79 3.84 0.83 o 6 7 0 244.49 259.40 6.64 o 7 7 0 3.99 3.16 1.32 o 8 7 0 7.03 11.02 2.74 o 9 7 0 8.12 9.06 1.71 o 0 8 0 1093.30 1139.73 22.78 o 1 8 0 35.32 39.73 1.26 o 2 8 0 108.13 107.03 2.34 o 3 8 0 115.54 107.05 2.38 o 4 8 0 255.97 269.14 4.77 o 5 8 0 66.11 53.22 1.93 o 6 8 0 204.39 196.89 4.86 o 7 8 0 6.55 4.95 1.91 o 8 8 0 77.84 75.62 4.32 o 1 9 0 114.02 118.17 2.49 o 2 9 0 16.28 16.69 1.24 o 3 9 0 59.38 60.66 1.96 o 4 9 0 76.14 66.99 2.32 o 5 9 0 83.45 85.60 3.12 o 6 9 0 13.58 12.42 1.70 o 0 10 0 904.79 913.03 24.58 o 1 10 0 127.09 121.18 3.47 o 2 10 0 282.69 302.07 6.87 o 3 10 0 81.33 86.28 5.05 o 4 10 0 67.19 68.63 3.66 o -12 0 1 11.34 12.35 3.79 o -10 0 1 494.51 526.20 17.54 o -8 0 1 792.12 779.77 20.11 o -6 0 1 640.10 650.20 17.23 o -4 0 1 708.78 753.03 23.18 o -2 0 1 711.49 647.49 37.69 o 2 0 1 349.07 340.68 10.46 o 4 0 1 1049.57 993.37 27.30 o 6 0 1 434.79 394.13 11.59 o 8 0 1 267.80 275.42 25.98 o 10 0 1 237.42 254.93 9.41 o 12 0 1 22.15 19.23 4.34 o -12 1 1 9.00 10.31 2.63 o -11 1 1 15.94 15.05 1.79 o -10 1 1 90.19 92.64 3.50 o -9 1 1 89.35 91.18 4.29 o -8 1 1 106.89 115.01 4.23 o -7 1 1 52.68 60.31 2.08 o -6 1 1 637.63 667.42 14.59 o -5 1 1 259.72 245.73 6.74 o -4 1 1 1199.70 1174.15 22.84 o -3 1 1 22.05 10.62 0.48 o -1 1 1 59.67 35.37 10.31 o 0 1 1 759.77 438.09 109.68 o 1 1 1 150.59 136.79 2.81 o 4 1 1 23.38 18.11 3.77 o 5 1 1 116.03 138.51 3.56 o 6 1 1 700.06 695.11 14.78 o 7 1 1 1022.85 1068.28 21.45 o 8 1 1 109.00 99.87 9.18 o 9 1 1 134.15 141.80 4.34 o 10 1 1 0.19 -0.90 1.44 o 11 1 1 8.49 0.93 2.39 o 12 1 1 35.26 28.23 3.02 o -12 2 1 19.16 24.77 1.92 o -11 2 1 35.94 30.57 2.20 o -10 2 1 494.62 524.17 11.28 o -9 2 1 134.46 132.89 5.61 o -8 2 1 677.43 701.41 14.19 o -7 2 1 5.82 7.99 1.09 o -6 2 1 568.82 589.57 10.43 o -5 2 1 214.92 184.90 3.42 o -4 2 1 929.48 973.11 21.22 o -3 2 1 201.36 186.05 3.16 o -2 2 1 1082.00 977.30 16.75 o -1 2 1 87.98 100.82 1.79 o 0 2 1 330.68 257.73 3.59 o 2 2 1 1040.24 988.84 16.31 o 4 2 1 205.73 152.37 4.00 o 6 2 1 28.11 17.70 1.09 o 7 2 1 100.59 106.23 2.94 o 8 2 1 229.87 217.89 5.38 o 9 2 1 8.31 8.32 1.82 o 10 2 1 99.18 94.07 3.49 o 11 2 1 1.10 0.81 1.58 o 12 2 1 2.23 1.98 2.20 o -12 3 1 6.02 3.90 2.03 o -11 3 1 36.82 32.10 1.79 o -10 3 1 130.01 121.67 3.12 o -9 3 1 145.35 160.69 3.68 o -8 3 1 31.06 31.61 1.34 o -7 3 1 42.37 44.99 1.42 o -6 3 1 180.22 186.98 3.56 o -5 3 1 455.18 476.66 8.83 o -4 3 1 327.49 361.78 6.44 o -3 3 1 91.62 98.49 2.60 o -2 3 1 0.95 1.25 0.38 o -1 3 1 885.27 840.88 12.80 o 0 3 1 415.61 386.97 5.57 o 1 3 1 119.39 120.42 1.85 o 2 3 1 1161.43 1220.18 17.43 o 3 3 1 2889.13 3058.34 89.06 o 4 3 1 307.90 274.42 4.88 o 5 3 1 2091.48 2116.57 33.35 o 6 3 1 108.76 95.75 4.15 o 7 3 1 276.57 290.65 5.51 o 8 3 1 78.35 78.70 2.59 o 9 3 1 8.97 7.60 0.92 o 10 3 1 3.78 5.78 1.15 o 11 3 1 14.93 12.90 2.30 o -12 4 1 13.30 10.90 2.52 o -11 4 1 190.00 185.35 6.44 o -10 4 1 92.63 85.01 3.68 o -9 4 1 127.30 124.07 3.04 o -8 4 1 256.86 241.06 4.95 o -7 4 1 1453.83 1526.97 30.13 o -6 4 1 250.42 252.57 5.24 o -5 4 1 134.74 121.13 2.27 o -4 4 1 52.90 58.88 1.63 o -3 4 1 808.08 748.28 10.55 o -2 4 1 738.25 699.37 9.99 o -1 4 1 623.50 677.11 9.08 o 0 4 1 3.25 3.07 0.39 o 1 4 1 280.60 260.90 3.93 o 2 4 1 339.76 302.91 4.06 o 3 4 1 2361.06 2515.28 53.99 o 4 4 1 67.86 86.47 2.66 o 5 4 1 1644.69 1683.19 30.08 o 6 4 1 1.53 -0.68 0.68 o 7 4 1 1.02 2.24 0.73 o 8 4 1 133.99 150.16 3.14 o 9 4 1 27.60 24.59 1.22 o 10 4 1 22.30 16.33 1.59 o 11 4 1 4.96 1.42 1.54 o -11 5 1 4.61 3.48 1.54 o -10 5 1 12.41 8.16 2.01 o -9 5 1 77.15 74.42 2.11 o -8 5 1 28.11 23.57 1.52 o -7 5 1 254.65 257.66 5.15 o -6 5 1 6.62 6.40 0.84 o -5 5 1 0.90 0.66 0.72 o -4 5 1 0.07 0.99 0.47 o -3 5 1 376.95 351.87 4.91 o -2 5 1 0.03 0.42 0.46 o -1 5 1 49.67 56.97 2.62 o 0 5 1 1409.47 1412.58 18.56 o 1 5 1 26.38 22.77 0.79 o 2 5 1 0.33 0.15 0.40 o 3 5 1 149.61 145.44 2.62 o 4 5 1 5.82 5.45 1.07 o 5 5 1 235.97 230.32 6.77 o 6 5 1 50.48 54.41 1.75 o 7 5 1 112.78 106.68 2.49 o 8 5 1 31.63 24.91 2.33 o 9 5 1 95.53 99.91 3.88 o 10 5 1 103.88 106.21 5.53 o -10 6 1 71.30 67.25 3.44 o -9 6 1 165.60 174.05 4.94 o -8 6 1 253.64 277.61 8.06 o -7 6 1 165.05 164.98 3.85 o -6 6 1 27.65 25.30 1.45 o -5 6 1 489.01 490.06 7.78 o -4 6 1 122.43 125.10 2.20 o -3 6 1 264.41 270.47 4.23 o -2 6 1 489.87 504.70 10.57 o -1 6 1 226.32 249.08 3.75 o 0 6 1 46.00 58.38 1.74 o 1 6 1 837.73 855.30 10.88 o 2 6 1 120.38 127.49 2.05 o 3 6 1 58.94 56.89 1.41 o 4 6 1 33.44 31.00 1.14 o 5 6 1 873.94 928.61 16.56 o 6 6 1 360.83 379.51 7.74 o 7 6 1 11.75 11.69 1.91 o 8 6 1 20.13 22.34 2.30 o 9 6 1 0.46 0.09 1.48 o 10 6 1 64.20 73.96 7.33 o -9 7 1 9.47 8.27 2.99 o -8 7 1 47.13 44.83 5.98 o -7 7 1 50.99 50.75 4.33 o -6 7 1 37.08 32.56 2.00 o -5 7 1 0.17 0.31 0.74 o -4 7 1 0.70 -0.67 0.75 o -3 7 1 80.17 77.23 1.70 o -2 7 1 74.78 72.26 1.55 o -1 7 1 11.32 12.83 1.14 o 0 7 1 1.20 2.96 0.64 o 1 7 1 17.70 13.94 1.04 o 2 7 1 372.74 396.11 5.92 o 3 7 1 1023.29 1027.41 16.15 o 4 7 1 3.39 2.05 1.45 o 5 7 1 52.37 41.70 1.47 o 6 7 1 196.58 198.57 4.73 o 7 7 1 183.14 175.36 5.38 o 8 7 1 78.41 73.44 6.74 o 9 7 1 4.76 4.81 1.67 o -8 8 1 233.58 258.83 15.31 o -7 8 1 22.79 24.40 2.14 o -6 8 1 54.05 58.79 2.80 o -5 8 1 37.34 34.55 2.03 o -4 8 1 408.53 406.28 6.71 o -3 8 1 182.00 190.31 3.57 o -2 8 1 519.47 526.48 8.45 o -1 8 1 192.52 195.84 3.27 o 0 8 1 604.62 600.16 8.81 o 1 8 1 3.11 4.41 0.81 o 2 8 1 252.39 273.85 4.40 o 3 8 1 701.82 717.03 12.18 o 4 8 1 28.88 30.03 1.47 o 5 8 1 47.37 41.19 2.09 o 6 8 1 152.00 157.00 8.26 o 7 8 1 32.53 30.79 3.24 o 8 8 1 39.57 40.09 3.90 o -7 9 1 23.00 20.53 2.57 o -6 9 1 0.62 0.14 1.27 o -5 9 1 66.58 61.58 2.33 o -4 9 1 72.59 63.08 2.09 o -3 9 1 137.25 134.85 3.08 o -2 9 1 100.35 99.30 3.41 o -1 9 1 3.06 5.09 1.17 o 0 9 1 168.94 166.86 3.41 o 1 9 1 30.46 30.08 1.32 o 2 9 1 174.80 182.46 3.84 o 3 9 1 112.34 103.01 4.05 o 4 9 1 154.63 153.31 6.73 o 5 9 1 2.60 1.26 1.57 o 6 9 1 91.78 82.01 5.43 o -4 10 1 52.16 48.15 2.51 o -3 10 1 202.54 221.20 5.56 o -2 10 1 317.84 328.29 7.20 o -1 10 1 103.03 102.08 3.15 o 0 10 1 385.99 380.53 8.24 o 1 10 1 30.18 32.79 1.87 o 2 10 1 24.94 22.76 1.83 o 3 10 1 9.14 8.69 3.20 o 4 10 1 62.94 64.07 3.66 o -12 0 2 64.53 59.50 5.72 o -10 0 2 282.48 310.05 10.65 o -8 0 2 104.28 99.19 4.42 o -6 0 2 375.29 382.88 10.11 o -4 0 2 427.38 409.83 10.24 o -2 0 2 1136.34 1146.63 67.24 o 2 0 2 3200.66 3134.04 129.99 o 4 0 2 43.75 40.97 2.04 o 6 0 2 2581.29 2654.48 102.43 o 8 0 2 307.20 314.98 16.51 o 10 0 2 275.37 271.04 14.14 o -13 1 2 6.18 2.20 2.80 o -12 1 2 69.05 58.59 2.92 o -11 1 2 8.26 7.82 1.53 o -10 1 2 25.37 19.76 1.45 o -9 1 2 77.24 77.86 3.14 o -8 1 2 55.46 57.87 1.74 o -7 1 2 150.05 140.33 3.01 o -6 1 2 62.80 61.53 1.48 o -5 1 2 320.58 329.25 6.19 o -4 1 2 28.21 45.58 7.72 o -3 1 2 20.12 28.63 0.76 o -1 1 2 1196.39 1133.54 23.65 o 0 1 2 857.54 833.70 18.44 o 1 1 2 95.70 95.89 3.18 o 2 1 2 251.14 231.49 4.64 o 4 1 2 609.30 564.04 13.39 o 5 1 2 18.76 14.97 1.68 o 6 1 2 1886.02 2033.47 41.90 o 7 1 2 525.44 541.15 11.64 o 9 1 2 4.52 1.17 5.21 o 10 1 2 101.06 84.23 3.91 o 11 1 2 6.95 1.69 1.76 o -13 2 2 41.11 46.80 9.29 o -12 2 2 80.65 74.09 2.72 o -11 2 2 21.42 24.19 1.74 o -10 2 2 603.45 624.79 13.31 o -9 2 2 201.21 206.36 5.05 o -8 2 2 135.18 137.18 2.89 o -7 2 2 22.53 26.72 0.89 o -6 2 2 1664.35 1645.70 30.00 o -5 2 2 895.83 875.64 14.77 o -4 2 2 1.63 0.05 0.68 o -3 2 2 133.16 164.42 3.15 o -2 2 2 336.27 306.22 5.10 o -1 2 2 3.78 7.36 0.46 o 0 2 2 469.99 486.07 7.53 o 1 2 2 91.12 91.99 1.63 o 2 2 2 323.67 327.85 6.14 o 3 2 2 632.03 612.50 11.69 o 4 2 2 277.69 316.57 6.08 o 5 2 2 653.45 684.24 14.92 o 6 2 2 513.35 498.61 10.39 o 7 2 2 108.33 105.83 3.33 o 8 2 2 188.31 175.40 4.67 o 9 2 2 19.07 21.53 1.80 o 10 2 2 13.13 8.61 2.67 o 11 2 2 67.98 67.33 6.48 o -12 3 2 8.74 5.22 1.41 o -11 3 2 1.15 2.95 1.02 o -10 3 2 4.63 1.94 0.88 o -9 3 2 16.64 18.06 1.05 o -8 3 2 219.36 211.46 4.17 o -7 3 2 38.82 36.42 1.32 o -6 3 2 31.15 32.93 1.11 o -5 3 2 716.99 683.74 11.23 o -3 3 2 99.08 81.62 1.85 o -2 3 2 130.46 132.48 2.06 o -1 3 2 607.00 547.17 7.67 o 0 3 2 424.96 422.01 6.11 o 1 3 2 605.81 620.38 9.29 o 2 3 2 2593.99 2929.84 72.29 o 4 3 2 81.20 85.80 1.98 o 5 3 2 440.31 432.44 7.68 o 6 3 2 7.29 10.48 1.02 o 7 3 2 240.30 248.92 5.02 o 8 3 2 304.13 284.38 5.75 o 9 3 2 94.67 92.32 3.15 o 10 3 2 24.99 25.75 3.27 o 11 3 2 49.62 46.84 2.62 o -12 4 2 5.10 3.57 2.22 o -11 4 2 109.35 101.58 5.02 o -10 4 2 79.53 74.59 2.81 o -9 4 2 157.77 149.90 3.35 o -8 4 2 240.80 246.23 5.13 o -7 4 2 1352.70 1424.20 25.78 o -6 4 2 157.80 154.78 3.50 o -5 4 2 2289.42 2294.52 42.94 o -4 4 2 1.84 0.81 0.50 o -3 4 2 49.93 45.79 1.33 o -2 4 2 5.99 8.16 2.59 o -1 4 2 251.50 276.10 4.13 o 0 4 2 372.99 355.24 4.93 o 1 4 2 51.71 49.34 0.98 o 2 4 2 49.04 51.07 1.02 o 3 4 2 118.79 124.24 3.06 o 4 4 2 48.49 37.57 1.29 o 5 4 2 58.90 56.36 1.95 o 6 4 2 13.37 8.60 1.43 o 7 4 2 2.21 0.53 1.10 o 8 4 2 2.64 4.49 0.89 o 9 4 2 3.53 3.32 0.98 o 10 4 2 0.45 -0.23 1.36 o 11 4 2 1.63 0.10 1.76 o -11 5 2 5.25 9.41 2.11 o -10 5 2 15.97 15.67 1.35 o -9 5 2 0.97 1.34 1.00 o -8 5 2 15.52 12.45 0.92 o -7 5 2 126.73 132.78 2.93 o -6 5 2 78.14 82.86 2.59 o -5 5 2 364.86 366.44 5.57 o -4 5 2 139.10 137.32 3.63 o -3 5 2 493.47 498.60 7.05 o -2 5 2 345.08 366.36 5.31 o -1 5 2 302.33 289.49 4.38 o 0 5 2 1077.50 1144.88 15.28 o 1 5 2 35.85 32.89 1.16 o 2 5 2 121.74 139.31 2.27 o 3 5 2 790.28 833.39 12.95 o 4 5 2 127.20 132.34 2.91 o 5 5 2 9.21 7.99 1.17 o 6 5 2 12.97 15.74 1.23 o 7 5 2 273.04 282.58 5.64 o 8 5 2 2.70 -0.35 0.80 o 9 5 2 251.89 251.23 7.76 o 10 5 2 45.26 45.92 3.66 o -11 6 2 0.04 -2.76 3.11 o -10 6 2 84.33 81.05 3.43 o -9 6 2 14.65 16.10 1.38 o -8 6 2 231.04 245.18 5.30 o -7 6 2 711.10 734.21 13.45 o -6 6 2 27.10 24.61 0.94 o -5 6 2 922.55 953.90 14.41 o -4 6 2 266.09 274.91 4.42 o -3 6 2 890.66 910.17 15.28 o -2 6 2 290.29 275.67 5.25 o -1 6 2 117.89 133.68 2.79 o 0 6 2 10.22 12.09 0.64 o 1 6 2 63.90 78.52 1.49 o 2 6 2 166.42 158.08 2.57 o 3 6 2 205.34 207.58 3.75 o 4 6 2 452.27 429.75 7.23 o 5 6 2 62.81 70.06 2.62 o 6 6 2 192.65 216.44 4.92 o 7 6 2 10.64 8.13 1.32 o 8 6 2 0.09 0.02 1.09 o 9 6 2 59.88 51.50 2.83 o -10 7 2 29.27 29.07 3.36 o -9 7 2 31.96 28.26 2.34 o -8 7 2 237.90 228.95 6.72 o -7 7 2 28.69 30.15 1.41 o -6 7 2 47.47 47.51 1.40 o -5 7 2 23.68 22.30 1.52 o -4 7 2 40.55 39.53 1.53 o -3 7 2 0.01 0.73 0.75 o -2 7 2 294.95 281.03 5.21 o -1 7 2 65.10 59.81 1.40 o 0 7 2 245.26 260.03 4.07 o 1 7 2 45.16 40.01 1.51 o 2 7 2 223.02 232.44 3.72 o 3 7 2 702.67 715.29 12.21 o 4 7 2 230.31 240.48 4.60 o 5 7 2 9.59 9.01 1.20 o 6 7 2 12.93 9.83 1.45 o 7 7 2 164.27 164.06 5.94 o 8 7 2 247.97 294.54 10.69 o -8 8 2 157.76 143.50 8.35 o -7 8 2 21.44 19.88 1.63 o -6 8 2 63.98 64.17 1.91 o -5 8 2 254.50 262.14 7.69 o -4 8 2 334.85 355.33 6.00 o -3 8 2 91.63 87.31 1.94 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