data_2105949 _cell_angle_alpha 91.809 _cell_angle_beta 109.675 _cell_angle_gamma 104.825 _cell_length_a 12.1351 _cell_length_b 13.2343 _cell_length_c 13.8728 _exptl_crystal_F_000 860.00 _reflns_d_resolution_high 0.7934 _[local]_cod_data_source_file bm50634sup6.hkl _[local]_cod_data_source_block 4 _shelx_title ' c13_30 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.11 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 839.34 598.33 13.24 o 3 0 0 2524.52 2381.64 44.46 o 4 0 0 406.06 515.42 24.64 o 5 0 0 5.40 100.56 13.79 o 6 0 0 403.48 453.38 26.12 o 7 0 0 2696.44 2369.35 60.76 o 8 0 0 24.35 62.54 13.75 o 9 0 0 1404.77 1367.46 68.00 o 10 0 0 169.53 248.39 34.96 o 11 0 0 531.58 443.47 67.35 o 12 0 0 4.55 -15.51 28.56 o 13 0 0 859.43 780.89 103.67 o -14 1 0 368.36 476.17 131.06 o -13 1 0 6.78 -17.65 30.43 o -12 1 0 446.95 485.52 71.29 o -11 1 0 2.94 6.53 27.11 o -10 1 0 1111.93 1165.82 80.24 o -9 1 0 571.85 689.44 59.18 o -8 1 0 2440.59 2680.34 75.80 o -7 1 0 1244.26 1041.34 41.45 o -6 1 0 6657.68 6557.41 135.02 o -5 1 0 699.44 625.68 26.80 o -4 1 0 2286.51 2677.97 51.63 o -3 1 0 248.93 276.56 15.10 o -2 1 0 6874.83 6592.95 74.87 o -1 1 0 36163.52 38035.98 1036.85 o 1 1 0 20731.43 23820.06 213.49 o 2 1 0 19.02 6.59 6.61 o 3 1 0 1081.93 820.31 27.62 o 4 1 0 725.90 638.77 32.18 o 5 1 0 8955.32 8006.60 124.44 o 6 1 0 141.23 156.05 18.11 o 7 1 0 712.14 833.55 39.82 o 8 1 0 244.40 188.41 22.12 o 9 1 0 69.70 50.36 23.46 o 10 1 0 926.00 911.09 86.09 o 11 1 0 0.36 -24.87 24.87 o 12 1 0 3207.22 3191.27 227.58 o 13 1 0 1.51 -28.30 32.90 o -14 2 0 704.38 618.34 116.66 o -13 2 0 341.33 389.91 67.61 o -12 2 0 764.64 748.16 139.79 o -11 2 0 613.77 474.63 63.48 o -10 2 0 188.86 205.53 35.88 o -9 2 0 577.36 541.85 52.25 o -8 2 0 22.81 36.88 13.79 o -7 2 0 6399.96 6368.03 112.22 o -6 2 0 39.06 56.14 17.85 o -5 2 0 19895.69 20740.34 306.56 o -4 2 0 7288.43 6657.05 160.70 o -3 2 0 4973.99 4430.02 113.32 o -2 2 0 1917.26 2634.97 73.79 o -1 2 0 3690.57 4467.90 51.96 o 0 2 0 243.15 181.96 14.99 o 1 2 0 5114.45 5816.15 77.82 o 2 2 0 9982.68 8863.80 117.37 o 3 2 0 3093.93 2719.44 62.49 o 4 2 0 474.11 583.59 31.43 o 5 2 0 615.56 601.93 34.74 o 6 2 0 11174.48 11229.00 170.78 o 7 2 0 485.21 554.60 36.94 o 8 2 0 879.54 957.27 58.66 o 9 2 0 44.93 59.72 16.34 o 10 2 0 338.67 458.83 61.59 o 11 2 0 909.36 745.52 80.96 o 12 2 0 3.66 32.86 52.68 o 13 2 0 516.21 393.05 127.09 o -14 3 0 98.65 -6.62 51.07 o -13 3 0 3021.33 3026.41 151.46 o -12 3 0 14.90 -7.96 24.04 o -11 3 0 92.83 23.04 23.11 o -10 3 0 127.06 256.91 40.06 o -9 3 0 50.53 38.15 21.75 o -8 3 0 1337.51 1339.76 47.44 o -7 3 0 381.36 434.49 24.82 o -6 3 0 7854.38 8052.61 228.70 o -5 3 0 3882.37 4151.20 75.46 o -4 3 0 471.91 913.54 39.85 o -3 3 0 634.60 1673.14 57.53 o -2 3 0 65.23 32.64 8.92 o -1 3 0 2768.59 1982.70 28.76 o 0 3 0 24368.43 25113.97 260.66 o 1 3 0 296.79 459.46 17.69 o 2 3 0 5768.93 5865.05 100.32 o 3 3 0 465.22 845.23 51.16 o 4 3 0 425.53 499.79 36.71 o 5 3 0 5121.25 5002.03 95.07 o 6 3 0 305.62 315.53 28.20 o 7 3 0 5908.90 5678.88 132.19 o 8 3 0 10.14 24.38 13.69 o 9 3 0 961.34 972.74 49.27 o 10 3 0 89.49 96.28 33.93 o 11 3 0 437.01 494.53 121.41 o 12 3 0 431.96 512.24 119.46 o -14 4 0 1279.69 1335.70 124.18 o -13 4 0 60.44 75.77 38.39 o -12 4 0 2201.56 2243.76 133.33 o -11 4 0 806.10 996.86 101.29 o -10 4 0 576.07 581.10 58.18 o -9 4 0 72.00 121.04 30.06 o -8 4 0 1997.56 1950.48 87.24 o -7 4 0 2031.03 1987.74 56.63 o -6 4 0 14.80 23.68 8.05 o -5 4 0 5880.20 5465.85 99.05 o -4 4 0 4416.10 3546.48 66.26 o -3 4 0 6934.38 6570.21 97.21 o -2 4 0 936.58 733.65 22.49 o -1 4 0 26242.53 26105.86 264.10 o 0 4 0 167.18 274.10 14.81 o 1 4 0 5615.95 5508.65 94.63 o 2 4 0 3411.54 3746.49 66.92 o 3 4 0 2910.81 3092.23 72.59 o 4 4 0 1111.88 1111.92 39.74 o 5 4 0 18.89 -6.70 10.86 o 6 4 0 5845.78 5897.71 114.12 o 7 4 0 133.31 149.37 22.02 o 8 4 0 1636.52 1611.85 60.40 o 9 4 0 814.41 834.98 59.30 o 10 4 0 1739.83 1793.53 125.69 o 11 4 0 57.42 61.13 29.17 o 12 4 0 452.83 549.37 78.72 o -14 5 0 17.99 -1.40 35.86 o -13 5 0 1256.88 1254.31 113.18 o -12 5 0 1.81 -7.54 21.07 o -11 5 0 1020.71 1107.28 81.55 o -10 5 0 838.07 891.40 71.29 o -9 5 0 1754.67 1829.32 90.15 o -8 5 0 1175.51 1368.58 51.91 o -7 5 0 4282.13 3888.03 107.99 o -6 5 0 482.22 567.83 31.68 o -5 5 0 676.61 680.76 53.46 o -4 5 0 6.02 8.57 7.72 o -3 5 0 555.30 497.97 23.93 o -2 5 0 5665.65 5697.60 85.31 o -1 5 0 42.74 119.62 7.69 o 0 5 0 23319.12 25229.10 261.10 o 1 5 0 265.62 324.07 25.13 o 2 5 0 2593.29 2451.54 53.68 o 3 5 0 375.82 384.45 29.08 o 4 5 0 4172.95 4056.61 83.08 o 5 5 0 177.82 163.10 30.38 o 6 5 0 665.45 778.72 46.90 o 7 5 0 1567.04 1646.37 60.63 o 8 5 0 734.64 814.35 59.15 o 9 5 0 1330.29 1396.14 74.13 o 10 5 0 43.61 44.61 26.19 o 11 5 0 978.03 856.83 87.88 o -14 6 0 63.08 71.00 45.78 o -13 6 0 388.85 463.13 66.64 o -12 6 0 1030.59 971.40 79.22 o -11 6 0 0.52 35.08 24.49 o -10 6 0 89.24 127.35 38.16 o -9 6 0 45.53 87.51 27.63 o -8 6 0 3233.49 3319.61 78.65 o -7 6 0 749.76 734.51 35.39 o -6 6 0 4365.20 4126.37 85.06 o -5 6 0 488.39 451.22 29.92 o -4 6 0 1360.18 1136.54 37.45 o -3 6 0 311.56 405.14 23.55 o -2 6 0 43.66 34.04 7.25 o -1 6 0 9652.19 9607.07 158.08 o 0 6 0 765.40 788.83 18.72 o 1 6 0 4568.09 4966.98 82.41 o 2 6 0 1578.51 1477.91 41.90 o 3 6 0 6947.59 6772.08 114.85 o 4 6 0 911.25 1067.99 43.81 o 5 6 0 9634.31 9686.99 184.56 o 6 6 0 696.94 778.27 47.21 o 7 6 0 111.32 128.31 20.98 o 8 6 0 577.22 584.75 52.10 o 9 6 0 106.88 115.35 37.18 o 10 6 0 207.16 241.97 39.96 o 11 6 0 770.44 791.05 158.08 o -14 7 0 564.13 449.86 70.28 o -13 7 0 202.17 218.89 44.40 o -12 7 0 252.57 257.12 44.41 o -11 7 0 1477.31 1430.92 93.92 o -10 7 0 307.05 284.60 55.26 o -9 7 0 314.19 262.95 71.02 o -8 7 0 8.19 21.49 10.66 o -7 7 0 3921.35 4016.69 88.96 o -6 7 0 417.83 550.76 39.45 o -5 7 0 4494.93 4591.89 90.09 o -4 7 0 1345.98 1290.23 41.41 o -3 7 0 5736.81 5321.46 90.08 o -2 7 0 2516.99 2387.12 39.58 o -1 7 0 3022.95 2867.41 71.76 o 0 7 0 69.07 166.76 11.88 o 1 7 0 240.55 294.67 20.47 o 2 7 0 6.58 16.76 8.83 o 3 7 0 75.91 77.15 14.10 o 4 7 0 5348.15 5146.14 102.62 o 5 7 0 44.69 56.83 16.21 o 6 7 0 853.03 886.71 81.92 o 7 7 0 21.56 73.98 17.14 o 8 7 0 399.79 473.30 48.93 o 9 7 0 332.23 293.32 72.42 o 10 7 0 992.52 1090.48 113.99 o -14 8 0 89.41 99.16 44.24 o -13 8 0 592.24 700.00 81.79 o -12 8 0 0.02 -10.07 48.54 o -11 8 0 1573.13 1507.93 97.40 o -10 8 0 857.93 811.92 69.25 o -9 8 0 131.54 63.19 36.19 o -8 8 0 667.99 662.08 36.53 o -7 8 0 23.95 14.71 17.56 o -6 8 0 5273.68 5272.92 104.70 o -5 8 0 4305.94 4742.25 94.16 o -4 8 0 3058.24 3197.01 69.15 o -3 8 0 4.19 -5.07 8.59 o -2 8 0 6428.11 5887.92 140.25 o -1 8 0 16.56 20.70 11.23 o 0 8 0 2823.66 2922.05 77.89 o 1 8 0 761.79 784.42 29.39 o 2 8 0 17.85 11.31 9.51 o 3 8 0 2010.23 2014.14 56.33 o 4 8 0 67.08 95.85 16.24 o 5 8 0 3530.39 3695.11 102.23 o 6 8 0 609.80 570.87 42.80 o 7 8 0 1279.26 1365.72 63.08 o 8 8 0 29.28 31.80 29.85 o 9 8 0 875.69 915.09 82.90 o 10 8 0 191.92 228.93 52.66 o -13 9 0 23.31 118.22 31.48 o -12 9 0 1570.12 1607.41 103.76 o -11 9 0 1332.75 1293.92 90.08 o -10 9 0 838.14 871.33 71.15 o -9 9 0 397.70 538.80 53.77 o -8 9 0 1579.90 1600.01 56.42 o -7 9 0 208.07 253.11 26.04 o -6 9 0 154.36 177.94 20.81 o -5 9 0 3465.70 3350.58 120.18 o -4 9 0 3.64 -7.58 7.58 o -3 9 0 1601.87 1581.75 49.61 o -2 9 0 68.24 55.39 16.23 o -1 9 0 3302.45 3002.08 97.41 o 0 9 0 506.09 665.19 46.13 o 1 9 0 861.42 896.11 65.71 o 2 9 0 184.15 236.66 28.78 o 3 9 0 710.30 841.67 55.28 o 4 9 0 2906.86 2809.18 89.12 o 5 9 0 1799.92 1801.72 84.38 o 6 9 0 1513.12 1369.30 73.98 o 7 9 0 616.40 549.86 61.38 o 8 9 0 92.25 144.33 35.88 o 9 9 0 2.40 -19.76 26.46 o -13 10 0 162.65 127.09 33.36 o -12 10 0 488.60 449.72 51.62 o -11 10 0 787.75 759.40 72.93 o -10 10 0 1.07 -14.32 23.21 o -9 10 0 3949.75 4090.72 127.72 o -8 10 0 22.30 42.01 13.89 o -7 10 0 741.36 765.86 45.01 o -6 10 0 2.88 5.29 11.15 o -5 10 0 1127.60 1156.18 56.36 o -4 10 0 778.65 763.95 52.53 o -3 10 0 727.67 756.61 51.32 o -2 10 0 4542.31 4522.70 110.88 o -1 10 0 2.96 8.37 12.83 o 0 10 0 1598.62 1737.92 64.62 o 1 10 0 267.51 296.31 33.15 o 2 10 0 572.61 631.58 49.45 o 3 10 0 445.43 479.15 43.15 o 4 10 0 2472.05 2320.65 82.95 o 5 10 0 305.35 411.24 48.01 o 6 10 0 2.34 -12.32 21.13 o 7 10 0 205.26 218.18 47.00 o 8 10 0 9.68 -26.70 26.70 o -13 11 0 12.22 -9.47 74.90 o -12 11 0 288.09 332.77 62.70 o -11 11 0 76.14 39.42 38.67 o -10 11 0 2013.72 2032.06 124.25 o -9 11 0 237.68 242.63 55.26 o -8 11 0 2233.57 2297.50 85.95 o -7 11 0 32.25 60.07 18.46 o -6 11 0 820.67 747.20 62.71 o -5 11 0 119.80 91.99 21.46 o -4 11 0 2107.70 1989.99 74.48 o -3 11 0 1676.76 1690.29 68.51 o -2 11 0 1435.73 1457.55 74.11 o -1 11 0 162.63 194.39 27.84 o 0 11 0 0.39 30.36 18.94 o 1 11 0 94.48 100.30 21.06 o 2 11 0 100.25 122.50 28.95 o 3 11 0 1908.82 2066.32 79.49 o 4 11 0 2.14 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20.31 o 0 13 0 845.13 974.92 65.63 o 1 13 0 160.93 81.51 21.22 o 2 13 0 289.66 295.80 34.82 o 3 13 0 954.91 992.32 68.70 o 4 13 0 42.68 -3.56 16.57 o 5 13 0 313.45 408.55 114.08 o -10 14 0 837.96 874.17 163.53 o -9 14 0 190.28 141.68 47.62 o -8 14 0 302.56 354.13 55.83 o -7 14 0 80.34 71.80 27.41 o -6 14 0 180.83 205.44 29.77 o -5 14 0 311.69 366.92 38.19 o -4 14 0 7.00 -1.01 15.45 o -3 14 0 3941.32 3878.35 117.33 o -2 14 0 182.25 179.40 27.98 o -1 14 0 1033.30 1095.71 71.71 o 0 14 0 133.57 156.64 24.88 o 1 14 0 868.61 847.29 64.02 o 2 14 0 333.69 311.31 75.56 o 3 14 0 61.26 18.69 21.14 o 4 14 0 266.48 267.02 38.27 o -9 15 0 1026.67 1054.59 198.95 o -8 15 0 16.79 -9.79 36.56 o -7 15 0 601.26 553.80 49.32 o -6 15 0 108.64 88.54 29.28 o -5 15 0 1590.05 1674.53 143.11 o -4 15 0 1186.33 1092.30 71.37 o -3 15 0 236.18 349.21 82.16 o -2 15 0 617.03 610.12 55.68 o -1 15 0 59.79 38.59 38.75 o 0 15 0 342.18 463.90 45.28 o 1 15 0 111.35 143.00 25.92 o 2 15 0 248.39 200.17 27.10 o -7 16 0 44.59 54.97 36.83 o -6 16 0 893.64 867.73 65.16 o -5 16 0 66.78 55.83 26.26 o -4 16 0 538.64 466.77 48.81 o -3 16 0 99.94 122.33 36.06 o -2 16 0 109.38 104.46 24.55 o -1 16 0 160.55 216.02 32.68 o 0 -16 1 101.50 152.53 40.28 o 1 -16 1 152.14 45.81 32.36 o 2 -16 1 612.32 643.57 81.37 o 3 -16 1 0.48 6.92 18.29 o 4 -16 1 437.52 440.94 71.51 o 5 -16 1 197.52 245.56 32.58 o 6 -16 1 57.41 56.90 27.97 o 7 -16 1 30.71 -8.35 35.30 o -2 -15 1 218.05 179.23 41.29 o -1 -15 1 18.46 -11.25 28.37 o 0 -15 1 85.63 118.22 23.29 o 1 -15 1 776.06 735.94 107.43 o 2 -15 1 190.16 204.70 32.89 o 3 -15 1 951.20 917.03 65.16 o 4 -15 1 5.52 21.89 17.65 o 5 -15 1 1121.07 1162.60 86.08 o 6 -15 1 79.29 67.47 34.34 o 7 -15 1 357.12 328.40 37.92 o 8 -15 1 215.88 151.46 33.85 o 9 -15 1 630.04 777.29 81.92 o -4 -14 1 290.56 305.19 50.54 o -3 -14 1 244.57 247.95 45.64 o -2 -14 1 8.68 -4.22 16.86 o -1 -14 1 735.74 882.48 64.38 o 0 -14 1 184.95 184.43 41.72 o 1 -14 1 319.43 285.50 35.04 o 2 -14 1 1419.20 1548.62 118.97 o 3 -14 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553.47 46.38 o 3 -12 1 666.30 786.67 62.56 o 4 -12 1 349.97 404.60 40.57 o 5 -12 1 2.90 -13.90 13.90 o 6 -12 1 243.08 284.54 35.57 o 7 -12 1 298.61 318.53 35.74 o 8 -12 1 865.23 764.60 76.60 o 9 -12 1 139.67 167.00 46.63 o 10 -12 1 221.59 274.30 56.56 o 11 -12 1 11.27 -22.73 36.32 o 12 -12 1 515.93 428.19 69.18 o -7 -11 1 739.03 751.93 79.79 o -6 -11 1 3.65 18.42 20.51 o -5 -11 1 723.57 718.84 57.59 o -4 -11 1 839.82 821.07 59.14 o -3 -11 1 479.33 499.22 44.91 o -2 -11 1 102.29 100.05 21.51 o -1 -11 1 54.69 32.26 15.30 o 0 -11 1 1870.96 1930.72 70.70 o 1 -11 1 623.36 701.52 50.52 o 2 -11 1 2237.76 2076.52 72.41 o 3 -11 1 76.09 120.90 23.20 o 4 -11 1 467.35 461.08 78.36 o 5 -11 1 35.80 54.74 17.65 o 6 -11 1 200.61 235.86 31.27 o 7 -11 1 76.12 58.90 20.56 o 8 -11 1 741.50 729.03 54.50 o 9 -11 1 440.57 443.06 65.07 o 10 -11 1 31.59 2.63 33.36 o 11 -11 1 1366.93 987.93 107.42 o 12 -11 1 43.82 -12.97 43.84 o -8 -10 1 208.62 241.49 48.02 o -7 -10 1 192.56 212.37 33.82 o -6 -10 1 2170.43 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