#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:45:48 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181878 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/59/2105983.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2105983 _cell_angle_alpha 90.000 _cell_angle_beta 103.395 _cell_angle_gamma 90.000 _cell_length_a 4.7294 _cell_length_b 19.1014 _cell_length_c 9.0705 _exptl_crystal_F_000 390.00 _reflns_d_resolution_high 0.7959 _cod_data_source_file gp50788sup9.hkl _cod_data_source_block 8 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k12_39 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 132.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 25.22 7.53 2.84 o 2 0 0 2551.77 2294.10 80.99 o 3 0 0 6318.70 6826.80 205.03 o 4 0 0 302.01 290.67 26.12 o 5 0 0 1.45 18.68 14.20 o 1 1 0 110.85 129.96 5.08 o 2 1 0 1966.00 1864.42 42.95 o 3 1 0 0.48 -0.41 3.33 o 4 1 0 110.66 118.78 11.68 o 5 1 0 484.71 493.00 42.73 o 1 2 0 5888.71 6280.26 161.31 o 2 2 0 1315.17 1278.67 32.70 o 3 2 0 358.05 384.97 16.12 o 4 2 0 2011.09 1827.35 58.17 o 5 2 0 241.57 196.00 22.36 o 1 3 0 4946.52 5313.56 109.36 o 2 3 0 2552.19 2522.54 60.64 o 3 3 0 356.35 362.21 14.58 o 4 3 0 13.46 6.15 6.07 o 5 3 0 548.05 574.22 34.40 o 0 4 0 31.51 47.64 3.72 o 1 4 0 1516.14 1476.34 35.61 o 2 4 0 147.40 174.70 8.76 o 3 4 0 4159.00 4115.39 98.22 o 4 4 0 40.08 24.49 7.81 o 5 4 0 862.02 840.50 43.30 o 1 5 0 3237.29 3575.96 81.00 o 2 5 0 912.68 929.18 30.58 o 3 5 0 58.43 67.88 7.23 o 4 5 0 671.17 672.91 33.10 o 5 5 0 44.07 46.00 14.47 o 0 6 0 3624.24 4265.74 125.22 o 1 6 0 4648.06 4894.47 101.75 o 2 6 0 4199.36 4155.33 104.72 o 3 6 0 299.70 305.16 18.65 o 4 6 0 1721.25 1664.61 60.35 o 5 6 0 197.49 234.13 21.70 o 1 7 0 529.58 468.85 14.43 o 2 7 0 709.04 666.79 25.88 o 3 7 0 182.09 163.06 13.66 o 4 7 0 379.23 405.93 25.05 o 5 7 0 204.25 193.80 19.56 o 0 8 0 335.18 370.26 16.08 o 1 8 0 312.97 299.19 10.52 o 2 8 0 371.65 347.36 14.90 o 3 8 0 301.33 263.77 22.19 o 4 8 0 11.55 16.82 7.95 o 5 8 0 253.07 241.94 26.76 o 1 9 0 1053.01 1001.24 25.08 o 2 9 0 499.65 499.17 22.41 o 3 9 0 657.89 667.43 30.47 o 4 9 0 6.70 8.65 6.76 o 5 9 0 336.52 374.47 28.14 o 0 10 0 880.82 838.54 30.78 o 1 10 0 3177.55 2971.10 65.14 o 2 10 0 703.74 686.12 24.13 o 3 10 0 253.77 230.34 16.63 o 4 10 0 437.79 408.24 25.44 o 5 10 0 320.95 344.33 25.41 o 1 11 0 643.81 591.11 18.12 o 2 11 0 402.30 385.51 20.53 o 3 11 0 0.14 -4.98 5.10 o 4 11 0 105.42 101.17 12.66 o 5 11 0 121.60 124.82 15.04 o 0 12 0 7026.70 7381.08 218.30 o 1 12 0 115.59 134.32 7.82 o 2 12 0 331.30 354.08 16.79 o 3 12 0 1663.82 1579.70 51.96 o 4 12 0 20.83 10.76 7.17 o 1 13 0 192.96 188.70 9.76 o 2 13 0 1210.39 1096.62 51.51 o 3 13 0 52.40 54.14 10.23 o 4 13 0 65.97 82.83 16.93 o 0 14 0 1498.41 1425.72 51.28 o 1 14 0 336.42 328.80 15.01 o 2 14 0 394.88 376.85 19.37 o 3 14 0 235.53 214.65 19.63 o 4 14 0 1418.95 1394.48 72.94 o 1 15 0 502.11 511.04 18.25 o 2 15 0 621.51 599.08 26.51 o 3 15 0 82.64 88.48 10.32 o 4 15 0 0.17 -6.66 6.66 o 0 16 0 3695.35 3782.69 119.76 o 1 16 0 267.40 258.17 14.18 o 2 16 0 139.79 143.25 11.87 o 3 16 0 2868.06 2744.02 79.33 o 4 16 0 114.16 106.03 13.75 o 1 17 0 97.05 98.63 8.61 o 2 17 0 71.87 56.94 8.19 o 3 17 0 45.78 51.23 9.22 o 4 17 0 2.33 -6.03 6.84 o 0 18 0 45.47 67.40 9.60 o 1 18 0 2292.76 2235.23 59.55 o 2 18 0 582.33 587.17 26.97 o 3 18 0 228.57 239.21 17.74 o 1 19 0 21.32 22.33 6.55 o 2 19 0 98.20 106.37 10.87 o 3 19 0 49.69 52.27 10.29 o 0 20 0 305.22 342.39 23.76 o 1 20 0 103.33 114.09 10.64 o 2 20 0 348.56 350.48 20.84 o 3 20 0 153.22 148.33 15.62 o 1 21 0 343.65 383.03 21.24 o 2 21 0 91.78 107.87 12.66 o 0 22 0 109.20 137.53 19.06 o 1 22 0 329.03 347.57 22.62 o 2 22 0 596.44 684.96 34.99 o 1 23 0 97.43 123.41 13.52 o -5 1 1 37.97 36.84 11.84 o -4 1 1 624.53 659.50 27.71 o -3 1 1 1519.99 1520.76 50.57 o -2 1 1 475.05 421.97 15.06 o -1 1 1 7.85 10.51 2.14 o 0 1 1 8413.54 9121.27 163.23 o 1 1 1 1138.21 1033.57 24.92 o 2 1 1 1460.64 1368.80 32.96 o 3 1 1 3847.33 3970.47 88.22 o 4 1 1 517.43 545.20 30.65 o 5 1 1 274.81 264.80 27.46 o -5 2 1 53.28 24.23 11.42 o -4 2 1 100.78 128.06 11.73 o -3 2 1 533.95 554.94 20.27 o -2 2 1 3023.15 3205.52 69.87 o -1 2 1 4.40 1.77 1.34 o 0 2 1 1835.49 1827.34 40.41 o 1 2 1 381.55 359.59 12.61 o 2 2 1 511.95 550.54 25.51 o 3 2 1 118.75 108.74 8.07 o 4 2 1 61.87 53.70 10.09 o 5 2 1 169.22 113.78 18.14 o -5 3 1 392.19 431.08 35.20 o -4 3 1 1302.87 1272.39 46.65 o -3 3 1 896.22 906.59 38.24 o -2 3 1 1212.45 1138.91 28.12 o -1 3 1 4745.02 4901.90 101.26 o 0 3 1 2631.58 2771.49 57.00 o 1 3 1 166.27 154.06 5.48 o 2 3 1 913.56 831.55 26.59 o 3 3 1 686.76 637.09 23.97 o 4 3 1 189.43 216.45 17.43 o 5 3 1 127.96 129.65 19.30 o -5 4 1 244.87 235.76 21.26 o -4 4 1 1.48 -3.40 5.48 o -3 4 1 89.48 99.99 7.26 o -2 4 1 3285.39 3577.51 83.75 o -1 4 1 4796.47 4646.23 96.52 o 0 4 1 0.45 -1.07 1.07 o 1 4 1 5268.56 5378.25 111.12 o 2 4 1 4.39 2.91 2.71 o 3 4 1 248.29 275.16 14.64 o 4 4 1 27.63 36.71 7.77 o 5 4 1 20.28 4.51 8.90 o -5 5 1 355.17 351.20 31.54 o -4 5 1 19.27 12.90 6.45 o -3 5 1 393.34 394.56 14.45 o -2 5 1 816.46 788.69 21.55 o -1 5 1 3930.17 3924.91 81.68 o 0 5 1 1624.66 1579.97 34.06 o 1 5 1 3052.24 3083.87 65.85 o 2 5 1 1238.26 1285.05 38.78 o 3 5 1 373.40 373.43 21.20 o 4 5 1 461.50 426.91 25.08 o 5 5 1 345.69 385.81 35.34 o -5 6 1 39.74 38.83 11.27 o -4 6 1 18.49 25.47 7.78 o -3 6 1 207.73 199.30 13.98 o -2 6 1 339.53 308.37 15.37 o -1 6 1 915.31 921.81 25.66 o 0 6 1 37.23 41.05 3.15 o 1 6 1 531.87 538.58 15.20 o 2 6 1 23.61 20.35 5.10 o 3 6 1 175.20 172.73 14.12 o 4 6 1 3.08 -0.24 6.74 o 5 6 1 74.05 59.33 12.14 o -5 7 1 565.43 556.03 34.80 o -4 7 1 99.17 93.74 12.00 o -3 7 1 229.70 221.58 15.74 o -2 7 1 2675.80 2710.00 60.72 o -1 7 1 2551.10 2479.39 53.77 o 0 7 1 336.62 390.47 11.24 o 1 7 1 5596.92 5843.55 121.90 o 2 7 1 1020.07 978.95 32.45 o 3 7 1 304.13 298.61 19.12 o 4 7 1 1088.68 1070.90 45.12 o 5 7 1 422.51 434.32 30.23 o -5 8 1 69.87 70.86 12.16 o -4 8 1 0.01 -5.84 5.84 o -3 8 1 195.76 180.90 14.18 o -2 8 1 86.46 75.63 5.61 o -1 8 1 1516.37 1439.68 33.46 o 0 8 1 428.43 435.95 12.50 o 1 8 1 142.00 133.47 7.17 o 2 8 1 166.51 149.40 11.39 o 3 8 1 135.71 127.05 12.41 o 4 8 1 91.01 94.75 12.46 o 5 8 1 95.52 99.34 15.01 o -5 9 1 563.80 547.04 31.95 o -4 9 1 328.79 308.79 21.53 o -3 9 1 1254.20 1239.49 42.93 o -2 9 1 1806.07 1853.60 46.97 o -1 9 1 159.24 149.78 7.70 o 0 9 1 496.66 460.19 13.46 o 1 9 1 673.52 726.76 21.64 o 2 9 1 296.24 273.32 13.71 o 3 9 1 109.32 108.39 11.49 o 4 9 1 55.82 33.56 10.21 o 5 9 1 145.32 168.05 17.70 o -5 10 1 294.07 309.59 24.13 o -4 10 1 41.28 37.49 9.78 o -3 10 1 13.98 2.77 5.53 o -2 10 1 285.48 263.03 11.37 o -1 10 1 5.43 9.67 2.91 o 0 10 1 810.44 894.97 23.15 o 1 10 1 1043.68 999.78 25.62 o 2 10 1 769.54 764.40 26.02 o 3 10 1 131.85 137.22 12.83 o 4 10 1 96.77 110.05 13.51 o 5 10 1 2.29 -4.29 8.57 o -5 11 1 64.08 76.57 18.36 o -4 11 1 1259.00 1281.75 49.94 o -3 11 1 5.66 10.31 6.40 o -2 11 1 703.42 714.26 24.52 o -1 11 1 747.37 728.76 20.59 o 0 11 1 359.77 370.12 12.96 o 1 11 1 823.82 753.79 21.15 o 2 11 1 1691.72 1678.90 50.40 o 3 11 1 747.79 734.32 33.27 o 4 11 1 449.93 451.29 27.39 o -5 12 1 39.13 33.62 12.30 o -4 12 1 186.52 169.21 16.09 o -3 12 1 38.52 40.21 8.43 o -2 12 1 447.06 418.03 18.39 o -1 12 1 465.23 439.90 15.23 o 0 12 1 301.13 326.09 12.66 o 1 12 1 2.04 7.74 2.77 o 2 12 1 1959.19 1882.23 67.77 o 3 12 1 147.69 145.69 14.04 o 4 12 1 4.28 17.86 8.41 o -4 13 1 181.88 200.02 17.07 o -3 13 1 1474.05 1406.91 56.94 o -2 13 1 207.30 195.98 13.88 o -1 13 1 100.95 104.64 7.08 o 0 13 1 3963.72 4074.32 88.68 o 1 13 1 22.30 19.96 3.88 o 2 13 1 143.87 148.97 12.65 o 3 13 1 2049.43 1995.18 61.98 o 4 13 1 22.78 22.76 8.41 o -4 14 1 3.20 2.65 8.78 o -3 14 1 43.05 41.99 7.47 o -2 14 1 718.60 755.98 26.91 o -1 14 1 76.61 74.58 6.26 o 0 14 1 145.26 155.89 10.05 o 1 14 1 374.00 369.20 15.03 o 2 14 1 112.55 90.80 9.55 o 3 14 1 7.76 4.10 6.13 o 4 14 1 98.76 97.12 13.27 o -4 15 1 426.00 406.55 24.89 o -3 15 1 383.80 407.04 22.42 o -2 15 1 330.68 331.75 22.89 o -1 15 1 1347.75 1332.82 34.95 o 0 15 1 490.01 506.95 18.52 o 1 15 1 728.23 769.19 26.27 o 2 15 1 251.28 247.82 15.53 o 3 15 1 49.45 52.63 11.54 o 4 15 1 456.02 450.98 33.84 o -4 16 1 37.67 26.23 9.49 o -3 16 1 245.24 244.21 16.81 o -2 16 1 1232.66 1206.37 40.42 o -1 16 1 179.17 171.24 10.23 o 0 16 1 7.65 0.80 3.11 o 1 16 1 358.23 349.91 18.10 o 2 16 1 29.51 20.35 5.54 o 3 16 1 26.48 12.12 6.59 o 4 16 1 43.56 59.68 13.10 o -4 17 1 15.96 26.24 9.03 o -3 17 1 746.79 726.01 44.66 o -2 17 1 13.11 24.25 6.04 o -1 17 1 391.03 408.87 24.85 o 0 17 1 2046.98 2140.82 53.00 o 1 17 1 208.47 202.83 13.06 o 2 17 1 264.57 251.02 16.51 o 3 17 1 1507.24 1364.69 48.78 o -3 18 1 22.13 16.52 7.07 o -2 18 1 62.83 75.49 10.35 o -1 18 1 125.35 147.79 12.64 o 0 18 1 38.52 52.44 6.07 o 1 18 1 70.03 56.25 7.27 o 2 18 1 524.07 494.26 24.82 o 3 18 1 64.72 61.10 9.58 o -3 19 1 1.30 -3.40 5.66 o -2 19 1 460.29 449.84 25.49 o -1 19 1 1386.05 1413.78 62.84 o 0 19 1 24.59 24.52 5.47 o 1 19 1 646.55 686.62 27.04 o 2 19 1 665.95 652.39 31.35 o 3 19 1 3.26 4.54 6.36 o -3 20 1 0.14 3.51 8.76 o -2 20 1 209.65 231.71 17.73 o -1 20 1 33.66 47.12 8.20 o 0 20 1 20.22 18.47 7.06 o 1 20 1 529.15 529.79 24.98 o 2 20 1 65.94 54.33 9.26 o 3 20 1 33.11 90.98 44.27 o -2 21 1 445.17 483.05 33.26 o -1 21 1 0.80 -5.21 5.73 o 0 21 1 444.89 488.07 25.81 o 1 21 1 185.11 203.39 15.81 o 2 21 1 147.26 137.06 13.15 o -2 22 1 49.15 55.61 12.35 o -1 22 1 332.78 400.00 28.58 o 0 22 1 178.11 195.95 21.05 o 1 22 1 147.19 153.88 17.99 o 2 22 1 489.30 486.77 41.56 o -1 23 1 161.27 208.13 29.08 o 0 23 1 41.93 87.09 15.71 o 1 23 1 853.47 903.92 49.07 o -5 0 2 333.96 371.72 72.70 o -4 0 2 387.45 382.19 26.55 o -3 0 2 1670.97 1519.25 56.98 o -2 0 2 215.73 225.84 15.96 o -1 0 2 199.83 203.98 21.40 o 0 0 2 395.42 494.62 17.15 o 1 0 2 141.56 162.69 11.34 o 2 0 2 577.77 548.56 24.12 o 3 0 2 5122.40 5076.78 156.65 o 4 0 2 475.00 549.69 38.59 o 5 0 2 777.93 815.21 171.59 o -5 1 2 20.67 12.02 9.91 o -4 1 2 132.40 145.94 11.38 o -3 1 2 275.25 270.60 13.82 o -2 1 2 1449.43 1433.52 35.24 o -1 1 2 3543.51 3846.70 92.64 o 0 1 2 103.81 95.96 4.02 o 1 1 2 876.91 878.68 21.05 o 2 1 2 833.52 774.75 22.06 o 3 1 2 170.60 188.99 11.20 o 4 1 2 346.81 367.55 24.97 o 5 1 2 216.92 190.28 28.63 o -5 2 2 18.85 25.33 8.84 o -4 2 2 1845.29 1836.90 51.18 o -3 2 2 47.29 48.86 7.01 o -2 2 2 2055.71 2013.43 54.05 o -1 2 2 6333.71 6587.56 142.87 o 0 2 2 25.53 15.48 1.67 o 1 2 2 1415.42 1343.48 30.58 o 2 2 2 1328.54 1262.39 31.09 o 3 2 2 0.78 0.93 4.03 o 4 2 2 690.01 663.94 35.44 o 5 2 2 158.72 136.08 19.93 o -5 3 2 1197.30 1187.18 63.52 o -4 3 2 600.84 590.14 25.91 o -3 3 2 693.93 701.06 22.97 o -2 3 2 3371.90 3512.02 76.68 o -1 3 2 96.73 119.12 5.67 o 0 3 2 475.17 532.14 16.36 o 1 3 2 12931.85 13674.64 276.52 o 2 3 2 682.93 616.74 18.73 o 3 3 2 0.69 2.79 3.60 o 4 3 2 485.05 521.72 30.85 o 5 3 2 173.51 197.60 26.88 o -5 4 2 242.20 261.35 32.21 o -4 4 2 87.82 103.37 11.97 o -3 4 2 2647.53 2666.49 61.88 o -2 4 2 1023.90 926.99 27.02 o -1 4 2 1022.58 1032.33 28.29 o 0 4 2 17559.20 19144.34 384.13 o 1 4 2 3.27 2.66 1.84 o 2 4 2 1174.51 1143.19 30.44 o 3 4 2 1702.39 1663.32 51.15 o 4 4 2 222.54 222.06 19.37 o 5 4 2 1.89 -3.15 9.27 o -5 5 2 126.97 119.38 15.18 o -4 5 2 38.46 21.32 6.48 o -3 5 2 38.91 34.01 4.64 o -2 5 2 6.23 18.70 3.24 o -1 5 2 775.94 672.13 21.27 o 0 5 2 0.51 0.39 1.35 o 1 5 2 952.13 1055.76 25.73 o 2 5 2 2064.45 2029.61 46.85 o 3 5 2 99.28 93.78 10.49 o 4 5 2 11.77 -1.78 6.91 o 5 5 2 744.65 750.92 41.84 o -5 6 2 782.03 785.56 41.73 o -4 6 2 1392.29 1398.94 50.62 o -3 6 2 90.92 93.67 7.75 o -2 6 2 459.26 468.12 19.80 o -1 6 2 4630.75 4593.70 102.59 o 0 6 2 1937.98 2053.53 44.35 o 1 6 2 6468.65 6776.89 140.49 o 2 6 2 3087.40 3223.87 77.10 o 3 6 2 67.45 74.22 11.19 o 4 6 2 2084.81 2198.69 69.40 o 5 6 2 398.17 386.96 29.42 o -5 7 2 428.79 447.99 28.24 o -4 7 2 0.19 -1.63 5.38 o -3 7 2 5.34 5.07 3.44 o -2 7 2 3174.57 3111.56 73.36 o -1 7 2 1539.36 1539.59 35.25 o 0 7 2 116.55 123.69 8.03 o 1 7 2 342.41 320.67 12.52 o 2 7 2 849.61 836.95 26.12 o 3 7 2 0.04 4.64 6.12 o 4 7 2 273.43 249.22 19.61 o 5 7 2 184.96 193.44 20.24 o -5 8 2 1058.32 1043.93 46.79 o -4 8 2 7.18 5.52 6.33 o -3 8 2 4155.70 4102.67 108.72 o -2 8 2 2578.03 2583.45 58.55 o -1 8 2 2493.86 2482.69 54.92 o 0 8 2 5126.53 4972.29 103.78 o 1 8 2 3476.46 3483.67 81.17 o 2 8 2 698.09 730.45 24.13 o 3 8 2 1848.28 1864.68 57.55 o 4 8 2 21.39 12.11 7.40 o 5 8 2 390.28 380.08 33.94 o -5 9 2 699.29 719.23 37.63 o -4 9 2 390.37 370.21 23.34 o -3 9 2 154.65 145.22 12.96 o -2 9 2 2541.48 2434.14 58.85 o -1 9 2 803.79 813.73 21.56 o 0 9 2 504.62 538.59 15.64 o 1 9 2 4736.67 4939.70 105.08 o 2 9 2 1102.66 1021.07 30.63 o 3 9 2 138.25 140.52 13.24 o 4 9 2 228.14 206.22 20.24 o -5 10 2 15.94 0.10 7.26 o -4 10 2 2111.36 2056.96 64.91 o -3 10 2 7.80 15.04 6.42 o -2 10 2 2851.00 2890.60 65.37 o -1 10 2 2383.45 2416.82 54.47 o 0 10 2 676.57 674.25 20.25 o 1 10 2 2126.56 2156.57 49.79 o 2 10 2 1326.39 1313.48 41.54 o 3 10 2 1.20 1.59 5.59 o 4 10 2 1552.17 1628.17 59.10 o -5 11 2 0.31 -7.89 7.89 o -4 11 2 0.10 -1.32 6.76 o -3 11 2 89.40 84.50 9.72 o -2 11 2 1.81 6.73 3.10 o -1 11 2 375.76 369.74 13.14 o 0 11 2 147.82 159.17 10.82 o 1 11 2 3.53 4.01 2.76 o 2 11 2 588.01 599.95 26.92 o 3 11 2 241.40 246.09 18.38 o 4 11 2 4.51 5.03 7.66 o -5 12 2 57.47 55.00 12.55 o -4 12 2 32.72 39.17 9.54 o -3 12 2 1294.37 1193.37 42.33 o -2 12 2 424.11 409.51 16.03 o -1 12 2 1.25 3.20 2.82 o 0 12 2 3996.26 4004.02 87.01 o 1 12 2 1.42 4.36 2.97 o 2 12 2 2.40 4.56 4.75 o 3 12 2 2097.01 2109.38 69.87 o 4 12 2 19.19 20.58 8.90 o -4 13 2 47.35 39.02 15.65 o -3 13 2 275.85 244.83 16.27 o -2 13 2 1274.49 1186.09 34.96 o -1 13 2 208.43 220.49 10.71 o 0 13 2 5.69 5.03 2.64 o 1 13 2 789.30 749.31 22.42 o 2 13 2 4.42 4.80 5.09 o 3 13 2 280.88 229.95 17.78 o 4 13 2 457.41 470.07 28.75 o -4 14 2 620.18 560.27 31.61 o -3 14 2 58.14 62.69 12.50 o -2 14 2 360.26 354.07 17.00 o -1 14 2 2747.01 2716.46 62.37 o 0 14 2 25.84 19.79 3.93 o 1 14 2 1281.11 1275.01 33.69 o 2 14 2 596.70 538.90 25.16 o 3 14 2 115.29 101.46 13.34 o 4 14 2 83.49 87.24 13.04 o -4 15 2 245.94 235.14 20.00 o -3 15 2 152.69 163.72 15.37 o -2 15 2 125.33 116.07 9.08 o -1 15 2 111.58 108.11 7.90 o 0 15 2 93.37 109.38 7.91 o 1 15 2 937.60 896.43 29.42 o 2 15 2 330.23 294.56 17.70 o 3 15 2 15.80 6.93 6.87 o 4 15 2 57.04 63.79 11.60 o -4 16 2 15.71 4.91 9.99 o -3 16 2 573.05 592.87 29.69 o -2 16 2 11.11 16.40 6.28 o -1 16 2 1.28 -3.00 3.00 o 0 16 2 933.67 938.68 27.15 o 1 16 2 1.37 4.38 3.90 o 2 16 2 337.73 292.92 17.93 o 3 16 2 874.50 882.23 37.06 o -4 17 2 0.48 -7.17 9.84 o -3 17 2 3.51 9.61 5.60 o -2 17 2 26.47 24.37 6.49 o -1 17 2 194.63 201.12 12.88 o 0 17 2 66.59 73.34 8.17 o 1 17 2 35.49 48.36 9.11 o 2 17 2 265.73 263.82 18.90 o 3 17 2 12.50 8.22 6.93 o -3 18 2 3.29 4.55 7.77 o -2 18 2 91.31 81.90 25.09 o -1 18 2 201.66 208.62 17.32 o 0 18 2 25.13 23.04 6.71 o 1 18 2 149.41 139.50 11.57 o 2 18 2 611.50 586.89 27.83 o 3 18 2 31.27 23.79 8.51 o -3 19 2 42.96 39.82 11.46 o -2 19 2 1298.54 1298.59 59.78 o -1 19 2 329.07 326.49 22.56 o 0 19 2 55.94 43.04 8.01 o 1 19 2 229.72 218.35 21.40 o 2 19 2 100.96 107.17 12.38 o 3 19 2 21.11 22.27 13.49 o -3 20 2 560.69 591.51 40.29 o -2 20 2 339.98 412.31 43.29 o -1 20 2 188.81 200.83 17.84 o 0 20 2 884.57 892.14 40.57 o 1 20 2 243.61 253.61 21.95 o 2 20 2 65.81 57.95 11.68 o -2 21 2 0.32 -6.64 7.20 o -1 21 2 3.95 -4.80 12.50 o 0 21 2 46.04 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