data_2107282 _cell_angle_alpha 104.562 _cell_angle_beta 91.987 _cell_angle_gamma 108.301 _cell_length_a 10.7862 _cell_length_b 12.2712 _cell_length_c 13.7402 _exptl_crystal_F_000 828.00 _reflns_d_resolution_high 0.6500 _cod_data_source_file eb5042RuBrNO2PCyp32BF4_PLIsup3.hkl _cod_data_source_block RuBrNO2PCyp32BF4_PLI _shelx_title ' exp_128 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 201.80 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13895.03 16252.34 253.81 o 3 0 0 18260.17 19847.65 314.24 o 4 0 0 50.49 58.21 7.59 o 5 0 0 17564.17 17869.21 505.45 o 6 0 0 12384.80 12878.77 195.08 o 7 0 0 2609.82 2482.70 86.46 o 8 0 0 9827.47 9395.51 157.42 o 9 0 0 1123.31 1079.96 41.72 o 10 0 0 1971.33 1900.02 80.60 o 11 0 0 3563.89 3199.36 115.33 o 12 0 0 767.04 704.91 55.12 o 13 0 0 1195.52 977.21 68.27 o 14 0 0 5.62 20.11 31.01 o 15 0 0 961.09 1126.09 119.83 o -15 1 0 109.39 205.86 57.78 o -14 1 0 16.16 51.35 35.42 o -13 1 0 831.17 791.16 89.24 o -12 1 0 126.98 85.30 23.55 o -11 1 0 1130.27 994.91 61.17 o -10 1 0 171.17 168.45 19.25 o -9 1 0 3016.26 2810.66 73.64 o -8 1 0 1764.72 1741.68 52.65 o -7 1 0 87.92 110.25 13.18 o -6 1 0 1812.26 1662.38 58.19 o -5 1 0 5812.08 5805.85 131.44 o -4 1 0 5093.54 4904.29 112.96 o -3 1 0 8187.88 8280.04 130.93 o -2 1 0 1811.41 2056.14 36.15 o 1 1 0 3672.73 4753.65 120.88 o 2 1 0 10386.41 12483.78 294.59 o 3 1 0 3846.65 4230.52 163.88 o 4 1 0 5022.03 5492.51 90.67 o 5 1 0 5541.73 5828.52 117.05 o 6 1 0 395.96 405.97 23.59 o 7 1 0 9104.14 9014.19 177.45 o 8 1 0 1259.10 1194.09 40.78 o 9 1 0 1014.36 938.96 53.24 o 10 1 0 2227.71 2181.13 88.23 o 11 1 0 686.51 673.51 51.83 o 12 1 0 2096.62 1956.56 93.02 o 13 1 0 734.68 536.08 76.86 o 14 1 0 293.53 310.65 69.23 o 15 1 0 1324.48 1176.23 123.63 o -16 2 0 388.20 383.50 75.02 o -15 2 0 325.06 250.18 56.39 o -14 2 0 86.59 128.82 45.75 o -13 2 0 85.65 70.04 34.69 o -12 2 0 489.93 408.71 59.98 o -11 2 0 121.35 78.81 26.49 o -10 2 0 1137.57 1054.92 55.09 o -9 2 0 1101.35 1086.25 44.36 o -8 2 0 37.99 29.48 9.24 o -7 2 0 4725.86 4422.56 137.91 o -6 2 0 5277.62 4910.95 163.57 o -5 2 0 89.11 92.95 9.74 o -4 2 0 4262.12 3981.14 125.39 o -3 2 0 2142.13 2107.52 35.86 o -2 2 0 1272.31 1233.00 28.07 o -1 2 0 207.65 271.20 11.14 o 0 2 0 319.37 453.72 29.32 o 1 2 0 1753.43 2247.75 40.71 o 2 2 0 1810.12 2183.23 83.10 o 3 2 0 243.38 297.23 29.21 o 4 2 0 1096.71 1252.62 70.77 o 5 2 0 31.07 35.56 6.71 o 6 2 0 74.19 101.66 12.54 o 7 2 0 394.73 468.08 33.09 o 8 2 0 533.18 463.71 52.72 o 9 2 0 239.45 274.49 44.82 o 10 2 0 1005.73 842.20 74.49 o 11 2 0 12.98 52.92 20.62 o 12 2 0 290.26 252.74 36.26 o 13 2 0 26.18 32.89 30.17 o 14 2 0 32.57 62.05 40.51 o -16 3 0 333.88 379.86 74.54 o -15 3 0 546.07 482.44 77.80 o -14 3 0 902.90 889.67 98.99 o -13 3 0 2.82 14.88 28.62 o -12 3 0 1477.28 1422.38 112.01 o -11 3 0 421.89 355.89 55.80 o -10 3 0 592.75 533.55 40.40 o -9 3 0 3047.55 2843.73 93.69 o -8 3 0 291.29 287.31 27.02 o -7 3 0 9125.25 8721.29 182.15 o -6 3 0 689.62 674.40 35.32 o -5 3 0 79.06 61.87 8.73 o -4 3 0 1096.72 1002.66 25.64 o -3 3 0 3513.94 3851.10 83.61 o -2 3 0 27360.43 29789.75 331.54 o -1 3 0 26283.74 31176.23 401.67 o 0 3 0 6861.38 8492.77 155.78 o 1 3 0 3659.85 4510.39 102.91 o 2 3 0 2102.25 2408.15 71.84 o 3 3 0 25.75 62.01 10.96 o 4 3 0 5159.98 5950.09 188.77 o 5 3 0 3516.99 4057.60 162.02 o 6 3 0 997.39 1075.35 69.25 o 7 3 0 595.74 532.67 31.38 o 8 3 0 12.23 23.15 20.04 o 9 3 0 345.52 275.82 48.23 o 10 3 0 444.76 370.72 55.86 o 11 3 0 7.94 30.59 18.63 o 12 3 0 15.64 38.26 30.81 o 13 3 0 545.09 651.92 84.42 o 14 3 0 242.72 191.21 48.64 o -16 4 0 447.97 302.59 67.42 o -15 4 0 1475.15 1354.96 130.75 o -14 4 0 577.56 509.55 76.24 o -13 4 0 1850.86 1829.16 89.17 o -12 4 0 2452.95 2381.43 86.64 o -11 4 0 199.56 205.34 22.54 o -10 4 0 3538.11 3523.00 90.04 o -9 4 0 1491.80 1427.12 51.61 o -8 4 0 2104.72 1958.62 58.57 o -7 4 0 6281.29 5799.48 111.07 o -6 4 0 0.45 1.39 6.25 o -5 4 0 453.60 308.65 15.73 o -4 4 0 8121.75 8064.29 124.52 o -3 4 0 1530.75 1474.60 29.42 o -2 4 0 28425.67 31520.37 318.57 o -1 4 0 2391.37 2769.43 80.45 o 0 4 0 8270.20 9939.58 186.76 o 1 4 0 22277.30 27315.39 448.71 o 2 4 0 186.17 187.38 13.07 o 3 4 0 1250.39 1308.90 44.41 o 4 4 0 9492.60 10471.15 294.97 o 5 4 0 2124.47 2426.69 81.23 o 6 4 0 1853.72 2030.73 78.32 o 7 4 0 283.24 324.86 47.23 o 8 4 0 292.54 289.20 45.98 o 9 4 0 623.50 570.32 66.68 o 10 4 0 514.04 473.99 63.88 o 11 4 0 973.00 760.13 69.43 o 12 4 0 70.34 25.08 27.65 o 13 4 0 896.22 774.10 95.51 o 14 4 0 29.83 43.46 36.43 o -16 5 0 726.72 620.89 92.64 o -15 5 0 443.23 302.29 60.08 o -14 5 0 88.15 116.37 37.68 o -13 5 0 4426.91 4327.63 208.62 o -12 5 0 0.08 2.23 11.75 o -11 5 0 3367.85 3195.96 90.75 o -10 5 0 2421.00 2270.15 72.29 o -9 5 0 186.17 145.45 18.00 o -8 5 0 14153.59 13245.32 333.66 o -7 5 0 2851.24 2673.13 70.03 o -6 5 0 1224.17 1143.16 34.57 o -5 5 0 21740.27 21227.01 257.82 o -4 5 0 2279.13 2241.42 41.71 o -3 5 0 7814.77 7755.55 135.01 o -2 5 0 40208.64 45019.95 505.86 o -1 5 0 109.78 97.76 14.11 o 0 5 0 15128.24 17474.27 308.85 o 1 5 0 4387.22 5206.04 142.87 o 2 5 0 2988.78 3574.52 72.72 o 3 5 0 8920.11 10287.08 197.54 o 4 5 0 219.54 210.03 20.01 o 5 5 0 5713.02 6323.81 217.98 o 6 5 0 3467.28 3692.62 200.32 o 7 5 0 27.87 40.17 23.58 o 8 5 0 2467.65 2750.33 148.90 o 9 5 0 33.16 43.14 33.10 o 10 5 0 2664.88 2792.12 164.17 o 11 5 0 317.29 194.28 53.36 o 12 5 0 157.86 170.36 47.28 o 13 5 0 404.13 451.46 82.40 o -16 6 0 358.19 317.62 68.31 o -15 6 0 672.87 593.25 88.23 o -14 6 0 383.29 296.91 59.17 o -13 6 0 736.88 669.62 43.88 o -12 6 0 34.02 48.17 20.37 o -11 6 0 1824.19 1740.07 66.50 o -10 6 0 1382.18 1212.02 64.46 o -9 6 0 1293.48 1248.64 51.40 o -8 6 0 2500.13 2413.21 71.73 o -7 6 0 271.02 256.34 17.46 o -6 6 0 10242.97 9396.33 139.05 o -5 6 0 12885.65 12411.05 227.48 o -4 6 0 234.00 210.40 12.75 o -3 6 0 18259.51 18829.86 302.32 o -2 6 0 1294.49 1410.87 46.00 o -1 6 0 8950.65 9750.76 161.96 o 0 6 0 5136.96 5545.02 105.50 o 1 6 0 217.40 220.42 23.04 o 2 6 0 12016.90 13924.05 211.29 o 3 6 0 2143.25 2416.91 72.70 o 4 6 0 2691.04 3019.02 84.08 o 5 6 0 5623.78 6218.42 221.19 o 6 6 0 438.32 501.21 40.44 o 7 6 0 1909.25 2032.25 88.66 o 8 6 0 2084.29 2188.56 136.38 o 9 6 0 305.30 254.36 52.76 o 10 6 0 2102.27 2029.94 145.34 o 11 6 0 72.22 80.79 32.92 o 12 6 0 2189.93 2081.85 158.52 o -16 7 0 379.68 325.67 65.30 o -15 7 0 176.01 121.32 39.75 o -14 7 0 686.85 611.54 82.29 o -13 7 0 0.74 -18.33 18.33 o -12 7 0 58.42 50.16 17.66 o -11 7 0 2493.71 2305.40 106.16 o -10 7 0 133.02 101.27 15.75 o -9 7 0 1722.72 1691.03 63.43 o -8 7 0 1314.84 1267.08 43.17 o -7 7 0 784.58 700.39 30.16 o -6 7 0 1417.02 1252.74 34.46 o -5 7 0 1392.26 1378.26 35.89 o -4 7 0 3721.94 3824.74 66.57 o -3 7 0 5341.34 5567.32 112.58 o -2 7 0 2920.49 3371.90 91.25 o -1 7 0 5020.89 5773.60 115.83 o 0 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349.71 327.61 26.96 o -8 11 0 1478.11 1494.70 54.73 o -7 11 0 1264.85 1311.59 58.76 o -6 11 0 468.27 400.73 33.09 o -5 11 0 1690.00 1661.90 66.61 o -4 11 0 773.83 812.53 60.36 o -3 11 0 7349.81 7710.83 164.54 o -2 11 0 286.31 294.16 28.69 o -1 11 0 562.43 580.28 38.08 o 0 11 0 4693.50 4969.74 123.53 o 1 11 0 40.56 47.52 23.87 o 2 11 0 1115.37 1178.29 75.45 o 3 11 0 541.61 558.57 74.61 o 4 11 0 742.96 839.98 60.40 o 5 11 0 387.44 493.09 76.51 o 6 11 0 58.80 103.10 46.62 o 7 11 0 692.82 795.54 69.00 o 8 11 0 469.30 487.76 120.71 o 9 11 0 1118.83 1138.71 122.01 o -15 12 0 8.35 24.08 24.08 o -14 12 0 30.99 41.00 25.87 o -13 12 0 111.01 159.16 38.34 o -12 12 0 540.96 564.70 47.20 o -11 12 0 1066.77 1146.76 52.82 o -10 12 0 303.14 290.26 26.52 o -9 12 0 491.70 477.68 33.31 o -8 12 0 725.91 741.80 67.30 o -7 12 0 582.91 518.17 39.33 o -6 12 0 1349.17 1257.12 60.98 o -5 12 0 1217.47 1182.69 58.74 o -4 12 0 174.36 161.26 24.14 o -3 12 0 1101.86 1142.46 95.12 o -2 12 0 1177.34 1157.16 73.65 o -1 12 0 475.17 452.67 36.03 o 0 12 0 35.86 71.40 18.16 o 1 12 0 53.70 103.18 28.01 o 2 12 0 135.90 145.57 31.99 o 3 12 0 172.48 99.15 39.27 o 4 12 0 71.73 90.29 41.50 o 5 12 0 1.08 -12.96 36.89 o 6 12 0 532.01 589.04 87.87 o 7 12 0 409.34 488.22 57.02 o 8 12 0 756.20 859.09 75.99 o -14 13 0 1029.51 1250.07 93.33 o -13 13 0 20.27 37.93 30.20 o -12 13 0 837.94 888.91 76.60 o -11 13 0 868.69 982.58 50.75 o -10 13 0 1901.14 1883.31 85.49 o -9 13 0 1593.98 1606.16 72.98 o -8 13 0 463.91 427.31 38.02 o -7 13 0 212.68 185.01 26.39 o -6 13 0 2913.96 2853.07 97.86 o -5 13 0 18.23 19.59 14.98 o -4 13 0 1301.41 1312.39 65.27 o -3 13 0 1425.32 1477.11 115.42 o -2 13 0 59.96 24.37 27.40 o -1 13 0 175.14 130.01 30.82 o 0 13 0 112.78 156.94 35.14 o 1 13 0 36.38 60.15 30.52 o 2 13 0 4.65 13.65 23.42 o 3 13 0 3.87 -22.40 36.17 o 4 13 0 235.97 113.43 42.65 o 5 13 0 20.87 3.65 34.93 o 6 13 0 440.80 604.99 95.97 o 7 13 0 624.15 677.91 68.75 o -14 14 0 983.19 1231.30 193.47 o -13 14 0 1164.45 1407.14 185.84 o 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