data_2107456 _cell_angle_alpha 90.000 _cell_angle_beta 103.908 _cell_angle_gamma 90.000 _cell_length_a 10.1156 _cell_length_b 28.8563 _cell_length_c 4.8378 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.2112 _cod_data_source_file bi5051dihydrate_mono_NEUTRONsup2.hkl _cod_data_source_block dihydrate_mono_NEUTRON _shelx_title ' carbamazepine dihydrate monoclinic P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 285.82 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -9 8 0 37464.50 39540.05 425.42 o -9 10 0 24412.77 23595.59 325.04 o -8 14 1 22742.47 24993.74 346.45 o -6 4 0 16310.76 15614.59 231.70 o -10 9 1 17020.21 16633.79 298.60 o -9 6 0 14111.36 13448.31 239.94 o -6 8 0 14867.03 16871.52 288.51 o -8 11 1 13831.17 14487.10 259.84 o -14 10 0 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