#------------------------------------------------------------------------------ #$Date: 2016-05-14 04:13:36 +0300 (Sat, 14 May 2016) $ #$Revision: 182941 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/74/2107499.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2107499 _cell_angle_alpha 93.043 _cell_angle_beta 104.723 _cell_angle_gamma 112.509 _cell_length_a 13.1577 _cell_length_b 13.7793 _cell_length_c 18.4731 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.7800 _cod_data_source_file xk5028CCDC1422434sup6.hkl _cod_data_source_block CCDC1422434 _shelx_title ' 15gtu46_L_AgTol_0m_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 395.62 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5922.71 6250.51 36.66 o 2 0 0 12782.30 12879.52 208.58 o 3 0 0 16805.27 17135.79 329.77 o 4 0 0 32549.50 32037.37 496.20 o 5 0 0 141.63 123.26 22.34 o 6 0 0 3331.91 3340.68 174.80 o 7 0 0 499.93 466.49 48.71 o 8 0 0 118.88 118.58 37.28 o 9 0 0 3810.36 3698.45 112.56 o 10 0 0 721.76 832.25 62.09 o 11 0 0 3747.76 3815.03 142.20 o 12 0 0 2094.49 2250.10 118.60 o 13 0 0 855.08 1070.70 112.69 o 14 0 0 417.42 812.80 123.95 o -15 1 0 218.67 216.84 169.68 o -14 1 0 343.74 429.54 105.87 o -13 1 0 2687.69 2501.86 128.09 o -12 1 0 1364.10 1537.62 132.36 o -11 1 0 1752.99 1762.83 80.02 o -10 1 0 17.02 4.56 26.70 o -9 1 0 3.28 21.23 21.81 o -8 1 0 4203.28 4099.41 82.58 o -7 1 0 34.07 56.52 13.77 o -6 1 0 1125.90 1114.73 37.29 o -5 1 0 10130.74 10329.48 143.60 o -4 1 0 592.57 538.25 12.19 o -3 1 0 4981.14 5190.95 88.50 o -2 1 0 4183.98 4251.69 86.87 o -1 1 0 50563.66 51971.21 1644.21 o 0 1 0 13856.06 13071.00 458.94 o 1 1 0 6792.45 6543.39 98.06 o 2 1 0 14028.79 14655.86 156.23 o 3 1 0 69629.55 68782.32 962.08 o 4 1 0 962.88 954.54 45.24 o 5 1 0 2313.10 2361.73 81.31 o 6 1 0 104.90 75.90 28.46 o 7 1 0 1218.48 1051.76 53.42 o 8 1 0 103.57 84.59 39.49 o 9 1 0 3084.97 2939.73 101.44 o 10 1 0 439.59 389.12 70.46 o 11 1 0 2848.10 2826.59 123.86 o 12 1 0 1320.55 1197.04 95.84 o 13 1 0 1817.47 1763.87 144.36 o 14 1 0 8.20 80.85 81.45 o -15 2 0 17.90 36.52 76.19 o -14 2 0 1213.80 1132.87 138.50 o -13 2 0 3661.58 3704.34 145.57 o -12 2 0 108.86 157.26 42.29 o -11 2 0 383.64 413.27 45.51 o -10 2 0 39.32 26.54 22.36 o -9 2 0 9906.97 9829.58 161.38 o -8 2 0 2789.01 2899.77 75.03 o -7 2 0 2353.99 2554.86 72.28 o -6 2 0 2508.33 2362.09 46.31 o -5 2 0 221.99 255.18 22.17 o -4 2 0 9876.10 10008.54 144.71 o -3 2 0 40.07 76.84 13.44 o -2 2 0 79896.17 78338.07 1057.52 o -1 2 0 4.04 6.50 9.06 o 0 2 0 27407.89 26709.89 313.29 o 1 2 0 3694.81 3642.32 47.05 o 2 2 0 156514.52 158509.70 1932.75 o 3 2 0 9711.54 10470.34 256.89 o 4 2 0 988.26 893.23 51.23 o 5 2 0 20023.03 20363.88 380.44 o 6 2 0 2327.96 2285.59 83.15 o 7 2 0 99.41 64.17 30.75 o 8 2 0 996.50 1056.18 69.66 o 9 2 0 453.04 410.89 57.49 o 10 2 0 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155.26 o 1 12 0 1664.04 1777.45 125.00 o 2 12 0 73.44 55.57 106.07 o 3 12 0 285.31 67.98 126.19 o 4 12 0 198.70 139.47 165.72 o 5 12 0 1050.75 1157.11 207.76 o 6 12 0 41.32 116.20 151.73 o -14 13 0 452.78 546.17 90.77 o -13 13 0 165.98 120.86 91.35 o -12 13 0 616.24 653.20 101.03 o -11 13 0 4429.85 4369.95 204.52 o -10 13 0 382.30 396.45 124.72 o -9 13 0 738.56 1076.35 147.94 o -8 13 0 9.73 39.37 84.20 o -7 13 0 754.10 958.51 130.31 o -6 13 0 582.16 691.50 126.19 o -5 13 0 12.17 1.14 89.18 o -4 13 0 218.52 172.91 92.74 o -3 13 0 1388.96 1313.28 167.42 o -2 13 0 1215.47 1110.79 159.37 o -1 13 0 381.58 224.56 118.42 o 0 13 0 3.03 1.40 107.94 o 1 13 0 10.75 83.83 109.98 o 2 13 0 3251.54 2973.58 256.52 o 3 13 0 0.28 0.47 109.18 o 4 13 0 214.68 191.40 152.85 o 5 13 0 1.74 90.57 144.23 o -14 14 0 87.12 1.24 119.83 o -13 14 0 383.96 229.43 123.50 o -12 14 0 1179.64 1274.64 196.27 o -11 14 0 1589.46 1394.32 282.86 o -10 14 0 2587.12 2546.57 298.48 o -9 14 0 1037.46 1259.29 299.80 o -8 14 0 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