#------------------------------------------------------------------------------
#$Date: 2016-05-28 04:36:26 +0300 (Sat, 28 May 2016) $
#$Revision: 183118 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/75/2107544.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2107544
_cell_angle_alpha                90.000
_cell_angle_beta                 105.035
_cell_angle_gamma                90.000
_cell_length_a                   8.2950
_cell_length_b                   11.7449
_cell_length_c                   10.0278
_exptl_crystal_F_000             672.00
_reflns_d_resolution_high        0.7608
_cod_data_source_file            xk5029aPd_2sup5.hkl
_cod_data_source_block           aPd_2
_shelx_title                     ' aPdCl29S2O-22 in P21/n No14'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            263.77
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 2 0 2680.80 3240.26 87.13 o
1 2 0 26.24 20.31 4.00 o
1 3 0 3147.65 2472.33 77.03 o
0 4 0 15360.34 17092.24 391.79 o
1 4 0 86.77 79.57 8.28 o
2 4 0 335.72 204.49 56.40 o
1 5 0 2612.07 2684.00 68.93 o
2 5 0 39.10 33.14 8.98 o
0 6 0 9258.83 10339.32 183.47 o
1 6 0 3489.03 3648.91 100.93 o
2 6 0 2813.21 2553.91 123.89 o
1 7 0 10480.03 11546.71 430.85 o
2 7 0 1483.03 1485.38 74.39 o
0 8 0 1995.93 2219.18 83.45 o
1 8 0 3696.79 3733.52 122.49 o
2 8 0 1072.20 1073.29 78.62 o
1 9 0 377.20 381.74 35.96 o
2 9 0 1178.75 1221.97 115.72 o
0 10 0 4732.23 5188.29 303.41 o
1 10 0 464.95 376.00 45.48 o
2 10 0 4746.82 4654.62 547.53 o
1 11 0 4985.62 5524.40 331.64 o
2 11 0 2193.77 2273.98 275.33 o
0 12 0 705.57 536.18 115.33 o
1 12 0 437.44 327.78 57.11 o
2 12 0 1380.14 1462.58 173.73 o
1 13 0 436.83 307.45 58.27 o
2 13 0 276.88 246.88 45.22 o
0 14 0 326.65 197.28 71.42 o
1 14 0 32.54 -13.52 28.07 o
2 14 0 2.85 -38.71 38.71 o
1 15 0 76.07 212.95 95.17 o
-1 0 1 18326.26 21122.12 387.08 o
-2 1 1 8191.59 5370.16 414.53 o
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-1 2 1 313.49 321.56 11.17 o
0 2 1 19791.72 14099.69 543.13 o
-2 3 1 3.73 1.71 3.84 o
-1 3 1 5725.21 6389.23 99.13 o
0 3 1 6567.14 5712.42 164.68 o
-2 4 1 1.26 4.04 2.95 o
-1 4 1 6051.95 6687.00 102.55 o
0 4 1 25213.73 23991.20 378.97 o
1 4 1 837.99 558.29 65.46 o
-3 5 1 1089.74 912.62 82.39 o
-2 5 1 18.21 18.52 4.61 o
-1 5 1 781.30 859.92 24.16 o
0 5 1 4306.77 3671.74 134.86 o
1 5 1 501.27 500.71 39.52 o
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0 6 1 6455.39 7065.45 251.14 o
1 6 1 3883.54 3384.54 129.69 o
-3 7 1 2070.59 2142.74 137.36 o
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-1 7 1 1197.42 1349.64 41.55 o
0 7 1 9944.18 10664.64 406.53 o
1 7 1 7480.19 7402.14 284.36 o
-3 8 1 1177.06 1254.13 86.61 o
-2 8 1 5073.09 5322.45 254.52 o
-1 8 1 229.24 235.29 23.65 o
0 8 1 6705.47 7049.28 272.96 o
1 8 1 5557.55 5431.07 240.69 o
2 8 1 2646.95 2783.21 342.77 o
-3 9 1 196.35 201.79 33.54 o
-2 9 1 1306.13 1257.56 67.75 o
-1 9 1 8471.81 8972.16 175.37 o
0 9 1 116.99 100.66 14.11 o
1 9 1 3874.21 4520.44 273.49 o
2 9 1 217.50 141.68 55.06 o
-3 10 1 1455.42 1912.82 126.90 o
-2 10 1 1004.28 979.09 62.19 o
-1 10 1 5769.97 5745.96 184.64 o
0 10 1 4389.47 4940.13 168.41 o
1 10 1 248.85 185.19 38.39 o
-3 11 1 501.36 590.55 70.59 o
-2 11 1 3640.36 3398.24 194.87 o
-1 11 1 2245.10 2320.82 128.16 o
0 11 1 1935.89 2159.73 130.33 o
1 11 1 41.13 42.14 15.98 o
2 11 1 329.11 236.55 68.24 o
-3 12 1 1742.29 2273.18 219.00 o
-2 12 1 195.71 212.19 37.91 o
-1 12 1 661.41 593.92 67.70 o
0 12 1 114.04 98.98 25.63 o
1 12 1 270.62 156.19 41.28 o
2 12 1 421.84 260.78 111.80 o
-3 13 1 87.48 83.78 44.99 o
-2 13 1 144.54 142.38 33.42 o
-1 13 1 12.74 -19.86 25.75 o
0 13 1 105.11 88.78 13.99 o
1 13 1 1468.77 1246.34 183.64 o
2 13 1 1.41 5.93 37.69 o
-2 14 1 401.26 363.41 58.38 o
-1 14 1 90.61 73.35 17.25 o
0 14 1 617.63 646.24 77.59 o
1 14 1 1127.25 1225.14 111.12 o
-2 15 1 60.68 -13.53 183.48 o
-1 15 1 434.57 294.49 222.02 o
0 15 1 120.89 93.37 55.58 o
1 15 1 984.28 700.36 380.95 o
-2 0 2 46.90 49.86 7.14 o
-3 1 2 853.25 715.73 41.29 o
-2 1 2 1230.45 1259.54 30.74 o
-1 1 2 1110.11 975.17 43.47 o
-3 2 2 27136.09 21099.66 847.04 o
-2 2 2 7905.49 8881.79 136.76 o
-1 2 2 14975.14 13678.57 327.79 o
-3 3 2 385.76 360.03 24.06 o
-2 3 2 4519.65 4701.73 93.76 o
-1 3 2 18297.75 18037.87 354.89 o
0 3 2 69577.05 48998.27 743.73 o
-4 4 2 2782.36 1965.96 244.22 o
-3 4 2 4668.99 4796.04 208.42 o
-2 4 2 137.94 143.20 11.22 o
-1 4 2 11150.75 11308.65 163.52 o
0 4 2 40.14 29.72 7.21 o
-4 5 2 1402.96 1407.69 140.32 o
-3 5 2 458.97 480.87 26.05 o
-2 5 2 413.08 426.91 20.34 o
-1 5 2 307.13 339.40 20.66 o
0 5 2 6955.18 5907.17 224.05 o
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-3 6 2 2165.43 2376.66 108.51 o
-2 6 2 320.62 317.83 21.01 o
-1 6 2 212.80 241.87 15.65 o
0 6 2 3378.64 3292.54 147.55 o
-4 7 2 3049.11 3676.93 276.49 o
-3 7 2 7443.41 7918.72 384.75 o
-2 7 2 2451.08 2566.88 74.18 o
-1 7 2 3.49 4.16 6.02 o
0 7 2 4838.82 4832.42 260.02 o
1 7 2 1234.98 1215.96 113.86 o
-4 8 2 478.03 497.19 58.77 o
-3 8 2 9404.11 9787.60 512.91 o
-2 8 2 1690.82 1653.27 67.00 o
-1 8 2 6347.45 7124.04 197.76 o
0 8 2 50.15 57.08 10.97 o
1 8 2 595.40 634.11 78.06 o
-4 9 2 6732.91 9585.09 1213.16 o
-3 9 2 126.47 110.82 19.56 o
-2 9 2 4362.90 4477.95 121.74 o
-1 9 2 2502.42 2777.80 91.23 o
0 9 2 2214.01 2633.17 137.02 o
1 9 2 613.56 609.29 62.02 o
-4 10 2 2680.38 3451.57 227.75 o
-3 10 2 1747.70 1875.81 129.82 o
-2 10 2 115.10 140.41 21.53 o
-1 10 2 1534.90 1768.12 81.76 o
0 10 2 38.30 53.85 18.86 o
1 10 2 2086.02 2336.83 247.98 o
-4 11 2 1259.60 1972.68 348.87 o
-3 11 2 275.31 282.12 38.94 o
-2 11 2 236.34 187.45 28.89 o
-1 11 2 55.00 39.33 12.17 o
0 11 2 41.60 52.24 19.11 o
1 11 2 641.98 459.44 106.36 o
-4 12 2 31.82 26.71 26.92 o
-3 12 2 268.20 274.86 47.43 o
-2 12 2 59.76 16.45 25.39 o
-1 12 2 650.35 598.09 70.59 o
0 12 2 247.09 201.37 37.67 o
1 12 2 108.67 59.55 42.28 o
-4 13 2 39.22 21.03 56.70 o
-3 13 2 201.63 228.76 45.59 o
-2 13 2 2956.38 2928.03 174.49 o
-1 13 2 1705.45 1596.57 121.70 o
0 13 2 1164.90 1154.02 115.38 o
1 13 2 120.87 85.51 67.31 o
-3 14 2 421.92 -44.64 110.88 o
-2 14 2 348.11 435.18 74.36 o
-1 14 2 3219.20 3029.18 168.74 o
0 14 2 0.02 -10.02 28.12 o
1 14 2 2749.20 3539.61 1449.54 o
-2 15 2 1783.38 1622.71 296.26 o
-1 15 2 96.27 -33.17 135.45 o
0 15 2 946.16 1106.41 270.77 o
-3 0 3 2102.42 2434.84 56.19 o
-1 0 3 30.72 40.93 15.67 o
-4 1 3 6883.20 5737.96 325.30 o
-3 1 3 4076.55 4201.45 105.57 o
-2 1 3 97.32 87.02 8.09 o
-1 1 3 1859.53 1422.20 94.19 o
-4 2 3 19332.25 17892.52 913.96 o
-3 2 3 3323.77 3464.74 92.78 o
-2 2 3 1882.89 2233.86 55.07 o
-1 2 3 8035.41 5730.04 157.00 o
-4 3 3 849.15 961.21 55.59 o
-3 3 3 18759.18 21767.92 223.49 o
-2 3 3 346.44 380.28 14.86 o
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-3 4 3 4644.88 4817.71 87.70 o
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-5 5 3 609.86 623.01 94.51 o
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0 5 3 33012.99 22517.73 677.06 o
-5 6 3 372.95 345.62 58.09 o
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-3 6 3 4512.52 4624.39 171.18 o
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0 6 3 21.69 20.28 9.36 o
-5 7 3 520.35 575.57 102.28 o
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-3 7 3 111.71 110.40 10.90 o
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-1 7 3 3769.90 3860.17 182.35 o
0 7 3 7469.39 7404.73 387.84 o
-5 8 3 169.88 124.41 41.36 o
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-3 8 3 1668.77 1755.80 70.29 o
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-1 8 3 703.33 715.63 46.04 o
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-4 9 3 169.54 165.92 29.72 o
-3 9 3 2803.17 3069.43 114.51 o
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-1 9 3 115.40 96.11 17.56 o
0 9 3 18.26 40.46 14.54 o
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-3 10 3 465.91 461.58 48.31 o
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-1 10 3 124.34 113.91 17.00 o
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-5 11 3 13.74 33.50 71.06 o
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