#------------------------------------------------------------------------------ #$Date: 2016-09-30 04:23:35 +0300 (Fri, 30 Sep 2016) $ #$Revision: 186841 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/79/2107969.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2107969 _cell_angle_alpha 92.496(6) _cell_angle_beta 91.452(6) _cell_angle_gamma 107.191(6) _cell_length_a 6.2535(7) _cell_length_b 7.2501(8) _cell_length_c 32.335(4) _exptl_crystal_F_000 496 _reflns_d_resolution_high 0.7564 _cod_data_source_file ps5052Z_TBDMSsup5.hkl _cod_data_source_block Z_TBDMS _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 157.04 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status _jana_refln_twin_domain 0 1 7 11.76 15.56 1.60 o 1 0 1 8 120.22 121.04 4.32 o 1 0 3 -6 88.27 93.15 3.33 o 1 0 3 -2 3186.58 3336.96 78.72 o 1 0 3 -1 1080.88 1122.69 24.61 o 1 0 3 0 1682.00 1629.97 35.46 o 1 0 3 1 232.68 195.10 4.49 o 1 0 3 2 1054.24 1075.33 22.29 o 1 0 3 3 444.40 412.83 9.74 o 1 1 -9 -8 133.78 148.37 13.19 o 1 1 -2 -5 1712.87 1708.76 32.23 o 1 1 -2 0 230.50 235.16 4.66 o 1 1 -2 3 799.17 726.11 14.06 o 1 1 -2 4 417.18 410.90 8.14 o 1 1 -2 5 2418.22 2409.33 45.33 o 1 1 0 -6 221.11 222.01 5.03 o 1 1 0 -4 4155.80 4008.39 80.62 o 1 1 0 -3 3154.91 2989.64 60.18 o 1 1 0 -2 4866.52 4598.71 92.63 o 1 1 0 -1 343.00 335.24 6.81 o 1 1 0 0 352.86 314.13 6.91 o 1 1 0 1 838.13 757.43 16.94 o 1 1 0 2 2072.04 1965.50 42.22 o 1 1 0 3 2802.99 2442.18 49.57 o 1 1 0 4 5136.34 4610.26 83.19 o 1 1 0 5 75.84 69.45 1.53 o 1 1 2 2 94.44 86.32 1.85 o 1 1 2 3 1683.89 1709.38 29.77 o 1 2 -1 -41 0.06 1.18 9.89 < 1 3 -6 -31 14.23 26.19 10.01 < 1 3 -4 -36 9.87 19.53 6.91 < 1 3 -1 39 51.12 47.50 10.53 o 1 3 0 -40 15.56 29.94 11.15 < 1 3 5 25 36.69 44.44 5.77 o 1 6 -2 -29 1.14 -0.35 5.25 < 1 6 1 -26 8.99 84.10 14.25 o 1 8 -3 7 303.60 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3518.37 83.14 o 1 -2 -4 3 285.34 254.81 6.02 o -2 2 4 0 285.34 254.81 6.02 o 1 -3 -4 3 568.66 566.87 16.01 o -2 3 4 0 568.66 566.87 16.01 o 1 -4 -4 4 82.72 105.56 9.64 o -2 4 4 0 82.72 105.56 9.64 o 1 -5 -4 4 10.71 13.17 3.58 o -2 5 4 0 10.71 13.17 3.58 o 1 -6 5 0 4.57 11.57 2.37 o -2 -6 5 0 4.57 11.57 2.37 o 1 -5 5 0 413.72 477.14 29.47 o -2 -5 5 0 413.72 477.14 29.47 o 1 4 -5 1 54.10 57.22 2.61 o -2 -4 5 0 54.10 57.22 2.61 o 1 3 -5 1 117.17 122.08 3.55 o -2 -3 5 0 117.17 122.08 3.55 o 1 2 -5 2 44.13 30.19 2.56 o -2 -2 5 0 44.13 30.19 2.56 o 1 1 -5 2 0.56 0.25 0.94 < -2 -1 5 0 0.56 0.25 0.94 < 1 -1 -5 3 468.26 423.92 9.20 o -2 1 5 0 468.26 423.92 9.20 o 1 -3 -5 4 800.91 717.28 39.19 o -2 3 5 0 800.91 717.28 39.19 o 1 -4 -5 4 112.92 138.43 11.62 o -2 4 5 0 112.92 138.43 11.62 o 1 -7 6 0 4.00 3.53 5.01 < -2 -7 6 0 4.00 3.53 5.01 < 1 5 -6 1 71.23 68.39 3.65 o -2 -5 6 0 71.23 68.39 3.65 o 1 4 -6 1 405.39 359.90 22.37 o -2 -4 6 0 405.39 359.90 22.37 o 1 3 -6 2 8.79 14.65 3.11 o -2 -3 6 0 8.79 14.65 3.11 o 1 2 -6 2 1163.10 1118.44 30.06 o -2 -2 6 0 1163.10 1118.44 30.06 o 1 0 -6 3 38.72 32.53 2.29 o -2 0 6 0 38.72 32.53 2.29 o 1 -2 -6 4 510.77 479.44 27.62 o -2 2 6 0 510.77 479.44 27.62 o 1 6 -7 1 3.79 4.88 3.26 < -2 -6 7 0 3.79 4.88 3.26 < 1 4 -7 2 4.62 24.74 6.02 o -2 -4 7 0 4.62 24.74 6.02 o 1 3 -7 2 256.68 271.14 12.55 o -2 -3 7 0 256.68 271.14 12.55 o 1 2 -7 3 123.02 130.44 13.93 o -2 -2 7 0 123.02 130.44 13.93 o 1 1 -7 3 78.63 86.96 3.95 o -2 -1 7 0 78.63 86.96 3.95 o 1 -1 -7 4 1175.88 1058.51 56.38 o -2 1 7 0 1175.88 1058.51 56.38 o 1 5 -8 2 231.69 174.34 13.81 o -2 -5 8 0 231.69 174.34 13.81 o 1 2 -8 3 595.94 556.71 26.56 o -2 -2 8 0 595.94 556.71 26.56 o 1 0 -8 4 183.61 195.67 9.22 o -2 0 8 0 183.61 195.67 9.22 o 1 4 -9 3 15.07 18.10 6.83 < -2 -4 9 0 15.07 18.10 6.83 < 1 3 -9 3 208.47 193.77 19.38 o -2 -3 9 0 208.47 193.77 19.38 o 1 1 -9 4 8.81 19.68 4.29 o -2 -1 9 0 8.81 19.68 4.29 o 1 1 -9 3 1.46 1.53 4.96 < -2 1 -9 1 1.46 1.53 4.96 < 1 3 -9 2 224.14 240.98 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1 1164.65 1171.57 21.68 o 1 0 0 1 0.02 0.02 0.02 < -2 0 0 1 0.02 0.02 0.02 < 1 -2 0 2 904.50 870.41 15.14 o -2 2 0 1 904.50 870.41 15.14 o 1 -3 0 2 32.15 34.63 1.41 o -2 3 0 1 32.15 34.63 1.41 o 1 -4 0 3 438.70 469.57 9.57 o -2 4 0 1 438.70 469.57 9.57 o 1 -5 0 3 8.00 1.13 1.46 < -2 5 0 1 8.00 1.13 1.46 < 1 -7 0 4 169.40 146.74 7.25 o -2 7 0 1 169.40 146.74 7.25 o 1 -8 1 2 36.18 39.41 7.99 o -2 -8 1 1 36.18 39.41 7.99 o 1 -6 1 1 311.88 330.33 9.91 o -2 -6 1 1 311.88 330.33 9.91 o 1 -5 1 1 38.09 44.79 7.05 o -2 -5 1 1 38.09 44.79 7.05 o 1 -4 1 0 274.16 241.72 5.48 o -2 -4 1 1 274.16 241.72 5.48 o 1 -3 1 0 2406.10 2443.51 42.59 o -2 -3 1 1 2406.10 2443.51 42.59 o 1 2 -1 1 23.71 23.63 2.74 o -2 -2 1 1 23.71 23.63 2.74 o 1 1 -1 1 1265.81 1198.08 23.43 o -2 -1 1 1 1265.81 1198.08 23.43 o 1 -1 -1 2 2353.67 2421.61 44.32 o -2 1 1 1 2353.67 2421.61 44.32 o 1 -2 -1 2 3730.03 3861.97 67.08 o -2 2 1 1 3730.03 3861.97 67.08 o 1 -3 -1 3 1180.85 1192.23 18.94 o -2 3 1 1 1180.85 1192.23 18.94 o 1 -4 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429.03 341.70 28.21 o -2 -6 2 24 429.03 341.70 28.21 o 1 5 -2 23 21.68 26.12 4.17 o -2 -5 2 24 21.68 26.12 4.17 o 1 4 -2 23 351.64 343.57 13.29 o -2 -4 2 24 351.64 343.57 13.29 o 1 3 -2 24 8.38 10.26 3.77 < -2 -3 2 24 8.38 10.26 3.77 < 1 2 -2 24 254.95 228.62 6.26 o -2 -2 2 24 254.95 228.62 6.26 o 1 0 -2 25 943.96 830.95 20.00 o -2 0 2 24 943.96 830.95 20.00 o 1 -2 -2 26 801.01 797.19 22.07 o -2 2 2 24 801.01 797.19 22.07 o 1 -3 -2 26 105.07 113.42 6.63 o -2 3 2 24 105.07 113.42 6.63 o 1 -5 -2 27 136.30 109.57 16.89 o -2 5 2 24 136.30 109.57 16.89 o 1 6 -3 23 44.53 33.39 5.18 o -2 -6 3 24 44.53 33.39 5.18 o 1 5 -3 23 201.31 200.06 18.42 o -2 -5 3 24 201.31 200.06 18.42 o 1 4 -3 24 1.55 6.44 4.22 < -2 -4 3 24 1.55 6.44 4.22 < 1 3 -3 24 7.01 6.95 2.17 o -2 -3 3 24 7.01 6.95 2.17 o 1 2 -3 25 297.25 263.02 14.03 o -2 -2 3 24 297.25 263.02 14.03 o 1 1 -3 25 1079.70 925.39 24.84 o -2 -1 3 24 1079.70 925.39 24.84 o 1 -1 -3 26 803.01 834.60 26.27 o -2 1 3 24 803.01 834.60 26.27 o 1 -2 -3 26 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12.97 o 1 2 4 22 24.32 31.84 2.74 o -2 -2 -4 25 24.32 31.84 2.74 o 1 1 4 23 209.49 240.73 16.77 o -2 -1 -4 25 209.49 240.73 16.77 o 1 0 4 23 123.68 110.12 4.12 o -2 0 -4 25 123.68 110.12 4.12 o 1 -2 4 24 15.74 14.28 2.05 o -2 2 -4 25 15.74 14.28 2.05 o 1 -3 4 24 108.53 117.34 4.93 o -2 3 -4 25 108.53 117.34 4.93 o 1 -5 4 25 1.25 1.23 3.38 < -2 5 -4 25 1.25 1.23 3.38 < 1 5 3 21 106.73 105.88 14.43 o -2 -5 -3 25 106.73 105.88 14.43 o 1 4 3 22 180.79 167.90 7.28 o -2 -4 -3 25 180.79 167.90 7.28 o 1 3 3 22 118.97 104.67 6.44 o -2 -3 -3 25 118.97 104.67 6.44 o 1 2 3 23 1177.22 1142.51 36.30 o -2 -2 -3 25 1177.22 1142.51 36.30 o 1 1 3 23 11.09 6.49 1.90 o -2 -1 -3 25 11.09 6.49 1.90 o 1 -1 3 24 744.19 708.33 17.61 o -2 1 -3 25 744.19 708.33 17.61 o 1 -2 3 24 203.34 206.38 10.56 o -2 2 -3 25 203.34 206.38 10.56 o 1 -3 3 25 145.92 136.31 4.96 o -2 3 -3 25 145.92 136.31 4.96 o 1 -4 3 25 1.92 1.41 2.66 < -2 4 -3 25 1.92 1.41 2.66 < 1 -6 3 26 17.93 19.56 4.04 o -2 6 -3 25 17.93 19.56 4.04 o 1 5 2 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112.56 142.82 3.53 o -2 1 -1 25 112.56 142.82 3.53 o 1 -2 1 25 21.44 24.37 3.08 o -2 2 -1 25 21.44 24.37 3.08 o 1 -3 1 26 203.70 209.68 6.17 o -2 3 -1 25 203.70 209.68 6.17 o 1 -4 1 26 9.70 12.48 2.34 o -2 4 -1 25 9.70 12.48 2.34 o 1 -6 1 27 9.28 10.06 4.74 < -2 6 -1 25 9.28 10.06 4.74 < 1 6 0 22 159.64 166.82 17.68 o -2 -6 0 25 159.64 166.82 17.68 o 1 5 0 23 278.44 294.77 11.25 o -2 -5 0 25 278.44 294.77 11.25 o 1 4 0 23 323.14 327.15 12.73 o -2 -4 0 25 323.14 327.15 12.73 o 1 3 0 24 313.28 290.50 7.62 o -2 -3 0 25 313.28 290.50 7.62 o 1 2 0 24 374.23 379.14 8.83 o -2 -2 0 25 374.23 379.14 8.83 o 1 0 0 25 45.33 73.22 2.29 o -2 0 0 25 45.33 73.22 2.29 o 1 -2 0 26 513.90 483.16 10.58 o -2 2 0 25 513.90 483.16 10.58 o 1 -3 0 26 121.00 114.51 4.24 o -2 3 0 25 121.00 114.51 4.24 o 1 -4 0 27 368.95 447.15 29.89 o -2 4 0 25 368.95 447.15 29.89 o 1 -5 0 27 14.96 18.03 4.14 o -2 5 0 25 14.96 18.03 4.14 o 1 6 -1 23 2.59 8.61 3.35 < -2 -6 1 25 2.59 8.61 3.35 < 1 5 -1 23 78.21 92.93 12.50 o -2 -5 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405.67 22.62 o 1 -5 -2 28 16.11 12.60 5.43 < -2 5 2 25 16.11 12.60 5.43 < 1 6 -3 24 5.81 2.00 4.22 < -2 -6 3 25 5.81 2.00 4.22 < 1 5 -3 24 4.03 13.74 6.83 < -2 -5 3 25 4.03 13.74 6.83 < 1 4 -3 25 1.65 2.27 3.60 < -2 -4 3 25 1.65 2.27 3.60 < 1 3 -3 25 148.89 133.08 5.25 o -2 -3 3 25 148.89 133.08 5.25 o 1 2 -3 26 67.50 49.99 5.65 o -2 -2 3 25 67.50 49.99 5.65 o 1 1 -3 26 363.72 309.24 9.45 o -2 -1 3 25 363.72 309.24 9.45 o 1 -1 -3 27 1.62 5.50 2.69 < -2 1 3 25 1.62 5.50 2.69 < 1 -2 -3 27 177.56 190.25 8.16 o -2 2 3 25 177.56 190.25 8.16 o 1 -3 -3 28 143.04 161.39 10.06 o -2 3 3 25 143.04 161.39 10.06 o 1 -4 -3 28 132.58 152.68 11.86 o -2 4 3 25 132.58 152.68 11.86 o 1 6 -4 24 46.12 46.51 10.04 o -2 -6 4 25 46.12 46.51 10.04 o 1 5 -4 25 1.49 0.91 3.35 < -2 -5 4 25 1.49 0.91 3.35 < 1 4 -4 25 90.42 84.72 6.93 o -2 -4 4 25 90.42 84.72 6.93 o 1 3 -4 26 55.04 49.79 10.68 o -2 -3 4 25 55.04 49.79 10.68 o 1 2 -4 26 284.61 256.54 9.08 o -2 -2 4 25 284.61 256.54 9.08 o 1 0 -4 27 372.21 345.64 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31.84 o -2 -5 1 28 405.63 404.64 31.84 o 1 4 -1 27 213.66 212.17 9.91 o -2 -4 1 28 213.66 212.17 9.91 o 1 3 -1 27 44.76 52.78 3.16 o -2 -3 1 28 44.76 52.78 3.16 o 1 2 -1 28 13.24 14.90 3.40 o -2 -2 1 28 13.24 14.90 3.40 o 1 1 -1 28 2.16 4.09 1.70 < -2 -1 1 28 2.16 4.09 1.70 < 1 -1 -1 29 134.57 132.29 4.24 o -2 1 1 28 134.57 132.29 4.24 o 1 -2 -1 29 265.89 251.48 9.52 o -2 2 1 28 265.89 251.48 9.52 o 1 -3 -1 30 132.62 99.02 14.13 o -2 3 1 28 132.62 99.02 14.13 o 1 -4 -1 30 4.68 5.89 3.92 < -2 4 1 28 4.68 5.89 3.92 < 1 6 -2 26 69.00 58.62 10.73 o -2 -6 2 28 69.00 58.62 10.73 o 1 5 -2 27 153.77 134.07 7.67 o -2 -5 2 28 153.77 134.07 7.67 o 1 4 -2 27 45.54 59.86 5.08 o -2 -4 2 28 45.54 59.86 5.08 o 1 3 -2 28 14.86 25.11 5.18 o -2 -3 2 28 14.86 25.11 5.18 o 1 2 -2 28 79.93 81.07 3.63 o -2 -2 2 28 79.93 81.07 3.63 o 1 0 -2 29 84.75 60.10 3.43 o -2 0 2 28 84.75 60.10 3.43 o 1 -2 -2 30 53.66 59.54 4.49 o -2 2 2 28 53.66 59.54 4.49 o 1 -3 -2 30 43.76 52.65 6.98 o -2 3 2 28 43.76 52.65 6.98 o 1 6 -3 27 232.99 254.37 14.53 o -2 -6 3 28 232.99 254.37 14.53 o 1 5 -3 27 29.29 34.80 8.21 o -2 -5 3 28 29.29 34.80 8.21 o 1 4 -3 28 4.36 10.43 5.06 < -2 -4 3 28 4.36 10.43 5.06 < 1 3 -3 28 2.89 2.00 2.24 < -2 -3 3 28 2.89 2.00 2.24 < 1 2 -3 29 347.90 281.60 15.29 o -2 -2 3 28 347.90 281.60 15.29 o 1 1 -3 29 278.32 245.34 8.73 o -2 -1 3 28 278.32 245.34 8.73 o 1 -1 -3 30 7.58 6.31 2.98 < -2 1 3 28 7.58 6.31 2.98 < 1 -2 -3 30 52.20 64.32 6.04 o -2 2 3 28 52.20 64.32 6.04 o 1 -3 -3 31 59.38 64.89 6.49 o -2 3 3 28 59.38 64.89 6.49 o 1 -4 -3 31 50.54 69.65 8.53 o -2 4 3 28 50.54 69.65 8.53 o 1 5 -4 28 3.56 20.03 4.19 o -2 -5 4 28 3.56 20.03 4.19 o 1 4 -4 28 1.14 1.46 3.92 < -2 -4 4 28 1.14 1.46 3.92 < 1 3 -4 29 415.63 361.43 34.75 o -2 -3 4 28 415.63 361.43 34.75 o 1 2 -4 29 79.17 77.44 5.43 o -2 -2 4 28 79.17 77.44 5.43 o 1 0 -4 30 48.01 37.63 3.80 o -2 0 4 28 48.01 37.63 3.80 o 1 -2 -4 31 69.15 77.46 4.66 o -2 2 4 28 69.15 77.46 4.66 o 1 -3 -4 31 165.64 200.31 10.43 o -2 3 4 28 165.64 200.31 10.43 o 1 5 -5 28 0.77 -0.44 5.77 < -2 -5 5 28 0.77 -0.44 5.77 < 1 4 -5 29 107.94 106.29 9.13 o -2 -4 5 28 107.94 106.29 9.13 o 1 3 -5 29 48.70 58.77 6.66 o -2 -3 5 28 48.70 58.77 6.66 o 1 2 -5 30 327.07 260.02 26.68 o -2 -2 5 28 327.07 260.02 26.68 o 1 1 -5 30 216.99 198.21 9.94 o -2 -1 5 28 216.99 198.21 9.94 o 1 -1 -5 31 25.31 26.09 3.55 o -2 1 5 28 25.31 26.09 3.55 o 1 -2 -5 31 29.64 38.28 8.46 o -2 2 5 28 29.64 38.28 8.46 o 1 4 -6 29 56.83 49.10 8.21 o -2 -4 6 28 56.83 49.10 8.21 o 1 3 -6 30 5.00 4.96 8.53 < -2 -3 6 28 5.00 4.96 8.53 < 1 2 -6 30 48.11 54.68 6.71 o -2 -2 6 28 48.11 54.68 6.71 o 1 0 -6 31 110.75 122.65 7.18 o -2 0 6 28 110.75 122.65 7.18 o 1 -1 7 26 140.57 162.60 8.63 o -2 1 -7 29 140.57 162.60 8.63 o 1 2 6 25 4.49 13.07 9.00 < -2 -2 -6 29 4.49 13.07 9.00 < 1 0 6 26 258.08 240.24 9.99 o -2 0 -6 29 258.08 240.24 9.99 o 1 -2 6 27 73.18 85.04 4.81 o -2 2 -6 29 73.18 85.04 4.81 o 1 -3 6 27 394.69 436.82 28.93 o -2 3 -6 29 394.69 436.82 28.93 o 1 2 5 26 73.34 84.96 8.21 o -2 -2 -5 29 73.34 84.96 8.21 o 1 1 5 26 103.09 95.05 5.20 o -2 -1 -5 29 103.09 95.05 5.20 o 1 -1 5 27 166.52 159.99 6.36 o -2 1 -5 29 166.52 159.99 6.36 o 1 -3 5 28 71.25 101.96 5.87 o -2 3 -5 29 71.25 101.96 5.87 o 1 -4 5 28 145.27 150.22 9.52 o -2 4 -5 29 145.27 150.22 9.52 o 1 3 4 26 8.00 11.00 3.23 o -2 -3 -4 29 8.00 11.00 3.23 o 1 2 4 26 148.05 158.23 6.88 o -2 -2 -4 29 148.05 158.23 6.88 o 1 1 4 27 144.51 154.34 13.24 o -2 -1 -4 29 144.51 154.34 13.24 o 1 0 4 27 4.13 2.79 1.95 < -2 0 -4 29 4.13 2.79 1.95 < 1 -2 4 28 88.52 97.44 4.27 o -2 2 -4 29 88.52 97.44 4.27 o 1 -3 4 28 616.30 621.52 26.93 o -2 3 -4 29 616.30 621.52 26.93 o 1 -5 4 29 128.78 150.00 9.25 o -2 5 -4 29 128.78 150.00 9.25 o 1 4 3 26 9.04 9.82 3.11 o -2 -4 -3 29 9.04 9.82 3.11 o 1 3 3 26 18.80 16.33 3.95 o -2 -3 -3 29 18.80 16.33 3.95 o 1 2 3 27 5.30 7.57 3.18 < -2 -2 -3 29 5.30 7.57 3.18 < 1 1 3 27 325.27 316.64 9.00 o -2 -1 -3 29 325.27 316.64 9.00 o 1 -1 3 28 398.23 386.51 10.48 o -2 1 -3 29 398.23 386.51 10.48 o 1 -2 3 28 387.39 378.67 17.34 o -2 2 -3 29 387.39 378.67 17.34 o 1 -3 3 29 162.06 171.23 7.42 o -2 3 -3 29 162.06 171.23 7.42 o 1 -4 3 29 232.03 232.79 9.74 o -2 4 -3 29 232.03 232.79 9.74 o 1 5 2 26 5.17 2.64 2.81 < -2 -5 -2 29 5.17 2.64 2.81 < 1 4 2 26 16.04 22.96 9.30 < -2 -4 -2 29 16.04 22.96 9.30 < 1 3 2 27 7.00 4.59 2.42 < -2 -3 -2 29 7.00 4.59 2.42 < 1 2 2 27 126.23 117.61 4.29 o -2 -2 -2 29 126.23 117.61 4.29 o 1 0 2 28 90.24 82.72 3.08 o -2 0 -2 29 90.24 82.72 3.08 o 1 -2 2 29 158.76 186.87 5.65 o -2 2 -2 29 158.76 186.87 5.65 o 1 -3 2 29 248.07 265.52 7.74 o -2 3 -2 29 248.07 265.52 7.74 o 1 -5 2 30 51.46 40.47 4.49 o -2 5 -2 29 51.46 40.47 4.49 o 1 5 1 26 25.65 32.36 9.45 o -2 -5 -1 29 25.65 32.36 9.45 o 1 4 1 27 30.07 28.14 3.28 o -2 -4 -1 29 30.07 28.14 3.28 o 1 3 1 27 27.59 24.02 2.81 o -2 -3 -1 29 27.59 24.02 2.81 o 1 2 1 28 193.47 170.71 8.36 o -2 -2 -1 29 193.47 170.71 8.36 o 1 1 1 28 113.26 103.36 3.55 o -2 -1 -1 29 113.26 103.36 3.55 o 1 -1 1 29 1044.62 1077.73 24.34 o -2 1 -1 29 1044.62 1077.73 24.34 o 1 -2 1 29 280.11 320.14 10.97 o -2 2 -1 29 280.11 320.14 10.97 o 1 -3 1 30 270.68 305.94 9.37 o -2 3 -1 29 270.68 305.94 9.37 o 1 -4 1 30 1.48 8.36 3.26 < -2 4 -1 29 1.48 8.36 3.26 < 1 5 0 27 229.50 261.20 10.33 o -2 -5 0 29 229.50 261.20 10.33 o 1 4 0 27 22.94 19.88 4.02 o -2 -4 0 29 22.94 19.88 4.02 o 1 3 0 28 160.23 173.52 8.41 o -2 -3 0 29 160.23 173.52 8.41 o 1 2 0 28 72.80 77.54 3.18 o -2 -2 0 29 72.80 77.54 3.18 o 1 0 0 29 1.25 4.46 1.38 o -2 0 0 29 1.25 4.46 1.38 o 1 -2 0 30 257.46 273.01 6.98 o -2 2 0 29 257.46 273.01 6.98 o 1 -3 0 30 19.72 23.58 2.61 o -2 3 0 29 19.72 23.58 2.61 o 1 -4 0 31 337.22 390.16 27.23 o -2 4 0 29 337.22 390.16 27.23 o 1 -5 0 31 113.47 104.89 8.19 o -2 5 0 29 113.47 104.89 8.19 o 1 6 -1 27 11.74 14.48 7.47 < -2 -6 1 29 11.74 14.48 7.47 < 1 5 -1 27 102.71 98.01 12.90 o -2 -5 1 29 102.71 98.01 12.90 o 1 4 -1 28 222.33 239.40 9.00 o -2 -4 1 29 222.33 239.40 9.00 o 1 3 -1 28 55.14 60.74 3.35 o -2 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159.39 8.16 o -2 -3 3 29 156.38 159.39 8.16 o 1 2 -3 30 241.20 209.51 12.55 o -2 -2 3 29 241.20 209.51 12.55 o 1 1 -3 30 473.85 398.94 12.97 o -2 -1 3 29 473.85 398.94 12.97 o 1 -1 -3 31 19.67 18.18 4.12 o -2 1 3 29 19.67 18.18 4.12 o 1 -2 -3 31 641.07 735.11 30.85 o -2 2 3 29 641.07 735.11 30.85 o 1 -3 -3 32 27.59 44.47 9.25 o -2 3 3 29 27.59 44.47 9.25 o 1 5 -4 29 134.97 147.19 10.09 o -2 -5 4 29 134.97 147.19 10.09 o 1 4 -4 29 389.07 359.85 23.63 o -2 -4 4 29 389.07 359.85 23.63 o 1 3 -4 30 181.41 127.70 17.09 o -2 -3 4 29 181.41 127.70 17.09 o 1 2 -4 30 212.26 218.34 9.96 o -2 -2 4 29 212.26 218.34 9.96 o 1 0 -4 31 8.06 6.34 2.96 < -2 0 4 29 8.06 6.34 2.96 < 1 -2 -4 32 63.00 74.46 4.76 o -2 2 4 29 63.00 74.46 4.76 o 1 -3 -4 32 286.84 347.30 20.94 o -2 3 4 29 286.84 347.30 20.94 o 1 5 -5 29 51.11 46.83 8.63 o -2 -5 5 29 51.11 46.83 8.63 o 1 4 -5 30 26.15 29.87 6.07 o -2 -4 5 29 26.15 29.87 6.07 o 1 3 -5 30 162.78 164.01 11.49 o -2 -3 5 29 162.78 164.01 11.49 o 1 2 -5 31 6.36 13.52 9.62 < -2 -2 5 29 6.36 13.52 9.62 < 1 1 -5 31 371.80 359.09 15.51 o -2 -1 5 29 371.80 359.09 15.51 o 1 -1 -5 32 9.53 4.49 2.96 < -2 1 5 29 9.53 4.49 2.96 < 1 -2 -5 32 63.55 67.65 10.21 o -2 2 5 29 63.55 67.65 10.21 o 1 3 -6 31 29.17 25.38 10.09 < -2 -3 6 29 29.17 25.38 10.09 < 1 2 -6 31 49.86 58.52 7.03 o -2 -2 6 29 49.86 58.52 7.03 o 1 0 -6 32 28.51 29.35 4.17 o -2 0 6 29 28.51 29.35 4.17 o 1 0 6 27 256.59 239.70 10.06 o -2 0 -6 30 256.59 239.70 10.06 o 1 -2 6 28 51.08 58.23 4.27 o -2 2 -6 30 51.08 58.23 4.27 o 1 -3 6 28 7.39 19.31 7.00 < -2 3 -6 30 7.39 19.31 7.00 < 1 2 5 27 60.36 62.25 7.42 o -2 -2 -5 30 60.36 62.25 7.42 o 1 1 5 27 136.91 142.67 6.58 o -2 -1 -5 30 136.91 142.67 6.58 o 1 -1 5 28 219.13 223.81 8.06 o -2 1 -5 30 219.13 223.81 8.06 o 1 -3 5 29 112.13 128.17 8.04 o -2 3 -5 30 112.13 128.17 8.04 o 1 -4 5 29 31.91 36.70 5.08 o -2 4 -5 30 31.91 36.70 5.08 o 1 3 4 27 87.58 92.68 5.43 o -2 -3 -4 30 87.58 92.68 5.43 o 1 2 4 27 54.69 53.42 4.14 o -2 -2 -4 30 54.69 53.42 4.14 o 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591.60 594.37 14.30 o 1 -3 2 30 16.19 14.60 2.71 o -2 3 -2 30 16.19 14.60 2.71 o 1 -5 2 31 10.67 9.64 3.65 < -2 5 -2 30 10.67 9.64 3.65 < 1 5 1 27 14.55 20.32 8.68 < -2 -5 -1 30 14.55 20.32 8.68 < 1 4 1 28 4.36 4.37 3.43 < -2 -4 -1 30 4.36 4.37 3.43 < 1 3 1 28 151.01 142.72 5.92 o -2 -3 -1 30 151.01 142.72 5.92 o 1 2 1 29 244.67 210.82 8.11 o -2 -2 -1 30 244.67 210.82 8.11 o 1 1 1 29 523.30 497.59 11.44 o -2 -1 -1 30 523.30 497.59 11.44 o 1 -1 1 30 368.04 417.27 10.41 o -2 1 -1 30 368.04 417.27 10.41 o 1 -2 1 30 77.73 78.57 5.43 o -2 2 -1 30 77.73 78.57 5.43 o 1 -3 1 31 376.49 407.13 11.44 o -2 3 -1 30 376.49 407.13 11.44 o 1 -4 1 31 88.08 91.20 5.89 o -2 4 -1 30 88.08 91.20 5.89 o 1 5 0 28 2.66 6.54 3.08 < -2 -5 0 30 2.66 6.54 3.08 < 1 4 0 28 218.81 209.43 9.54 o -2 -4 0 30 218.81 209.43 9.54 o 1 3 0 29 23.59 29.59 4.00 o -2 -3 0 30 23.59 29.59 4.00 o 1 2 0 29 377.16 368.80 8.88 o -2 -2 0 30 377.16 368.80 8.88 o 1 0 0 30 1171.98 1165.23 22.66 o -2 0 0 30 1171.98 1165.23 22.66 o 1 -2 0 31 643.32 655.31 14.35 o -2 2 0 30 643.32 655.31 14.35 o 1 -3 0 31 108.88 109.38 5.28 o -2 3 0 30 108.88 109.38 5.28 o 1 -5 0 32 2.66 13.79 4.69 < -2 5 0 30 2.66 13.79 4.69 < 1 6 -1 28 32.33 17.31 10.16 < -2 -6 1 30 32.33 17.31 10.16 < 1 5 -1 28 158.69 154.44 16.47 o -2 -5 1 30 158.69 154.44 16.47 o 1 4 -1 29 2.05 6.14 2.81 < -2 -4 1 30 2.05 6.14 2.81 < 1 3 -1 29 282.27 273.14 8.09 o -2 -3 1 30 282.27 273.14 8.09 o 1 2 -1 30 90.99 78.13 5.43 o -2 -2 1 30 90.99 78.13 5.43 o 1 1 -1 30 415.34 392.36 9.74 o -2 -1 1 30 415.34 392.36 9.74 o 1 -1 -1 31 477.73 486.57 12.90 o -2 1 1 30 477.73 486.57 12.90 o 1 -2 -1 31 155.04 166.84 6.88 o -2 2 1 30 155.04 166.84 6.88 o 1 -3 -1 32 542.64 421.85 34.35 o -2 3 1 30 542.64 421.85 34.35 o 1 -4 -1 32 19.41 37.12 5.85 o -2 4 1 30 19.41 37.12 5.85 o 1 5 -2 29 34.52 38.72 5.38 o -2 -5 2 30 34.52 38.72 5.38 o 1 4 -2 29 160.04 153.92 7.77 o -2 -4 2 30 160.04 153.92 7.77 o 1 3 -2 30 15.12 17.39 4.59 o -2 -3 2 30 15.12 17.39 4.59 o 1 2 -2 30 613.49 530.54 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7.94 o 1 -1 -3 39 59.39 65.43 7.82 o -2 1 3 37 59.39 65.43 7.82 o 1 2 -4 38 25.48 36.53 5.50 o -2 -2 4 37 25.48 36.53 5.50 o 1 0 4 36 95.38 100.11 5.20 o -2 0 -4 38 95.38 100.11 5.20 o 1 -2 4 37 22.11 33.98 7.92 o -2 2 -4 38 22.11 33.98 7.92 o 1 1 3 36 109.28 100.43 5.23 o -2 -1 -3 38 109.28 100.43 5.23 o 1 -1 3 37 251.93 230.10 11.10 o -2 1 -3 38 251.93 230.10 11.10 o 1 -2 3 37 50.10 49.92 8.73 o -2 2 -3 38 50.10 49.92 8.73 o 1 2 2 36 395.80 416.48 12.50 o -2 -2 -2 38 395.80 416.48 12.50 o 1 0 2 37 338.69 318.07 13.79 o -2 0 -2 38 338.69 318.07 13.79 o 1 -2 2 38 344.38 356.84 13.07 o -2 2 -2 38 344.38 356.84 13.07 o 1 -3 2 38 8.87 13.89 3.55 o -2 3 -2 38 8.87 13.89 3.55 o 1 3 1 36 276.12 312.57 11.34 o -2 -3 -1 38 276.12 312.57 11.34 o 1 2 1 37 140.01 149.36 9.32 o -2 -2 -1 38 140.01 149.36 9.32 o 1 1 1 37 254.66 249.04 9.03 o -2 -1 -1 38 254.66 249.04 9.03 o 1 -1 1 38 293.17 292.64 12.08 o -2 1 -1 38 293.17 292.64 12.08 o 1 -2 1 38 3.02 9.84 5.45 < -2 2 -1 38 3.02 9.84 5.45 < 1 -3 1 39 355.97 342.86 11.96 o -2 3 -1 38 355.97 342.86 11.96 o 1 3 0 37 42.38 49.25 7.40 o -2 -3 0 38 42.38 49.25 7.40 o 1 2 0 37 311.16 322.83 12.73 o -2 -2 0 38 311.16 322.83 12.73 o 1 0 0 38 1462.47 1441.47 46.76 o -2 0 0 38 1462.47 1441.47 46.76 o 1 -2 0 39 129.83 134.68 7.87 o -2 2 0 38 129.83 134.68 7.87 o 1 -3 0 39 0.65 6.63 10.80 < -2 3 0 38 0.65 6.63 10.80 < 1 3 -1 37 324.12 323.70 14.13 o -2 -3 1 38 324.12 323.70 14.13 o 1 2 -1 38 3.05 1.58 4.74 < -2 -2 1 38 3.05 1.58 4.74 < 1 1 -1 38 262.78 241.72 14.43 o -2 -1 1 38 262.78 241.72 14.43 o 1 -1 -1 39 149.76 141.32 8.04 o -2 1 1 38 149.76 141.32 8.04 o 1 -2 -1 39 106.09 135.20 12.21 o -2 2 1 38 106.09 135.20 12.21 o 1 3 -2 37 8.53 4.78 9.27 < -2 -3 2 38 8.53 4.78 9.27 < 1 3 -2 38 10.33 6.04 3.80 < -2 -3 2 38 10.33 6.04 3.80 < 1 2 -2 38 325.99 315.51 13.71 o -2 -2 2 38 325.99 315.51 13.71 o 1 0 -2 39 87.41 100.38 7.15 o -2 0 2 38 87.41 100.38 7.15 o 1 2 -3 39 41.24 39.48 12.68 o -2 -2 3 38 41.24 39.48 12.68 o 1 1 -3 39 34.40 35.19 4.51 o -2 -1 3 38 34.40 35.19 4.51 o 1 1 3 37 61.24 61.43 4.37 o -2 -1 -3 39 61.24 61.43 4.37 o 1 -1 3 38 30.68 27.52 4.64 o -2 1 -3 39 30.68 27.52 4.64 o 1 -2 3 38 35.96 56.03 8.53 o -2 2 -3 39 35.96 56.03 8.53 o 1 2 2 37 10.54 17.21 3.16 o -2 -2 -2 39 10.54 17.21 3.16 o 1 0 2 38 59.34 71.64 5.89 o -2 0 -2 39 59.34 71.64 5.89 o 1 -2 2 39 35.03 22.27 3.92 o -2 2 -2 39 35.03 22.27 3.92 o 1 2 1 38 153.97 172.88 10.36 o -2 -2 -1 39 153.97 172.88 10.36 o 1 1 1 38 120.92 102.42 5.28 o -2 -1 -1 39 120.92 102.42 5.28 o 1 -1 1 39 40.20 34.28 4.44 o -2 1 -1 39 40.20 34.28 4.44 o 1 -2 1 39 76.03 90.76 9.10 o -2 2 -1 39 76.03 90.76 9.10 o 1 3 0 38 0.47 -2.15 4.88 < -2 -3 0 39 0.47 -2.15 4.88 < 1 2 0 38 88.41 89.72 5.97 o -2 -2 0 39 88.41 89.72 5.97 o 1 0 0 39 17.48 33.27 4.00 o -2 0 0 39 17.48 33.27 4.00 o 1 -2 0 40 24.60 18.15 4.39 o -2 2 0 39 24.60 18.15 4.39 o 1 3 -1 38 254.65 245.27 11.74 o -2 -3 1 39 254.65 245.27 11.74 o 1 2 -1 39 70.08 72.29 8.21 o -2 -2 1 39 70.08 72.29 8.21 o 1 1 -1 39 33.58 19.58 5.18 o -2 -1 1 39 33.58 19.58 5.18 o 1 -1 -1 40 18.91 25.70 4.14 o -2 1 1 39 18.91 25.70 4.14 o 1 -2 -1 40 61.95 73.20 9.59 o -2 2 1 39 61.95 73.20 9.59 o 1 2 -2 39 23.83 18.52 4.39 o -2 -2 2 39 23.83 18.52 4.39 o 1 0 -2 40 15.45 9.64 3.06 o -2 0 2 39 15.45 9.64 3.06 o 1 1 -3 40 34.98 34.45 4.96 o -2 -1 3 39 34.98 34.45 4.96 o 1 -1 3 39 38.22 41.38 5.38 o -2 1 -3 40 38.22 41.38 5.38 o 1 0 2 39 10.34 9.62 3.87 < -2 0 -2 40 10.34 9.62 3.87 < 1 -2 2 40 51.30 42.10 5.11 o -2 2 -2 40 51.30 42.10 5.11 o 1 2 1 39 59.70 54.50 6.29 o -2 -2 -1 40 59.70 54.50 6.29 o 1 1 1 39 14.32 22.22 3.85 o -2 -1 -1 40 14.32 22.22 3.85 o 1 -1 1 40 7.27 10.78 3.85 < -2 1 -1 40 7.27 10.78 3.85 < 1 -2 1 40 57.86 66.91 7.94 o -2 2 -1 40 57.86 66.91 7.94 o 1 2 0 39 36.59 29.35 4.34 o -2 -2 0 40 36.59 29.35 4.34 o 1 0 0 40 29.43 36.57 4.14 o -2 0 0 40 29.43 36.57 4.14 o 1 -2 0 41 84.66 72.68 15.69 o -2 2 0 40 84.66 72.68 15.69 o 1 2 -1 40 60.29 44.44 7.28 o -2 -2 1 40 60.29 44.44 7.28 o 1 1 -1 40 6.20 13.47 4.91 < -2 -1 1 40 6.20 13.47 4.91 < 1 -1 -1 41 36.76 39.29 4.86 o -2 1 1 40 36.76 39.29 4.86 o 1 2 -2 40 51.39 46.24 5.62 o -2 -2 2 40 51.39 46.24 5.62 o 1 0 -2 41 1.89 4.98 3.28 < -2 0 2 40 1.89 4.98 3.28 < 1 0 2 40 1.53 3.21 3.63 < -2 0 -2 41 1.53 3.21 3.63 < 1 1 1 40 33.33 38.05 4.83 o -2 -1 -1 41 33.33 38.05 4.83 o 1 -1 1 41 57.84 76.21 5.85 o -2 1 -1 41 57.84 76.21 5.85 o 1 2 0 40 76.34 67.58 10.65 o -2 -2 0 41 76.34 67.58 10.65 o 1 0 0 41 0.03 2.74 3.11 < -2 0 0 41 0.03 2.74 3.11 < 1 1 -1 41 67.75 53.10 6.81 o -2 -1 1 41 67.75 53.10 6.81 o 1 0 0 42 192.71 199.96 17.78 o -2 0 0 42 192.71 199.96 17.78 o 1