#------------------------------------------------------------------------------ #$Date: 2016-12-02 04:09:55 +0200 (Fri, 02 Dec 2016) $ #$Revision: 188821 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/80/2108023.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108023 _cell_angle_alpha 90.000 _cell_angle_beta 101.367 _cell_angle_gamma 90.000 _cell_length_a 15.9394 _cell_length_b 5.0180 _cell_length_c 12.9310 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7903 _cod_data_source_file eb5052M155sup3.hkl _cod_data_source_block M155 _shelx_title ' M155_1a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 139.05 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7006.50 1933.24 1495.98 o 3 0 0 344.05 327.85 2.43 o 4 0 0 382.57 411.39 4.24 o 5 0 0 6282.09 5798.17 13.52 o 6 0 0 2802.80 2778.80 15.27 o 7 0 0 1458.67 1369.36 12.35 o 8 0 0 1422.03 1687.33 13.27 o 9 0 0 895.94 986.93 7.44 o 10 0 0 887.81 829.92 8.34 o 11 0 0 8.95 12.92 1.29 o 12 0 0 1.40 4.94 1.02 o 13 0 0 625.72 638.79 8.91 o 14 0 0 676.97 671.27 20.57 o 15 0 0 782.35 848.23 17.76 o 16 0 0 95.01 115.84 5.44 o 17 0 0 211.94 189.78 9.12 o 18 0 0 30.65 35.58 4.69 o 19 0 0 85.31 86.47 7.68 o 1 1 0 1245.14 1236.95 7.44 o 2 1 0 5.85 14.65 0.51 o 3 1 0 7.20 4.19 0.57 o 4 1 0 701.86 729.86 5.18 o 5 1 0 565.21 582.98 4.37 o 6 1 0 1551.83 1551.49 10.33 o 7 1 0 0.41 0.52 0.25 o 8 1 0 864.06 918.32 6.37 o 9 1 0 25.37 20.76 0.70 o 10 1 0 17.26 20.02 0.78 o 11 1 0 24.50 22.33 1.12 o 12 1 0 227.48 215.26 3.94 o 13 1 0 0.03 -0.50 0.63 o 14 1 0 0.70 0.01 0.67 o 15 1 0 46.26 41.69 1.99 o 16 1 0 36.20 30.18 1.82 o 17 1 0 56.68 51.25 2.90 o 18 1 0 3.04 3.12 1.23 o 19 1 0 47.90 60.97 4.60 o 0 2 0 5772.54 5482.23 22.03 o 1 2 0 4202.23 4110.32 15.86 o 2 2 0 207.60 182.00 1.97 o 3 2 0 810.83 840.22 4.39 o 4 2 0 273.11 293.85 2.92 o 5 2 0 800.32 771.55 5.47 o 6 2 0 533.49 525.23 4.25 o 7 2 0 451.74 430.24 4.02 o 8 2 0 55.94 61.54 1.51 o 9 2 0 50.87 48.07 1.39 o 10 2 0 18.89 17.50 0.92 o 11 2 0 505.12 508.08 6.80 o 12 2 0 872.85 896.22 8.55 o 13 2 0 67.83 71.33 2.56 o 14 2 0 308.16 322.74 6.35 o 15 2 0 267.75 270.75 6.36 o 16 2 0 135.66 142.56 4.57 o 17 2 0 11.64 13.76 2.55 o 18 2 0 28.60 34.39 2.89 o 1 3 0 162.89 168.72 2.27 o 2 3 0 152.98 148.39 2.48 o 3 3 0 34.96 32.77 1.31 o 4 3 0 2299.35 2470.57 10.96 o 5 3 0 937.10 967.43 7.99 o 6 3 0 2.57 2.63 0.65 o 7 3 0 515.46 510.21 5.28 o 8 3 0 0.27 0.39 0.58 o 9 3 0 314.63 310.57 4.72 o 10 3 0 265.18 272.83 4.64 o 11 3 0 9.57 8.82 1.30 o 12 3 0 528.11 557.92 11.98 o 13 3 0 456.83 449.20 7.76 o 14 3 0 39.82 40.49 2.50 o 15 3 0 0.42 -0.05 1.41 o 16 3 0 20.88 21.28 2.35 o 17 3 0 1.59 1.18 1.63 o 0 4 0 322.43 315.70 7.85 o 1 4 0 293.55 290.41 5.34 o 2 4 0 62.19 65.09 2.59 o 3 4 0 22.42 24.12 1.34 o 4 4 0 167.38 181.01 3.47 o 5 4 0 267.12 276.62 4.34 o 6 4 0 462.30 460.31 5.26 o 7 4 0 366.52 359.20 4.73 o 8 4 0 767.99 774.45 7.05 o 9 4 0 338.82 334.94 4.75 o 10 4 0 149.97 136.35 3.73 o 11 4 0 13.87 15.26 1.65 o 12 4 0 34.97 32.32 2.70 o 13 4 0 235.01 246.46 7.27 o 14 4 0 201.74 200.91 6.77 o 15 4 0 98.49 97.68 8.13 o 1 5 0 71.60 71.87 3.15 o 2 5 0 93.17 103.32 3.73 o 3 5 0 142.27 157.08 4.58 o 4 5 0 19.49 27.64 2.02 o 5 5 0 1.49 1.38 0.82 o 6 5 0 17.60 16.07 2.14 o 7 5 0 23.89 26.54 2.09 o 8 5 0 83.70 80.39 3.45 o 9 5 0 28.21 32.16 2.31 o 10 5 0 0.03 -1.03 1.09 o 11 5 0 0.00 1.94 1.70 o 0 6 0 146.40 129.78 9.83 o 1 6 0 376.57 415.68 12.21 o 2 6 0 179.14 180.18 9.23 o 3 6 0 24.82 31.34 3.48 o 4 6 0 15.60 10.97 3.06 o -19 1 1 128.77 139.58 7.28 o -18 1 1 73.05 86.20 3.65 o -17 1 1 144.15 149.32 4.12 o -16 1 1 243.43 227.52 4.87 o -15 1 1 0.78 3.22 0.81 o -14 1 1 109.76 104.97 3.08 o -13 1 1 130.07 119.06 3.17 o -12 1 1 495.46 489.70 6.02 o -11 1 1 173.67 177.01 3.45 o -10 1 1 119.46 102.27 1.96 o -9 1 1 66.89 59.90 1.16 o -8 1 1 3954.22 3952.99 17.47 o -7 1 1 239.90 245.95 1.97 o -6 1 1 4838.43 4644.68 17.30 o -5 1 1 95.20 149.69 1.53 o -4 1 1 145.42 107.76 1.37 o -3 1 1 12767.45 11309.55 51.73 o -2 1 1 10954.65 10431.40 33.70 o -1 1 1 5371.60 5379.55 11.71 o 0 1 1 813.42 714.38 4.62 o 1 1 1 4774.77 4733.08 19.50 o 2 1 1 2148.55 2037.49 14.25 o 3 1 1 1066.56 1110.37 8.75 o 4 1 1 191.59 158.54 1.81 o 5 1 1 149.61 131.40 1.62 o 6 1 1 10.53 29.84 0.84 o 7 1 1 749.08 684.69 3.86 o 8 1 1 47.48 54.86 1.17 o 9 1 1 347.14 363.89 3.11 o 10 1 1 978.73 955.13 5.26 o 11 1 1 1116.84 1136.26 10.35 o 12 1 1 1482.62 1487.86 18.34 o 13 1 1 927.35 915.04 11.58 o 14 1 1 65.39 74.94 2.57 o 15 1 1 13.02 9.64 1.28 o 16 1 1 0.01 -0.79 0.79 o 17 1 1 69.00 72.42 3.25 o 18 1 1 68.74 64.73 4.77 o 19 1 1 38.00 48.70 5.86 o -18 2 1 10.61 10.90 1.85 o -17 2 1 2.03 2.73 1.05 o -16 2 1 192.71 171.90 5.00 o -15 2 1 20.59 23.22 2.58 o -14 2 1 4.61 4.26 1.07 o -13 2 1 14.02 17.41 1.61 o -12 2 1 933.18 938.09 14.84 o -11 2 1 346.25 349.42 5.91 o -10 2 1 139.77 144.40 3.13 o -9 2 1 156.41 152.83 2.25 o -8 2 1 419.81 429.02 3.61 o -7 2 1 173.58 206.94 2.55 o -6 2 1 0.17 2.00 0.35 o -5 2 1 13.51 15.28 0.67 o -4 2 1 80.27 86.77 1.43 o -3 2 1 767.10 786.64 3.71 o -2 2 1 12.68 14.96 0.64 o -1 2 1 1625.14 1659.20 9.09 o 0 2 1 1510.44 1608.39 4.93 o 1 2 1 3521.96 3743.83 17.88 o 2 2 1 2766.21 2771.60 15.09 o 3 2 1 1342.39 1414.75 9.74 o 4 2 1 30.52 42.58 1.10 o 5 2 1 64.20 79.14 1.68 o 6 2 1 227.64 228.00 2.92 o 7 2 1 2.07 2.45 0.46 o 8 2 1 0.03 0.44 0.35 o 9 2 1 92.64 84.30 1.88 o 10 2 1 108.21 118.11 2.30 o 11 2 1 165.05 167.64 3.94 o 12 2 1 179.43 184.23 4.32 o 13 2 1 1.82 2.24 0.90 o 14 2 1 13.03 13.89 1.44 o 15 2 1 0.44 0.15 0.74 o 16 2 1 32.54 31.75 2.23 o 17 2 1 41.62 49.60 3.34 o 18 2 1 14.17 23.93 4.75 o -17 3 1 228.23 251.52 13.00 o -16 3 1 223.79 227.82 7.13 o -15 3 1 100.57 106.38 4.72 o -14 3 1 0.16 -0.24 1.16 o -13 3 1 72.81 69.80 3.14 o -12 3 1 202.91 197.00 5.00 o -11 3 1 212.23 216.38 5.05 o -10 3 1 521.69 529.79 7.61 o -9 3 1 515.24 508.08 5.48 o -8 3 1 535.32 537.53 5.53 o -7 3 1 367.21 370.32 4.50 o -6 3 1 34.37 34.96 1.30 o -5 3 1 91.56 88.15 1.97 o -4 3 1 1315.32 1259.90 9.53 o -3 3 1 2252.56 2272.38 11.88 o -2 3 1 2340.16 2413.48 9.85 o -1 3 1 1573.84 1615.93 7.34 o 0 3 1 546.98 536.16 5.90 o 1 3 1 2.42 2.71 0.36 o 2 3 1 316.23 326.37 3.62 o 3 3 1 799.50 800.22 6.82 o 4 3 1 1415.08 1443.56 8.40 o 5 3 1 1401.00 1420.86 8.47 o 6 3 1 1567.68 1545.18 9.38 o 7 3 1 758.37 764.74 6.50 o 8 3 1 361.01 353.59 5.02 o 9 3 1 2.81 3.24 0.64 o 10 3 1 121.11 126.57 2.91 o 11 3 1 510.39 519.93 8.83 o 12 3 1 383.32 383.27 7.88 o 13 3 1 355.46 357.73 8.69 o 14 3 1 123.84 124.29 4.57 o 15 3 1 18.66 20.23 2.65 o 16 3 1 1.69 4.49 2.84 o -14 4 1 56.42 51.94 3.47 o -13 4 1 21.51 20.94 2.35 o -12 4 1 123.41 124.69 4.33 o -11 4 1 106.76 113.57 3.60 o -10 4 1 21.36 21.43 1.88 o -9 4 1 71.26 74.64 2.48 o -8 4 1 353.65 349.76 4.72 o -7 4 1 234.04 222.15 3.70 o -6 4 1 82.08 83.21 2.27 o -5 4 1 39.93 35.06 1.62 o -4 4 1 69.53 75.92 2.50 o -3 4 1 299.72 312.99 4.84 o -2 4 1 62.13 60.08 2.52 o -1 4 1 24.34 22.63 1.60 o 0 4 1 42.99 46.74 2.24 o 1 4 1 112.30 122.48 3.17 o 2 4 1 43.83 53.89 2.80 o 3 4 1 1.00 2.56 0.74 o 4 4 1 167.46 185.06 3.92 o 5 4 1 32.91 28.90 1.63 o 6 4 1 49.00 50.30 1.94 o 7 4 1 3.07 1.96 0.64 o 8 4 1 84.41 81.68 2.52 o 9 4 1 0.51 1.52 0.77 o 10 4 1 234.39 228.98 5.41 o 11 4 1 23.87 22.98 2.01 o 12 4 1 9.89 4.64 1.34 o 13 4 1 0.02 -0.36 0.95 o 14 4 1 16.87 17.35 2.17 o 15 4 1 1.29 -2.08 2.08 o -11 5 1 213.10 208.17 8.33 o -10 5 1 138.93 136.60 6.68 o -9 5 1 193.21 196.52 5.40 o -8 5 1 0.05 1.23 1.02 o -7 5 1 109.69 107.02 4.52 o -6 5 1 36.11 36.67 2.35 o -5 5 1 46.83 49.60 2.63 o -4 5 1 196.99 188.74 5.04 o -3 5 1 52.79 57.30 2.82 o -2 5 1 11.06 14.53 1.96 o -1 5 1 28.80 33.55 2.20 o 0 5 1 193.69 208.18 5.20 o 1 5 1 139.49 145.69 4.40 o 2 5 1 10.64 12.57 1.40 o 3 5 1 76.01 82.37 3.37 o 4 5 1 199.80 203.91 4.70 o 5 5 1 223.87 230.88 7.02 o 6 5 1 298.48 315.35 6.74 o 7 5 1 77.07 76.81 3.95 o 8 5 1 9.68 5.72 1.14 o 9 5 1 10.25 11.72 1.61 o 10 5 1 14.44 13.82 1.93 o 11 5 1 67.50 72.97 6.92 o -5 6 1 16.81 9.41 2.94 o -4 6 1 17.97 17.50 2.78 o -3 6 1 33.32 29.03 3.42 o -2 6 1 23.44 26.92 3.34 o -1 6 1 12.83 16.29 2.82 o 0 6 1 33.33 30.61 3.40 o 1 6 1 41.19 42.10 4.05 o 2 6 1 41.71 35.94 4.58 o 3 6 1 8.15 4.20 2.13 o -19 0 2 137.41 142.00 9.85 o -18 0 2 37.19 48.24 5.57 o -17 0 2 10.61 8.94 2.01 o -16 0 2 300.06 270.49 8.39 o -15 0 2 280.84 271.16 6.33 o -14 0 2 673.39 645.58 10.76 o -13 0 2 368.00 367.56 7.82 o -12 0 2 432.30 440.35 7.09 o -11 0 2 1226.66 1255.69 22.50 o -10 0 2 798.29 869.36 17.04 o -9 0 2 3090.37 3107.65 26.36 o -8 0 2 182.80 175.81 3.53 o -7 0 2 581.44 701.95 7.90 o -6 0 2 2038.10 1692.03 9.67 o -5 0 2 381.72 279.14 3.68 o -4 0 2 7189.46 6863.02 68.51 o -3 0 2 7490.87 7168.08 23.01 o -2 0 2 2768.53 2712.21 36.78 o -1 0 2 4.31 5.98 0.80 o 0 0 2 982.64 824.20 32.53 o 1 0 2 6137.34 5965.47 53.51 o 2 0 2 13317.02 12053.04 63.94 o 3 0 2 6026.29 5368.21 23.95 o 4 0 2 14110.13 11998.61 38.51 o 5 0 2 0.24 5.70 1.61 o 6 0 2 8469.38 8669.54 57.83 o 7 0 2 2893.92 2949.28 25.03 o 8 0 2 686.34 742.04 6.41 o 9 0 2 3217.78 3131.83 20.35 o 10 0 2 1741.82 1678.72 19.85 o 11 0 2 2552.36 2605.80 30.16 o 12 0 2 257.59 279.80 4.89 o 13 0 2 353.09 371.55 6.97 o 14 0 2 180.11 136.44 5.67 o 15 0 2 604.36 545.30 15.80 o 16 0 2 137.92 142.37 8.53 o -19 1 2 12.84 17.42 2.26 o -18 1 2 19.00 24.98 2.42 o -17 1 2 0.11 2.07 1.10 o -16 1 2 88.67 88.39 3.09 o -15 1 2 7.86 10.80 1.20 o -14 1 2 19.39 23.95 1.58 o -13 1 2 474.98 473.83 7.13 o -12 1 2 37.34 38.34 1.77 o -11 1 2 266.23 270.72 4.30 o -10 1 2 128.96 127.45 2.53 o -9 1 2 329.08 348.14 3.82 o -8 1 2 2367.24 2314.41 14.64 o -7 1 2 117.91 121.52 1.45 o -6 1 2 89.61 104.89 1.29 o -5 1 2 1189.92 1174.61 9.06 o -4 1 2 20.85 29.01 0.66 o -3 1 2 149.81 152.61 2.46 o -2 1 2 4995.80 4939.58 10.68 o -1 1 2 3964.39 3957.62 13.41 o 0 1 2 11.03 17.20 0.44 o 1 1 2 246.64 230.01 2.18 o 2 1 2 974.94 910.97 5.84 o 3 1 2 1490.66 1521.38 7.72 o 4 1 2 41.11 47.66 1.04 o 5 1 2 1767.96 1699.22 10.16 o 6 1 2 12.81 15.78 0.63 o 7 1 2 1820.20 1911.76 9.21 o 8 1 2 64.07 58.38 1.19 o 9 1 2 37.36 34.20 0.97 o 10 1 2 0.79 1.31 0.38 o 11 1 2 102.61 104.58 1.82 o 12 1 2 61.62 57.55 1.88 o 13 1 2 79.39 67.36 2.66 o 14 1 2 1.22 2.04 1.42 o 15 1 2 14.11 11.59 1.33 o 16 1 2 0.27 -1.44 1.50 o 17 1 2 14.52 15.30 3.45 o -18 2 2 160.99 160.28 6.00 o -17 2 2 16.34 14.89 2.06 o -16 2 2 0.82 2.08 1.11 o -15 2 2 16.42 13.97 1.43 o -14 2 2 216.89 211.22 5.18 o -13 2 2 127.67 126.79 3.87 o -12 2 2 28.72 29.65 1.91 o -11 2 2 748.73 764.35 8.71 o -10 2 2 581.36 627.55 7.58 o -9 2 2 66.73 70.64 3.27 o -8 2 2 204.61 212.88 2.72 o -7 2 2 20.57 12.71 0.70 o -6 2 2 148.76 182.86 2.66 o -5 2 2 1747.70 1718.48 11.74 o -4 2 2 428.39 389.63 3.14 o -3 2 2 658.79 590.66 4.94 o -2 2 2 190.50 194.57 2.10 o -1 2 2 1028.37 1097.04 4.83 o 0 2 2 797.18 818.22 4.95 o 1 2 2 14.10 12.33 0.58 o 2 2 2 329.62 268.68 2.41 o 3 2 2 2783.89 2744.23 14.40 o 4 2 2 419.93 378.70 3.31 o 5 2 2 236.37 208.35 2.82 o 6 2 2 0.34 0.32 0.41 o 7 2 2 11.93 13.08 0.84 o 8 2 2 538.66 540.17 4.67 o 9 2 2 1142.30 1127.34 7.39 o 10 2 2 913.87 916.95 6.55 o 11 2 2 11.42 11.74 0.82 o 12 2 2 476.37 481.84 6.22 o 13 2 2 27.28 26.15 1.76 o 14 2 2 25.25 24.71 1.85 o 15 2 2 168.36 166.10 5.42 o 16 2 2 220.23 211.15 6.28 o 17 2 2 46.82 47.67 4.06 o -17 3 2 3.86 6.68 2.61 o -16 3 2 2.52 4.21 1.49 o -15 3 2 1.26 3.07 1.47 o -14 3 2 154.80 159.72 4.84 o -13 3 2 0.03 1.04 0.97 o -12 3 2 545.97 560.84 8.38 o -11 3 2 98.12 99.68 3.48 o -10 3 2 0.66 1.50 0.87 o -9 3 2 502.37 514.31 6.07 o -8 3 2 69.02 66.71 1.96 o -7 3 2 20.57 24.03 1.20 o -6 3 2 49.52 45.81 1.48 o -5 3 2 316.55 314.71 3.99 o -4 3 2 146.46 159.14 2.79 o -3 3 2 65.31 82.17 1.81 o -2 3 2 790.44 819.31 5.46 o -1 3 2 490.09 529.45 4.30 o 0 3 2 1863.21 1959.29 8.09 o 1 3 2 218.46 243.08 3.24 o 2 3 2 119.03 146.05 2.53 o 3 3 2 100.87 107.13 2.20 o 4 3 2 654.92 668.89 5.12 o 5 3 2 44.82 41.32 1.34 o 6 3 2 2.65 2.89 0.59 o 7 3 2 29.27 30.63 1.39 o 8 3 2 0.71 1.57 0.64 o 9 3 2 45.06 47.81 2.00 o 10 3 2 1835.88 1872.19 14.55 o 11 3 2 1166.31 1163.96 14.55 o 12 3 2 155.42 147.53 4.91 o 13 3 2 137.57 138.02 4.90 o 14 3 2 0.25 1.62 1.15 o 15 3 2 85.44 88.28 7.45 o 16 3 2 21.08 26.02 4.63 o -14 4 2 8.85 12.62 2.96 o -13 4 2 67.04 56.56 3.59 o -12 4 2 634.06 676.69 11.59 o -11 4 2 35.60 33.07 2.02 o -10 4 2 28.85 32.65 2.18 o -9 4 2 37.28 36.63 1.95 o -8 4 2 115.67 109.01 2.89 o -7 4 2 312.38 294.65 4.64 o -6 4 2 1037.82 1043.02 8.52 o -5 4 2 401.24 414.15 5.30 o -4 4 2 670.72 664.78 7.18 o -3 4 2 482.06 482.14 6.96 o -2 4 2 395.08 417.02 6.45 o -1 4 2 162.33 164.54 3.64 o 0 4 2 33.51 38.50 1.83 o 1 4 2 208.90 219.59 4.20 o 2 4 2 689.56 714.80 7.57 o 3 4 2 363.00 353.29 5.36 o 4 4 2 393.56 398.63 5.74 o 5 4 2 235.46 220.28 4.34 o 6 4 2 11.72 11.81 1.32 o 7 4 2 28.84 31.08 1.79 o 8 4 2 268.95 263.97 5.03 o 9 4 2 177.92 173.17 4.16 o 10 4 2 145.02 132.95 3.72 o 11 4 2 370.62 364.97 8.09 o 12 4 2 11.95 10.90 2.01 o 13 4 2 1.84 1.91 1.52 o 14 4 2 5.95 9.69 2.84 o -12 5 2 20.87 14.27 3.31 o -11 5 2 3.75 -1.26 2.54 o -10 5 2 6.66 5.36 2.16 o -9 5 2 74.80 68.42 3.76 o -8 5 2 55.92 58.79 2.96 o -7 5 2 25.42 27.64 2.06 o -6 5 2 52.69 49.53 2.67 o -5 5 2 114.93 115.88 4.01 o -4 5 2 10.95 7.88 1.21 o -3 5 2 0.17 1.20 0.75 o -2 5 2 49.45 41.22 2.43 o -1 5 2 614.25 640.07 13.11 o 0 5 2 21.15 22.56 1.87 o 1 5 2 9.67 6.34 1.15 o 2 5 2 50.36 43.65 2.23 o 3 5 2 28.57 28.44 1.84 o 4 5 2 3.97 4.67 1.05 o 5 5 2 0.29 -0.50 0.81 o 6 5 2 26.79 31.22 2.61 o 7 5 2 19.76 12.78 1.78 o 8 5 2 62.13 64.84 3.72 o 9 5 2 71.86 68.27 3.89 o 10 5 2 32.33 27.50 2.75 o 11 5 2 4.44 3.20 3.79 o -5 6 2 386.05 367.94 16.25 o -4 6 2 211.49 211.18 12.27 o -3 6 2 44.15 52.60 4.52 o -2 6 2 251.50 246.34 9.42 o -1 6 2 0.92 -0.09 1.04 o 0 6 2 251.56 260.34 9.73 o 1 6 2 73.62 79.84 5.43 o -19 1 3 82.23 89.04 4.50 o -18 1 3 31.55 26.77 2.54 o -17 1 3 99.07 98.34 3.42 o -16 1 3 259.96 256.65 5.23 o -15 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