#------------------------------------------------------------------------------ #$Date: 2017-03-15 09:03:47 +0200 (Wed, 15 Mar 2017) $ #$Revision: 194251 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/80/2108036.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108036 _cell_angle_alpha 90.000 _cell_angle_beta 93.368 _cell_angle_gamma 90.000 _cell_length_a 10.7807 _cell_length_b 28.8937 _cell_length_c 14.8900 _exptl_crystal_F_000 2232.00 _reflns_d_resolution_high 0.7483 _cod_data_source_file xm50051gsup8.hkl _cod_data_source_block 1g _shelx_title ' db132 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 496.04 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 25693.70 19727.00 442.60 o 6 0 0 164033.52 167504.08 3281.60 o 8 0 0 43142.79 38641.61 877.90 o 10 0 0 165.36 231.74 33.65 o 12 0 0 1407.76 1157.19 82.23 o 14 0 0 878.40 1731.12 246.93 o 2 1 0 316.04 412.58 27.56 o 4 1 0 881.98 646.05 25.26 o 5 1 0 68450.55 58318.90 818.83 o 6 1 0 7515.14 7825.09 286.35 o 7 1 0 397.05 331.27 22.99 o 8 1 0 11179.63 10922.24 325.16 o 9 1 0 9623.65 9506.96 146.58 o 10 1 0 232.23 154.09 21.25 o 11 1 0 944.08 841.33 39.27 o 12 1 0 159.88 183.60 39.45 o 13 1 0 3.83 124.79 44.87 o 14 1 0 655.84 2339.35 265.13 o 1 2 0 41089.24 39923.56 390.61 o 3 2 0 28683.93 32360.74 923.61 o 4 2 0 10136.25 7244.77 221.78 o 5 2 0 1582.66 2294.55 126.96 o 6 2 0 13.03 176.95 36.67 o 7 2 0 9248.91 8471.28 110.61 o 8 2 0 3223.76 3834.10 101.29 o 9 2 0 6530.08 6515.46 121.98 o 10 2 0 127.52 280.19 36.41 o 11 2 0 1112.10 1135.82 45.38 o 12 2 0 197.98 391.27 46.40 o 13 2 0 85.60 198.36 63.91 o 14 2 0 592.98 775.47 176.75 o 2 3 0 62427.98 66857.88 698.93 o 3 3 0 24470.30 16660.18 194.26 o 4 3 0 126391.70 122868.69 1359.08 o 5 3 0 26973.67 30440.83 355.95 o 6 3 0 38644.74 37738.15 466.87 o 7 3 0 3484.05 2869.00 45.72 o 8 3 0 5947.86 5606.57 84.61 o 9 3 0 3838.00 3617.34 64.68 o 10 3 0 10058.91 9200.58 125.70 o 11 3 0 1396.83 1352.73 88.93 o 12 3 0 3084.86 2665.70 102.53 o 13 3 0 161.80 701.80 150.76 o 1 4 0 64283.72 61876.92 678.68 o 3 4 0 2172.09 2934.33 52.98 o 4 4 0 504.17 512.33 17.35 o 5 4 0 22144.71 23113.38 271.24 o 6 4 0 176.06 667.85 28.46 o 7 4 0 23589.03 21699.66 246.34 o 8 4 0 1225.22 1284.74 44.61 o 9 4 0 6885.77 6319.56 86.05 o 10 4 0 1418.99 1478.32 58.25 o 11 4 0 266.47 248.32 37.07 o 12 4 0 608.21 699.18 62.13 o 13 4 0 1031.80 1156.71 253.43 o 14 4 0 16.45 127.36 77.98 o 1 5 0 8950.41 11225.22 103.21 o 2 5 0 9518.18 8072.55 75.39 o 3 5 0 1882.57 910.40 16.32 o 4 5 0 8148.83 9427.15 154.75 o 5 5 0 8500.04 9364.70 165.66 o 6 5 0 861.11 680.73 57.50 o 7 5 0 447.09 806.56 48.50 o 8 5 0 87.03 97.54 17.81 o 9 5 0 1499.95 1664.38 63.01 o 10 5 0 527.79 527.16 36.04 o 11 5 0 1.75 -9.63 32.34 o 12 5 0 2.06 37.42 88.53 o 13 5 0 441.09 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8 0 878.77 822.74 14.30 o 3 8 0 1345.50 2299.77 55.26 o 4 8 0 3382.17 3868.31 50.69 o 5 8 0 86.06 331.96 18.82 o 6 8 0 522.23 663.80 30.56 o 7 8 0 2268.81 2074.54 47.62 o 8 8 0 0.05 16.85 17.51 o 9 8 0 49.00 250.21 38.27 o 10 8 0 7.28 26.41 22.56 o 11 8 0 20.20 268.35 53.50 o 12 8 0 370.47 499.86 74.55 o 13 8 0 2.16 355.53 101.13 o 14 8 0 32.61 200.14 85.78 o 1 9 0 5765.74 6776.16 63.99 o 2 9 0 28201.32 26990.12 301.33 o 3 9 0 24931.49 24004.54 238.66 o 4 9 0 45549.25 46285.29 488.95 o 5 9 0 12417.44 11768.37 163.11 o 6 9 0 8199.79 7521.26 88.77 o 7 9 0 292.76 225.45 16.77 o 8 9 0 403.51 465.17 31.57 o 9 9 0 8456.31 7526.14 104.37 o 10 9 0 1708.24 1631.75 56.08 o 11 9 0 4474.72 4112.61 120.43 o 12 9 0 442.11 589.58 85.67 o 13 9 0 60.85 86.74 109.17 o 0 10 0 46382.95 43600.46 654.87 o 1 10 0 36490.59 37785.97 384.43 o 2 10 0 23851.35 24452.91 253.55 o 3 10 0 26246.19 27507.81 272.97 o 4 10 0 27.88 101.41 10.33 o 5 10 0 1085.56 1192.84 27.89 o 6 10 0 9549.69 9173.85 104.60 o 7 10 0 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0 474.31 636.38 77.28 o 13 12 0 837.88 1032.59 96.30 o 1 13 0 353.09 220.23 21.71 o 2 13 0 60776.75 61945.16 673.14 o 3 13 0 12141.93 12477.07 139.76 o 4 13 0 66181.14 65409.96 689.88 o 5 13 0 7275.13 6907.80 90.32 o 6 13 0 13428.59 12224.82 165.17 o 7 13 0 1934.90 1691.05 47.97 o 8 13 0 356.22 443.06 36.87 o 9 13 0 472.03 390.18 50.08 o 10 13 0 1300.38 1310.34 76.39 o 11 13 0 685.85 736.30 132.78 o 12 13 0 579.55 906.98 95.00 o 13 13 0 600.02 807.43 99.47 o 0 14 0 36642.47 36637.31 593.29 o 1 14 0 21713.55 23709.25 272.55 o 2 14 0 8895.31 9259.92 105.82 o 3 14 0 2825.79 2685.28 62.40 o 4 14 0 101.77 266.63 21.03 o 5 14 0 53.53 446.94 22.43 o 6 14 0 1670.29 1556.04 71.68 o 7 14 0 23.81 34.37 19.90 o 8 14 0 1955.69 1862.10 51.58 o 9 14 0 299.70 452.97 50.37 o 10 14 0 123.98 214.21 58.85 o 11 14 0 1115.62 1388.84 92.81 o 12 14 0 9.86 44.83 56.75 o 13 14 0 1103.06 1433.65 104.20 o 1 15 0 12566.88 13357.29 171.62 o 2 15 0 13.79 51.76 8.40 o 3 15 0 92300.67 88648.29 963.34 o 4 15 0 33.23 62.15 11.57 o 5 15 0 58855.18 57720.76 646.82 o 6 15 0 265.81 262.30 27.88 o 7 15 0 2166.16 1979.85 47.65 o 8 15 0 172.20 221.22 34.06 o 9 15 0 4797.22 4588.32 86.89 o 10 15 0 284.23 244.24 66.43 o 11 15 0 3393.01 3393.57 198.14 o 12 15 0 28.29 107.34 57.81 o 13 15 0 704.40 1011.99 119.57 o 0 16 0 102522.44 102244.34 1671.92 o 1 16 0 204.08 372.63 19.77 o 2 16 0 32536.45 32867.36 327.74 o 3 16 0 1108.79 1313.62 28.25 o 4 16 0 216.15 203.41 15.15 o 5 16 0 1409.43 1839.95 82.34 o 6 16 0 9551.05 9006.81 141.62 o 7 16 0 955.31 903.01 36.90 o 8 16 0 10893.10 10206.24 153.42 o 9 16 0 275.21 212.24 45.06 o 10 16 0 1538.86 1516.26 87.17 o 11 16 0 165.22 178.05 56.83 o 12 16 0 17.74 67.37 57.61 o 13 16 0 325.76 382.09 96.17 o 1 17 0 625.42 530.74 20.56 o 2 17 0 94.09 72.77 13.02 o 3 17 0 3913.37 3896.29 52.97 o 4 17 0 1489.65 1269.13 31.74 o 5 17 0 16.64 65.87 20.45 o 6 17 0 2041.24 2201.03 82.60 o 7 17 0 1513.47 1588.31 63.18 o 8 17 0 690.43 879.11 45.66 o 9 17 0 1561.61 1662.69 85.83 o 10 17 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