#------------------------------------------------------------------------------ #$Date: 2017-05-12 20:32:45 +0300 (Fri, 12 May 2017) $ #$Revision: 196647 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/80/2108042.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108042 _chemical_formula_sum 'Al4.847 Si1.153 O9.577' _chemical_name_common '2/1 Mullite' _space_group_ssg_name Pbam(\a01/2)0ss _symmetry_cell_setting orthorhombic _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 7.5817(6) _cell_length_b 7.6752(7) _cell_length_c 2.8843(3) _cell_modulation_dimension 1 _cod_data_source_file dq5021Isup2.hkl _cod_data_source_block I loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,-x2,x3,x3-x4+1/2 3 -x1+1/2,x2+1/2,-x3,-x4+1/2 4 x1+1/2,-x2+1/2,-x3,-x3+x4 5 -x1,-x2,-x3,-x4 6 x1,x2,-x3,-x3+x4+1/2 7 x1+1/2,-x2+1/2,x3,x4+1/2 8 -x1+1/2,x2+1/2,x3,x3-x4 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.300100 0.000000 0.500000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 1 0 800.10 945.13 12.94 o 0 0 2 0 5298.15 4431.60 20.47 o 0 0 3 0 170.74 181.34 2.92 o 0 0 4 0 888.47 887.96 7.89 o 0 1 1 -1 86.16 71.99 8.62 o 0 1 2 -1 81.18 84.06 10.78 o 0 1 3 -1 7.31 3.02 6.90 < 0 2 0 0 0.66 2.13 1.77 < 0 2 1 -1 23.42 12.07 11.21 < 0 2 1 0 7.01 15.95 1.73 o 0 2 2 -1 7.13 6.47 8.19 < 0 2 2 0 0.14 -0.27 1.99 < 0 2 3 -1 8.86 6.90 12.93 < 0 2 3 0 46.34 48.92 2.08 o 0 2 4 0 0.05 -0.40 1.24 < 0 3 1 -1 48.53 46.13 8.62 o 0 3 3 -1 39.92 43.97 9.05 o 0 4 0 0 165.67 175.00 4.43 o 0 4 1 -1 7.91 0.00 6.90 < 0 4 1 0 1517.75 1423.12 13.38 o 0 4 2 -1 2.15 -8.62 12.93 < 0 4 2 0 46.34 37.58 2.26 o 0 4 3 -1 9.50 4.31 11.64 < 0 4 3 0 413.21 417.50 6.03 o 0 4 4 0 6.76 5.50 2.26 < 0 5 1 -1 62.37 57.77 7.76 o 0 5 2 -1 78.13 79.32 9.48 o 0 5 3 -1 10.57 3.02 9.05 < 0 6 0 0 458.79 410.19 6.12 o 0 6 1 -1 65.02 64.66 8.19 o 0 6 1 0 7.60 7.58 1.73 o 0 6 2 -1 30.43 27.16 11.21 < 0 6 2 0 274.52 283.62 5.05 o 0 6 3 -1 34.06 38.37 12.93 < 0 6 3 0 0.99 1.86 1.77 < 0 7 1 -1 4.80 10.35 8.62 < 0 7 2 -1 1.41 21.99 12.50 < 0 8 0 0 0.21 -3.01 2.04 < 0 8 1 -1 0.90 7.33 9.92 < 0 8 1 0 320.90 328.20 5.67 o 0 8 2 -1 2.95 0.43 12.50 < 0 8 2 0 0.26 0.09 1.95 < 0 8 3 0 133.03 137.20 3.68 o 0 9 1 -1 26.45 37.94 7.76 o 0 10 0 0 9.37 10.41 1.55 o 0 10 1 0 190.24 207.40 4.56 o 0 10 2 0 6.40 6.29 1.99 o 0 10 3 0 82.73 82.21 3.32 o 0 12 0 0 85.62 71.08 2.79 o 0 12 1 0 16.72 16.44 1.73 o 1 0 0 1 171.41 150.45 10.35 o 1 0 1 -1 31.25 22.42 11.21 < 1 0 1 1 20.47 29.75 11.64 < 1 0 2 -1 8.76 9.48 11.21 < 1 0 2 1 85.94 87.94 10.78 o 1 0 3 -1 13.80 10.35 8.19 < 1 1 0 0 382.79 428.31 4.17 o 1 1 0 1 1.55 -1.29 5.60 < 1 1 1 -1 26.42 21.55 7.76 < 1 1 1 0 658.90 656.32 3.55 o 1 1 1 1 2.92 0.00 7.76 < 1 1 2 -1 43.08 36.64 10.78 o 1 1 2 0 125.06 118.10 2.17 o 1 1 2 1 0.03 3.88 7.33 < 1 1 3 -1 0.93 -3.88 6.90 < 1 1 3 0 173.62 170.93 1.55 o 1 1 4 0 29.41 31.77 1.15 o 1 1 5 0 22.23 22.16 1.77 o 1 2 0 0 665.49 739.68 7.98 o 1 2 0 1 11.58 6.04 7.33 < 1 2 1 -1 1.74 -1.29 12.07 < 1 2 1 0 1143.67 1133.87 5.45 o 1 2 1 1 5.85 6.04 8.19 < 1 2 2 -1 4.09 3.02 9.05 < 1 2 2 0 266.47 251.63 2.70 o 1 2 2 1 3.85 -3.45 8.62 < 1 2 3 -1 5.17 -6.47 8.19 < 1 2 3 0 220.97 210.06 2.04 o 1 2 4 0 56.82 58.36 1.37 o 1 2 5 0 45.30 42.28 2.61 o 1 3 0 0 430.47 420.51 5.14 o 1 3 0 1 37.47 31.90 8.19 o 1 3 1 -1 1.53 0.00 7.76 < 1 3 1 0 2.80 2.97 0.97 o 1 3 1 1 16.89 15.95 10.78 < 1 3 2 0 344.82 336.31 3.28 o 1 3 2 1 12.44 10.35 9.48 < 1 3 3 -1 0.43 7.76 8.62 < 1 3 3 0 0.53 0.09 1.42 < 1 3 4 0 82.10 79.90 1.86 o 1 3 5 0 0.13 0.53 1.02 < 1 4 0 0 95.98 107.82 2.88 o 1 4 0 1 8.68 9.05 8.62 < 1 4 1 -1 8.59 15.09 9.05 < 1 4 1 0 52.53 48.08 2.13 o 1 4 1 1 27.62 36.64 12.50 < 1 4 2 -1 13.60 14.66 8.62 < 1 4 2 0 12.78 12.54 1.02 o 1 4 2 1 0.28 2.16 9.48 < 1 4 3 -1 0.49 8.62 10.78 < 1 4 3 0 13.70 14.71 1.95 o 1 4 4 0 3.84 4.25 1.02 o 1 5 0 0 75.57 70.24 2.57 o 1 5 0 1 10.04 15.52 8.62 < 1 5 1 -1 12.42 11.64 7.76 < 1 5 1 0 984.22 994.72 7.31 o 1 5 1 1 7.04 5.17 9.92 < 1 5 2 -1 15.01 17.24 8.62 < 1 5 2 0 41.77 42.54 1.46 o 1 5 2 1 6.27 -4.74 11.21 < 1 5 3 -1 2.48 14.66 10.78 < 1 5 3 0 274.53 279.59 2.84 o 1 5 4 0 8.89 9.04 1.37 o 1 6 0 0 227.16 210.19 2.79 o 1 6 0 1 0.34 -8.19 6.47 < 1 6 1 -1 13.55 7.33 6.90 < 1 6 1 0 2.46 3.81 0.93 o 1 6 1 1 0.10 -5.17 11.21 < 1 6 2 -1 2.88 7.76 9.92 < 1 6 2 0 111.56 114.82 2.08 o 1 6 2 1 1.43 7.33 10.78 < 1 6 3 -1 13.02 13.36 11.64 < 1 6 3 0 1.39 3.24 1.15 < 1 6 4 0 25.85 20.30 2.04 o 1 7 0 0 42.45 36.43 1.46 o 1 7 0 1 20.47 11.64 7.76 < 1 7 1 -1 1.22 -3.88 7.76 < 1 7 1 0 272.41 271.66 3.63 o 1 7 1 1 14.25 12.93 10.78 < 1 7 2 -1 1.36 -13.36 12.07 < 1 7 2 0 19.88 21.27 1.68 o 1 7 3 0 101.79 99.93 2.53 o 1 8 0 0 261.70 263.59 2.97 o 1 8 0 1 2.89 -18.97 9.48 < 1 8 1 -1 2.64 3.88 8.62 < 1 8 1 0 42.02 42.45 1.91 o 1 8 1 1 0.31 -12.07 13.36 < 1 8 2 -1 6.16 5.60 14.23 < 1 8 2 0 149.69 154.44 2.84 o 1 8 3 0 13.37 15.29 1.64 o 1 9 0 0 328.54 336.23 2.75 o 1 9 0 1 5.33 1.29 7.33 < 1 9 1 -1 21.55 31.90 7.76 o 1 9 1 0 25.34 25.79 1.68 o 1 9 2 0 202.51 207.00 3.15 o 1 9 3 0 11.37 11.57 1.68 o 1 10 0 0 139.32 141.68 2.30 o 1 10 1 0 33.15 30.05 1.68 o 1 10 2 0 92.67 88.85 2.30 o 1 10 3 0 16.02 15.42 1.60 o 1 11 0 0 23.53 22.34 1.42 o 1 11 1 0 4.56 5.63 1.24 o 1 11 2 0 16.59 15.11 2.26 o 1 11 3 0 1.48 1.33 2.04 < 1 12 0 0 6.96 5.45 1.06 o 1 12 1 0 27.61 25.30 1.46 o 1 12 2 0 4.82 2.61 2.30 < 1 13 0 0 10.28 11.26 2.08 o 1 13 1 0 46.44 48.70 1.60 o 2 0 0 0 29.56 34.17 1.46 o 2 0 1 0 856.53 812.67 6.69 o 2 0 2 0 5.73 5.27 1.20 o 2 0 3 0 285.52 282.25 2.88 o 2 0 4 0 0.44 2.17 1.55 < 2 0 5 0 54.44 52.20 3.10 o 2 1 0 0 1266.58 1554.56 7.00 o 2 1 0 1 1.95 0.43 6.04 < 2 1 1 -1 14.35 17.67 6.90 < 2 1 1 0 74.64 89.47 1.33 o 2 1 1 1 0.33 -1.72 6.47 < 2 1 2 -1 2.32 2.59 7.76 < 2 1 2 0 448.01 389.98 2.61 o 2 1 2 1 10.82 9.48 7.33 < 2 1 3 -1 10.78 18.11 7.33 < 2 1 3 0 1.65 1.60 0.80 < 2 1 4 0 74.00 71.04 1.55 o 2 1 5 0 0.03 1.82 1.51 < 2 2 0 0 1101.49 1281.44 7.13 o 2 2 0 1 21.07 17.67 7.33 < 2 2 1 -1 38.53 37.94 7.76 o 2 2 1 0 18.66 16.57 0.93 o 2 2 1 1 18.01 14.66 6.47 < 2 2 2 -1 33.77 30.61 8.62 o 2 2 2 0 482.58 434.25 2.35 o 2 2 2 1 5.61 15.95 7.76 < 2 2 3 -1 14.58 4.74 7.33 < 2 2 3 0 11.08 9.62 1.29 o 2 2 4 0 90.49 95.15 1.68 o 2 2 5 0 3.09 2.75 1.33 < 2 3 0 0 1027.21 1216.52 9.66 o 2 3 0 1 112.22 115.10 9.48 o 2 3 1 -1 1.42 9.48 7.76 < 2 3 1 0 0.07 -0.35 1.46 < 2 3 1 1 84.83 90.96 10.35 o 2 3 2 -1 19.78 29.31 10.35 < 2 3 2 0 238.33 231.99 2.44 o 2 3 2 1 28.50 39.66 13.36 < 2 3 3 -1 0.62 12.07 11.64 < 2 3 3 0 0.06 1.55 1.20 < 2 3 4 0 49.74 48.57 1.64 o 2 4 0 0 472.72 482.33 5.89 o 2 4 0 1 3.51 11.21 7.33 < 2 4 1 -1 87.92 81.04 10.35 o 2 4 1 0 83.31 77.82 2.44 o 2 4 1 1 4.91 17.67 10.35 < 2 4 2 -1 65.72 60.35 10.78 o 2 4 2 0 221.51 209.61 2.70 o 2 4 2 1 0.43 7.76 10.35 < 2 4 3 -1 24.83 16.38 10.78 < 2 4 3 0 33.07 37.27 1.86 o 2 4 4 0 46.56 45.82 1.55 o 2 5 0 0 511.96 493.95 5.54 o 2 5 0 1 48.67 45.26 8.19 o 2 5 1 -1 22.61 30.18 8.62 o 2 5 1 0 1018.34 974.38 5.72 o 2 5 1 1 11.55 22.42 9.92 < 2 5 2 -1 13.67 21.55 10.35 < 2 5 2 0 275.53 261.95 2.84 o 2 5 2 1 40.85 44.83 12.07 o 2 5 3 -1 10.36 13.79 11.64 < 2 5 3 0 302.33 290.40 2.88 o 2 5 4 0 69.44 68.42 1.68 o 2 6 0 0 71.03 67.98 1.60 o 2 6 0 1 55.56 52.59 7.33 o 2 6 1 -1 10.26 12.50 6.04 < 2 6 1 0 207.71 206.56 2.70 o 2 6 1 1 32.55 50.44 10.35 o 2 6 2 -1 3.93 -3.45 10.78 < 2 6 2 0 36.82 35.63 1.46 o 2 6 3 -1 5.06 5.17 11.21 < 2 6 3 0 74.87 76.22 1.77 o 2 6 4 0 9.82 10.99 2.13 o 2 7 0 0 116.81 117.53 2.17 o 2 7 0 1 2.26 0.00 6.90 < 2 7 1 -1 3.39 -0.43 7.33 < 2 7 1 0 151.11 153.69 2.44 o 2 7 1 1 2.38 0.86 11.21 < 2 7 2 -1 14.56 -0.43 11.64 < 2 7 2 0 68.65 71.44 1.73 o 2 7 3 0 55.98 56.28 1.68 o 2 8 0 0 203.88 203.85 2.66 o 2 8 0 1 13.13 18.11 9.05 < 2 8 1 -1 0.15 8.19 9.92 < 2 8 1 0 22.73 22.29 1.64 o 2 8 2 -1 0.61 -27.16 13.36 < 2 8 2 0 120.87 122.58 2.61 o 2 8 3 0 9.19 6.82 1.68 o 2 8 4 0 36.08 40.77 2.44 o 2 9 0 0 55.90 56.46 1.73 o 2 9 1 0 86.98 86.24 3.10 o 2 9 2 0 37.14 29.65 2.61 o 2 9 3 0 41.36 52.20 2.66 o 2 10 0 0 38.81 38.07 1.55 o 2 10 1 0 34.70 33.33 2.48 o 2 10 2 0 24.49 30.31 2.44 o 2 10 3 0 16.17 16.62 2.13 o 2 11 0 0 17.07 17.19 1.33 o 2 11 1 0 66.00 64.79 1.68 o 2 11 2 0 9.64 12.59 2.22 o 2 12 0 0 20.68 18.66 1.24 o 2 12 1 0 28.71 27.43 1.42 o 2 12 2 0 14.06 18.35 2.35 o 2 13 0 0 0.89 4.92 1.82 < 2 13 1 0 28.12 25.70 1.42 o 3 0 0 1 37.95 26.73 7.76 o 3 0 1 -1 31.84 28.45 7.76 o 3 0 1 1 74.64 50.87 21.55 < 3 0 2 1 11.46 9.48 10.35 < 3 0 3 -1 7.01 16.38 9.48 < 3 1 0 0 30.88 25.57 1.24 o 3 1 0 1 20.47 18.54 6.47 < 3 1 1 -1 51.20 43.97 6.04 o 3 1 1 0 333.30 347.97 2.26 o 3 1 1 1 2.93 6.90 5.17 < 3 1 2 -1 53.23 59.49 6.47 o 3 1 2 0 106.90 98.96 1.46 o 3 1 2 1 16.85 23.28 7.33 o 3 1 3 -1 19.94 25.00 7.33 o 3 1 3 0 56.57 51.67 1.11 o 3 1 4 0 24.48 24.55 1.51 o 3 1 5 0 16.03 18.83 1.29 o 3 2 0 0 158.34 164.94 1.95 o 3 2 0 1 144.86 140.54 8.19 o 3 2 1 -1 4.17 1.72 8.19 < 3 2 1 0 359.06 356.43 3.15 o 3 2 1 1 69.10 71.13 6.90 o 3 2 2 -1 5.02 6.47 6.47 < 3 2 2 0 82.52 72.94 1.02 o 3 2 2 1 59.33 59.92 9.05 o 3 2 3 -1 13.22 22.42 7.76 < 3 2 3 0 87.40 86.33 2.30 o 3 2 4 0 19.98 17.28 1.24 o 3 3 0 0 63.15 63.81 1.77 o 3 3 0 1 6.13 23.28 11.21 < 3 3 1 -1 75.91 67.25 10.78 o 3 3 1 0 2317.28 2181.67 11.52 o 3 3 1 1 0.24 -0.43 8.19 < 3 3 2 -1 54.20 66.39 10.35 o 3 3 2 0 34.28 31.95 1.33 o 3 3 2 1 5.62 8.19 9.48 < 3 3 3 -1 19.61 22.42 10.78 < 3 3 3 0 631.73 638.06 3.63 o 3 3 4 0 6.19 6.51 0.97 o 3 4 0 0 4.63 4.08 0.97 o 3 4 0 1 18.52 19.40 9.92 < 3 4 1 -1 39.43 30.61 9.05 o 3 4 1 0 160.75 160.34 2.70 o 3 4 1 1 2.77 -4.74 7.76 < 3 4 2 -1 22.47 35.35 11.21 o 3 4 2 0 7.22 7.71 1.11 o 3 4 2 1 15.90 13.79 12.93 < 3 4 3 -1 17.70 27.16 12.07 < 3 4 3 0 43.28 48.61 1.86 o 3 4 4 0 0.98 -0.66 1.51 < 3 5 0 0 344.46 338.35 3.10 o 3 5 0 1 2.76 0.00 7.76 < 3 5 1 -1 15.27 6.04 6.90 < 3 5 1 0 27.94 31.55 1.73 o 3 5 1 1 0.38 -1.72 11.64 < 3 5 2 -1 8.50 4.74 8.62 < 3 5 2 0 207.21 202.88 2.61 o 3 5 2 1 2.34 3.45 13.79 < 3 5 3 -1 5.56 9.48 10.35 < 3 5 3 0 8.18 6.69 1.46 o 3 5 4 0 59.64 59.65 2.84 o 3 6 0 0 13.08 12.63 1.11 o 3 6 0 1 44.29 37.50 8.19 o 3 6 1 -1 1.43 3.45 6.47 < 3 6 1 0 40.25 38.38 1.86 o 3 6 1 1 45.20 54.32 14.23 o 3 6 2 -1 7.78 14.23 10.78 < 3 6 2 0 5.09 6.65 1.60 o 3 6 3 0 13.59 14.98 1.68 o 3 6 4 0 1.34 0.44 1.91 < 3 7 0 0 932.20 980.45 5.58 o 3 7 0 1 3.80 1.29 8.19 < 3 7 1 -1 9.79 12.50 7.33 < 3 7 1 0 0.01 -0.35 1.24 < 3 7 1 1 3.42 -5.17 14.66 < 3 7 2 -1 7.77 18.97 15.09 < 3 7 2 0 544.72 545.79 4.83 o 3 7 3 0 0.15 4.79 1.46 o 3 7 4 0 169.81 158.21 3.81 o 3 8 0 0 7.90 10.24 1.37 o 3 8 0 1 0.55 -18.11 8.19 < 3 8 1 -1 4.69 8.62 9.05 < 3 8 1 0 22.35 26.90 1.68 o 3 8 2 0 4.27 1.73 1.46 < 3 8 3 0 10.56 11.08 1.51 o 3 8 4 0 0.81 -0.13 2.04 < 3 9 0 0 21.93 23.40 1.60 o 3 9 1 0 141.50 144.12 3.90 o 3 9 2 0 12.24 9.44 2.26 o 3 9 3 0 53.55 54.77 2.97 o 3 10 0 0 29.70 28.98 1.82 o 3 10 1 0 0.01 -0.09 1.46 < 3 10 2 0 20.43 19.01 2.35 o 3 10 3 0 0.00 -0.40 1.91 < 3 11 0 0 41.56 36.92 1.91 o 3 11 1 0 60.48 59.38 2.17 o 3 11 2 0 27.83 24.95 2.66 o 3 12 0 0 1.53 3.72 1.91 < 3 12 1 0 3.69 4.25 1.46 < 3 13 0 0 38.08 36.25 2.79 o 3 13 1 0 0.07 0.97 1.11 < 4 0 0 0 716.74 889.55 5.89 o 4 0 1 0 581.07 512.25 5.14 o 4 0 2 0 206.34 220.34 4.83 o 4 0 3 0 221.71 222.42 3.24 o 4 0 4 0 47.66 51.76 3.06 o 4 1 0 0 88.79 100.24 1.64 o 4 1 0 1 1.53 2.59 8.19 < 4 1 1 -1 1.19 3.02 5.60 < 4 1 1 0 51.55 48.92 1.20 o 4 1 1 1 0.04 -3.45 6.90 < 4 1 2 -1 0.55 1.29 5.60 < 4 1 2 0 47.45 42.85 0.97 o 4 1 2 1 4.43 0.43 8.19 < 4 1 3 -1 3.12 -6.47 8.19 < 4 1 3 0 17.19 17.28 1.42 o 4 1 4 0 9.10 10.06 1.29 o 4 2 0 0 813.72 854.19 5.27 o 4 2 0 1 3.47 6.47 6.47 < 4 2 1 -1 17.05 12.07 6.47 < 4 2 1 0 666.11 629.11 3.28 o 4 2 1 1 1.18 2.59 6.04 < 4 2 2 -1 15.66 12.93 6.47 < 4 2 2 0 345.17 328.69 2.30 o 4 2 2 1 2.56 -10.78 8.62 < 4 2 3 -1 3.21 4.74 7.76 < 4 2 3 0 173.16 162.73 2.30 o 4 2 4 0 64.56 61.51 1.46 o 4 3 0 0 0.08 0.89 1.11 < 4 3 0 1 0.02 -0.86 7.76 < 4 3 1 -1 7.77 14.23 10.78 < 4 3 1 0 0.16 0.22 1.33 < 4 3 1 1 3.92 6.04 7.33 < 4 3 2 -1 0.03 -1.29 7.76 < 4 3 2 0 0.00 -0.49 0.75 < 4 3 2 1 2.46 -3.88 11.64 < 4 3 3 -1 8.17 15.95 10.35 < 4 3 3 0 0.02 1.11 1.06 < 4 3 4 0 0.09 -1.15 1.15 < 4 4 0 0 646.81 633.32 4.92 o 4 4 0 1 4.59 14.66 9.05 < 4 4 1 -1 0.07 -3.88 9.48 < 4 4 1 0 151.01 141.37 2.92 o 4 4 1 1 0.99 7.76 8.62 < 4 4 2 -1 0.97 2.59 8.62 < 4 4 2 0 360.44 341.14 3.99 o 4 4 2 1 4.01 -4.74 14.23 < 4 4 3 -1 0.47 -3.88 12.50 < 4 4 3 0 37.73 36.47 1.82 o 4 4 4 0 87.96 93.55 2.30 o 4 5 0 0 147.22 147.31 2.13 o 4 5 0 1 2.34 -6.04 7.76 < 4 5 1 -1 0.00 -3.45 6.90 < 4 5 1 0 108.44 100.69 2.53 o 4 5 1 1 3.99 12.50 13.36 < 4 5 2 -1 0.99 9.48 12.07 < 4 5 2 0 82.97 83.85 2.22 o 4 5 3 -1 0.45 4.31 12.93 < 4 5 3 0 39.47 38.60 1.86 o 4 5 4 0 22.67 20.92 2.35 o 4 6 0 0 66.08 73.03 1.77 o 4 6 0 1 1.65 -6.04 9.48 < 4 6 1 -1 5.12 3.45 7.76 < 4 6 1 0 308.12 325.32 3.99 o 4 6 1 1 4.00 -14.66 14.66 < 4 6 2 -1 0.95 -6.90 13.36 < 4 6 2 0 35.33 38.51 1.91 o 4 6 3 0 105.74 112.47 2.53 o 4 6 4 0 14.87 12.98 2.35 o 4 7 0 0 55.52 60.45 2.39 o 4 7 0 1 27.15 42.68 9.05 o 4 7 1 -1 23.14 31.04 9.05 o 4 7 1 0 31.47 33.55 1.55 o 4 7 1 1 9.01 22.42 13.36 < 4 7 2 -1 7.61 0.86 15.52 < 4 7 2 0 31.98 31.42 1.82 o 4 7 3 0 11.52 12.19 1.55 o 4 7 4 0 8.75 4.83 2.26 < 4 8 0 0 138.31 140.35 2.84 o 4 8 0 1 26.76 30.61 9.48 o 4 8 1 -1 0.00 9.48 7.76 < 4 8 1 0 20.40 18.79 1.37 o 4 8 2 0 86.43 93.51 2.44 o 4 8 3 0 7.47 7.84 1.42 o 4 9 0 0 14.27 14.62 1.37 o 4 9 1 0 27.28 28.72 1.86 o 4 9 2 0 9.39 9.57 1.60 o 4 9 3 0 12.75 17.33 2.53 o 4 10 0 0 152.72 157.99 2.84 o 4 10 1 0 12.09 10.68 1.55 o 4 10 2 0 96.78 105.43 3.37 o 4 10 3 0 4.42 5.50 2.04 < 4 11 0 0 12.23 10.90 1.51 o 4 11 1 0 20.39 19.72 1.55 o 4 11 2 0 7.52 4.56 2.04 < 4 12 0 0 2.63 3.72 2.22 < 4 12 1 0 197.32 185.99 2.97 o 4 12 2 0 2.06 2.04 1.60 < 5 0 0 1 48.51 48.28 7.76 o 5 0 1 -1 25.32 25.43 12.50 < 5 0 1 1 35.27 42.68 6.90 o 5 0 2 -1 37.06 37.07 10.78 o 5 0 2 1 19.44 7.33 8.62 < 5 0 3 -1 1.04 -4.31 10.78 < 5 1 0 0 51.99 49.68 1.46 o 5 1 0 1 100.91 111.22 6.04 o 5 1 1 -1 73.09 75.01 7.76 o 5 1 1 0 274.66 260.18 1.86 o 5 1 1 1 78.44 89.67 6.90 o 5 1 2 -1 32.36 40.52 6.04 o 5 1 2 0 39.49 41.26 1.02 o 5 1 2 1 37.49 44.83 8.62 o 5 1 3 -1 41.53 46.99 9.48 o 5 1 3 0 82.76 76.93 1.60 o 5 1 4 0 9.69 9.26 1.02 o 5 2 0 0 901.82 915.57 4.21 o 5 2 0 1 6.73 3.45 5.17 < 5 2 1 -1 0.70 -0.86 5.60 < 5 2 1 0 1148.05 1092.34 5.14 o 5 2 1 1 25.94 12.93 8.19 < 5 2 2 -1 1.94 11.21 7.76 < 5 2 2 0 464.67 447.33 3.19 o 5 2 2 1 0.03 -16.38 12.07 < 5 2 3 -1 0.39 -3.88 9.48 < 5 2 3 0 350.50 344.25 3.86 o 5 2 4 0 118.07 109.19 1.73 o 5 3 0 0 252.75 254.60 2.48 o 5 3 0 1 1.97 0.43 7.33 < 5 3 1 -1 12.74 19.40 8.19 < 5 3 1 0 228.91 241.30 3.68 o 5 3 1 1 0.59 0.86 9.05 < 5 3 2 -1 3.52 0.86 8.19 < 5 3 2 0 138.10 138.53 2.22 o 5 3 2 1 0.98 28.45 20.69 < 5 3 3 -1 10.05 -2.59 14.23 < 5 3 3 0 69.19 69.04 2.17 o 5 3 4 0 36.35 38.42 1.82 o 5 4 0 0 13.90 16.49 1.42 o 5 4 0 1 13.39 18.11 7.76 < 5 4 1 -1 0.86 4.31 7.33 < 5 4 1 0 184.68 188.12 2.66 o 5 4 1 1 7.27 12.93 10.78 < 5 4 2 -1 5.48 4.31 8.19 < 5 4 2 0 13.23 14.49 2.44 o 5 4 3 -1 0.48 -12.07 16.38 < 5 4 3 0 57.99 65.90 2.92 o 5 4 4 0 1.01 0.62 1.46 < 5 5 0 0 34.73 36.16 1.42 o 5 5 0 1 3.96 -4.74 6.90 < 5 5 1 -1 0.28 -4.31 7.33 < 5 5 1 0 54.99 54.07 1.60 o 5 5 1 1 2.31 15.52 9.48 < 5 5 2 -1 0.07 4.74 10.78 < 5 5 2 0 23.48 28.89 1.73 o 5 5 3 0 18.35 13.16 2.61 o 5 5 4 0 8.01 4.08 1.99 < 5 6 0 0 3.69 2.75 1.42 < 5 6 0 1 6.73 16.38 8.62 < 5 6 1 -1 0.17 -13.79 8.62 < 5 6 1 0 53.53 60.23 1.82 o 5 6 1 1 0.90 -9.92 12.93 < 5 6 2 -1 2.03 -9.92 14.66 < 5 6 2 0 1.87 0.27 1.46 < 5 6 3 0 21.14 21.85 2.66 o 5 6 4 0 0.37 2.39 1.91 < 5 7 0 0 197.48 196.50 4.56 o 5 7 0 1 35.26 57.77 9.92 o 5 7 1 -1 37.79 46.56 9.05 o 5 7 1 0 89.38 104.14 2.13 o 5 7 2 0 122.58 126.30 2.66 o 5 7 3 0 34.05 36.52 1.86 o 5 7 4 0 41.20 42.28 2.61 o 5 8 1 0 11.96 12.23 1.37 o 5 8 2 0 76.84 81.94 2.26 o 5 8 3 0 2.98 3.19 1.46 < 5 9 0 0 2.34 4.17 1.51 < 5 9 1 0 27.73 30.45 1.86 o 5 9 2 0 1.50 3.68 1.55 < 5 9 3 0 11.92 11.52 1.73 o 5 10 0 0 95.88 100.02 3.41 o 5 10 1 0 25.20 25.13 1.82 o 5 10 2 0 67.20 75.65 2.26 o 5 10 3 0 13.45 11.17 2.17 o 5 11 0 0 26.64 27.17 2.57 o 5 11 1 0 64.93 58.85 3.01 o 5 11 2 0 18.45 21.23 2.39 o 5 12 0 0 8.51 9.97 2.35 o 5 12 1 0 23.81 28.54 1.77 o 6 0 0 0 1009.51 978.76 7.05 o 6 0 1 0 18.68 18.08 0.89 o 6 0 2 0 529.27 506.00 3.77 o 6 0 3 0 5.33 6.96 1.24 o 6 0 4 0 135.45 129.85 2.66 o 6 1 0 0 363.39 375.93 2.84 o 6 1 0 1 21.14 16.38 5.60 < 6 1 1 -1 5.88 6.04 4.74 < 6 1 1 0 0.54 0.35 0.49 < 6 1 1 1 24.45 24.57 5.17 o 6 1 2 -1 0.06 -2.59 5.17 < 6 1 2 0 180.57 168.53 1.64 o 6 1 3 -1 6.79 15.95 8.19 < 6 1 3 0 0.57 0.35 0.89 < 6 1 4 0 39.95 38.82 1.86 o 6 2 0 0 170.43 167.51 1.64 o 6 2 0 1 26.82 28.45 5.60 o 6 2 1 -1 19.18 14.66 5.17 < 6 2 1 0 83.56 88.54 1.37 o 6 2 1 1 22.49 21.12 7.76 < 6 2 2 -1 14.32 14.23 7.76 < 6 2 2 0 90.16 87.48 1.95 o 6 2 2 1 9.72 15.95 18.97 < 6 2 3 -1 7.00 -11.21 19.40 < 6 2 3 0 30.56 30.18 2.70 o 6 2 4 0 25.10 24.86 1.42 o 6 3 0 0 151.94 167.74 2.22 o 6 3 0 1 14.19 3.88 6.47 < 6 3 1 -1 3.79 8.19 6.90 < 6 3 1 0 1.65 2.75 0.93 < 6 3 1 1 2.54 28.45 10.35 < 6 3 2 -1 5.17 13.79 9.92 < 6 3 2 0 77.82 77.46 1.82 o 6 3 3 0 0.05 -2.75 2.13 < 6 3 4 0 27.22 27.34 1.42 o 6 4 0 0 0.10 -0.53 1.37 < 6 4 0 1 14.30 20.69 7.76 < 6 4 1 -1 0.28 1.72 9.05 < 6 4 1 0 364.51 371.19 3.01 o 6 4 1 1 14.64 12.93 9.92 < 6 4 2 -1 0.56 -17.67 9.48 < 6 4 2 0 0.02 0.80 1.42 < 6 4 3 0 137.30 144.78 3.77 o 6 4 4 0 0.00 -1.06 1.46 < 6 5 0 0 45.10 48.84 2.22 o 6 5 0 1 0.28 9.48 9.48 < 6 5 1 -1 13.61 24.14 9.05 < 6 5 1 0 165.45 176.73 2.22 o 6 5 1 1 0.01 -26.30 13.79 < 6 5 2 -1 1.58 28.88 14.23 < 6 5 2 0 28.50 28.72 2.30 o 6 5 3 0 65.72 64.44 2.92 o 6 5 4 0 9.06 9.08 2.35 o 6 6 0 0 316.45 335.03 4.12 o 6 6 0 1 0.07 1.72 9.05 < 6 6 1 -1 0.47 6.90 8.62 < 6 6 1 0 0.75 3.06 1.29 < 6 6 2 0 183.80 195.92 4.39 o 6 6 3 0 1.15 -0.27 2.17 < 6 7 0 0 54.33 56.37 2.22 o 6 7 1 -1 18.73 28.02 9.48 < 6 7 1 0 76.79 84.20 2.04 o 6 7 2 0 34.21 36.65 3.01 o 6 7 3 0 33.39 30.62 2.61 o 6 8 0 0 18.00 17.95 1.64 o 6 8 1 0 46.10 50.17 1.46 o 6 8 2 0 10.21 11.21 1.60 o 6 8 3 0 23.19 28.05 2.39 o 6 9 0 0 13.39 13.69 1.73 o 6 9 1 0 27.39 31.55 1.55 o 6 9 2 0 9.81 10.55 1.73 o 6 9 3 0 14.92 13.96 1.77 o 6 10 0 0 0.26 1.73 1.29 < 6 10 1 0 143.80 145.27 2.84 o 6 10 2 0 0.17 -0.58 2.61 < 6 11 0 0 0.50 0.53 2.17 < 6 11 1 0 14.77 17.64 1.73 o 6 12 0 0 97.04 104.72 3.37 o 6 12 1 0 13.23 13.92 1.55 o 7 0 0 1 0.29 2.16 8.62 < 7 0 1 -1 7.68 12.50 10.35 < 7 0 1 1 0.20 6.90 9.05 < 7 0 2 -1 0.02 -14.23 7.76 < 7 1 0 0 98.04 103.61 1.95 o 7 1 0 1 22.50 10.78 5.60 < 7 1 1 -1 20.35 27.59 6.04 o 7 1 1 0 168.56 164.63 1.29 o 7 1 1 1 26.55 25.87 6.47 o 7 1 2 -1 11.79 30.18 6.47 o 7 1 2 0 57.37 62.88 1.29 o 7 1 3 0 52.89 58.23 1.73 o 7 1 4 0 23.60 24.82 2.66 o 7 2 0 0 37.50 34.74 0.93 o 7 2 0 1 0.01 -6.90 5.60 < 7 2 1 -1 5.00 8.19 5.17 < 7 2 1 0 9.85 10.15 0.71 o 7 2 1 1 1.44 -8.19 7.76 < 7 2 2 -1 4.24 16.81 7.76 < 7 2 2 0 21.38 20.08 0.97 o 7 2 2 1 1.04 -30.61 22.42 < 7 2 3 -1 1.46 -14.23 20.26 < 7 2 3 0 3.52 1.33 1.55 < 7 2 4 0 5.38 6.56 1.55 o 7 3 0 0 412.33 408.73 4.56 o 7 3 0 1 2.94 -6.04 6.04 < 7 3 1 -1 1.22 0.86 6.47 < 7 3 1 0 48.13 50.25 1.29 o 7 3 1 1 5.03 21.55 9.05 < 7 3 2 -1 0.43 12.93 8.62 < 7 3 2 0 247.06 262.00 2.48 o 7 3 3 0 18.18 21.67 2.35 o 7 3 4 0 68.94 66.65 1.42 o 7 4 0 0 101.52 100.07 2.66 o 7 4 0 1 23.29 32.76 9.05 o 7 4 1 -1 9.35 6.47 8.62 < 7 4 1 0 24.18 24.91 1.20 o 7 4 2 -1 19.16 7.33 9.48 < 7 4 2 0 58.86 56.24 2.22 o 7 4 3 0 8.97 7.98 2.39 o 7 4 4 0 17.06 16.97 1.37 o 7 5 0 0 26.03 27.08 1.95 o 7 5 0 1 11.27 25.43 9.48 < 7 5 1 -1 1.11 -2.59 9.48 < 7 5 1 0 337.07 366.14 3.10 o 7 5 2 0 15.11 16.04 2.30 o 7 5 3 0 142.73 152.89 3.99 o 7 5 4 0 3.61 8.11 1.95 o 7 6 0 0 21.38 19.23 1.42 o 7 6 1 -1 1.14 1.29 9.48 < 7 6 1 0 0.29 -1.46 1.29 < 7 6 2 0 13.86 17.06 2.39 o 7 6 3 0 0.09 0.71 1.95 < 7 7 0 0 125.71 129.62 2.79 o 7 7 1 0 274.26 297.76 3.15 o 7 7 2 0 83.29 91.03 2.57 o 7 7 3 0 124.28 136.89 3.90 o 7 8 0 0 1.61 1.77 2.48 < 7 8 1 0 14.06 15.60 1.51 o 7 8 2 0 1.04 0.66 1.29 < 7 8 3 0 7.13 8.82 2.26 o 7 9 0 0 197.07 178.59 4.03 o 7 9 1 0 2.18 5.89 2.22 < 7 9 2 0 131.54 133.66 2.30 o 7 10 0 0 1.22 0.49 1.91 < 7 10 1 0 8.22 9.66 2.75 o 7 10 2 0 0.93 0.75 2.35 < 7 11 0 0 6.54 6.34 1.91 o 7 11 1 0 6.16 0.22 2.13 < 8 0 0 0 783.81 887.47 6.20 o 8 0 1 0 4.41 5.05 0.97 o 8 0 2 0 462.62 489.03 4.43 o 8 0 3 0 1.33 1.55 1.37 < 8 1 0 0 162.80 178.77 2.17 o 8 1 0 1 0.77 -2.16 6.90 < 8 1 1 -1 3.21 7.76 6.47 < 8 1 1 0 111.83 115.84 1.24 o 8 1 1 1 3.43 6.47 17.67 < 8 1 2 -1 0.22 -2.16 6.47 < 8 1 2 0 94.50 98.03 1.68 o 8 1 3 0 39.72 37.98 1.60 o 8 2 0 0 0.64 2.39 1.02 < 8 2 0 1 19.90 18.97 6.90 < 8 2 1 -1 5.98 1.29 6.04 < 8 2 1 0 31.28 33.99 0.97 o 8 2 2 -1 6.34 10.35 7.33 < 8 2 2 0 0.50 1.86 0.84 < 8 2 2 1 10.12 -0.43 19.40 < 8 2 3 -1 1.97 -9.92 21.12 < 8 2 3 0 11.48 10.24 1.73 o 8 2 4 0 0.24 0.97 2.04 < 8 3 0 0 23.84 25.30 1.46 o 8 3 0 1 0.50 0.86 8.62 < 8 3 1 -1 23.31 37.07 7.76 o 8 3 1 0 18.12 18.39 0.93 o 8 3 2 0 15.74 15.73 0.97 o 8 3 3 0 9.44 8.73 1.64 o 8 3 4 0 7.21 6.29 1.51 o 8 4 0 0 67.26 66.96 1.86 o 8 4 1 -1 1.14 12.07 8.62 < 8 4 1 0 189.68 194.86 2.04 o 8 4 2 0 39.66 40.33 1.60 o 8 4 3 0 83.96 86.59 1.99 o 8 5 0 0 201.30 212.89 3.24 o 8 5 1 0 160.72 171.41 2.04 o 8 5 2 0 128.10 136.45 1.99 o 8 5 3 0 70.56 75.87 2.26 o 8 6 0 0 46.97 48.79 2.04 o 8 6 1 0 8.03 7.84 1.24 o 8 6 2 0 26.98 33.02 1.73 o 8 6 3 0 5.42 6.56 1.77 o 8 7 0 0 54.51 54.64 2.13 o 8 7 1 0 26.17 27.12 1.64 o 8 7 2 0 35.30 36.60 1.64 o 8 7 3 0 11.28 11.66 1.42 o 8 8 0 0 13.88 11.79 2.79 o 8 8 1 0 41.26 43.21 1.99 o 8 8 2 0 8.72 10.46 1.55 o 8 9 0 0 4.11 2.35 2.17 < 8 9 1 0 15.53 20.83 2.39 o 8 9 2 0 3.11 4.87 1.42 o 8 10 0 0 44.15 33.10 2.53 o 8 10 1 0 12.49 14.27 2.75 o 9 0 1 -1 0.02 13.36 9.48 < 9 1 0 0 112.02 119.88 1.86 o 9 1 1 -1 5.60 2.16 6.90 < 9 1 1 0 25.18 24.95 0.84 o 9 1 2 0 69.52 67.63 1.77 o 9 1 3 0 10.82 11.74 1.46 o 9 2 0 0 103.60 110.66 2.13 o 9 2 1 -1 0.49 -8.62 6.90 < 9 2 1 0 166.56 176.73 1.55 o 9 2 2 0 67.21 72.15 1.55 o 9 2 3 0 75.84 84.69 2.26 o 9 3 0 0 0.00 -2.39 2.22 < 9 3 1 0 119.76 129.62 1.73 o 9 3 2 0 0.01 0.18 0.84 < 9 3 3 0 49.75 52.03 1.91 o 9 4 0 0 1.33 3.72 1.51 < 9 4 1 0 16.39 15.64 1.29 o 9 4 2 0 1.60 0.84 0.93 < 9 4 3 0 4.84 7.89 1.55 o 9 5 0 0 51.25 49.19 2.17 o 9 5 1 0 64.38 68.82 1.51 o 9 5 2 0 33.96 35.45 1.33 o 9 5 3 0 29.23 29.74 1.95 o 9 6 0 0 45.43 41.57 1.86 o 9 6 1 0 0.29 -0.44 1.11 < 9 6 2 0 29.79 33.55 1.55 o 9 6 3 0 0.04 0.44 1.06 < 9 7 0 0 57.06 57.83 2.04 o 9 7 1 0 1.39 1.33 1.29 < 9 7 2 0 38.98 46.62 1.73 o 9 8 0 0 56.98 50.87 2.57 o 9 8 1 0 6.20 6.65 1.33 o 9 8 2 0 37.14 39.13 1.60 o 9 9 0 0 3.02 0.49 1.99 < 9 9 1 0 93.12 97.27 2.39 o 9 10 0 0 47.29 41.97 2.35 o 10 0 0 0 126.87 102.01 4.03 o 10 0 1 0 459.37 486.59 3.59 o 10 0 2 0 85.06 86.77 3.24 o 10 1 0 0 1.32 2.84 1.02 < 10 1 1 0 41.12 41.04 1.06 o 10 1 2 0 0.80 -1.20 1.29 < 10 1 3 0 20.19 22.16 2.39 o 10 2 0 0 108.98 120.01 2.57 o 10 2 1 0 6.78 5.58 0.89 o 10 2 2 0 66.83 65.28 1.64 o 10 2 3 0 4.65 6.69 1.46 o 10 3 0 0 14.65 12.94 1.68 o 10 3 1 0 5.22 6.38 1.11 o 10 3 2 0 10.79 10.99 1.11 o 10 3 3 0 1.88 0.31 1.37 < 10 4 0 0 147.73 143.67 2.97 o 10 4 1 0 0.62 0.62 1.29 < 10 4 2 0 96.88 93.29 1.46 o 10 4 3 0 0.20 1.82 1.37 < 10 5 0 0 0.22 3.19 1.51 < 10 5 1 0 11.16 11.08 1.46 o 10 5 2 0 0.15 -0.27 0.97 < 10 6 0 0 0.56 -0.53 1.33 < 10 6 1 0 73.13 74.76 1.82 o 10 6 2 0 0.17 0.97 1.55 < 10 7 0 0 0.05 1.33 1.33 < 10 7 1 0 1.74 -1.95 1.33 < 10 7 2 0 0.07 -0.31 1.24 < 10 8 0 0 100.80 88.63 2.84 o 10 8 1 0 0.02 0.04 1.15 < 11 1 0 0 30.71 26.19 1.68 o 11 1 1 0 12.03 10.72 0.89 o 11 1 2 0 18.81 20.08 1.77 o 11 1 3 0 7.34 10.37 2.13 o 11 2 0 0 43.48 40.33 1.91 o 11 2 1 0 27.93 25.35 1.11 o 11 2 2 0 29.14 34.12 2.39 o 11 3 0 0 0.07 -3.81 1.42 < 11 3 1 0 165.51 156.48 2.04 o 11 3 2 0 0.01 -0.53 1.24 < 11 4 0 0 11.89 9.22 1.73 o 11 4 1 0 2.43 3.72 1.06 o 11 4 2 0 7.46 6.91 1.29 o 11 5 0 0 47.60 46.49 1.99 o 11 5 1 0 6.68 7.58 1.11 o 11 5 2 0 34.75 31.51 1.86 o 11 6 0 0 0.03 -0.49 1.42 < 11 6 1 0 6.92 5.41 1.51 o 11 6 2 0 0.00 -0.93 1.55 < 11 7 0 0 82.31 76.53 3.24 o 11 7 1 0 6.91 7.22 1.29 o 12 0 0 0 12.34 13.25 1.42 o 12 0 1 0 0.08 0.49 1.02 < 12 0 2 0 7.66 10.10 2.04 o 12 1 0 0 14.11 11.30 1.46 o 12 1 1 0 6.90 6.96 0.93 o 12 1 2 0 8.87 10.68 2.04 o 12 2 0 0 21.22 15.78 2.48 o 12 2 1 0 72.97 67.89 1.46 o 12 2 2 0 14.70 15.69 1.46 o 12 3 0 0 1.17 3.15 1.51 < 12 3 1 0 0.51 -0.49 1.02 < 12 3 2 0 1.18 -2.30 2.08 < 12 4 0 0 6.92 4.34 1.55 < 12 4 1 0 2.04 2.04 1.11 < 12 5 0 0 74.50 77.02 2.22 o 12 5 1 0 57.46 57.17 1.42 o 12 6 0 0 57.31 53.31 2.04 o 13 1 0 0 1.18 1.37 1.46 < 13 1 1 0 30.86 27.56 1.73 o 13 2 0 0 11.18 9.08 1.55 o 13 2 1 0 24.07 24.37 1.29 o 13 3 0 0 120.92 119.88 2.53 o 13 3 1 0 9.97 10.10 2.08 o