#------------------------------------------------------------------------------ #$Date: 2017-07-25 11:51:14 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/80/2108097.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108097 _cell_angle_alpha 69.762 _cell_angle_beta 69.338 _cell_angle_gamma 69.366 _cell_length_a 13.7266 _cell_length_b 16.9157 _cell_length_c 16.9080 _exptl_crystal_F_000 1824.00 _reflns_d_resolution_high 0.7505 _cod_data_source_file eb5059mn2293sup2.hkl _cod_data_source_block mn2293 _shelx_title ' mn2293 in P-1 [Ni(Hpydc)2] . 3 H2O low temp form' _shelx_refln_list_code 4 _shelx_f_calc_maximum 344.70 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7.77 60.90 9.06 o 2 0 0 67192.84 71562.09 1557.15 o 3 0 0 10.14 48.53 2.74 o 4 0 0 1200.95 1579.38 25.55 o 5 0 0 32.73 33.54 4.29 o 6 0 0 44181.08 46103.82 717.36 o 7 0 0 86.21 86.79 5.23 o 8 0 0 12422.60 11508.37 179.04 o 9 0 0 0.24 20.16 2.46 o 10 0 0 3845.13 3894.30 63.06 o 11 0 0 66.54 66.35 7.41 o 12 0 0 11698.19 11387.25 207.17 o 13 0 0 1.59 30.82 7.26 o 14 0 0 6788.70 6763.48 126.23 o 15 0 0 10.69 34.98 10.35 o 16 0 0 2320.67 2403.06 63.13 o -16 1 0 801.80 780.39 40.76 o -15 1 0 281.67 257.41 15.07 o -14 1 0 363.60 362.17 13.40 o -13 1 0 329.15 316.33 11.69 o -12 1 0 610.63 573.45 15.65 o -11 1 0 4.86 10.35 3.74 o -10 1 0 794.48 789.53 15.80 o -9 1 0 249.26 253.59 7.07 o -8 1 0 142.28 147.26 5.42 o -7 1 0 36.51 33.58 2.80 o -6 1 0 1433.04 1469.12 24.58 o -5 1 0 59.02 68.44 2.71 o -4 1 0 442.67 456.47 8.41 o -3 1 0 320.13 306.15 6.16 o -2 1 0 796.02 815.98 13.25 o -1 1 0 90.46 118.54 3.74 o 1 1 0 213.87 225.26 4.48 o 2 1 0 237.59 247.84 11.76 o 3 1 0 422.95 404.48 7.12 o 4 1 0 603.95 698.60 19.59 o 5 1 0 12.57 23.83 2.21 o 6 1 0 334.33 354.55 7.42 o 7 1 0 186.10 195.14 5.11 o 8 1 0 271.53 257.04 6.91 o 9 1 0 433.53 442.89 9.67 o 10 1 0 273.29 267.53 12.74 o 11 1 0 151.09 152.42 7.40 o 12 1 0 466.27 457.38 13.40 o 13 1 0 866.64 839.90 23.22 o 14 1 0 277.42 260.73 11.91 o 15 1 0 58.39 55.91 8.23 o 16 1 0 103.19 112.27 11.41 o -16 2 0 23.83 29.76 10.35 o -15 2 0 6252.71 6299.84 146.38 o -14 2 0 26.70 23.91 5.45 o -13 2 0 5309.71 5458.88 102.84 o -12 2 0 763.73 699.54 18.13 o -11 2 0 8993.44 9074.24 165.59 o -10 2 0 150.09 153.41 6.29 o -9 2 0 16790.49 17056.22 264.43 o -8 2 0 35.80 42.64 3.23 o -7 2 0 1371.16 1018.33 18.11 o -6 2 0 1734.77 1890.38 31.05 o -5 2 0 2135.17 1805.49 29.76 o -4 2 0 11926.95 12375.92 191.49 o -3 2 0 13517.14 12278.95 189.39 o -2 2 0 27290.00 27860.94 441.57 o -1 2 0 32360.13 34015.78 524.66 o 0 2 0 2115.98 2195.04 34.29 o 2 2 0 477.86 490.63 8.23 o 3 2 0 74776.34 75179.27 1337.64 o 4 2 0 35010.88 37782.57 692.48 o 5 2 0 42526.35 42843.27 662.77 o 6 2 0 816.29 917.13 18.17 o 7 2 0 39121.51 39606.95 611.18 o 8 2 0 83.98 68.73 6.39 o 9 2 0 4291.10 4230.68 67.75 o 10 2 0 1317.73 1409.49 29.11 o 11 2 0 7471.44 7492.79 137.19 o 12 2 0 492.24 540.90 14.60 o 13 2 0 11955.41 11784.71 214.13 o 14 2 0 771.28 748.31 25.15 o 15 2 0 3777.54 3773.45 91.94 o 16 2 0 14.29 13.99 7.15 o -15 3 0 625.99 641.75 33.64 o -14 3 0 223.84 214.35 10.94 o -13 3 0 921.32 886.75 22.15 o -12 3 0 306.56 305.52 11.44 o -11 3 0 17.02 31.83 4.69 o -10 3 0 298.83 289.47 8.23 o -9 3 0 569.21 579.80 15.92 o -8 3 0 148.11 153.49 5.47 o -7 3 0 326.23 342.01 9.71 o -6 3 0 3031.05 3050.22 49.17 o -5 3 0 898.36 873.53 15.53 o -4 3 0 1036.95 1082.48 18.43 o -3 3 0 279.74 280.73 6.44 o -2 3 0 1556.16 1481.74 23.77 o -1 3 0 660.05 635.23 10.66 o 0 3 0 23.56 26.41 1.49 o 1 3 0 15.09 26.57 1.29 o 2 3 0 427.88 440.97 8.03 o 3 3 0 445.30 450.96 7.91 o 4 3 0 1104.50 1169.64 19.08 o 5 3 0 425.26 436.77 8.20 o 6 3 0 503.06 495.23 9.50 o 7 3 0 313.33 280.21 6.24 o 8 3 0 188.06 173.54 7.66 o 9 3 0 364.59 354.97 7.99 o 10 3 0 508.71 540.27 13.85 o 11 3 0 98.21 118.28 6.64 o 12 3 0 166.39 165.21 8.44 o 13 3 0 407.57 416.35 13.28 o 14 3 0 6.32 10.65 5.89 o 15 3 0 102.60 104.61 10.49 o 16 3 0 161.76 139.65 12.33 o -15 4 0 105.22 106.10 14.23 o -14 4 0 2348.95 2514.03 63.58 o -13 4 0 190.42 225.11 10.69 o -12 4 0 6799.18 6950.26 129.23 o -11 4 0 5.32 10.78 3.74 o -10 4 0 11517.28 11551.52 180.98 o -9 4 0 830.46 799.54 16.17 o -8 4 0 12042.72 11426.97 178.55 o -7 4 0 813.53 832.10 15.68 o -6 4 0 13637.56 13242.17 205.40 o -5 4 0 9472.67 9873.91 153.64 o -4 4 0 16353.14 16257.00 251.17 o -3 4 0 11324.02 11516.60 178.23 o -2 4 0 9102.90 8954.87 138.77 o -1 4 0 27068.86 27775.29 429.88 o 0 4 0 75836.13 75823.45 1349.34 o 1 4 0 4065.52 4270.41 66.47 o 2 4 0 8033.24 7633.56 118.23 o 3 4 0 619.23 650.31 11.15 o 4 4 0 172.37 164.28 6.34 o 5 4 0 1609.61 1374.04 22.63 o 6 4 0 26061.26 26191.01 403.84 o 7 4 0 1116.40 1221.72 20.99 o 8 4 0 22814.62 21901.42 338.02 o 9 4 0 3190.24 3448.87 55.61 o 10 4 0 12688.02 12834.79 231.32 o 11 4 0 10.06 8.46 3.43 o 12 4 0 6943.41 6892.24 127.22 o 13 4 0 2536.07 2684.97 53.24 o 14 4 0 4992.47 4847.13 113.90 o 15 4 0 512.70 510.59 20.57 o 16 4 0 5367.31 5339.06 126.71 o 17 4 0 13.57 23.84 18.76 o -14 5 0 79.40 98.70 16.17 o -13 5 0 14.21 8.56 5.89 o -12 5 0 462.37 455.79 21.35 o -11 5 0 4.60 1.98 3.94 o -10 5 0 55.60 49.92 4.34 o -9 5 0 203.30 210.81 8.03 o -8 5 0 134.25 149.59 5.82 o -7 5 0 2311.98 2289.73 38.33 o -6 5 0 1945.28 1975.33 33.14 o -5 5 0 1127.52 1200.73 21.02 o -4 5 0 522.47 581.25 11.12 o -3 5 0 161.27 145.26 4.17 o -2 5 0 384.16 419.55 8.07 o -1 5 0 1406.99 1431.30 23.11 o 0 5 0 123.97 149.28 3.94 o 1 5 0 2855.34 2893.32 45.61 o 2 5 0 807.20 832.04 14.06 o 3 5 0 1972.46 1940.19 31.21 o 4 5 0 146.59 155.68 4.02 o 5 5 0 1253.30 1226.62 20.69 o 6 5 0 331.44 339.00 7.07 o 7 5 0 414.94 392.80 16.29 o 8 5 0 261.88 247.17 6.11 o 9 5 0 115.70 129.62 4.74 o 10 5 0 191.31 195.51 7.56 o 11 5 0 672.48 650.82 16.10 o 12 5 0 99.40 107.31 6.64 o 13 5 0 646.36 621.24 38.82 o 14 5 0 510.13 505.24 20.07 o 15 5 0 108.34 112.47 10.86 o 16 5 0 93.75 89.79 10.49 o 17 5 0 253.97 239.11 16.47 o -14 6 0 253.68 274.47 15.99 o -13 6 0 2712.40 2782.36 69.07 o -12 6 0 662.54 697.77 23.32 o -11 6 0 8057.46 8294.45 155.25 o -10 6 0 115.46 124.46 6.29 o -9 6 0 13242.83 13094.36 204.91 o -8 6 0 319.78 290.33 8.07 o -7 6 0 15790.78 15215.95 236.61 o -6 6 0 40.33 53.70 5.04 o -5 6 0 5740.97 5572.92 88.14 o -4 6 0 3861.52 3941.49 62.74 o -3 6 0 47459.40 46807.21 724.87 o -2 6 0 1854.79 1674.66 27.64 o -1 6 0 43031.86 41621.75 644.01 o 0 6 0 904.33 1002.97 15.14 o 1 6 0 4764.09 4246.24 76.93 o 2 6 0 10836.64 10968.83 169.66 o 3 6 0 2832.72 2637.23 42.05 o 4 6 0 1297.19 1417.17 23.45 o 5 6 0 24654.50 25002.26 385.57 o 6 6 0 794.32 761.34 13.70 o 7 6 0 28739.12 29135.11 449.61 o 8 6 0 10053.61 10496.78 163.50 o 9 6 0 16036.21 15804.23 245.02 o 10 6 0 2267.61 2330.79 45.52 o 11 6 0 4414.85 4500.64 84.39 o 12 6 0 707.16 645.87 16.53 o 13 6 0 6561.45 6513.98 149.58 o 14 6 0 217.44 222.54 13.63 o 15 6 0 5610.51 5618.47 131.74 o 16 6 0 299.52 317.66 17.31 o 17 6 0 2946.06 2966.37 76.39 o -14 7 0 18.10 12.45 7.15 o -13 7 0 274.93 284.31 16.17 o -12 7 0 385.90 343.45 16.39 o -11 7 0 42.04 57.02 6.20 o -10 7 0 811.95 752.88 19.16 o -9 7 0 33.47 34.41 4.69 o -8 7 0 1181.68 1142.58 21.49 o -7 7 0 2026.22 1961.98 33.79 o -6 7 0 600.80 550.55 11.59 o -5 7 0 1525.79 1520.95 30.09 o -4 7 0 1668.97 1773.05 29.74 o -3 7 0 547.83 569.68 10.94 o -2 7 0 1978.61 1989.66 48.73 o -1 7 0 540.78 631.57 11.59 o 0 7 0 2368.72 2602.85 41.88 o 1 7 0 101.81 92.47 2.95 o 2 7 0 3536.88 3621.17 57.25 o 3 7 0 1186.33 1225.94 20.70 o 4 7 0 1686.09 1773.11 29.27 o 5 7 0 1695.98 1731.17 28.62 o 6 7 0 1000.81 1026.69 20.66 o 7 7 0 1412.51 1560.85 26.51 o 8 7 0 1890.32 1930.67 33.24 o 9 7 0 49.81 52.30 3.33 o 10 7 0 395.75 390.08 15.70 o 11 7 0 417.47 401.59 11.76 o 12 7 0 457.37 450.16 13.28 o 13 7 0 574.51 555.19 20.07 o 14 7 0 39.81 57.42 12.94 o 15 7 0 160.84 151.88 25.23 o 16 7 0 47.28 39.73 8.66 o 17 7 0 386.35 364.22 19.65 o -13 8 0 91.62 86.83 9.57 o -12 8 0 2298.58 2281.40 58.53 o -11 8 0 87.83 80.84 7.78 o -10 8 0 7693.62 7554.30 139.93 o -9 8 0 403.16 403.59 12.66 o -8 8 0 225.00 221.61 9.13 o -7 8 0 7509.33 7435.23 136.20 o -6 8 0 6391.83 6275.03 99.61 o -5 8 0 7118.09 6724.86 106.08 o -4 8 0 15143.00 14306.87 222.05 o -3 8 0 1153.70 1122.16 19.84 o -2 8 0 3556.33 2907.55 46.87 o -1 8 0 7672.56 8027.80 125.01 o 0 8 0 35584.95 35540.34 549.24 o 1 8 0 7058.68 6822.29 106.58 o 2 8 0 25898.46 25083.91 387.51 o 3 8 0 637.10 634.60 11.96 o 4 8 0 18777.76 18079.65 279.31 o 5 8 0 181.40 226.68 7.84 o 6 8 0 26156.61 26036.76 401.58 o 7 8 0 5664.99 6036.45 95.25 o 8 8 0 22136.58 22150.73 342.38 o 9 8 0 17.74 29.07 4.11 o 10 8 0 5224.03 5354.59 99.59 o 11 8 0 61.24 81.90 5.88 o 12 8 0 8890.54 9116.58 167.06 o 13 8 0 2425.90 2511.15 63.11 o 14 8 0 8864.00 9100.25 206.76 o 15 8 0 878.70 904.33 30.15 o 16 8 0 4164.12 4216.72 147.50 o -13 9 0 48.69 50.46 12.94 o -12 9 0 139.99 150.84 11.41 o -11 9 0 656.70 645.49 18.65 o -10 9 0 10.85 4.04 4.23 o -9 9 0 1015.22 961.78 23.37 o -8 9 0 300.31 299.70 10.83 o -7 9 0 3.81 4.98 3.43 o -6 9 0 821.34 808.24 19.10 o -5 9 0 1418.38 1427.32 25.35 o -4 9 0 1288.65 1307.21 23.22 o -3 9 0 310.78 288.68 8.03 o -2 9 0 183.49 174.81 5.15 o -1 9 0 270.12 260.73 6.48 o 0 9 0 535.44 542.81 12.19 o 1 9 0 2621.13 2651.07 43.00 o 2 9 0 205.52 211.34 5.59 o 3 9 0 795.93 887.99 21.29 o 4 9 0 254.95 255.76 9.34 o 5 9 0 133.73 150.62 4.82 o 6 9 0 913.83 984.48 17.93 o 7 9 0 264.27 238.79 6.73 o 8 9 0 763.45 808.80 15.64 o 9 9 0 66.88 73.81 3.88 o 10 9 0 136.16 141.55 7.13 o 11 9 0 70.96 61.33 5.26 o 12 9 0 307.86 308.07 11.64 o 13 9 0 191.53 201.94 12.71 o 14 9 0 75.89 71.44 9.01 o 15 9 0 275.51 283.29 15.83 o 16 9 0 9.69 17.58 7.74 o -12 10 0 864.21 870.77 42.70 o -11 10 0 1749.32 1780.58 40.32 o -10 10 0 536.97 502.64 19.97 o -9 10 0 6473.45 6375.37 119.51 o -8 10 0 385.00 397.97 15.12 o -7 10 0 5572.38 5348.63 100.08 o -6 10 0 443.41 470.17 13.31 o -5 10 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772.77 14.97 o 0 11 0 1927.40 1892.23 32.12 o 1 11 0 3092.14 3049.00 49.61 o 2 11 0 1630.04 1546.28 26.49 o 3 11 0 452.59 492.07 12.10 o 4 11 0 239.59 247.13 6.90 o 5 11 0 1081.56 1073.06 19.55 o 6 11 0 1076.01 1103.70 20.04 o 7 11 0 290.09 293.44 8.03 o 8 11 0 1132.50 1146.10 21.00 o 9 11 0 328.88 345.75 9.14 o 10 11 0 1120.86 1105.37 24.59 o 11 11 0 264.10 273.90 10.31 o 12 11 0 282.36 273.26 26.52 o 13 11 0 56.72 53.94 12.94 o 14 11 0 70.46 59.80 9.01 o 15 11 0 6.05 13.99 7.15 o 16 11 0 96.74 75.30 9.94 o -11 12 0 946.42 987.86 32.94 o -10 12 0 2773.52 2770.85 70.90 o -9 12 0 4478.43 4395.80 105.67 o -8 12 0 2093.23 2048.82 53.98 o -7 12 0 4723.80 4590.84 113.86 o -6 12 0 2830.57 2718.54 54.23 o -5 12 0 1526.05 1455.59 31.54 o -4 12 0 12073.01 11723.46 212.88 o -3 12 0 701.12 605.57 20.44 o -2 12 0 4763.50 4581.17 85.86 o -1 12 0 2909.26 2890.07 55.48 o 0 12 0 4556.71 4387.41 70.64 o 1 12 0 1833.27 1819.82 31.18 o 2 12 0 5103.98 4721.55 75.51 o 3 12 0 364.32 350.66 8.45 o 4 12 0 18833.22 18337.05 284.32 o 5 12 0 780.73 789.36 15.51 o 6 12 0 14881.93 15071.40 234.35 o 7 12 0 2398.55 2395.81 40.58 o 8 12 0 4043.88 4040.63 65.66 o 9 12 0 433.27 407.23 10.27 o 10 12 0 2152.38 2231.56 44.78 o 11 12 0 788.96 797.86 19.80 o 12 12 0 5844.14 6066.31 139.50 o 13 12 0 2367.68 2357.51 59.88 o 14 12 0 1480.26 1601.72 60.81 o 15 12 0 105.22 121.16 11.19 o 16 12 0 1120.74 1161.48 36.56 o -10 13 0 1032.28 1041.03 34.30 o -9 13 0 213.68 191.98 14.16 o -8 13 0 260.35 279.57 16.47 o -7 13 0 135.95 129.91 11.41 o -6 13 0 296.42 311.58 18.11 o -5 13 0 598.12 545.78 20.57 o -4 13 0 2611.24 2544.55 63.58 o -3 13 0 474.91 434.90 13.13 o -2 13 0 318.30 278.43 9.69 o -1 13 0 100.46 97.86 6.26 o 0 13 0 250.98 269.67 9.58 o 1 13 0 828.77 717.66 14.58 o 2 13 0 1439.21 1355.71 24.34 o 3 13 0 1986.77 1937.92 33.12 o 4 13 0 1040.28 1023.39 19.18 o 5 13 0 1167.13 1148.99 21.33 o 6 13 0 151.41 132.89 5.77 o 7 13 0 1055.08 1038.67 19.87 o 8 13 0 221.58 205.42 7.55 o 9 13 0 591.23 593.89 15.31 o 10 13 0 439.68 435.30 13.14 o 11 13 0 124.07 127.16 7.56 o 12 13 0 977.54 972.35 29.64 o 13 13 0 657.30 629.29 23.21 o 14 13 0 69.33 71.54 9.57 o 15 13 0 309.94 295.88 17.31 o -9 14 0 1904.93 1850.33 52.15 o -8 14 0 1012.06 1032.07 33.85 o -7 14 0 2224.18 2123.22 56.72 o -6 14 0 94.19 87.38 10.06 o -5 14 0 3353.08 3356.29 82.34 o -4 14 0 1987.02 1870.34 49.86 o -3 14 0 6728.69 6382.61 147.29 o -2 14 0 2083.80 2075.36 53.52 o -1 14 0 3471.60 3299.67 79.58 o 0 14 0 167.05 165.35 13.97 o 1 14 0 26.76 30.75 4.20 o 2 14 0 185.35 215.80 8.71 o 3 14 0 3943.88 3907.38 57.15 o 4 14 0 1093.83 1066.99 20.34 o 5 14 0 3112.89 3162.32 52.38 o 6 14 0 2261.05 2249.92 38.63 o 7 14 0 2795.02 2710.86 45.75 o 8 14 0 94.24 105.94 5.77 o 9 14 0 1735.39 1763.31 31.67 o 10 14 0 1696.05 1742.69 36.33 o 11 14 0 1619.03 1658.07 43.89 o 12 14 0 1254.84 1258.00 36.06 o 13 14 0 1438.76 1503.82 41.56 o 14 14 0 86.09 96.19 10.26 o 15 14 0 1509.34 1530.30 44.31 o -8 15 0 72.90 46.75 9.70 o -7 15 0 395.43 379.97 23.94 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531.10 559.71 23.21 o 6 15 20 1494.75 1640.00 46.14 o 7 15 20 322.71 320.27 18.03 o 8 15 20 2250.78 2266.97 59.88 o 9 15 20 1998.13 2174.06 58.05 o 10 15 20 598.04 626.74 25.42 o 11 15 20 1110.09 1183.75 42.05 o 5 16 20 166.34 147.50 19.41 o 6 16 20 992.68 996.20 32.90 o 7 16 20 81.35 106.33 11.79 o 8 16 20 1426.66 1488.95 43.80 o 9 16 20 7.55 18.89 9.01 o 10 16 20 909.64 875.86 33.64 o 3 0 21 470.65 463.82 22.64 o 4 0 21 760.61 866.88 46.58 o 5 0 21 634.01 642.80 27.45 o 6 0 21 49.10 46.66 11.41 o 2 1 21 213.33 220.49 15.83 o 3 1 21 710.07 813.51 29.64 o 4 1 21 218.52 231.60 24.58 o 5 1 21 12.11 18.11 9.15 o 6 1 21 281.19 306.67 20.13 o 7 1 21 59.28 63.83 11.89 o 8 1 21 108.36 119.83 14.23 o 1 2 21 2.36 12.94 9.15 o 2 2 21 693.70 707.97 32.99 o 3 2 21 242.20 283.44 17.68 o 4 2 21 966.58 906.99 46.58 o 5 2 21 597.12 639.61 26.48 o 6 2 21 171.93 197.07 24.58 o 7 2 21 93.88 95.25 25.23 o 8 2 21 944.43 950.83 47.87 o 9 2 21 737.96 658.10 31.05 o 1 3 21 42.56 46.31 9.94 o 2 3 21 385.31 415.37 20.98 o 3 3 21 109.74 128.57 12.33 o 4 3 21 1320.25 1399.95 60.81 o 5 3 21 348.53 367.97 20.57 o 6 3 21 1543.95 1564.07 82.16 o 7 3 21 874.56 900.47 32.47 o 8 3 21 18.94 24.58 10.06 o 9 3 21 239.12 235.28 17.82 o 10 3 21 21.13 23.94 10.06 o 0 4 21 679.70 762.38 45.28 o 1 4 21 11.92 7.12 16.17 o 2 4 21 22.41 37.08 8.66 o 3 4 21 59.37 68.04 11.64 o 4 4 21 224.51 213.49 22.00 o 5 4 21 441.78 484.44 29.76 o 6 4 21 69.64 82.17 11.89 o 7 4 21 208.76 205.02 22.64 o 8 4 21 178.95 193.00 16.47 o 9 4 21 1936.23 1966.74 80.87 o 10 4 21 146.24 151.07 14.64 o 0 5 21 294.27 349.34 27.17 o 1 5 21 77.55 76.47 10.49 o 2 5 21 461.42 477.12 37.52 o 3 5 21 631.01 671.51 37.52 o 4 5 21 152.56 163.72 14.16 o 5 5 21 511.92 547.95 23.79 o 6 5 21 95.69 96.64 16.17 o 7 5 21 244.50 230.96 16.47 o 8 5 21 316.33 338.22 20.57 o 9 5 21 555.17 564.98 26.06 o 10 5 21 59.91 56.02 11.41 o 11 5 21 839.83 904.44 43.34 o 0 6 21 104.87 113.86 16.82 o 1 6 21 830.46 896.64 41.40 o 2 6 21 264.09 249.79 15.99 o 3 6 21 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2126.44 2099.76 58.55 o 8 6 22 368.21 360.89 21.49 o 9 6 22 969.01 965.39 35.21 o 4 7 22 321.24 375.22 28.46 o 5 7 22 321.68 310.55 18.74 o 6 7 22 266.13 279.72 18.74 o 7 7 22 2234.54 2211.70 150.09 o 8 7 22 587.83 656.73 76.98 o 9 7 22 4185.05 4316.81 192.78 o 5 8 22 563.89 608.11 36.23 o 6 8 22 456.44 509.89 23.32 o 7 8 22 967.26 938.17 76.98 o 8 8 22 714.30 713.79 28.32 o 9 8 22 2444.89 2619.03 69.98 o 5 9 22 365.26 370.04 29.76 o 6 9 22 906.26 934.16 46.58 o 7 9 22 232.09 247.92 38.82 o 8 9 22 648.15 705.98 28.32 o 9 9 22 1971.66 2065.35 161.09 o 5 10 22 72.61 59.52 15.53 o 6 10 22 287.59 278.18 25.88 o 7 10 22 486.16 511.07 34.93 o 8 10 22 597.20 602.94 37.52 o 9 10 22 19.00 19.08 9.01 o 5 11 22 1207.64 1176.57 36.06 o 6 11 22 233.37 234.80 34.29 o 7 11 22 1033.89 1067.43 51.75 o 8 11 22 159.92 164.32 22.00 o 9 11 22 2430.46 2679.58 102.21 o 7 12 22 679.84 695.29 32.99 o 8 12 22 16.59 23.29 14.23 o