#------------------------------------------------------------------------------ #$Date: 2017-07-25 11:51:43 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199055 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/81/2108100.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108100 _cell_angle_alpha 77.490 _cell_angle_beta 71.742 _cell_angle_gamma 76.504 _cell_length_a 13.6173 _cell_length_b 14.3205 _cell_length_c 15.4896 _exptl_crystal_F_000 1454.12 _reflns_d_resolution_high 0.6800 _cod_data_source_file rm5002p_1_newsup3.hkl _cod_data_source_block p_1_new _shelx_title ' p_1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 405.15 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 387.91 140.78 3.58 o 2 0 0 468.69 618.51 13.05 o 3 0 0 3711.69 3994.33 72.92 o 4 0 0 5166.74 4735.44 87.25 o 5 0 0 4403.85 4271.54 80.08 o 6 0 0 3350.07 3142.00 61.08 o 7 0 0 5102.26 5506.09 103.69 o 8 0 0 3434.43 3451.87 68.67 o 9 0 0 6451.18 6694.43 127.27 o 10 0 0 254.21 238.29 13.18 o 11 0 0 205.34 246.40 14.59 o 12 0 0 2171.35 2144.14 50.03 o 13 0 0 5.35 54.84 14.31 o 14 0 0 366.07 362.45 31.00 o 15 0 0 445.50 417.29 33.38 o 16 0 0 2.03 2.38 14.31 o 17 0 0 415.76 425.64 39.34 o 18 0 0 367.29 350.52 35.77 o -18 1 0 2.24 33.38 16.69 o -17 1 0 20.33 57.23 17.88 o -16 1 0 82.13 79.88 19.08 o -15 1 0 33.25 58.42 16.69 o -14 1 0 257.78 289.72 28.61 o -13 1 0 41.31 57.23 15.50 o -12 1 0 46.79 50.31 9.27 o -11 1 0 44.69 53.78 9.54 o -10 1 0 7488.74 7245.83 138.23 o -9 1 0 2232.37 1889.85 60.21 o -8 1 0 4870.94 4839.81 93.57 o -7 1 0 407.36 499.85 15.95 o -6 1 0 3325.78 3471.40 67.43 o -5 1 0 229.09 303.10 10.51 o -4 1 0 9532.88 9932.43 179.15 o -3 1 0 2022.93 1737.49 34.14 o -2 1 0 8133.68 9114.61 162.71 o -1 1 0 35752.54 33495.05 639.05 o 1 1 0 59624.80 51251.65 920.17 o 2 1 0 9665.33 11969.57 212.03 o 3 1 0 22937.96 24266.02 606.86 o 4 1 0 3876.36 4524.56 83.04 o 5 1 0 11.37 18.37 3.72 o 6 1 0 3.79 58.42 8.35 o 7 1 0 820.42 730.11 18.84 o 8 1 0 189.81 154.53 9.16 o 9 1 0 2434.80 2495.17 52.19 o 10 1 0 1949.21 2035.22 44.96 o 11 1 0 220.30 239.64 22.65 o 12 1 0 139.94 140.69 19.08 o 13 1 0 1054.70 1105.22 48.88 o 14 1 0 1444.42 1511.78 62.00 o 15 1 0 50.48 65.57 16.69 o 16 1 0 32.64 72.73 19.08 o 17 1 0 24.36 44.11 17.88 o 18 1 0 27.50 28.61 16.69 o -17 2 0 39.86 66.77 19.08 o -16 2 0 452.86 493.59 36.96 o -15 2 0 761.12 720.12 41.73 o -14 2 0 78.87 73.92 17.88 o -13 2 0 27.34 36.13 9.67 o -12 2 0 452.75 386.92 18.49 o -11 2 0 154.39 179.42 13.41 o -10 2 0 743.23 779.34 24.77 o -9 2 0 9938.69 9482.31 177.45 o -8 2 0 889.99 755.70 22.33 o -7 2 0 5120.80 5367.60 102.43 o -6 2 0 2201.29 2092.98 44.25 o -5 2 0 2365.24 2605.57 51.84 o -4 2 0 5472.04 5729.48 106.22 o -3 2 0 1726.54 2125.06 42.15 o -2 2 0 10119.26 11658.16 208.23 o -1 2 0 3113.31 3419.42 63.23 o 0 2 0 8660.21 9208.99 164.40 o 1 2 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1958.20 39.20 o -1 3 0 1122.07 1024.41 23.85 o 0 3 0 4513.21 4584.83 84.31 o 1 3 0 8.15 11.92 3.37 o 2 3 0 1376.61 1328.09 26.55 o 3 3 0 4727.69 5965.79 107.90 o 4 3 0 472.20 399.91 10.86 o 5 3 0 1440.12 2043.33 40.36 o 6 3 0 561.00 883.09 20.54 o 7 3 0 126.84 118.16 7.45 o 8 3 0 813.97 687.18 18.32 o 9 3 0 1141.72 987.80 25.12 o 10 3 0 10873.12 10930.03 201.00 o 11 3 0 50.32 50.07 13.11 o 12 3 0 337.74 331.45 27.42 o 13 3 0 1391.72 1236.37 52.46 o 14 3 0 642.75 753.51 40.54 o 15 3 0 1747.65 1770.50 70.34 o 16 3 0 47.96 75.11 20.27 o 17 3 0 665.64 840.54 47.69 o 18 3 0 1084.04 1324.60 64.38 o -17 4 0 336.05 320.72 34.58 o -16 4 0 609.11 569.90 40.54 o -15 4 0 373.05 395.83 36.96 o -14 4 0 1567.74 1473.63 63.19 o -13 4 0 135.32 105.20 12.56 o -12 4 0 125.64 131.30 13.41 o -11 4 0 513.40 474.66 26.23 o -10 4 0 670.47 542.40 35.17 o -9 4 0 65.78 81.80 11.92 o -8 4 0 830.59 748.74 33.38 o -7 4 0 762.84 814.67 24.02 o -6 4 0 2443.15 2119.71 46.37 o -5 4 0 6047.86 5878.51 111.70 o -4 4 0 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198.12 295.68 13.05 o -4 5 0 6382.43 5912.38 112.55 o -3 5 0 777.35 533.00 16.42 o -2 5 0 12820.63 14205.62 256.71 o -1 5 0 2.73 6.36 3.72 o 0 5 0 4769.16 4498.10 85.57 o 1 5 0 3462.95 3673.79 70.82 o 2 5 0 1793.95 2066.79 42.15 o 3 5 0 200.02 399.53 13.71 o 4 5 0 808.15 1069.64 24.40 o 5 5 0 4575.66 4135.85 78.35 o 6 5 0 490.04 812.70 20.54 o 7 5 0 3091.14 3306.16 64.39 o 8 5 0 331.85 299.05 12.03 o 9 5 0 8076.98 8374.99 155.46 o 10 5 0 1626.99 1578.55 56.04 o 11 5 0 345.96 379.14 26.23 o 12 5 0 232.68 253.95 23.85 o 13 5 0 936.65 920.42 44.11 o 14 5 0 80.23 96.57 19.08 o 15 5 0 497.93 538.90 36.96 o 16 5 0 2.97 23.85 14.31 o 17 5 0 1438.42 1404.48 64.38 o 18 5 0 2568.11 2811.34 102.53 o -16 6 0 1.94 5.96 15.50 o -15 6 0 303.83 314.76 33.38 o -14 6 0 1322.17 1519.65 47.19 o -13 6 0 350.27 428.58 35.77 o -12 6 0 33.22 39.36 13.71 o -11 6 0 546.37 532.78 24.02 o -10 6 0 32.52 47.54 9.67 o -9 6 0 2021.45 1820.17 46.37 o -8 6 0 19.18 10.87 7.75 o -7 6 0 375.06 348.44 43.52 o -6 6 0 5225.41 5430.53 107.07 o -5 6 0 5527.13 5347.85 104.96 o -4 6 0 616.86 611.72 19.80 o -3 6 0 1849.32 2117.28 45.94 o -2 6 0 6.43 29.20 13.11 o -1 6 0 10223.33 10439.62 191.79 o 0 6 0 235.70 293.59 12.20 o 1 6 0 703.09 570.53 16.86 o 2 6 0 13.86 1.19 4.22 o 3 6 0 1913.31 2252.67 49.48 o 4 6 0 6283.18 6243.04 116.33 o 5 6 0 13575.25 15118.10 271.88 o 6 6 0 379.21 405.86 26.23 o 7 6 0 4045.79 3961.71 77.05 o 8 6 0 70.48 48.74 8.35 o 9 6 0 222.77 201.11 22.65 o 10 6 0 448.35 512.67 28.61 o 11 6 0 23.26 81.07 14.31 o 12 6 0 8.47 25.04 11.92 o 13 6 0 1699.02 1726.39 65.57 o 14 6 0 0.30 23.85 13.11 o 15 6 0 515.06 603.28 38.15 o 16 6 0 4.52 17.88 13.11 o 17 6 0 4.27 0.00 14.31 o 18 6 0 8.36 46.50 17.88 o -15 7 0 672.03 813.12 48.88 o -14 7 0 23.51 32.31 13.71 o -13 7 0 229.03 288.84 21.49 o -12 7 0 37.68 48.87 11.36 o -11 7 0 733.91 706.07 44.11 o -10 7 0 2229.45 2260.57 56.06 o -9 7 0 977.77 934.65 31.19 o -8 7 0 799.46 761.67 26.55 o -7 7 0 4203.80 4106.63 86.41 o -6 7 0 1617.72 1537.79 39.20 o -5 7 0 343.64 303.65 28.02 o -4 7 0 2325.00 2032.82 48.29 o -3 7 0 3337.74 3357.40 97.77 o -2 7 0 3329.14 3152.58 65.33 o -1 7 0 3.70 4.44 4.58 o 0 7 0 6730.73 6894.76 130.25 o 1 7 0 10769.62 12020.80 220.04 o 2 7 0 452.68 598.73 22.06 o 3 7 0 11762.03 12763.10 232.26 o 4 7 0 158.88 160.33 10.12 o 5 7 0 483.11 378.18 18.48 o 6 7 0 3286.12 3105.23 62.32 o 7 7 0 692.38 740.16 25.63 o 8 7 0 4443.39 4694.03 90.94 o 9 7 0 1047.63 1042.03 41.73 o 10 7 0 1610.17 1602.39 57.23 o 11 7 0 506.03 512.67 31.00 o 12 7 0 56.76 100.15 17.88 o 13 7 0 1169.59 1098.07 50.07 o 14 7 0 242.98 329.06 29.81 o 15 7 0 69.38 95.38 20.27 o 16 7 0 17.91 19.08 16.69 o 17 7 0 37.15 13.11 15.50 o 18 7 0 171.42 201.49 29.81 o -15 8 0 63.52 48.88 20.27 o -14 8 0 1122.75 1355.21 118.63 o -13 8 0 65.56 93.24 15.17 o -12 8 0 223.32 248.43 20.64 o -11 8 0 557.11 517.17 28.02 o -10 8 0 3.06 15.84 8.82 o -9 8 0 1644.38 1591.60 44.25 o -8 8 0 1097.42 996.12 32.45 o -7 8 0 24.07 53.07 9.67 o -6 8 0 1031.41 1064.48 97.17 o -5 8 0 600.63 671.00 28.02 o -4 8 0 862.96 770.91 27.42 o -3 8 0 44.61 49.66 7.98 o -2 8 0 2854.21 2572.20 56.48 o -1 8 0 1017.73 998.39 27.39 o 0 8 0 350.09 321.04 13.89 o 1 8 0 6339.88 6627.82 126.46 o 2 8 0 7419.35 7721.25 145.42 o 3 8 0 8.56 24.59 22.65 o 4 8 0 4887.23 4752.35 92.31 o 5 8 0 2739.55 2852.25 59.00 o 6 8 0 9.05 7.15 5.06 o 7 8 0 2465.62 2280.19 48.81 o 8 8 0 1617.78 1557.61 38.15 o 9 8 0 287.60 308.79 22.65 o 10 8 0 150.41 116.84 16.69 o 11 8 0 12.14 15.50 10.73 o 12 8 0 254.61 230.11 23.85 o 13 8 0 5.31 9.54 13.11 o 14 8 0 659.48 753.51 42.92 o 15 8 0 703.59 758.28 44.11 o 16 8 0 209.45 299.26 31.00 o 17 8 0 0.07 -10.73 14.31 o 18 8 0 158.53 270.64 32.19 o -14 9 0 966.63 980.38 39.62 o -13 9 0 75.65 87.36 15.17 o -12 9 0 126.17 153.35 23.25 o -11 9 0 306.37 328.21 27.42 o -10 9 0 541.90 527.64 25.70 o -9 9 0 752.95 750.69 29.51 o -8 9 0 2523.67 2503.62 61.12 o -7 9 0 219.75 264.67 18.11 o -6 9 0 62.95 64.78 10.31 o -5 9 0 2852.05 2623.06 60.68 o -4 9 0 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227.84 32.19 o -2 10 0 967.92 975.25 29.92 o -1 10 0 2426.50 2269.61 52.69 o 0 10 0 1270.45 1236.05 33.72 o 1 10 0 111.16 201.94 13.89 o 2 10 0 233.86 242.05 15.17 o 3 10 0 1099.69 1056.19 29.92 o 4 10 0 44.80 100.05 10.01 o 5 10 0 8951.59 8983.22 169.45 o 6 10 0 1188.79 1086.32 29.85 o 7 10 0 132.15 136.57 11.36 o 8 10 0 3120.30 3151.14 97.77 o 9 10 0 1845.90 1638.16 60.81 o 10 10 0 2907.40 2789.88 90.61 o 11 10 0 108.33 103.73 17.88 o 12 10 0 500.59 411.33 32.19 o 13 10 0 810.68 745.16 41.73 o 14 10 0 1388.42 1201.80 56.04 o 15 10 0 72.28 102.53 20.27 o 16 10 0 199.23 199.11 26.23 o 17 10 0 201.55 168.11 25.04 o 18 10 0 1307.05 1186.30 71.54 o -13 11 0 328.41 263.49 33.38 o -12 11 0 8.47 17.54 11.71 o -11 11 0 597.50 620.64 30.35 o -10 11 0 216.23 198.73 19.39 o -9 11 0 57.77 41.76 13.71 o -8 11 0 43.15 32.28 10.86 o -7 11 0 1571.57 1480.49 44.25 o -6 11 0 1053.14 1017.64 50.67 o -5 11 0 2357.60 2246.55 93.59 o -4 11 0 38.90 49.71 16.10 o -3 11 0 60.45 77.84 14.31 o -2 11 0 22.11 11.33 7.59 o -1 11 0 37.79 41.63 10.13 o 0 11 0 490.11 440.49 19.39 o 1 11 0 47.45 91.16 10.51 o 2 11 0 362.85 380.20 18.11 o 3 11 0 1278.84 1239.48 34.53 o 4 11 0 3638.31 3319.78 71.23 o 5 11 0 4995.39 5175.19 103.69 o 6 11 0 190.78 179.07 39.94 o 7 11 0 164.39 141.09 15.50 o 8 11 0 945.01 994.34 44.11 o 9 11 0 2834.84 2504.93 84.65 o 10 11 0 194.40 177.65 21.46 o 11 11 0 407.89 423.25 31.00 o 12 11 0 1263.01 1325.79 57.23 o 13 11 0 1755.63 1658.43 67.96 o 14 11 0 123.04 144.26 23.85 o 15 11 0 521.79 579.44 41.73 o 16 11 0 164.11 152.61 26.23 o 17 11 0 76.96 65.57 22.65 o -12 12 0 99.16 92.67 18.53 o -11 12 0 20.27 19.98 10.51 o -10 12 0 3645.72 3816.17 92.31 o -9 12 0 85.62 73.40 20.86 o -8 12 0 367.36 383.91 25.70 o -7 12 0 227.02 207.13 18.84 o -6 12 0 1131.05 1054.90 36.22 o -5 12 0 251.57 257.65 19.80 o -4 12 0 24.38 16.52 8.82 o -3 12 0 336.62 329.16 22.06 o -2 12 0 1684.27 1660.00 45.50 o -1 12 0 767.79 777.29 28.23 o 0 12 0 53.75 72.07 10.96 o 1 12 0 2265.75 2312.68 55.64 o 2 12 0 2.62 2.95 7.13 o 3 12 0 1773.75 1599.95 42.57 o 4 12 0 2402.61 2205.05 53.11 o 5 12 0 2797.89 2586.72 59.84 o 6 12 0 2049.18 2059.47 50.11 o 7 12 0 177.42 111.70 12.03 o 8 12 0 459.85 476.90 32.19 o 9 12 0 726.19 662.90 38.15 o 10 12 0 643.64 637.86 36.96 o 11 12 0 44.56 52.46 16.69 o 12 12 0 26.87 17.88 14.31 o 13 12 0 98.03 81.07 20.27 o 14 12 0 88.05 129.96 23.85 o 15 12 0 316.12 325.49 34.58 o 16 12 0 28.92 42.92 17.88 o 17 12 0 247.68 284.95 35.77 o -11 13 0 18.96 12.66 12.20 o -10 13 0 644.82 613.74 32.79 o -9 13 0 547.83 610.69 31.61 o -8 13 0 81.39 66.64 13.89 o -7 13 0 460.21 408.04 26.55 o -6 13 0 0.36 12.52 9.27 o -5 13 0 37.33 38.57 11.92 o -4 13 0 2075.44 1990.67 53.94 o -3 13 0 106.01 110.95 22.65 o -2 13 0 52.43 55.57 17.88 o -1 13 0 217.02 238.07 23.25 o 0 13 0 622.20 568.09 24.02 o 1 13 0 1949.53 1855.18 48.90 o 2 13 0 197.92 232.52 17.27 o 3 13 0 64.69 82.02 10.96 o 4 13 0 249.94 283.51 20.86 o 5 13 0 2152.17 2123.09 53.09 o 6 13 0 1682.71 1653.63 44.21 o 7 13 0 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