#------------------------------------------------------------------------------
#$Date: 2018-01-26 09:51:48 +0200 (Fri, 26 Jan 2018) $
#$Revision: 205694 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/81/2108192.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108192
_cell_angle_alpha                90.000
_cell_angle_beta                 91.425
_cell_angle_gamma                90.000
_cell_length_a                   8.9902
_cell_length_b                   15.1990
_cell_length_c                   10.7569
_exptl_crystal_F_000             992.00
_reflns_d_resolution_high        0.8409
_cod_data_source_file            lo50142sup5.hkl
_cod_data_source_block           2
_shelx_title                     ' exp_1651 in P21/n No14'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            345.17
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 32249.10 38824.70 969.53 o
4 0 0 83783.22 83257.24 2677.77 o
6 0 0 1492.33 2046.27 499.37 o
8 0 0 957.42 757.42 388.03 o
10 0 0 414.38 974.77 764.03 o
2 1 0 15713.38 16061.22 467.26 o
3 1 0 11547.55 11296.68 531.10 o
4 1 0 44393.36 43904.64 1072.96 o
5 1 0 19392.41 19341.84 897.35 o
6 1 0 3703.91 3255.99 384.76 o
7 1 0 10596.79 9944.27 735.96 o
8 1 0 8629.05 11586.20 1696.88 o
9 1 0 3915.84 4354.63 740.40 o
10 1 0 911.11 1535.05 599.65 o
1 2 0 90665.73 79897.07 2128.63 o
2 2 0 6611.01 6687.87 272.99 o
3 2 0 54670.56 58302.92 1170.22 o
4 2 0 5088.42 5097.88 368.36 o
5 2 0 1315.30 1816.74 319.62 o
6 2 0 4858.31 4516.34 490.34 o
7 2 0 298.13 116.90 160.06 o
8 2 0 38.20 -8.69 273.44 o
9 2 0 1965.55 2261.16 603.63 o
10 2 0 21.61 40.08 320.78 o
1 3 0 1454.67 1807.58 122.63 o
2 3 0 233.83 389.97 86.74 o
3 3 0 18446.84 16955.02 628.17 o
4 3 0 20563.59 21206.02 858.00 o
5 3 0 6790.17 7420.71 590.24 o
6 3 0 6654.03 6725.19 545.28 o
7 3 0 4224.02 4026.27 487.65 o
8 3 0 15737.00 16794.88 1129.51 o
9 3 0 2692.64 3081.30 544.73 o
10 3 0 1695.98 1701.36 548.93 o
0 4 0 47459.93 50498.52 1895.09 o
1 4 0 115.92 165.72 33.91 o
2 4 0 600.21 866.37 143.22 o
3 4 0 14295.57 14825.78 635.40 o
4 4 0 9240.55 9334.82 568.00 o
5 4 0 84.07 190.51 98.32 o
6 4 0 775.19 845.11 256.76 o
7 4 0 1439.73 1688.78 250.40 o
8 4 0 2926.76 3423.06 487.94 o
9 4 0 782.89 775.64 306.53 o
10 4 0 955.54 1131.06 374.45 o
1 5 0 6677.50 6906.27 329.40 o
2 5 0 177.67 79.38 56.58 o
3 5 0 1704.17 1914.84 223.16 o
4 5 0 5922.79 5741.21 453.27 o
5 5 0 22493.06 23802.76 1012.48 o
6 5 0 1780.98 1654.15 323.42 o
7 5 0 17027.69 19932.62 1132.72 o
8 5 0 3295.88 3380.28 521.08 o
9 5 0 5356.73 5196.01 1099.12 o
10 5 0 988.06 922.86 374.37 o
0 6 0 20421.65 19609.16 899.51 o
1 6 0 21748.08 24508.52 730.00 o
2 6 0 1222.68 1394.96 189.59 o
3 6 0 19522.57 20509.62 1222.00 o
4 6 0 3620.33 3277.82 344.39 o
5 6 0 6696.86 6301.21 629.20 o
6 6 0 24.18 5.75 122.87 o
7 6 0 9.54 386.91 428.47 o
8 6 0 490.33 371.36 226.18 o
9 6 0 1192.50 756.33 439.72 o
10 6 0 745.49 730.06 298.47 o
1 7 0 283.56 208.79 32.36 o
2 7 0 5988.72 5616.48 394.11 o
3 7 0 512.59 418.83 131.51 o
4 7 0 24834.28 24939.92 1664.54 o
5 7 0 1368.50 1047.43 318.95 o
6 7 0 18904.56 19483.72 1224.79 o
7 7 0 1342.42 1134.16 536.25 o
8 7 0 12467.74 15773.23 1597.43 o
9 7 0 1394.92 742.55 728.90 o
0 8 0 55543.77 57612.64 1825.23 o
1 8 0 11370.09 10707.34 716.66 o
2 8 0 16480.62 19145.08 1537.74 o
3 8 0 12909.81 12918.76 1063.12 o
4 8 0 17599.69 18992.56 1270.44 o
5 8 0 273.09 74.14 161.26 o
6 8 0 649.33 501.93 233.59 o
7 8 0 630.44 537.98 210.00 o
8 8 0 495.85 650.90 530.08 o
9 8 0 970.39 261.36 1477.60 o
1 9 0 2934.73 2610.46 342.28 o
2 9 0 340.22 792.69 539.52 o
3 9 0 12121.80 13232.61 1133.45 o
4 9 0 809.34 848.93 292.15 o
5 9 0 13415.63 10797.38 2052.98 o
6 9 0 68.19 197.77 97.63 o
7 9 0 13247.92 14676.97 1081.15 o
8 9 0 336.23 150.10 662.26 o
9 9 0 3589.04 1137.68 2369.75 o
0 10 0 7043.62 6496.05 703.75 o
1 10 0 12934.18 13244.32 889.60 o
2 10 0 9325.15 10292.65 1284.85 o
3 10 0 6500.46 6350.75 809.44 o
4 10 0 515.31 1313.67 1431.33 o
5 10 0 1363.45 397.56 227.70 o
6 10 0 330.55 235.84 140.49 o
7 10 0 39.29 -127.17 262.29 o
8 10 0 47.32 443.05 1627.29 o
1 11 0 274.06 219.59 137.91 o
2 11 0 4541.64 4537.38 527.39 o
3 11 0 26.83 -177.89 183.50 o
4 11 0 4931.27 6348.25 890.70 o
5 11 0 80.18 39.75 232.04 o
6 11 0 8045.22 6908.60 1894.25 o
7 11 0 5.35 -164.79 358.80 o
8 11 0 2768.30 1314.81 1873.62 o
0 12 0 7413.58 8383.34 917.74 o
1 12 0 5419.38 5477.40 508.50 o
2 12 0 3918.63 3901.92 724.42 o
3 12 0 3668.68 3567.49 1161.55 o
4 12 0 1589.55 1488.45 1236.20 o
5 12 0 78.51 105.95 126.08 o
6 12 0 213.23 251.20 192.30 o
7 12 0 33.79 -406.28 397.14 o
1 13 0 2057.41 2199.32 408.86 o
2 13 0 147.94 332.04 247.92 o
3 13 0 2356.17 2418.85 636.53 o
4 13 0 7.72 1479.17 1304.27 o
5 13 0 4698.61 1644.35 556.40 o
6 13 0 393.79 -19.64 136.31 o
7 13 0 3358.76 1984.76 2307.87 o
0 14 0 6741.91 8596.08 1619.38 o
1 14 0 3435.11 4490.35 874.70 o
2 14 0 8891.72 10130.46 905.67 o
3 14 0 2112.81 2271.15 758.06 o
4 14 0 1864.16 1440.27 1052.19 o
5 14 0 179.81 47.27 165.25 o
6 14 0 215.53 45.95 188.35 o
1 15 0 116.08 411.19 396.63 o
2 15 0 1742.69 1895.53 551.35 o
3 15 0 439.43 374.53 337.21 o
4 15 0 3333.24 1613.66 871.40 o
5 15 0 177.26 89.75 183.96 o
0 16 0 1453.32 1581.42 672.72 o
1 16 0 5681.96 5276.44 956.59 o
2 16 0 326.89 847.83 430.83 o
3 16 0 4106.74 4508.00 1246.16 o
4 16 0 180.30 -76.01 114.50 o
1 17 0 577.94 646.40 277.92 o
2 17 0 142.97 812.05 486.52 o
3 17 0 913.11 1205.87 578.14 o
0 18 0 1611.57 991.26 432.65 o
-9 0 1 1467.14 2399.78 710.31 o
-7 0 1 583.15 586.94 355.47 o
-5 0 1 21215.69 19168.95 973.86 o
-3 0 1 46070.24 46969.78 2044.95 o
3 0 1 74359.37 79783.19 1531.24 o
5 0 1 3120.88 2583.75 595.24 o
7 0 1 609.91 616.68 351.03 o
9 0 1 735.01 1054.24 650.47 o
-10 1 1 1771.99 2289.81 699.65 o
-9 1 1 7168.94 7215.25 856.69 o
-8 1 1 13679.15 13498.10 1055.33 o
-7 1 1 7102.48 6529.74 674.21 o
-6 1 1 7283.05 7548.75 707.20 o
-5 1 1 14762.14 15130.75 604.80 o
-4 1 1 13531.25 14025.91 568.06 o
-3 1 1 14316.75 14856.52 800.71 o
-2 1 1 6357.93 6862.35 686.28 o
2 1 1 11067.24 10590.65 318.82 o
3 1 1 60253.31 59581.88 1008.50 o
4 1 1 40524.40 39927.87 1538.87 o
5 1 1 9825.12 9687.38 712.30 o
6 1 1 13282.82 12877.59 826.37 o
7 1 1 7493.09 7840.84 636.91 o
8 1 1 9813.10 10164.51 864.40 o
9 1 1 1730.25 1524.72 477.07 o
10 1 1 1739.05 1989.72 836.20 o
-10 2 1 1403.79 1648.05 523.13 o
-9 2 1 250.76 328.32 193.72 o
-8 2 1 79.02 80.79 328.56 o
-7 2 1 74.61 -135.89 271.13 o
-6 2 1 901.86 903.41 241.05 o
-5 2 1 3.78 -77.58 110.89 o
-4 2 1 37361.09 37768.46 1203.59 o
-3 2 1 3074.64 3025.60 275.44 o
-2 2 1 17329.22 19568.72 1026.55 o
-1 2 1 2347.62 2318.15 252.97 o
1 2 1 67.53 234.81 75.39 o
2 2 1 46684.19 45150.63 1192.37 o
3 2 1 18234.58 17872.64 691.69 o
4 2 1 8580.27 9578.07 532.20 o
5 2 1 3087.46 2659.80 340.30 o
6 2 1 883.97 507.66 233.63 o
7 2 1 3936.50 3940.05 491.72 o
8 2 1 4546.94 4719.60 563.75 o
9 2 1 2.94 101.47 597.74 o
10 2 1 1050.37 1287.42 541.25 o
-10 3 1 1805.94 1425.04 486.78 o
-9 3 1 5579.66 5421.32 729.93 o
-8 3 1 5587.54 5271.65 616.82 o
-7 3 1 5175.17 5348.87 810.66 o
-6 3 1 3918.35 3729.15 424.94 o
-5 3 1 19522.91 19645.13 959.41 o
-4 3 1 7059.29 8179.72 534.94 o
-3 3 1 170.56 155.35 74.72 o
-2 3 1 6637.62 6465.68 269.85 o
-1 3 1 883.01 877.12 184.26 o
0 3 1 221.22 185.42 44.37 o
1 3 1 3196.79 3075.72 209.96 o
2 3 1 4520.22 4367.86 226.88 o
3 3 1 25908.03 24938.33 728.22 o
4 3 1 15941.47 16017.09 672.90 o
5 3 1 19010.22 18810.63 899.40 o
6 3 1 4734.42 4407.16 425.12 o
7 3 1 21015.63 22416.94 1077.16 o
8 3 1 2183.01 2586.57 487.91 o
9 3 1 6571.26 7013.35 941.42 o
10 3 1 578.40 826.52 970.40 o
-10 4 1 327.40 98.62 284.97 o
-9 4 1 425.03 203.93 133.50 o
-8 4 1 300.46 223.74 160.94 o
-7 4 1 71.71 529.67 247.68 o
-6 4 1 70.59 -15.62 137.49 o
-5 4 1 12461.04 13645.09 772.40 o
-4 4 1 4135.25 4150.55 373.55 o
-3 4 1 4283.67 4470.31 295.79 o
-2 4 1 940.65 622.95 119.88 o
-1 4 1 48593.89 48837.23 1477.27 o
0 4 1 4145.14 4807.12 568.58 o
1 4 1 11992.05 19475.60 2535.32 o
2 4 1 88.42 84.92 31.85 o
3 4 1 17538.33 17371.52 630.94 o
4 4 1 1912.33 1609.61 184.22 o
5 4 1 4004.50 3908.95 400.53 o
6 4 1 1636.92 1731.99 247.71 o
7 4 1 1490.00 1848.88 297.03 o
8 4 1 128.76 644.93 424.80 o
9 4 1 1862.10 2271.36 532.79 o
10 4 1 142.50 514.16 406.84 o
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8 5 1 10289.56 11522.96 1800.27 o
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-10 6 1 968.02 309.15 675.60 o
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-6 6 1 1120.22 985.66 336.87 o
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-1 6 1 7706.25 7521.43 384.17 o
0 6 1 32002.33 32301.94 959.62 o
1 6 1 614.55 848.76 334.87 o
2 6 1 31755.95 25447.06 1393.65 o
3 6 1 3754.50 3065.73 254.88 o
4 6 1 6021.49 6361.27 449.07 o
5 6 1 2648.55 1994.10 417.71 o
6 6 1 2454.52 2428.28 327.55 o
7 6 1 46.02 -4.76 107.18 o
8 6 1 1426.14 1390.92 548.68 o
9 6 1 1358.94 1359.96 593.42 o
10 6 1 2163.70 2860.05 652.98 o
-9 7 1 7282.39 4955.93 3797.76 o
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-7 7 1 20594.80 23390.80 1349.52 o
-6 7 1 2058.55 1515.31 496.69 o
-5 7 1 33986.14 36939.46 1442.76 o
-4 7 1 2491.59 1017.47 561.49 o
-3 7 1 19265.29 19225.51 918.17 o
-2 7 1 122.89 319.20 97.74 o
-1 7 1 576.79 315.86 72.36 o
0 7 1 145.31 239.75 187.44 o
1 7 1 169.22 700.14 350.16 o
2 7 1 34.82 61.47 64.35 o
3 7 1 15089.17 12703.66 1187.26 o
4 7 1 323.45 278.55 90.06 o
5 7 1 7269.38 6561.50 782.19 o
6 7 1 1592.71 906.82 349.33 o
7 7 1 11307.11 9699.57 1625.63 o
8 7 1 1154.83 1402.80 601.63 o
9 7 1 3198.26 6773.31 1222.59 o
-9 8 1 438.65 312.88 670.84 o
-8 8 1 74.71 246.08 822.92 o
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-5 8 1 14162.43 15784.21 1176.32 o
-4 8 1 6829.97 6337.98 566.79 o
-3 8 1 15982.57 17773.49 773.77 o
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-1 8 1 50257.78 55342.31 1714.87 o
0 8 1 16113.79 14469.05 839.94 o
1 8 1 20028.65 19981.44 866.57 o
2 8 1 11037.02 8788.39 909.91 o
3 8 1 6115.93 4498.67 528.08 o
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5 8 1 5361.37 5039.50 741.97 o
6 8 1 10.69 -64.16 171.50 o
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8 8 1 375.26 359.52 442.99 o
9 8 1 401.81 709.53 314.29 o
-9 9 1 122.23 186.18 708.14 o
-8 9 1 7205.29 3321.88 4353.93 o
-7 9 1 139.70 -165.64 217.97 o
-6 9 1 21671.30 22298.71 1244.18 o
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-3 9 1 481.93 659.46 150.31 o
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0 9 1 930.23 1158.33 205.50 o
1 9 1 32.79 -56.58 126.37 o
2 9 1 8850.44 7822.56 812.98 o
3 9 1 4445.76 3292.37 507.62 o
4 9 1 9147.74 8024.40 1813.73 o
5 9 1 6.34 93.85 97.93 o
6 9 1 15406.40 14145.29 1817.20 o
7 9 1 409.76 68.30 293.39 o
8 9 1 3100.37 3043.15 1205.16 o
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-7 10 1 685.10 1515.22 432.99 o
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5 10 1 83.44 206.95 141.66 o
6 10 1 12.01 -213.31 175.06 o
7 10 1 47.71 191.76 239.72 o
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-8 11 1 6.80 211.36 400.00 o
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0 11 1 1257.50 1361.22 636.37 o
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-5 15 1 3502.22 1921.60 1631.33 o
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-1 15 1 320.70 325.73 286.17 o
0 15 1 128.90 223.77 566.30 o
1 15 1 266.45 75.18 129.64 o
2 15 1 523.55 825.25 285.31 o
3 15 1 3185.15 3824.69 601.60 o
4 15 1 82.36 157.04 143.15 o
5 15 1 3166.66 111.91 554.90 o
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0 16 1 3705.62 3248.84 783.58 o
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2 16 1 4778.54 4248.09 956.56 o
3 16 1 549.95 1051.12 466.05 o
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