#------------------------------------------------------------------------------
#$Date: 2018-03-28 07:48:05 +0300 (Wed, 28 Mar 2018) $
#$Revision: 207151 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/82/2108226.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108226
_cod_data_source_file            xk5046Xsup11.hkl
_cod_data_source_block           X
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
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1 1 0 5415.06 5794.78 52.03 o
0 3 0 4718.65 4592.22 36.93 o
-2 4 0 30302.60 29239.10 329.09 o
2 2 0 30121.80 29418.10 185.88 o
-1 5 0 8362.44 8185.42 96.08 o
1 4 0 8328.94 8314.13 103.32 o
-3 6 0 33820.50 34227.90 368.88 o
3 3 0 34120.30 34930.60 369.75 o
0 6 0 14666.90 14574.40 123.39 o
-2 7 0 19829.50 19510.00 160.91 o
2 5 0 19830.90 19609.60 132.03 o
-4 8 0 4667.33 4534.02 89.13 o
4 4 0 4623.98 4523.96 67.92 o
-1 8 0 829.98 823.90 46.21 o
1 7 0 841.47 867.37 44.67 o
-3 9 0 2674.54 2601.68 33.94 o
3 6 0 2659.37 2518.72 102.03 o
0 9 0 19788.50 19287.60 164.51 o
-5 10 0 2987.65 2994.08 56.08 o
5 5 0 2996.20 2992.50 57.19 o
-2 10 0 765.22 747.73 23.91 o
2 8 0 758.14 731.79 24.14 o
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4 7 0 7540.97 7467.83 58.01 o
-1 11 0 715.05 740.70 30.72 o
1 10 0 725.02 742.78 35.12 o
-6 12 0 1929.32 1851.40 70.79 o
6 6 0 1912.13 1780.19 53.75 o
-3 12 0 1222.04 1305.21 36.50 o
3 9 0 1235.94 1288.59 34.06 o
0 12 0 275.06 285.24 32.64 o
-5 13 0 1049.68 1062.07 34.73 o
5 8 0 1055.61 1052.63 33.86 o
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2 11 0 5541.85 5336.03 303.96 o
-7 14 0 3498.79 3412.13 70.26 o
7 7 0 3497.23 3488.39 107.96 o
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4 10 0 1117.40 1015.18 67.47 o
-1 14 0 316.59 315.66 40.29 o
1 13 0 313.90 262.47 44.93 o
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6 9 0 1929.51 1837.31 105.38 o
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3 12 0 498.86 444.35 44.93 o
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5 11 0 1062.28 1032.92 59.90 o
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2 14 0 893.96 896.51 39.41 o
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7 10 0 658.65 663.27 37.24 o
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4 13 0 470.98 435.25 38.61 o
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1 16 0 965.33 989.55 44.79 o
-9 18 0 1828.14 1881.18 70.84 o
9 9 0 1825.88 1833.56 62.40 o
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6 12 0 280.08 272.93 37.64 o
-3 18 0 243.80 265.91 35.22 o
3 15 0 242.67 249.95 42.08 o
0 18 0 893.18 940.13 62.05 o
-8 19 0 16.47 34.97 34.31 <
8 11 0 16.51 37.16 32.81 <
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5 14 0 596.97 630.01 48.22 o
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2 17 0 33.69 40.81 31.81 <
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10 10 0 12.55 31.44 41.75 <
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7 13 0 2172.60 2135.08 58.18 o
-4 20 0 657.66 714.18 37.04 o
4 16 0 656.68 597.31 45.57 o
-1 20 0 6.96 13.91 36.89 <
1 19 0 6.72 28.15 35.81 <
-9 21 0 42.65 49.69 35.99 <
9 12 0 43.63 42.56 33.01 <
-6 21 0 162.44 179.67 30.84 o
6 15 0 160.23 135.96 35.80 o
-3 21 0 88.56 98.87 30.47 o
3 18 0 89.83 95.04 47.91 <
0 21 0 8.37 12.18 25.95 <
-11 22 0 1049.88 1157.21 72.79 o
11 11 0 1051.01 1059.50 57.57 o
-8 22 0 101.38 122.81 40.76 o
8 14 0 101.39 101.61 42.54 <
-5 22 0 91.72 77.49 45.07 <
5 17 0 92.00 73.03 35.67 <
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2 20 0 875.01 740.73 107.97 o
-10 23 0 296.81 286.32 33.08 o
10 13 0 294.20 237.84 38.62 o
-7 23 0 103.27 104.73 43.32 <
7 16 0 104.42 98.89 33.73 <
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4 19 0 484.27 357.37 56.55 o
-12 24 0 165.61 178.59 38.16 o
12 12 0 167.01 140.52 36.84 o
-9 24 0 175.86 166.82 24.20 o
9 15 0 176.05 168.64 30.24 o
-6 24 0 92.64 109.16 23.51 o
6 18 0 93.14 104.31 22.93 o
-11 25 0 51.88 53.45 20.83 <
11 14 0 51.52 55.34 28.14 <
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8 17 0 209.19 195.83 55.40 o
0 2 1 40235.10 39598.40 350.18 o
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-3 2 1 10966.00 11129.80 82.84 o
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-1 4 1 5529.79 5360.87 51.63 o
1 3 1 5535.19 5385.16 36.82 o
-3 5 1 9081.55 8938.18 71.21 o
-5 3 1 9021.37 9036.24 60.05 o
0 5 1 7672.58 7677.95 80.48 o
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1 6 1 8164.18 8134.16 86.13 o
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3 5 1 13574.60 13393.80 127.43 o
0 8 1 678.40 667.26 39.04 o
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2 7 1 8654.67 8601.55 142.35 o
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4 6 1 1754.72 1732.23 31.71 o
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1 9 1 286.96 318.57 21.98 o
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-11 9 1 12148.10 11988.90 151.89 o
-6 11 1 3024.78 2981.66 38.47 o
-11 6 1 3028.31 3019.58 44.04 o
-3 11 1 975.85 946.02 26.60 o
3 8 1 973.95 950.25 27.20 o
0 11 1 8908.56 8854.21 98.97 o
-11 12 1 347.90 362.27 32.59 o
-12 11 1 342.37 333.64 26.55 o
-8 12 1 4305.65 4172.23 97.17 o
-12 8 1 4276.35 4252.16 48.73 o
-5 12 1 1831.70 1891.77 37.34 o
5 7 1 1846.95 1825.15 37.14 o
-2 12 1 1866.62 1736.88 99.50 o
2 10 1 1848.99 1817.52 42.07 o
-13 13 1 1094.23 1087.11 47.84 o
-10 13 1 835.04 805.06 49.26 o
-13 10 1 840.48 870.54 50.42 o
-7 13 1 1130.88 1179.85 33.23 o
-13 7 1 1142.29 1209.33 44.88 o
-4 13 1 4070.02 4049.05 63.07 o
4 9 1 4075.17 4044.30 50.51 o
-1 13 1 1222.77 1284.67 44.78 o
1 12 1 1233.06 1234.71 41.90 o
-12 14 1 587.69 592.25 44.21 o
-14 12 1 580.32 557.18 48.74 o
-9 14 1 627.22 625.67 33.26 o
-14 9 1 630.65 565.29 31.39 o
-6 14 1 4797.17 4713.52 61.47 o
6 8 1 4774.69 4648.48 64.09 o
-3 14 1 380.66 375.95 40.36 o
3 11 1 379.05 335.23 35.13 o
0 14 1 134.11 147.13 40.79 o
-14 15 1 2447.90 2448.15 74.56 o
-15 14 1 2461.85 2534.87 61.42 o
-11 15 1 2111.03 2119.73 61.38 o
-15 11 1 2109.00 2036.13 51.18 o
-8 15 1 1085.19 1019.58 38.97 o
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2 13 1 1011.56 1051.63 57.71 o
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-16 13 1 689.61 719.17 38.00 o
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-16 10 1 658.80 618.31 44.84 o
-7 16 1 1400.39 1203.34 72.66 o
7 9 1 1399.08 1219.69 69.69 o
-4 16 1 484.78 513.03 44.14 o
4 12 1 484.15 494.50 45.16 o
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1 15 1 979.65 935.17 44.69 o
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-6 17 1 374.25 397.38 37.04 o
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3 14 1 1151.52 1204.06 44.81 o
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-14 18 1 359.26 374.35 37.09 o
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-11 18 1 1933.60 1955.89 43.58 o
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-8 18 1 531.58 525.87 36.37 o
8 10 1 525.78 501.54 36.40 o
-5 18 1 996.02 1057.42 50.31 o
5 13 1 995.27 1010.96 51.71 o
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2 16 1 934.55 975.97 46.53 o
-19 19 1 19.27 38.22 29.42 <
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-13 19 1 371.53 352.86 35.93 o
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-19 10 1 21.60 40.56 35.81 <
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4 15 1 521.02 512.38 53.90 o
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9 11 1 1204.14 1249.66 42.85 o
-6 20 1 41.57 52.27 33.50 <
6 14 1 40.93 64.20 35.48 <
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3 17 1 33.47 49.64 37.16 <
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1 2 2 4847.81 5025.63 40.40 o
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0 4 2 21957.80 21917.90 121.90 o
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-5 13 15 107.62 109.39 34.77 o
5 8 15 109.77 109.97 29.92 o
-2 13 15 417.60 383.09 39.18 o
2 11 15 417.07 373.37 32.47 o
-13 14 15 136.53 134.11 17.56 o
-14 13 15 134.88 138.96 17.67 o
-10 14 15 151.23 161.03 23.85 o
-14 10 15 149.31 150.77 24.01 o
-7 14 15 58.03 49.07 30.36 <
7 7 15 59.17 67.32 27.15 <
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4 10 15 199.48 182.14 29.66 o
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1 13 15 99.75 81.18 27.94 <
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6 9 15 105.80 95.32 22.84 o
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3 12 15 193.24 138.84 33.31 o
0 15 15 64.06 48.03 22.51 <
-14 16 15 49.54 74.53 30.77 <
-16 14 15 48.75 44.13 21.80 <
-11 16 15 168.27 153.42 16.47 o
-16 11 15 168.51 163.36 18.47 o
-8 16 15 248.92 209.50 21.84 o
8 8 15 246.89 227.81 22.86 o
-5 16 15 99.48 79.14 22.33 o
5 11 15 99.35 85.84 20.35 o
2 14 15 46.09 20.65 32.46 <
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-17 10 15 69.08 66.50 19.79 o
-7 17 15 123.10 131.69 36.17 o
7 10 15 124.26 116.70 25.24 o
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0 2 16 1344.05 1251.98 52.30 o
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-4 4 16 762.55 749.78 37.89 o
-1 4 16 321.74 304.11 29.27 o
1 3 16 325.93 343.32 30.42 o
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-5 3 16 124.70 132.73 28.12 o
0 5 16 648.47 651.47 32.79 o
-5 6 16 268.85 272.75 33.54 o
-6 5 16 271.64 267.78 31.37 o
-2 6 16 341.55 314.78 29.22 o
2 4 16 342.50 291.66 28.94 o
-7 7 16 1027.46 1015.64 36.61 o
-4 7 16 94.86 96.65 28.61 o
-7 4 16 94.04 97.38 25.22 o
-1 7 16 138.07 162.18 29.07 o
1 6 16 136.17 150.75 26.95 o
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-8 6 16 117.64 125.80 25.68 o
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3 5 16 261.42 231.96 23.64 o
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-10 7 16 128.83 149.46 32.78 o
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4 6 16 274.31 298.84 31.55 o
-1 10 16 76.09 65.20 26.04 <
1 9 16 77.42 79.19 33.22 <
-9 11 16 550.13 558.32 26.78 o
-11 9 16 550.56 547.28 29.49 o
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-11 6 16 179.51 183.52 25.77 o
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0 11 16 717.56 669.83 32.60 o
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4 9 16 255.77 230.29 30.15 o
-1 13 16 95.03 94.63 26.12 o
1 12 16 96.37 74.69 25.19 <
-12 14 16 46.27 47.54 16.36 <
-14 12 16 45.57 33.17 21.83 <
-9 14 16 84.25 77.42 20.00 o
-14 9 16 84.34 89.78 22.91 o
-6 14 16 193.08 153.76 24.01 o
6 8 16 191.21 183.25 21.08 o
-3 14 16 44.99 37.02 22.79 <
3 11 16 44.46 39.12 19.17 <
-11 15 16 138.63 111.37 20.11 o
-15 11 16 138.28 145.23 21.04 o
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-15 8 16 65.11 72.76 18.92 o
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5 10 16 71.24 62.63 22.08 <
7 9 16 246.11 276.40 33.65 o
0 1 17 9.70 28.44 34.56 <
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-1 3 17 200.18 193.36 27.77 o
1 2 17 197.24 183.37 29.30 o
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0 4 17 441.19 434.34 29.02 o
-5 5 17 240.12 273.06 33.08 o
-2 5 17 148.57 149.47 23.71 o
2 3 17 146.60 142.96 30.15 o
-4 6 17 191.00 207.72 33.65 o
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-1 6 17 282.27 285.78 33.79 o
1 5 17 285.14 290.36 38.86 o
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3 4 17 80.29 63.42 30.31 <
0 7 17 231.49 250.88 36.26 o
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-8 5 17 377.61 394.67 32.91 o
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4 5 17 224.18 233.37 25.97 o
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1 8 17 49.87 47.38 29.46 <
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1 11 17 22.65 8.08 27.18 <
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6 7 17 68.32 57.86 17.62 o
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3 10 17 51.88 53.68 25.01 <
-8 14 17 251.18 199.80 24.03 o
-14 8 17 249.19 257.60 24.49 o
-5 14 17 30.36 13.33 32.27 <
5 9 17 30.53 27.61 29.81 <
0 0 18 1045.93 749.98 84.68 o
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1 1 18 73.06 69.13 35.09 <
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0 3 18 52.12 31.00 27.61 <
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1 4 18 103.64 91.42 37.24 <
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3 3 18 282.63 304.45 31.04 o
0 6 18 127.71 109.06 27.64 o
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2 5 18 211.76 221.95 34.60 o
-7 8 18 96.15 94.60 20.71 o
-8 7 18 97.52 88.31 20.79 o
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4 4 18 100.89 100.95 26.42 o
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1 7 18 98.88 89.55 24.22 o
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3 6 18 20.87 32.90 22.70 <
0 9 18 533.96 441.47 46.22 o
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-10 8 18 12.54 13.04 20.46 <
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5 5 18 91.85 94.16 21.22 o
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2 8 18 39.62 31.56 20.95 <
-10 11 18 31.19 35.96 17.42 <
-11 10 18 31.78 48.45 21.68 <
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4 7 18 222.88 180.51 38.71 o
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1 10 18 16.66 33.91 29.73 <
-6 12 18 134.26 108.06 19.33 o
6 6 18 132.85 153.26 34.46 o
-1 1 19 20.73 26.57 30.33 <
0 2 19 365.71 237.12 36.01 o
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-3 2 19 32.18 15.02 36.59 <
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1 3 19 156.47 117.36 37.76 o
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0 5 19 31.23 38.69 30.41 <
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-7 4 19 105.59 75.90 20.95 o
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1 6 19 67.65 48.24 21.64 <
-6 8 19 23.10 12.62 19.68 <
-8 6 19 22.76 19.05 15.22 <
-3 8 19 209.20 181.47 23.02 o
3 5 19 210.99 144.82 51.74 <
0 8 19 4.12 1.99 29.65 <
-5 9 19 79.98 78.62 18.62 o
-9 5 19 80.03 54.17 20.85 <
2 7 19 192.32 173.18 32.38 o
0 1 20 3.65 8.61 28.10 <
-2 2 20 391.47 200.07 26.09 o
-1 3 20 11.80 5.38 36.56 <
1 2 20 11.48 9.41 21.45 <
-3 4 20 118.71 44.73 34.40 <
-4 3 20 120.12 52.45 21.59 <
0 4 20 134.77 81.80 34.33 <
-5 5 20 62.42 12.62 29.21 <
-2 5 20 32.49 4.02 31.42 <
2 3 20 32.33 16.87 30.18 <
loop_
_twin_refln_datum_id
_twin_refln_individual_id
_twin_refln_index_h
_twin_refln_index_k
_twin_refln_index_l
_twin_refln_f_squared_calc
_twin_refln_f_squared_meas
_twin_refln_f_squared_sigma
_twin_refln_include_status
? ? ? ? ? ? ? ? ?