#------------------------------------------------------------------------------ #$Date: 2018-06-26 18:29:20 +0300 (Tue, 26 Jun 2018) $ #$Revision: 208648 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/82/2108259.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108259 _cell_angle_alpha 112.713 _cell_angle_beta 106.080 _cell_angle_gamma 105.946 _cell_length_a 14.5961 _cell_length_b 14.7434 _cell_length_c 15.2140 _exptl_crystal_F_000 1304.00 _reflns_d_resolution_high 0.7495 _cod_data_source_file lo5021IIIsup4.hkl _cod_data_source_block III _shelx_title ' Fe_A26_60 in P-1 #2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 303.64 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 17835.58 17377.30 223.93 o 2 0 0 5292.68 5110.72 52.53 o 3 0 0 435.15 460.06 14.57 o 4 0 0 8285.07 8618.97 75.60 o 5 0 0 674.73 583.87 16.85 o 6 0 0 5984.81 5759.37 69.90 o 7 0 0 112.93 118.05 23.48 o 8 0 0 762.11 739.04 37.11 o 9 0 0 1099.23 1104.30 57.50 o 10 0 0 4581.84 4493.30 90.28 o 11 0 0 8226.27 8287.99 139.98 o 12 0 0 440.02 392.20 36.68 o 13 0 0 37.21 44.56 25.16 o 14 0 0 5.32 8.88 31.00 o 15 0 0 100.92 123.88 42.83 o 16 0 0 382.54 331.55 57.82 o -17 1 0 112.21 111.99 47.54 o -16 1 0 2.95 0.95 38.98 o -15 1 0 425.11 455.99 54.37 o -14 1 0 13.22 5.85 38.73 o -13 1 0 1352.17 1317.67 55.79 o -12 1 0 81.75 46.75 21.26 o -11 1 0 248.47 252.66 35.24 o -10 1 0 347.67 325.31 37.71 o -9 1 0 6423.69 6117.91 86.75 o -8 1 0 4838.80 4643.40 67.48 o -7 1 0 155.07 168.56 12.03 o -6 1 0 1324.04 1332.27 26.44 o -5 1 0 81.29 29.18 12.16 o -4 1 0 19892.03 20468.25 211.96 o -3 1 0 27185.34 28091.62 282.71 o -2 1 0 13166.02 13751.49 129.95 o -1 1 0 0.02 -6.62 6.62 o 0 1 0 24257.56 23767.51 475.56 o 2 1 0 4060.23 4353.31 48.84 o 3 1 0 8105.48 7992.83 81.20 o 4 1 0 3566.36 3392.12 45.55 o 5 1 0 299.54 331.76 18.07 o 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