#------------------------------------------------------------------------------ #$Date: 2018-12-07 05:36:04 +0200 (Fri, 07 Dec 2018) $ #$Revision: 212435 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/83/2108339.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108339 _cell_angle_alpha 66.778(3) _cell_angle_beta 82.477(3) _cell_angle_gamma 86.204(3) _cell_formula_units_Z 4 _cell_length_a 8.9492(7) _cell_length_b 14.5926(12) _cell_length_c 15.0762(12) _cell_volume 1793.5(3) _cod_data_source_file dk5074odba-dsup6.hkl _cod_data_source_block odba-d loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2302.36 1970.65 16.20 o 3 0 0 2770.69 2479.33 22.08 o 4 0 0 3931.23 4163.62 32.39 o 5 0 0 3038.73 2779.67 24.29 o 6 0 0 1668.46 1544.43 18.40 o 7 0 0 2032.81 2156.90 25.76 o 8 0 0 348.43 398.25 16.93 o 9 0 0 636.04 578.61 29.45 o 10 0 0 43.25 0.00 25.03 < 11 0 0 12.74 50.79 27.24 < 12 0 0 5.09 94.23 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21 196.40 252.50 106.00 < 4 9 21 98.78 0.74 103.80 < -1 10 21 132.32 22.08 131.03 < 0 10 21 0.50 14.72 109.68 < 1 10 21 54.70 13.25 122.94 < 2 10 21 199.73 230.41 113.37 < 3 10 21 40.09 -81.71 100.11 < 4 10 21 639.18 646.33 117.78 o -2 11 21 110.29 -2.94 139.87 < -1 11 21 106.21 182.56 135.45 < 0 11 21 67.50 169.31 85.39 < 1 11 21 0.74 36.81 80.24 < 2 11 21 0.05 260.59 106.74 < 3 11 21 94.08 217.90 108.95 < 4 11 21 9.08 10.31 106.00 < -2 12 21 5.57 39.75 147.96 < -1 12 21 76.97 123.67 142.07 < 0 12 21 6.38 100.85 89.07 < 1 12 21 254.21 178.88 86.86 < 2 12 21 37.16 80.98 84.66 < 3 12 21 703.10 766.32 124.41 o -1 13 21 6.55 131.77 146.49 < 0 13 21 101.69 -5.15 144.28 < 1 13 21 278.94 313.60 92.02 o 2 13 21 66.98 151.65 88.34 < 3 13 21 1.99 -25.76 109.68 < 0 14 21 748.90 823.74 161.95 o 1 14 21 365.46 371.75 98.64 o 2 14 21 206.67 150.91 92.75 < 3 14 21 21.59 -37.54 137.66 < 1 15 21 76.83 176.67 100.11 < 2 15 21 36.56 27.24 142.81 < 3 15 21 30.43 -16.93 146.49 < 2 4 22 46.63 21.35 133.24 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