#------------------------------------------------------------------------------
#$Date: 2019-03-14 05:33:07 +0200 (Thu, 14 Mar 2019) $
#$Revision: 214119 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/83/2108369.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108369
_chemical_compound_source        ?
_chemical_formula_analytical     ?
_chemical_formula_iupac          ?
_chemical_formula_moiety         ?
_chemical_formula_structural     'W O3 N2 H4'
_chemical_formula_sum            'H4 N2 O3 W'
_chemical_formula_weight         263.88
_chemical_melting_point          ?
_chemical_name_common            ?
_chemical_name_systematic        N2H4WO3
_reflns_number_total             1763
_cod_data_source_file            yb5016Isup2.hkl
_cod_data_source_block           I
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-y,x-y,z+2/3
-x+y,-x,z+1/3
y,x,-z
x-y,-y,-z+1/3
-x,-x+y,-z+2/3
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_d_spacing
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_include_status
6 7 2 0.443532 82.9968 0.0977 o
7 6 2 0.443532 27.1807 0.032 o
5 7 8 0.443977 58.1157 0.3551 o
7 5 8 0.443977 261.9294 1.6003 o
4 1 19 0.44427 161.4135 3.3304 o
1 4 19 0.44427 63.7244 1.3148 o
2 6 16 0.44436 65.7297 1.8771 o
6 2 16 0.44436 151.2256 4.3174 o
3 9 6 0.444464 48.815 1.933 o
9 3 6 0.444464 65.1096 2.5783 o
4 5 15 0.444651 33.4696 2.0332 o
5 4 15 0.444651 7.6677 0.4658 o
6 7 1 0.445075 11.4915 1.0664 o
7 6 1 0.445075 49.0702 4.5536 o
0 3 20 0.445084 44.5683 4.1502 o
3 0 20 0.445084 229.3799 21.3598 o
7 6 0 0.445593 189.0531 17.0894 o
2 9 9 0.445674 13.3902 1.2711 o
9 2 9 0.445674 51.9883 4.9351 o
6 6 8 0.445722 126.7073 14.4379 o
1 5 18 0.445917 297.9734 59.0433 o
5 1 18 0.445917 274.7529 54.4422 o
1 9 11 0.445974 48.5526 10.3009 o
5 6 11 0.445974 135.3324 28.712 o
6 5 11 0.445974 133.9015 28.4084 o
9 1 11 0.445974 117.53 24.935 o
2 10 3 0.446188 1.6627 0.3675 o
10 2 3 0.446188 16.4233 3.6297 o
2 8 12 0.446324 185.3402 37.619 o
8 2 12 0.446324 99.1497 20.1247 o
3 8 10 0.446345 11.6754 2.3265 o
8 3 10 0.446345 79.1491 15.7719 o
4 8 7 0.446489 12.3094 2.1121 o
8 4 7 0.446489 3.1464 0.5399 o
4 6 13 0.447397 246.0843 42.7069 o
6 4 13 0.447397 270.4038 46.9274 o
2 3 19 0.447789 235.1897 38.2003 o
3 2 19 0.447789 190.2069 30.894 o
0 11 4 0.447835 29.255 4.668 o
11 0 4 0.447835 0.7682 0.1226 o
1 10 7 0.448265 320.353 35.0499 o
10 1 7 0.448265 165.0182 18.0547 o
1 2 20 0.448622 49.3502 6.1449 o
2 1 20 0.448622 16.4333 2.0462 o
2 10 2 0.448816 64.3745 10.134 o
10 2 2 0.448816 60.6999 9.5555 o
5 5 13 0.449184 98.4258 21.9922 o
2 7 14 0.449211 17.8441 4.0503 o
7 2 14 0.449211 45.6169 10.3541 o
0 7 16 0.449673 101.9413 23.0667 o
3 5 16 0.449673 64.375 14.5664 o
5 3 16 0.449673 51.5082 11.655 o
7 0 16 0.449673 43.552 9.8547 o
2 5 17 0.450108 13.9224 3.7054 o
5 2 17 0.450108 13.4608 3.5825 o
3 9 5 0.450238 37.5032 10.8976 o
9 3 5 0.450238 91.3689 26.5497 o
2 10 1 0.450414 142.2982 44.0666 o
10 2 1 0.450414 408.3022 126.4422 o
10 2 0 0.450951 102.869 31.0737 o
0 10 9 0.451035 0.9298 0.2851 o
10 0 9 0.451035 11.5279 3.535 o
2 4 18 0.451287 101.5619 33.1347 o
4 2 18 0.451287 47.7701 15.5851 o
4 4 16 0.451487 19.271 6.6303 o
0 11 3 0.451568 130.454 46.0692 o
11 0 3 0.451568 61.4221 21.6909 o
0 9 12 0.451708 48.4145 18.1329 o
9 0 12 0.451708 2.363 0.885 o
1 7 15 0.451793 313.9525 123.3125 o
7 1 15 0.451793 18.5697 7.2937 o
5 7 7 0.45188 75.1559 31.357 o
7 5 7 0.45188 147.8955 61.7059 o
1 8 13 0.452821 99.7161 62.2232 o
8 1 13 0.452821 115.878 72.3083 o
3 3 18 0.453121 81.3183 45.2887 o
0 4 19 0.453228 25.4262 13.6463 o
4 0 19 0.453228 36.082 19.3653 o
4 8 6 0.453433 899.6471 476.9878 o
8 4 6 0.453433 928.552 492.313 o
4 7 10 0.453569 9.7339 5.3833 o
7 4 10 0.453569 24.5704 13.5886 o
6 6 7 0.453721 267.5239 162.1725 o
3 4 17 0.453768 43.2756 27.1418 o
4 3 17 0.453768 34.074 21.3707 o
0 2 20 0.454092 35.0263 28.0103 o
2 0 20 0.454092 12.3149 9.8481 o
0 11 2 0.454292 2.0309 1.8452 o
11 0 2 0.454292 11.7083 10.6378 o
0 8 14 0.454702 42.6404 44.8629 o
8 0 14 0.454702 35.3054 37.1455 o
2 9 8 0.454769 20.8561 22.0308 o
9 2 8 0.454769 21.4347 22.6421 o
3 9 4 0.455133 81.5811 83.7817 o
9 3 4 0.455133 78.7705 80.8952 o
1 10 6 0.455293 109.7956 111.8327 o
10 1 6 0.455293 75.8276 77.2345 o
3 7 12 0.455408 50.1277 51.2518 o
7 3 12 0.455408 29.7688 30.4364 o
0 6 17 0.455633 51.89 55.1252 o
6 0 17 0.455633 474.4473 504.0278 o
0 11 1 0.45595 108.7385 130.0407 o
11 0 1 0.45595 247.5546 296.0511 o
1 1 20 0.45596 16.5587 19.8732 o
11 0 0 0.456507 148.5432 172.8112 o
3 6 14 0.456578 0.3234 0.3612 o
6 3 14 0.456578 68.893 76.9574 o
3 8 9 0.456594 131.9526 145.9944 o
8 3 9 0.456594 133.235 147.4134 o
0 5 18 0.456856 31.0099 29.5492 o
5 0 18 0.456856 170.5188 162.4864 o
1 9 10 0.457316 181.2234 174.4171 o
5 6 10 0.457316 9.3062 8.9567 o
6 5 10 0.457316 46.5303 44.7828 o
9 1 10 0.457316 104.8407 100.9031 o
2 8 11 0.458821 276.6019 129.9552 o
8 2 11 0.458821 232.1975 109.0854 o
1 3 19 0.45887 221.444 96.7345 o
3 1 19 0.45887 54.7861 23.9325 o
3 9 3 0.459053 269.5103 95.2174 o
9 3 3 0.459053 67.5908 23.8797 o
5 7 6 0.459083 31.8602 10.9855 o
7 5 6 0.459083 28.2145 9.7285 o
4 8 5 0.459569 16.4701 5.2892 o
8 4 5 0.459569 7.2639 2.3327 o
0 1 20 0.459766 75.3126 25.0763 o
1 0 20 0.459766 233.0752 77.6053 o
4 5 14 0.4604 59.0503 12.5823 o
5 4 14 0.4604 348.3358 74.2228 o
0 10 8 0.46047 119.1135 22.6292 o
10 0 8 0.46047 137.6567 26.152 o
2 2 19 0.460797 323.8198 34.4278 o
1 6 16 0.460897 0.1555 0.0144 o
6 1 16 0.460897 47.4921 4.4116 o
6 6 6 0.461013 133.5773 11.1338 o
4 6 12 0.461133 1.1563 0.0918 o
6 4 12 0.461133 26.6861 2.1197 o
2 6 15 0.461223 119.002 9.4414 o
6 2 15 0.461223 59.1119 4.6898 o
1 10 5 0.461506 169.1915 16.2177 o
10 1 5 0.461506 202.642 19.424 o
3 9 2 0.461916 183.9839 30.1562 o
9 3 2 0.461916 58.3061 9.5568 o
5 5 12 0.46309 284.8521 39.6569 o
2 9 7 0.463275 11.3525 1.5612 o
9 2 7 0.463275 55.7484 7.6666 o
3 9 1 0.46366 140.404 25.8079 o
9 3 1 0.46366 100.4703 18.4676 o
9 3 0 0.464245 46.9676 9.2176 o
2 7 13 0.464289 52.503 10.324 o
7 2 13 0.464289 204.4973 40.2118 o
4 7 9 0.464337 94.7713 18.6432 o
7 4 9 0.464337 170.3226 33.5055 o
1 4 18 0.464612 48.0714 9.3019 o
4 1 18 0.464612 0.4156 0.0804 o
0 9 11 0.464676 107.9238 20.7325 o
9 0 11 0.464676 63.4589 12.1906 o
4 8 4 0.464779 27.0685 5.116 o
8 4 4 0.464779 7.2465 1.3696 o
1 5 17 0.46531 67.7421 11.0024 o
5 1 17 0.46531 59.0427 9.5895 o
5 7 5 0.465454 220.536 30.6181 o
7 5 5 0.465454 50.524 7.0145 o
3 8 8 0.46639 53.7222 7.1158 o
8 3 8 0.46639 181.6678 24.0628 o
0 3 19 0.46673 15.7783 1.6551 o
3 0 19 0.46673 326.4201 34.2401 o
1 10 4 0.466782 33.2896 3.3265 o
10 1 4 0.466782 136.1715 13.6071 o
1 8 12 0.467079 23.8459 1.9628 o
8 1 12 0.467079 17.8979 1.4732 o
0 7 15 0.467172 13.7221 1.1217 o
3 5 15 0.467172 54.0112 4.4152 o
5 3 15 0.467172 132.3328 10.8178 o
7 0 15 0.467172 177.9737 14.5488 o
6 6 5 0.467466 298.1074 25.4779 o
1 7 14 0.468341 123.5413 19.3817 o
7 1 14 0.468341 134.1633 21.0481 o
1 9 9 0.468359 24.5514 3.9056 o
5 6 9 0.468359 35.4143 5.6336 o
6 5 9 0.468359 19.7546 3.1425 o
9 1 9 0.468359 6.3777 1.0145 o
2 3 18 0.468641 105.6604 19.3272 o
3 2 18 0.468641 173.2504 31.6906 o
3 7 11 0.468707 122.1655 22.5249 o
7 3 11 0.468707 81.3314 14.9959 o
2 5 16 0.468864 54.0144 9.7411 o
5 2 16 0.468864 88.9093 16.0341 o
4 8 3 0.468955 75.2341 13.1022 o
8 4 3 0.468955 72.5337 12.6319 o
4 4 15 0.469207 62.3343 9.11 o
0 10 7 0.469305 229.6193 30.4924 o
10 0 7 0.469305 253.223 33.6269 o
0 8 13 0.47036 0.9885 0.1611 o
8 0 13 0.47036 9.0823 1.4801 o
1 2 19 0.470815 187.0405 35.1607 o
2 1 19 0.470815 170.4034 32.0332 o
5 7 4 0.470869 140.5737 26.3643 o
7 5 4 0.470869 71.8923 13.4832 o
1 10 3 0.471014 46.1928 8.5378 o
10 1 3 0.471014 0.2067 0.0382 o
2 9 6 0.471046 74.8527 13.7732 o
9 2 6 0.471046 138.9799 25.5728 o
2 8 10 0.471198 82.5011 14.833 o
8 2 10 0.471198 40.6082 7.301 o
2 4 17 0.471421 454.0266 79.1238 o
4 2 17 0.471421 95.1338 16.5791 o
4 8 2 0.472009 9.2261 1.7487 o
8 4 2 0.472009 11.4501 2.1702 o
3 6 13 0.472437 211.961 50.1457 o
6 3 13 0.472437 13.9538 3.3012 o
6 6 4 0.472952 136.1168 35.0474 o
3 4 16 0.473006 22.8725 5.9041 o
4 3 16 0.473006 55.7012 14.3782 o
3 3 17 0.473513 47.5736 12.321 o
4 8 1 0.473869 8.9615 2.2541 o
8 4 1 0.473869 30.1139 7.5744 o
1 10 2 0.474108 42.8517 10.3392 o
10 1 2 0.474108 30.0804 7.2578 o
8 4 0 0.474495 486.5222 108.339 o
4 7 8 0.47465 88.0722 18.891 o
7 4 8 0.47465 86.0293 18.4528 o
0 4 18 0.474886 478.0024 95.8365 o
4 0 18 0.474886 515.2914 103.3127 o
4 6 11 0.474955 275.9072 54.0913 o
6 4 11 0.474955 294.5043 57.7372 o
0 6 16 0.475119 40.4904 7.5187 o
6 0 16 0.475119 28.2781 5.251 o
5 7 3 0.475213 105.0959 18.8877 o
7 5 3 0.475213 139.1262 25.0036 o
3 8 7 0.475577 129.1806 20.0827 o
8 3 7 0.475577 111.6658 17.3598 o
1 10 1 0.475994 125.0103 13.689 o
10 1 1 0.475994 152.6769 16.7186 o
10 1 0 0.476627 134.8901 8.3645 o
4 5 13 0.476675 168.5669 10.3385 o
5 4 13 0.476675 120.0219 7.3611 o
5 5 11 0.477094 29.6828 1.7911 o
0 2 19 0.477149 509.6768 30.8605 o
2 0 19 0.477149 230.7608 13.9724 o
6 6 3 0.477356 11.8427 0.7308 o
0 10 6 0.477389 318.8174 19.7128 o
10 0 6 0.477389 493.4808 30.5124 o
0 9 10 0.477547 132.2661 8.1042 o
9 0 10 0.477547 5.6948 0.3489 o
0 5 17 0.47778 8.0964 0.5099 o
5 0 17 0.47778 2.9962 0.1887 o
2 9 5 0.477935 20.306 1.3526 o
9 2 5 0.477935 2.1895 0.1458 o
5 7 2 0.478391 81.7845 7.2236 o
7 5 2 0.478391 161.6303 14.2759 o
2 6 14 0.478871 80.0228 7.7848 o
6 2 14 0.478871 68.662 6.6796 o
1 9 8 0.478949 1.7285 0.1642 o
9 1 8 0.478949 30.4346 2.8907 o
5 6 8 0.478949 72.5173 6.8875 o
6 5 8 0.478949 8.6834 0.8247 o
1 1 19 0.479318 352.0836 29.6881 o
2 7 12 0.479695 114.2096 10.201 o
7 2 12 0.479695 178.5595 15.9486 o
1 6 15 0.479796 67.6658 6.1018 o
6 1 15 0.479796 6.5066 0.5867 o
5 7 1 0.480329 265.6734 21.5128 o
7 5 1 0.480329 121.9952 9.8785 o
6 6 2 0.480577 21.0955 1.8375 o
7 5 0 0.48098 42.3673 5.0959 o
1 3 18 0.481388 52.4711 6.7468 o
3 1 18 0.481388 17.172 2.208 o
1 8 11 0.48146 89.5284 11.114 o
8 1 11 0.48146 162.9145 20.2241 o
3 7 10 0.481926 0.4534 0.0462 o
7 3 10 0.481926 5.5133 0.5616 o
6 6 1 0.482542 388.2545 40.0976 o
6 6 0 0.483202 38.0372 6.7973 o
2 8 9 0.483305 43.1391 7.5602 o
8 2 9 0.483305 13.8177 2.4215 o
2 2 18 0.483615 14.4873 2.211 o
0 1 19 0.483745 370.1634 52.4097 o
1 0 19 0.483745 99.5502 14.0948 o
2 9 4 0.483803 7.0204 0.9585 o
9 2 4 0.483803 52.5879 7.1801 o
3 8 6 0.483995 105.1185 12.3736 o
8 3 6 0.483995 51.4274 6.0536 o
4 7 7 0.484345 1.2864 0.1195 o
7 4 7 0.484345 113.5248 10.5471 o
0 10 5 0.484565 294.7014 29.3767 o
10 0 5 0.484565 193.2221 19.2609 o
1 7 13 0.485505 192.1369 32.3935 o
7 1 13 0.485505 34.919 5.8872 o
0 7 14 0.48554 246.4384 41.6046 o
5 3 14 0.48554 182.1369 30.749 o
7 0 14 0.48554 0.0796 0.0134 o
3 5 14 0.48554 269.3949 45.4802 o
1 5 16 0.486123 66.7926 10.7981 o
5 1 16 0.486123 97.967 15.838 o
0 8 12 0.486399 632.7064 92.5981 o
8 0 12 0.486399 591.2095 86.5249 o
1 4 17 0.486673 93.6249 11.5384 o
4 1 17 0.486673 78.7969 9.711 o
4 4 14 0.487825 14.7827 1.829 o
2 9 3 0.48852 13.4409 1.309 o
9 2 3 0.48852 103.0959 10.0402 o
3 6 12 0.488697 230.9012 22.8076 o
6 3 12 0.488697 197.024 19.4613 o
4 6 10 0.488725 96.0417 9.524 o
6 4 10 0.488725 32.5943 3.2322 o
2 5 15 0.488804 33.9213 3.3962 o
5 2 15 0.488804 107.13 10.7259 o
1 9 7 0.488915 59.3177 5.9966 o
5 6 7 0.488915 90.7566 9.1749 o
6 5 7 0.488915 20.6771 2.0903 o
9 1 7 0.488915 71.8768 7.2663 o
0 9 9 0.490164 19.9446 4.2569 o
9 0 9 0.490164 0.0372 0.0079 o
0 3 18 0.490487 0.3423 0.0918 o
3 0 18 0.490487 60.0702 16.1131 o
0 10 4 0.490683 157.331 38.4325 o
10 0 4 0.490683 62.1827 15.1899 o
5 5 10 0.491056 84.5105 12.1117 o
2 3 17 0.491309 24.7848 2.615 o
3 2 17 0.491309 99.3698 10.4844 o
3 8 5 0.491478 151.5169 14.6429 o
8 3 5 0.491478 70.4277 6.8063 o
2 9 2 0.491974 4.4098 0.5731 o
9 2 2 0.491974 139.1252 18.0799 o
2 4 16 0.493104 50.0992 9.518 o
4 2 16 0.493104 89.8649 17.0729 o
7 4 6 0.493246 21.3321 3.7248 o
4 7 6 0.493246 17.7588 3.1009 o
4 5 12 0.493393 51.9842 8.6455 o
5 4 12 0.493393 5.9709 0.993 o
3 4 15 0.493503 443.7448 74.4003 o
4 3 15 0.493503 41.3053 6.9254 o
2 9 1 0.494082 190.4249 52.7365 o
9 2 1 0.494082 208.0412 57.6152 o
9 2 0 0.494791 86.5278 26.7924 o
7 3 9 0.494902 7.1986 2.2682 o
3 7 9 0.494902 18.4823 5.8237 o
2 8 8 0.494968 248.8766 79.7755 o
8 2 8 0.494968 246.6197 79.052 o
1 2 18 0.495235 112.1998 41.6832 o
2 1 18 0.495235 91.0308 33.8187 o
2 7 11 0.495313 34.9815 13.8887 o
7 2 11 0.495313 32.8643 13.0481 o
3 3 16 0.495499 66.4587 31.7781 o
0 10 3 0.495606 7.5169 4.0271 o
10 0 3 0.495606 3.0247 1.6205 o
1 8 10 0.495821 151.9904 99.7228 o
8 1 10 0.495821 8.2387 5.4055 o
0 6 15 0.495903 10.9269 7.6192 o
6 0 15 0.495903 10.5394 7.3489 o
2 6 13 0.497265 423.1878 114.6413 o
6 2 13 0.497265 380.5753 103.1037 o
3 8 4 0.497866 98.9209 17.9632 o
8 3 4 0.497866 29.7655 5.4052 o
1 9 6 0.498075 514.8508 102.1454 o
5 6 6 0.498075 185.3403 36.7712 o
6 5 6 0.498075 150.5492 29.8687 o
9 1 6 0.498075 378.6833 75.1301 o
0 4 17 0.49852 103.6391 32.4604 o
4 0 17 0.49852 100.135 31.3629 o
0 10 2 0.499214 201.9756 141.5172 o
10 0 2 0.499214 115.786 81.1272 o
1 6 14 0.499759 25.5254 23.0663 o
6 1 14 0.499759 49.131 44.3977 o
0 5 16 0.500395 15.1721 10.3896 o
5 0 16 0.500395 85.1003 58.2754 o
4 7 5 0.501174 52.0448 15.7037 o
7 4 5 0.501174 2.5478 0.7687 o
0 10 1 0.501417 439.9663 109.3224 o
10 0 1 0.501417 116.1117 28.8513 o
10 0 0 0.502158 1.5529 0.1444 o
4 6 9 0.502274 1.3052 0.1111 o
6 4 9 0.502274 11.5738 0.9852 o
0 9 8 0.502343 188.302 15.5154 o
9 0 8 0.502343 255.1578 21.024 o
0 2 18 0.502622 59.0238 4.9217 o
2 0 18 0.502622 91.987 7.6704 o
0 8 11 0.502704 1.9257 0.1733 o
8 0 11 0.502704 2.3369 0.2103 o
3 8 3 0.50301 336.3876 50.5451 o
8 3 3 0.50301 80.6863 12.1238 o
1 7 12 0.503204 2.2802 0.4625 o
7 1 12 0.503204 17.4403 3.5375 o
0 7 13 0.504744 98.5975 6.9514 o
3 5 13 0.504744 151.8507 10.7059 o
5 3 13 0.504744 159.7304 11.2615 o
7 0 13 0.504744 360.6439 25.4264 o
5 5 9 0.504805 16.464 1.0858 o
1 1 18 0.505159 177.2213 10.0906 o
3 6 11 0.505242 21.2302 1.1438 o
6 3 11 0.505242 106.22 5.7226 o
2 8 7 0.505991 283.6328 30.2893 o
8 2 7 0.505991 351.2638 37.5116 o
1 3 17 0.506057 131.4913 15.9815 o
3 1 17 0.506057 81.2765 9.8784 o
1 9 5 0.506242 51.838 8.6134 o
5 6 5 0.506242 23.513 3.9069 o
6 5 5 0.506242 62.759 10.428 o
9 1 5 0.506242 15.0952 2.5082 o
3 8 2 0.506783 152.745 46.9202 o
8 3 2 0.506783 23.2191 7.1324 o
4 4 13 0.507314 54.1349 18.9263 o
3 7 8 0.507446 368.002 122.0428 o
7 3 8 0.507446 194.8706 64.6261 o
4 7 4 0.507952 37.5937 7.6721 o
7 4 4 0.507952 60.4533 12.3372 o
1 5 15 0.508455 83.8354 8.8305 o
5 1 15 0.508455 46.7776 4.9271 o
2 2 17 0.508646 276.5615 24.0922 o
3 8 1 0.509089 187.1037 11.1981 o
8 3 1 0.509089 56.7236 3.3949 o
8 3 0 0.509864 9.9842 0.8146 o
2 5 14 0.509963 86.795 7.5242 o
5 2 14 0.509963 134.8107 11.6866 o
1 8 9 0.509985 26.5375 2.3341 o
8 1 9 0.509986 186.5672 16.4102 o
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