#------------------------------------------------------------------------------ #$Date: 2020-03-17 07:55:29 +0200 (Tue, 17 Mar 2020) $ #$Revision: 249434 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/85/2108590.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108590 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.3296 _cell_length_b 16.3759 _cell_length_c 31.1186 _exptl_crystal_F_000 3576.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file rm5026Isup2.hkl _cod_data_source_block I _shelx_title ' CF solution in P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 496.35 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 486.59 531.40 21.28 o 6 0 0 246362.27 246084.95 1209.66 o 8 0 0 40.54 71.74 20.16 o 10 0 0 1471.07 1594.37 53.39 o 12 0 0 1883.80 2034.36 71.92 o 14 0 0 3196.41 3476.70 103.48 o 16 0 0 1161.11 1148.55 60.59 o 18 0 0 158.60 124.42 27.40 o 20 0 0 767.67 757.87 60.65 o 3 1 0 7282.46 7485.08 46.47 o 4 1 0 57007.83 55888.13 260.44 o 5 1 0 60699.05 59639.41 232.59 o 6 1 0 181.46 168.48 6.95 o 7 1 0 1901.00 1721.98 43.77 o 8 1 0 15941.89 17213.52 188.16 o 9 1 0 18969.04 18867.70 100.27 o 10 1 0 163.84 186.42 14.01 o 11 1 0 3526.31 3487.42 64.71 o 12 1 0 3332.97 3138.62 63.28 o 13 1 0 387.65 333.32 24.88 o 14 1 0 1509.83 1465.12 47.18 o 15 1 0 1560.65 1558.08 53.20 o 16 1 0 1234.78 1080.03 43.74 o 17 1 0 155.16 150.64 21.32 o 18 1 0 586.75 611.42 35.67 o 19 1 0 315.59 359.20 28.81 o 20 1 0 1665.70 1785.08 66.68 o 2 2 0 4800.18 5228.44 29.31 o 3 2 0 30084.21 30042.61 139.78 o 4 2 0 43252.13 44060.40 181.53 o 5 2 0 31220.88 28372.45 136.23 o 6 2 0 29620.72 29328.04 157.70 o 7 2 0 11568.52 11871.63 70.72 o 8 2 0 6577.32 6687.18 56.28 o 9 2 0 4115.35 4223.31 59.71 o 10 2 0 15281.74 15103.59 103.71 o 11 2 0 2858.62 2925.13 131.13 o 12 2 0 741.73 748.03 41.47 o 13 2 0 2.86 0.03 12.51 o 14 2 0 261.27 386.08 27.77 o 15 2 0 802.27 699.54 34.87 o 16 2 0 25.55 16.56 15.83 o 17 2 0 70.84 55.21 17.09 o 18 2 0 0.35 24.98 16.13 o 19 2 0 247.69 249.85 25.89 o 20 2 0 127.28 124.05 22.33 o 1 3 0 8413.14 7888.20 37.42 o 2 3 0 72568.52 74709.20 302.78 o 3 3 0 14722.35 14528.03 78.40 o 4 3 0 263.85 252.10 10.53 o 5 3 0 6253.87 7185.51 53.65 o 6 3 0 3701.85 4343.97 40.18 o 7 3 0 280.14 435.97 22.10 o 8 3 0 19765.35 21242.01 126.85 o 9 3 0 1445.55 1754.20 33.10 o 10 3 0 4552.18 4700.92 50.40 o 11 3 0 3207.78 3208.41 47.80 o 12 3 0 47.14 73.61 10.46 o 13 3 0 113.38 131.19 16.93 o 14 3 0 5701.61 5528.56 92.30 o 15 3 0 52.62 65.74 17.09 o 16 3 0 9732.04 9825.11 135.21 o 17 3 0 565.42 595.94 37.03 o 18 3 0 281.91 236.76 27.27 o 19 3 0 73.10 65.69 18.19 o 20 3 0 975.70 1137.20 74.71 o 0 4 0 22522.94 25722.63 286.39 o 1 4 0 4152.03 4467.73 31.46 o 2 4 0 22778.91 23478.04 118.56 o 3 4 0 9247.16 9707.05 66.88 o 4 4 0 63824.76 65239.32 280.60 o 5 4 0 4500.64 4579.00 45.80 o 6 4 0 408.00 492.50 19.69 o 7 4 0 3773.28 3963.73 41.13 o 8 4 0 711.72 725.52 25.57 o 9 4 0 14514.33 13602.22 131.89 o 10 4 0 3601.82 3756.20 62.98 o 11 4 0 101.11 79.63 8.31 o 12 4 0 30.19 36.37 7.07 o 13 4 0 4439.43 4147.40 61.26 o 14 4 0 11.34 5.56 8.51 o 15 4 0 447.37 434.06 32.47 o 16 4 0 153.66 193.07 24.00 o 17 4 0 49.91 27.13 14.49 o 18 4 0 502.55 556.18 34.92 o 19 4 0 25.86 32.85 33.64 o 20 4 0 249.68 311.61 29.48 o 1 5 0 4509.14 4891.15 45.92 o 2 5 0 183.81 138.43 14.04 o 3 5 0 5098.41 5095.75 41.80 o 4 5 0 18490.57 18928.39 111.25 o 5 5 0 404.57 402.19 19.84 o 6 5 0 1086.58 944.60 23.31 o 7 5 0 544.69 622.21 14.20 o 8 5 0 14856.39 16064.97 181.05 o 9 5 0 448.52 466.68 20.36 o 10 5 0 33.98 50.72 14.19 o 11 5 0 340.59 379.49 20.85 o 12 5 0 181.23 137.02 13.13 o 13 5 0 900.32 863.97 24.44 o 14 5 0 6.58 3.82 9.77 o 15 5 0 795.26 790.85 38.65 o 16 5 0 2340.35 2320.83 64.31 o 17 5 0 37.43 51.78 16.26 o 18 5 0 194.64 210.16 45.06 o 19 5 0 0.48 4.53 14.79 o 0 6 0 9162.96 9590.00 77.84 o 1 6 0 10085.29 10640.66 126.51 o 2 6 0 8705.45 8577.44 106.59 o 3 6 0 10298.77 9712.10 71.39 o 4 6 0 33459.48 35636.84 188.94 o 5 6 0 8618.48 9456.23 78.72 o 6 6 0 832.23 781.48 21.72 o 7 6 0 4956.91 4879.67 68.94 o 8 6 0 2348.64 2489.94 61.03 o 9 6 0 209.16 208.68 20.99 o 10 6 0 701.45 643.20 29.06 o 11 6 0 3150.77 2942.59 81.44 o 12 6 0 989.88 914.53 32.84 o 13 6 0 429.48 374.16 25.38 o 14 6 0 715.21 719.90 32.38 o 15 6 0 6.74 11.57 13.16 o 16 6 0 25.46 52.81 17.65 o 17 6 0 25.67 34.75 15.81 o 18 6 0 12.26 14.31 13.71 o 19 6 0 111.05 121.66 32.10 o 1 7 0 290.74 256.69 30.06 o 2 7 0 722.43 857.90 41.20 o 3 7 0 10183.18 9409.08 113.21 o 4 7 0 926.08 1033.79 21.76 o 5 7 0 225.62 274.15 16.38 o 6 7 0 1103.42 1129.34 70.20 o 7 7 0 2786.22 2879.04 67.71 o 8 7 0 187.83 220.81 20.96 o 9 7 0 444.57 415.34 26.21 o 10 7 0 107.99 64.50 12.04 o 11 7 0 246.46 255.18 17.52 o 12 7 0 2405.33 2502.50 58.81 o 13 7 0 436.23 409.10 26.55 o 14 7 0 7.29 16.31 12.69 o 15 7 0 10.76 10.40 13.72 o 16 7 0 2.82 12.25 14.31 o 17 7 0 182.68 212.21 31.92 o 18 7 0 34.68 26.56 18.87 o 19 7 0 48.37 92.99 20.34 o 0 8 0 5622.11 6384.44 79.28 o 1 8 0 280.28 276.61 12.48 o 2 8 0 1180.07 1163.01 22.07 o 3 8 0 1277.79 1545.62 25.03 o 4 8 0 467.64 417.11 33.79 o 5 8 0 3818.10 3925.52 67.56 o 6 8 0 1770.96 1774.04 51.33 o 7 8 0 206.56 183.04 20.13 o 8 8 0 544.10 595.11 59.45 o 9 8 0 8.63 19.35 14.99 o 10 8 0 629.36 631.71 36.77 o 11 8 0 375.03 417.77 28.25 o 12 8 0 835.52 811.22 31.84 o 13 8 0 354.84 333.53 25.22 o 14 8 0 164.06 188.27 24.45 o 15 8 0 96.29 111.06 18.19 o 16 8 0 216.03 199.32 23.66 o 17 8 0 35.77 31.51 20.14 o 18 8 0 22.38 35.14 16.69 o 1 9 0 2.31 4.51 6.61 o 2 9 0 389.31 427.48 18.42 o 3 9 0 394.61 382.58 14.98 o 4 9 0 448.79 488.85 44.55 o 5 9 0 200.52 175.05 23.87 o 6 9 0 97.58 105.34 21.68 o 7 9 0 381.94 415.04 30.45 o 8 9 0 47.13 25.85 15.74 o 9 9 0 690.15 732.90 59.84 o 10 9 0 919.88 1013.94 45.11 o 11 9 0 23.95 9.64 17.23 o 12 9 0 341.07 355.56 26.10 o 13 9 0 114.63 113.40 18.13 o 14 9 0 10.02 8.35 17.54 o 15 9 0 2.30 13.53 14.62 o 16 9 0 5.13 9.66 13.18 o 17 9 0 2.73 25.53 25.83 o 18 9 0 0.42 0.00 13.30 o 0 10 0 127.30 140.51 29.99 o 1 10 0 134.20 141.80 11.52 o 2 10 0 26.36 27.93 12.84 o 3 10 0 21.94 32.27 8.76 o 4 10 0 1872.30 1752.20 32.41 o 5 10 0 1475.87 1423.14 90.56 o 6 10 0 318.55 299.18 42.36 o 7 10 0 256.57 296.90 36.57 o 8 10 0 60.18 82.17 16.76 o 9 10 0 73.54 88.79 32.63 o 10 10 0 773.79 771.90 41.33 o 11 10 0 125.68 91.57 21.58 o 12 10 0 23.56 63.82 26.88 o 13 10 0 2.34 16.91 16.43 o 14 10 0 1.98 16.88 15.82 o 15 10 0 51.34 57.38 21.29 o 16 10 0 264.71 312.31 27.14 o 17 10 0 0.30 0.68 14.69 o 1 11 0 1869.19 1758.23 85.34 o 2 11 0 137.96 161.58 30.20 o 3 11 0 277.77 282.38 20.77 o 4 11 0 3.23 11.32 7.35 o 5 11 0 607.11 624.93 38.63 o 6 11 0 6.87 31.59 27.76 o 7 11 0 1.00 4.80 24.22 o 8 11 0 489.11 490.63 63.47 o 9 11 0 446.69 423.30 45.90 o 10 11 0 2.01 7.34 17.86 o 11 11 0 32.10 9.99 17.51 o 12 11 0 508.41 550.41 30.84 o 13 11 0 146.83 171.68 20.41 o 14 11 0 32.06 53.88 16.47 o 15 11 0 20.32 36.65 14.59 o 16 11 0 1.07 0.04 14.44 o 17 11 0 160.40 163.73 33.77 o 0 12 0 2739.17 2964.57 122.68 o 1 12 0 30.07 20.58 8.43 o 2 12 0 488.37 409.73 47.36 o 3 12 0 246.50 231.28 21.55 o 4 12 0 810.39 727.18 21.94 o 5 12 0 695.17 689.62 23.06 o 6 12 0 464.16 491.03 22.92 o 7 12 0 352.67 370.15 56.88 o 8 12 0 497.51 490.26 69.37 o 9 12 0 1097.43 1195.12 99.69 o 10 12 0 0.35 0.70 17.66 o 11 12 0 298.68 369.44 32.50 o 12 12 0 965.10 924.81 52.13 o 13 12 0 21.21 39.76 14.04 o 14 12 0 45.65 74.40 22.89 o 15 12 0 0.05 0.03 13.81 o 16 12 0 52.68 52.23 16.59 o 1 13 0 1887.26 1675.41 69.39 o 2 13 0 18.02 18.60 9.84 o 3 13 0 866.40 916.04 31.92 o 4 13 0 151.84 148.10 18.40 o 5 13 0 1228.59 1136.83 40.51 o 6 13 0 56.58 70.89 12.11 o 7 13 0 1118.90 1186.78 70.90 o 8 13 0 104.13 161.72 48.01 o 9 13 0 447.17 542.12 75.87 o 10 13 0 636.58 766.83 88.05 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16 0 1189.02 1053.50 62.35 o 3 16 0 98.23 64.19 45.02 o 4 16 0 209.58 102.92 41.68 o 5 16 0 55.74 74.25 39.36 o 6 16 0 125.83 163.23 47.11 o 7 16 0 487.54 478.86 73.81 o 8 16 0 259.88 295.43 61.22 o 9 16 0 100.52 139.64 47.20 o 10 16 0 4.39 8.21 29.39 o 11 16 0 628.88 799.55 98.40 o 12 16 0 86.93 167.31 54.86 o 1 17 0 37.84 19.45 21.88 o 2 17 0 122.51 141.32 30.43 o 3 17 0 203.73 213.10 36.79 o 4 17 0 0.01 15.35 25.63 o 5 17 0 184.43 197.48 46.84 o 6 17 0 240.93 182.06 50.58 o 7 17 0 29.80 30.15 28.92 o 8 17 0 591.33 579.48 80.35 o 9 17 0 13.27 18.79 33.30 o 10 17 0 165.39 84.73 33.28 o 11 17 0 4.57 20.48 39.64 o 0 18 0 1.31 21.36 35.54 o 1 18 0 24.23 6.59 19.39 o 2 18 0 33.82 34.93 40.74 o 3 18 0 241.76 255.83 37.07 o 4 18 0 358.09 285.01 38.43 o 5 18 0 70.12 99.37 40.67 o 6 18 0 10.83 0.04 32.77 o 7 18 0 357.59 382.37 68.75 o 8 18 0 82.88 79.46 38.55 o 9 18 0 188.94 238.06 60.87 o 1 19 0 7.93 2.00 23.11 o 2 19 0 98.04 156.65 33.84 o 3 19 0 28.89 29.67 21.39 o 4 19 0 82.25 156.12 48.62 o 5 19 0 233.39 298.21 42.48 o 6 19 0 5.61 25.90 26.95 o 7 19 0 31.75 9.23 33.19 o 0 20 0 6.51 12.48 29.45 o 1 20 0 70.41 44.30 34.08 o 2 20 0 462.00 525.35 55.48 o 3 20 0 132.59 139.86 35.17 o 4 20 0 39.29 104.54 33.53 o 3 0 1 636.03 763.36 9.70 o 4 0 1 1506.01 1400.77 12.85 o 5 0 1 33.14 36.10 6.25 o 6 0 1 619.00 573.28 10.24 o 7 0 1 0.18 6.33 5.44 o 8 0 1 1092.97 1089.73 23.05 o 9 0 1 1853.19 2057.16 31.99 o 10 0 1 666.55 688.67 28.44 o 11 0 1 197.41 191.11 15.00 o 12 0 1 14.37 25.42 12.57 o 13 0 1 35.63 48.30 12.79 o 14 0 1 0.12 18.02 17.76 o 15 0 1 591.77 616.39 45.57 o 16 0 1 8.51 22.27 14.77 o 17 0 1 26.55 42.12 30.48 o 18 0 1 98.28 136.80 19.67 o 19 0 1 133.55 130.33 20.81 o 20 0 1 0.31 8.18 15.03 o -20 1 1 13.47 27.02 15.25 o -19 1 1 193.48 191.31 22.50 o -18 1 1 361.80 391.20 29.39 o -17 1 1 19.47 5.49 14.98 o -16 1 1 127.08 183.80 21.98 o -15 1 1 218.00 185.64 20.32 o -14 1 1 841.33 814.53 36.41 o -13 1 1 348.56 355.40 23.92 o -12 1 1 674.62 633.86 29.15 o -11 1 1 452.49 454.85 25.68 o -10 1 1 532.22 493.13 22.86 o -9 1 1 1566.11 1640.75 23.36 o -8 1 1 939.64 979.92 17.54 o -7 1 1 182.35 191.27 6.38 o -6 1 1 1057.51 1079.12 16.84 o -5 1 1 719.39 850.15 13.63 o -4 1 1 1505.80 1468.38 12.75 o -3 1 1 688.01 766.48 10.08 o 3 1 1 684.87 784.08 11.85 o 4 1 1 1490.95 1448.51 15.43 o 5 1 1 727.09 866.69 13.67 o 6 1 1 1069.88 1045.36 26.73 o 7 1 1 179.49 186.35 10.34 o 8 1 1 919.72 967.05 22.02 o 9 1 1 1549.38 1655.99 26.89 o 10 1 1 530.66 510.72 18.78 o 11 1 1 461.87 457.54 24.20 o 12 1 1 688.89 698.19 30.58 o 13 1 1 345.12 371.32 23.82 o 14 1 1 850.69 863.27 37.51 o 15 1 1 221.42 193.18 21.25 o 16 1 1 130.03 152.32 20.09 o 17 1 1 18.71 41.36 15.91 o 18 1 1 361.21 355.05 55.77 o 19 1 1 195.56 179.31 22.69 o 20 1 1 11.93 23.04 15.62 o -20 2 1 49.09 92.32 20.31 o -19 2 1 101.39 135.79 44.40 o -18 2 1 89.16 123.53 21.34 o -17 2 1 19.07 7.17 14.49 o -16 2 1 24.22 33.80 16.05 o -15 2 1 580.29 527.39 29.37 o -14 2 1 1837.90 1840.26 53.05 o -13 2 1 72.36 71.69 14.19 o -12 2 1 71.17 66.85 9.41 o -11 2 1 339.05 311.01 15.75 o -10 2 1 255.81 234.05 10.45 o -9 2 1 1114.57 1121.15 21.61 o -8 2 1 384.10 412.91 10.75 o -7 2 1 726.14 835.90 16.31 o -6 2 1 88.20 86.53 6.34 o -5 2 1 1658.38 1616.35 24.56 o -4 2 1 5028.64 5056.70 42.54 o -3 2 1 6092.18 5899.46 39.85 o -2 2 1 48.23 28.45 4.83 o 2 2 1 47.30 29.14 4.80 o 3 2 1 6047.29 5731.46 38.69 o 4 2 1 4990.94 5026.99 36.31 o 5 2 1 1661.33 1606.79 25.53 o 6 2 1 80.46 80.57 5.72 o 7 2 1 731.03 819.18 18.32 o 8 2 1 403.47 395.32 10.77 o 9 2 1 1125.61 1049.96 35.62 o 10 2 1 258.20 249.09 13.10 o 11 2 1 351.95 281.79 19.14 o 12 2 1 71.53 83.62 16.50 o 13 2 1 73.97 53.80 13.14 o 14 2 1 1859.75 1848.51 52.62 o 15 2 1 582.98 562.12 30.47 o 16 2 1 22.57 19.41 15.46 o 17 2 1 21.05 49.91 17.55 o 18 2 1 88.61 86.71 25.20 o 19 2 1 102.09 107.50 24.25 o 20 2 1 54.09 64.55 18.82 o -20 3 1 259.02 291.58 28.50 o -19 3 1 16.45 43.39 15.68 o -18 3 1 311.37 366.68 67.84 o -17 3 1 188.09 208.81 25.04 o -16 3 1 801.97 813.70 40.22 o -15 3 1 240.68 223.60 23.35 o -14 3 1 1748.61 1648.25 66.33 o -13 3 1 63.44 50.51 10.45 o -12 3 1 219.57 206.73 14.27 o -11 3 1 816.63 801.87 21.96 o -10 3 1 4501.19 4488.08 50.80 o -9 3 1 1691.48 1652.10 30.44 o -8 3 1 3428.65 3568.02 39.33 o -7 3 1 546.19 641.25 19.84 o -6 3 1 3276.38 3433.43 38.37 o -5 3 1 1633.20 1673.24 26.62 o -4 3 1 967.58 1004.03 14.51 o -3 3 1 3107.76 3230.74 27.91 o -2 3 1 10177.58 9876.13 69.99 o -1 3 1 1399.80 1510.70 35.69 o 0 3 1 1992.65 1867.66 18.51 o 1 3 1 1418.11 1535.12 32.30 o 2 3 1 10155.92 9907.35 70.16 o 3 3 1 3102.80 3269.15 28.22 o 4 3 1 995.41 1029.21 16.38 o 5 3 1 1620.68 1664.19 25.73 o 6 3 1 3366.23 3511.06 56.41 o 7 3 1 533.45 624.00 21.09 o 8 3 1 3404.81 3636.17 55.82 o 9 3 1 1710.56 1731.81 36.49 o 10 3 1 4544.55 4329.41 50.49 o 11 3 1 809.32 788.56 24.45 o 12 3 1 237.18 221.04 23.12 o 13 3 1 59.82 44.17 12.79 o 14 3 1 1764.05 1762.34 64.79 o 15 3 1 239.30 267.56 24.56 o 16 3 1 781.72 782.01 39.41 o 17 3 1 181.72 186.92 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4844.99 80.71 o 5 8 4 143.75 163.41 20.96 o 6 8 4 1004.47 1063.15 38.06 o 7 8 4 928.47 858.49 41.34 o 8 8 4 792.61 822.52 38.10 o 9 8 4 1774.92 1584.41 68.63 o 10 8 4 887.60 901.08 29.61 o 11 8 4 3603.52 3418.40 66.17 o 12 8 4 7.13 5.62 13.70 o 13 8 4 472.25 516.42 57.37 o 14 8 4 22.02 21.10 15.45 o 15 8 4 330.73 322.83 26.55 o 16 8 4 119.41 121.85 39.24 o 17 8 4 561.14 568.34 34.11 o 18 8 4 575.49 554.06 53.28 o -18 9 4 294.89 315.70 29.43 o -17 9 4 205.16 226.96 24.81 o -16 9 4 110.57 80.17 17.09 o -15 9 4 241.74 220.69 32.38 o -14 9 4 550.43 479.61 30.05 o -13 9 4 512.95 476.57 30.97 o -12 9 4 541.15 470.75 25.18 o -11 9 4 822.62 815.41 42.08 o -10 9 4 1563.70 1509.35 51.81 o -9 9 4 2989.74 3028.60 73.47 o -8 9 4 525.11 581.70 60.87 o -7 9 4 1300.14 1257.31 81.09 o -6 9 4 660.86 702.39 60.00 o -5 9 4 1478.70 1473.82 88.24 o -4 9 4 1598.63 1597.61 48.21 o -3 9 4 1844.28 1760.05 86.48 o -2 9 4 788.43 813.70 29.17 o -1 9 4 3633.81 3560.04 38.75 o 0 9 4 2417.75 2263.88 64.07 o 1 9 4 3596.79 3549.24 44.58 o 2 9 4 772.88 692.61 25.65 o 3 9 4 1831.54 1906.42 32.82 o 4 9 4 1567.75 1679.75 45.02 o 5 9 4 1443.47 1533.47 49.54 o 6 9 4 640.35 644.40 33.13 o 7 9 4 1323.55 1419.76 101.18 o 8 9 4 520.68 543.87 33.57 o 9 9 4 2986.10 2988.53 75.36 o 10 9 4 1579.51 1509.63 39.15 o 11 9 4 807.49 733.86 28.38 o 12 9 4 550.56 492.79 27.50 o 13 9 4 507.91 510.65 30.49 o 14 9 4 550.37 508.18 30.51 o 15 9 4 240.29 263.76 24.15 o 16 9 4 115.01 111.20 18.19 o 17 9 4 202.59 224.32 36.47 o 18 9 4 292.52 377.88 46.95 o -17 10 4 293.30 357.35 29.99 o -16 10 4 212.75 206.00 24.59 o -15 10 4 8.30 13.37 13.54 o -14 10 4 19.47 15.37 14.39 o -13 10 4 876.81 895.31 38.92 o -12 10 4 155.84 174.20 39.46 o -11 10 4 1809.90 1747.49 62.35 o -10 10 4 333.99 285.75 28.23 o -9 10 4 136.00 108.05 31.52 o -8 10 4 33.81 53.62 31.78 o -7 10 4 1509.06 1543.39 92.48 o -6 10 4 2416.03 2377.53 112.31 o -5 10 4 3419.97 3494.02 128.45 o -4 10 4 355.16 240.76 19.76 o -3 10 4 4762.52 5085.97 158.09 o -2 10 4 1328.54 1430.04 59.92 o -1 10 4 560.80 584.95 37.67 o 0 10 4 2589.55 2520.60 49.86 o 1 10 4 585.37 588.25 19.65 o 2 10 4 1299.08 1410.34 29.05 o 3 10 4 4760.71 5207.05 70.11 o 4 10 4 338.26 325.34 24.45 o 5 10 4 3412.23 3420.06 70.76 o 6 10 4 2419.28 2485.51 65.31 o 7 10 4 1542.92 1462.38 49.27 o 8 10 4 34.33 31.61 15.22 o 9 10 4 134.69 168.22 22.22 o 10 10 4 346.51 315.17 31.10 o 11 10 4 1827.45 1773.41 47.11 o 12 10 4 160.62 209.54 22.49 o 13 10 4 891.68 916.06 39.80 o 14 10 4 22.30 34.45 16.00 o 15 10 4 9.12 18.09 13.71 o 16 10 4 212.19 227.63 35.95 o 17 10 4 298.39 335.36 41.53 o -17 11 4 277.71 330.59 30.11 o -16 11 4 420.21 539.02 55.17 o -15 11 4 56.67 62.69 18.54 o -14 11 4 101.90 155.16 28.35 o -13 11 4 83.30 81.21 17.98 o -12 11 4 981.48 957.11 86.35 o -11 11 4 3.22 1.53 32.38 o -10 11 4 92.87 101.50 35.28 o -9 11 4 1693.87 1400.87 102.38 o -8 11 4 1420.35 1370.58 92.70 o -7 11 4 354.12 341.74 50.26 o -6 11 4 403.77 463.83 54.76 o -5 11 4 2081.37 2023.36 125.59 o -4 11 4 2264.95 2303.51 115.66 o -3 11 4 688.73 535.13 52.55 o -2 11 4 3009.93 3030.38 42.81 o -1 11 4 1906.65 1880.71 33.78 o 0 11 4 374.54 287.30 47.47 o 1 11 4 1930.20 1904.85 53.16 o 2 11 4 3062.73 3017.45 91.17 o 3 11 4 684.65 591.47 21.86 o 4 11 4 2252.83 2390.10 59.51 o 5 11 4 2038.67 2111.66 46.61 o 6 11 4 401.85 474.22 30.73 o 7 11 4 350.06 314.26 63.62 o 8 11 4 1435.10 1391.97 51.61 o 9 11 4 1706.81 1594.50 80.51 o 10 11 4 87.37 112.03 36.18 o 11 11 4 2.37 16.46 19.60 o 12 11 4 970.74 1010.22 36.67 o 13 11 4 80.50 77.48 17.61 o 14 11 4 98.27 101.98 18.82 o 15 11 4 54.06 62.17 26.27 o 16 11 4 424.70 455.78 47.84 o 17 11 4 276.95 309.56 42.52 o -16 12 4 296.45 297.25 41.28 o -15 12 4 151.46 144.32 30.82 o -14 12 4 111.80 75.15 35.90 o -13 12 4 605.41 598.84 76.16 o -12 12 4 200.25 223.56 50.25 o -11 12 4 505.79 450.30 70.22 o -10 12 4 146.43 155.83 41.18 o -9 12 4 156.28 111.64 40.73 o -8 12 4 172.58 114.03 37.85 o -7 12 4 2942.23 2941.96 145.94 o -6 12 4 913.55 982.98 22.54 o -5 12 4 213.83 163.98 35.08 o -4 12 4 901.22 825.30 69.85 o -3 12 4 271.30 257.32 31.55 o -2 12 4 2292.77 2252.12 40.13 o -1 12 4 44.69 73.57 9.13 o 0 12 4 3615.01 3408.16 136.36 o 1 12 4 45.69 66.41 12.90 o 2 12 4 2306.11 2261.59 60.68 o 3 12 4 261.75 261.33 19.75 o 4 12 4 884.67 824.92 30.63 o 5 12 4 208.79 174.38 44.33 o 6 12 4 914.13 1007.26 35.21 o 7 12 4 2934.59 2933.73 89.14 o 8 12 4 166.78 165.78 23.17 o 9 12 4 151.35 116.76 23.04 o 10 12 4 150.24 169.16 26.29 o 11 12 4 511.97 480.61 83.39 o 12 12 4 202.20 199.14 19.92 o 13 12 4 605.38 625.64 49.44 o 14 12 4 116.84 94.50 24.48 o 15 12 4 153.02 224.58 35.48 o 16 12 4 298.14 292.05 40.80 o -15 13 4 91.25 88.01 27.52 o -14 13 4 57.83 49.21 41.86 o -13 13 4 345.22 340.12 63.21 o -12 13 4 51.07 55.11 34.34 o -11 13 4 356.23 370.30 62.98 o -10 13 4 1537.45 1625.10 118.67 o -9 13 4 92.46 84.40 40.49 o -8 13 4 23.61 20.24 29.19 o -7 13 4 585.58 543.41 19.53 o -6 13 4 1770.90 1779.63 110.46 o -5 13 4 2439.53 2314.06 126.76 o -4 13 4 296.70 248.50 49.00 o -3 13 4 181.07 193.71 20.16 o -2 13 4 474.38 421.28 31.02 o -1 13 4 1515.56 1512.28 66.78 o 0 13 4 312.15 361.65 55.23 o 1 13 4 1512.28 1487.49 93.97 o 2 13 4 463.46 388.50 52.92 o 3 13 4 176.34 220.47 45.54 o 4 13 4 297.33 262.41 21.11 o 5 13 4 2403.06 2343.99 109.64 o 6 13 4 1793.20 1838.37 86.00 o 7 13 4 577.71 537.38 35.22 o 8 13 4 23.81 104.09 42.20 o 9 13 4 97.15 74.48 31.18 o 10 13 4 1528.44 1535.60 63.11 o 11 13 4 352.28 379.44 35.02 o 12 13 4 51.60 67.14 15.74 o 13 13 4 349.63 372.18 35.41 o 14 13 4 59.58 55.18 23.21 o 15 13 4 90.76 97.25 29.13 o -14 14 4 58.11 54.39 20.00 o -13 14 4 130.75 178.24 47.34 o -12 14 4 33.88 0.04 29.84 o -11 14 4 341.32 542.12 75.61 o -10 14 4 137.92 101.30 39.00 o -9 14 4 125.50 205.84 48.45 o -8 14 4 1818.10 1738.14 122.21 o -7 14 4 1789.90 1749.44 114.98 o -6 14 4 113.75 144.78 43.76 o -5 14 4 805.26 954.19 81.63 o -4 14 4 464.85 524.28 48.40 o -3 14 4 308.63 297.90 36.62 o -2 14 4 96.88 114.10 36.16 o -1 14 4 1228.72 1087.98 75.22 o 0 14 4 141.05 123.32 41.89 o 1 14 4 1208.77 1117.61 87.69 o 2 14 4 96.18 91.79 37.29 o 3 14 4 321.56 336.19 57.88 o 4 14 4 471.71 544.59 65.36 o 5 14 4 808.91 878.50 44.69 o 6 14 4 112.27 137.92 38.04 o 7 14 4 1770.86 1781.73 48.97 o 8 14 4 1808.76 1835.93 53.35 o 9 14 4 121.50 161.05 52.33 o 10 14 4 137.73 102.81 39.77 o 11 14 4 346.38 375.61 39.06 o 12 14 4 34.08 45.47 29.53 o 13 14 4 130.14 97.16 57.76 o 14 14 4 58.79 62.78 26.15 o -13 15 4 220.78 244.67 57.25 o -12 15 4 22.99 33.78 34.91 o -11 15 4 9.51 10.27 29.92 o -10 15 4 18.36 0.35 34.65 o -9 15 4 195.41 185.50 46.06 o -8 15 4 240.28 321.12 61.64 o -7 15 4 62.67 40.14 32.01 o -6 15 4 159.71 143.27 44.61 o -5 15 4 352.13 433.56 42.24 o -4 15 4 249.26 260.72 37.17 o -3 15 4 173.01 133.57 28.65 o -2 15 4 344.96 342.94 39.12 o -1 15 4 151.12 105.98 27.79 o 0 15 4 7.74 7.09 22.84 o 1 15 4 146.87 200.96 47.48 o 2 15 4 343.08 491.26 67.95 o 3 15 4 174.09 177.34 44.82 o 4 15 4 246.72 259.39 53.72 o 5 15 4 341.27 340.02 58.77 o 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14.26 21.06 o 7 1 28 495.17 454.58 43.73 o 8 1 28 145.58 194.99 34.09 o 9 1 28 83.93 72.31 26.42 o 10 1 28 114.36 89.04 31.83 o 11 1 28 145.41 166.45 35.13 o 12 1 28 69.27 48.70 28.23 o 13 1 28 54.80 49.05 28.91 o 14 1 28 409.27 457.20 54.73 o -14 2 28 130.35 150.07 38.41 o -13 2 28 111.24 85.34 27.52 o -12 2 28 67.40 67.58 31.61 o -11 2 28 366.66 412.38 39.57 o -10 2 28 362.34 376.09 46.86 o -9 2 28 1569.24 1524.38 70.96 o -8 2 28 512.95 498.68 58.08 o -7 2 28 29.39 36.37 29.24 o -6 2 28 262.40 220.69 30.19 o -5 2 28 76.17 81.28 21.93 o -4 2 28 1862.16 1567.25 58.07 o -3 2 28 355.98 453.70 37.98 o -2 2 28 1492.26 1344.84 36.86 o -1 2 28 737.16 771.40 23.86 o 0 2 28 1.48 19.71 9.69 o 1 2 28 747.21 799.44 25.53 o 2 2 28 1515.59 1417.67 42.83 o 3 2 28 354.43 451.12 53.01 o 4 2 28 1878.51 1792.40 47.92 o 5 2 28 72.21 69.12 14.28 o 6 2 28 255.82 247.30 28.82 o 7 2 28 28.16 17.87 15.27 o 8 2 28 521.82 558.39 50.32 o 9 2 28 1573.13 1489.77 80.53 o 10 2 28 358.40 320.63 42.22 o 11 2 28 371.60 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