#------------------------------------------------------------------------------ #$Date: 2020-05-16 08:18:03 +0300 (Sat, 16 May 2020) $ #$Revision: 252091 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/86/2108606.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108606 _cell_angle_alpha 90.000 _cell_angle_beta 94.612 _cell_angle_gamma 90.000 _cell_length_a 7.8461 _cell_length_b 20.3590 _cell_length_c 29.1890 _exptl_crystal_F_000 2224.00 _reflns_d_resolution_high 0.7651 _cod_data_source_file um5038Isup2.hkl _cod_data_source_block I _shelx_title ' 1 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 538.19 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3751.94 3520.48 62.20 o 2 0 0 77792.80 80580.23 1977.94 o 3 0 0 1399.38 1231.54 102.63 o 4 0 0 176.47 165.71 20.80 o 5 0 0 244.84 296.27 34.21 o 6 0 0 47.76 27.26 17.83 o 7 0 0 5961.04 6160.83 220.81 o 8 0 0 69.06 93.30 46.65 o 9 0 0 697.15 506.92 68.42 o 10 0 0 3.12 0.00 52.87 o 1 1 0 19794.36 19605.16 281.14 o 2 1 0 1043.91 790.12 22.03 o 3 1 0 2527.12 2235.34 36.42 o 4 1 0 3181.15 2838.70 32.52 o 5 1 0 200.69 236.51 16.34 o 6 1 0 2392.82 2328.99 56.28 o 7 1 0 732.35 728.84 42.84 o 8 1 0 1582.85 1475.47 69.24 o 9 1 0 37.29 26.24 34.98 o 10 1 0 15.22 18.13 38.44 o 0 2 0 3135.05 2441.32 93.30 o 1 2 0 7956.69 8599.48 179.32 o 2 2 0 10348.71 10358.67 159.98 o 3 2 0 6891.10 6348.98 102.68 o 4 2 0 9294.78 9542.64 140.42 o 5 2 0 1325.11 1120.69 32.77 o 6 2 0 23.57 9.47 14.64 o 7 2 0 10.71 22.18 25.22 o 8 2 0 578.86 618.95 48.38 o 9 2 0 3.24 18.95 34.98 o 10 2 0 449.98 456.44 54.98 o 1 3 0 4769.68 4037.64 53.68 o 2 3 0 289645.84 300036.22 5096.89 o 3 3 0 4.46 27.99 8.24 o 4 3 0 4205.15 4465.16 81.25 o 5 3 0 3022.03 3201.12 44.66 o 6 3 0 50.35 51.91 16.48 o 7 3 0 1005.25 928.51 58.32 o 8 3 0 2.51 25.46 29.63 o 9 3 0 96.28 122.98 65.31 o 10 3 0 45.33 77.83 42.84 o 0 4 0 6944.23 8089.01 376.31 o 1 4 0 46238.80 48614.23 871.41 o 2 4 0 3558.94 3522.85 89.25 o 3 4 0 329.66 354.75 27.45 o 4 4 0 469.74 464.06 17.78 o 5 4 0 826.29 762.33 25.70 o 6 4 0 150.76 144.85 20.27 o 7 4 0 241.23 235.71 24.72 o 8 4 0 5.88 21.77 30.79 o 9 4 0 4.89 3.21 34.03 o 10 4 0 124.81 172.39 51.31 o 1 5 0 1814.98 1978.48 78.18 o 2 5 0 87.81 38.59 6.84 o 3 5 0 5110.92 5575.71 99.39 o 4 5 0 8188.93 8452.92 175.55 o 5 5 0 810.75 659.85 39.50 o 6 5 0 1505.92 1521.07 37.44 o 7 5 0 587.18 579.38 30.52 o 8 5 0 114.39 40.43 31.83 o 9 5 0 265.92 298.90 43.82 o 10 5 0 185.64 161.87 46.02 o 0 6 0 17616.68 19673.62 441.61 o 1 6 0 2561.30 2629.48 37.62 o 2 6 0 9038.51 9158.94 153.08 o 3 6 0 235.01 289.63 18.42 o 4 6 0 10558.36 10834.14 328.90 o 5 6 0 5397.64 5496.63 92.65 o 6 6 0 50.36 26.74 14.20 o 7 6 0 15.43 0.00 15.39 o 8 6 0 279.93 299.45 39.40 o 9 6 0 4.20 3.02 36.23 o 1 7 0 17413.49 18129.56 376.04 o 2 7 0 17.87 53.66 6.47 o 3 7 0 441.92 575.83 43.36 o 4 7 0 158.25 220.02 17.29 o 5 7 0 761.10 701.28 26.03 o 6 7 0 1564.13 1511.28 39.08 o 7 7 0 637.04 682.10 28.75 o 8 7 0 6.91 15.22 18.82 o 9 7 0 186.47 195.19 55.98 o 0 8 0 1012.00 1020.07 31.10 o 1 8 0 656.78 602.17 34.21 o 2 8 0 5463.26 5783.02 80.56 o 3 8 0 1675.55 1900.26 36.10 o 4 8 0 668.03 717.01 41.38 o 5 8 0 611.70 666.56 24.59 o 6 8 0 2605.33 2413.48 53.76 o 7 8 0 460.37 456.97 26.36 o 8 8 0 230.08 184.36 22.81 o 9 8 0 456.04 403.94 50.44 o 1 9 0 489.28 709.02 46.65 o 2 9 0 1821.24 1781.14 47.00 o 3 9 0 5506.96 5261.39 82.62 o 4 9 0 1122.97 1182.13 57.99 o 5 9 0 2765.39 2481.67 52.07 o 6 9 0 13.42 45.93 17.07 o 7 9 0 363.63 398.52 28.28 o 8 9 0 192.40 178.86 24.11 o 9 9 0 1.52 0.00 37.19 o 0 10 0 11.95 0.00 21.77 o 1 10 0 452.62 552.06 21.99 o 2 10 0 1332.86 1485.62 25.90 o 3 10 0 1113.89 1043.78 31.05 o 4 10 0 123.65 128.94 21.60 o 5 10 0 398.19 341.28 19.20 o 6 10 0 1008.92 1018.92 37.56 o 7 10 0 3.45 0.00 17.27 o 8 10 0 130.85 107.54 23.14 o 9 10 0 6.64 16.77 25.55 o 1 11 0 247.81 213.02 14.29 o 2 11 0 3563.32 3619.39 54.21 o 3 11 0 4951.27 4659.48 75.00 o 4 11 0 2652.15 2545.38 56.54 o 5 11 0 1166.91 1312.77 52.07 o 6 11 0 1041.41 1024.82 38.60 o 7 11 0 406.15 427.72 26.50 o 8 11 0 412.35 347.38 28.33 o 9 11 0 100.98 62.14 30.77 o 0 12 0 205.05 195.93 27.99 o 1 12 0 3172.94 3168.50 64.27 o 2 12 0 1217.27 1302.26 29.66 o 3 12 0 902.35 922.35 42.20 o 4 12 0 2016.11 1876.19 44.44 o 5 12 0 231.19 237.44 20.48 o 6 12 0 722.77 767.26 33.71 o 7 12 0 98.89 162.01 22.94 o 8 12 0 8.09 17.51 21.95 o 9 12 0 133.53 119.09 33.50 o 1 13 0 6178.97 5763.06 121.57 o 2 13 0 1.76 11.28 9.44 o 3 13 0 794.61 842.90 43.54 o 4 13 0 847.90 823.99 27.51 o 5 13 0 324.54 288.82 23.07 o 6 13 0 2224.28 2288.89 54.04 o 7 13 0 8.07 24.84 20.19 o 8 13 0 86.00 96.84 24.11 o 0 14 0 8826.22 8821.40 167.70 o 1 14 0 939.04 864.99 35.09 o 2 14 0 8162.46 8038.25 118.74 o 3 14 0 1589.57 1709.24 38.27 o 4 14 0 3158.59 2949.14 61.62 o 5 14 0 2129.35 2095.74 49.49 o 6 14 0 63.65 47.41 19.92 o 7 14 0 1109.15 1212.21 43.55 o 8 14 0 67.38 57.32 23.84 o 1 15 0 1057.75 1273.38 37.27 o 2 15 0 3.04 24.04 11.98 o 3 15 0 258.79 298.15 19.63 o 4 15 0 1258.99 1180.61 38.85 o 5 15 0 534.21 572.30 33.22 o 6 15 0 51.30 37.92 19.92 o 7 15 0 106.62 125.72 23.28 o 8 15 0 131.83 130.35 26.50 o 0 16 0 73.63 40.43 24.88 o 1 16 0 3237.38 3167.71 60.90 o 2 16 0 9.85 19.97 11.48 o 3 16 0 2106.22 1968.07 67.18 o 4 16 0 2557.14 2568.28 60.60 o 5 16 0 47.64 21.48 18.84 o 6 16 0 572.45 470.41 29.93 o 7 16 0 20.10 5.93 21.78 o 8 16 0 56.62 115.25 26.15 o 1 17 0 3250.31 3289.72 67.96 o 2 17 0 1555.91 1499.50 43.18 o 3 17 0 1813.78 1731.88 44.61 o 4 17 0 220.42 232.97 21.89 o 5 17 0 39.59 61.67 20.48 o 6 17 0 80.42 100.93 24.69 o 7 17 0 7.58 36.43 24.31 o 0 18 0 236.22 391.86 49.76 o 1 18 0 703.88 745.18 32.77 o 2 18 0 665.05 670.30 27.84 o 3 18 0 1119.28 986.63 35.25 o 4 18 0 88.35 118.34 24.69 o 5 18 0 49.88 33.95 19.85 o 6 18 0 0.98 35.47 21.78 o 7 18 0 51.29 90.60 25.61 o 1 19 0 0.22 11.86 15.90 o 2 19 0 76.55 71.87 15.39 o 3 19 0 437.28 453.63 28.73 o 4 19 0 1485.44 1431.57 45.00 o 5 19 0 67.43 44.71 21.09 o 6 19 0 33.52 26.82 26.45 o 7 19 0 74.24 51.56 29.05 o 0 20 0 8239.92 8734.58 251.91 o 1 20 0 1124.95 1126.14 42.40 o 2 20 0 477.08 465.37 30.89 o 3 20 0 14.37 32.72 26.90 o 4 20 0 0.33 30.39 22.79 o 5 20 0 70.72 88.94 32.77 o 6 20 0 10.32 10.78 32.12 o 1 21 0 2299.01 2350.56 90.19 o 2 21 0 151.34 172.70 32.99 o 3 21 0 12.53 1.44 28.34 o 4 21 0 0.27 1.67 28.34 o 5 21 0 6.31 12.01 31.38 o 6 21 0 184.41 203.43 65.31 o 0 22 0 6.72 24.88 37.32 o 1 22 0 306.20 307.10 39.04 o 2 22 0 1151.19 1226.33 96.41 o 3 22 0 168.13 120.16 31.83 o 4 22 0 328.23 256.01 119.73 o 5 22 0 238.28 237.64 38.87 o 1 23 0 42.01 49.45 24.49 o 2 23 0 1608.02 1791.46 121.29 o 3 23 0 42.42 37.00 35.76 o 4 23 0 1.79 0.00 31.38 o 5 23 0 211.82 260.69 41.98 o 0 24 0 296.01 363.87 52.87 o 1 24 0 0.00 0.00 29.63 o 2 24 0 27.67 26.43 30.79 o 3 24 0 430.79 510.55 48.23 o 4 24 0 1.16 16.17 32.12 o 1 25 0 61.99 97.96 35.19 o 2 25 0 403.24 457.12 46.18 o 3 25 0 2.75 23.32 34.98 o 0 26 0 11.87 0.00 43.54 o 1 26 0 12.42 18.66 32.99 o 2 26 0 55.28 99.52 37.38 o -10 1 1 0.48 6.04 38.44 o -9 1 1 23.07 0.00 32.99 o -8 1 1 732.43 824.15 54.98 o -7 1 1 0.63 7.77 24.19 o -6 1 1 73.85 62.22 16.89 o -5 1 1 431.51 361.04 19.75 o -4 1 1 1459.41 1285.32 23.72 o -3 1 1 4238.56 3977.97 74.06 o -2 1 1 7725.15 6947.06 68.03 o -1 1 1 18555.85 21415.50 292.98 o 1 1 1 7552.61 7614.62 78.42 o 2 1 1 16669.46 17189.04 308.72 o 3 1 1 10723.45 10897.12 225.11 o 4 1 1 1595.28 1677.70 33.39 o 5 1 1 1849.73 1886.93 37.97 o 6 1 1 4899.55 4642.50 88.73 o 7 1 1 1503.04 1536.93 65.86 o 8 1 1 197.68 164.66 48.20 o 9 1 1 1.97 0.00 34.03 o 10 1 1 401.30 337.51 49.44 o -10 2 1 59.65 73.08 45.09 o -9 2 1 66.11 125.64 38.44 o -8 2 1 368.37 397.07 42.84 o -7 2 1 123.47 127.03 27.42 o -6 2 1 173.27 172.49 18.74 o -5 2 1 216.18 270.49 10.97 o -4 2 1 4669.20 4368.96 45.71 o -3 2 1 49.04 60.41 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2619.19 2875.35 104.18 o 0 7 1 33.86 35.87 16.38 o 1 7 1 3854.93 4222.50 126.62 o 2 7 1 4541.13 4749.96 84.20 o 3 7 1 2751.26 2874.26 41.05 o 4 7 1 3.40 11.87 13.68 o 5 7 1 24.89 11.15 13.17 o 6 7 1 328.94 283.92 26.48 o 7 7 1 625.22 611.12 28.04 o 8 7 1 81.78 93.38 24.13 o 9 7 1 75.92 129.02 40.64 o -9 8 1 326.56 378.12 49.15 o -8 8 1 107.34 101.89 21.19 o -7 8 1 175.19 196.86 20.79 o -6 8 1 1581.44 1566.20 41.00 o -5 8 1 861.24 905.71 75.86 o -4 8 1 2956.49 2789.64 59.54 o -3 8 1 8861.20 9381.30 132.37 o -2 8 1 24733.46 25331.19 379.68 o -1 8 1 1988.04 1730.57 75.84 o 0 8 1 4814.14 4567.13 112.15 o 1 8 1 894.99 757.30 35.62 o 2 8 1 1166.00 1065.68 15.65 o 3 8 1 2144.79 2390.38 52.39 o 4 8 1 3204.82 3358.76 92.36 o 5 8 1 4336.58 4459.66 96.29 o 6 8 1 695.60 681.98 28.08 o 7 8 1 739.09 764.52 31.48 o 8 8 1 227.03 263.44 24.84 o 9 8 1 220.73 244.01 45.04 o -9 9 1 2.47 0.00 37.19 o -8 9 1 198.52 211.90 25.20 o -7 9 1 1655.68 1602.83 44.86 o -6 9 1 748.43 810.62 38.60 o -5 9 1 45.25 57.82 14.20 o -4 9 1 354.54 374.53 18.56 o -3 9 1 2146.52 2183.13 41.31 o -2 9 1 820.19 670.63 23.20 o -1 9 1 12147.80 12152.72 272.66 o 0 9 1 1265.57 1125.95 34.58 o 1 9 1 9107.35 10164.37 169.84 o 2 9 1 10972.86 10398.04 161.98 o 3 9 1 1348.91 1308.35 26.04 o 4 9 1 1351.73 1556.55 41.54 o 5 9 1 210.75 227.65 19.59 o 6 9 1 5499.99 5435.78 92.98 o 7 9 1 90.83 90.09 22.00 o 8 9 1 297.63 214.41 24.31 o 9 9 1 44.86 36.70 38.44 o -9 10 1 7.42 1.46 37.19 o -8 10 1 61.93 69.44 21.71 o -7 10 1 252.09 211.60 22.14 o -6 10 1 2012.56 1893.02 69.13 o -5 10 1 2041.07 2163.94 53.87 o -4 10 1 496.90 460.77 26.63 o -3 10 1 2980.51 3165.09 52.34 o -2 10 1 3251.98 3473.37 74.54 o -1 10 1 5233.02 4958.47 128.63 o 0 10 1 2040.20 2181.31 45.92 o 1 10 1 12916.13 12721.37 231.80 o 2 10 1 16935.93 17582.41 241.80 o 3 10 1 2748.05 2404.79 46.24 o 4 10 1 790.94 755.89 44.75 o 5 10 1 0.22 13.39 15.96 o 6 10 1 206.65 206.07 21.16 o 7 10 1 0.95 13.89 19.20 o 8 10 1 791.33 778.77 35.29 o 9 10 1 5.21 15.10 26.65 o -9 11 1 2.83 0.82 26.65 o -8 11 1 2.16 12.95 21.10 o -7 11 1 943.07 992.84 37.10 o -6 11 1 200.17 167.39 21.49 o -5 11 1 2402.03 2301.73 49.93 o -4 11 1 97.43 79.34 16.61 o -3 11 1 23.23 22.33 9.71 o -2 11 1 1.84 16.28 7.82 o -1 11 1 0.83 5.09 11.95 o 0 11 1 6345.63 6607.40 96.00 o 1 11 1 3819.09 4013.97 88.79 o 2 11 1 9244.67 9631.58 135.03 o 3 11 1 1091.10 950.27 34.17 o 4 11 1 1438.38 1532.15 64.26 o 5 11 1 1808.78 1834.39 62.42 o 6 11 1 1324.43 1389.73 42.61 o 7 11 1 488.90 501.37 29.28 o 8 11 1 13.60 13.44 21.10 o 9 11 1 178.78 248.66 31.92 o -9 12 1 120.83 166.29 30.88 o -8 12 1 148.76 108.48 28.83 o -7 12 1 56.21 72.79 21.43 o -6 12 1 6.61 35.09 17.93 o -5 12 1 582.60 558.76 32.32 o -4 12 1 1064.14 935.53 27.44 o -3 12 1 3437.34 3432.29 53.99 o -2 12 1 4665.40 4433.13 75.80 o -1 12 1 2270.75 2223.13 98.34 o 0 12 1 5430.29 5003.38 91.32 o 1 12 1 162.88 148.85 28.69 o 2 12 1 2546.85 2489.75 56.73 o 3 12 1 244.72 238.39 12.68 o 4 12 1 603.89 613.32 33.28 o 5 12 1 673.06 650.69 26.51 o 6 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