#------------------------------------------------------------------------------
#$Date: 2020-11-12 07:12:31 +0200 (Thu, 12 Nov 2020) $
#$Revision: 259105 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/86/2108686.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108686
_cell_angle_alpha                112.261
_cell_angle_beta                 106.134
_cell_angle_gamma                97.765
_cell_length_a                   9.2229
_cell_length_b                   12.2226
_cell_length_c                   13.0730
_exptl_crystal_F_000             664.00
_reflns_d_resolution_high        0.8652
_cod_data_source_file            rm50375sup6.hkl
_cod_data_source_block           5
_shelx_title                     ' cu_20141008LZY18_0m in P1   New: P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            169.90
_shelx_f_squared_multiplier      1.000
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 18531.11 21251.37 963.63 o
2 0 0 9157.35 10423.04 381.97 o
3 0 0 905.99 876.44 47.39 o
4 0 0 885.33 893.50 39.05 o
5 0 0 193.61 131.16 10.99 o
6 0 0 41.03 20.47 8.72 o
7 0 0 0.23 4.96 4.46 o
8 0 0 10.82 10.50 7.77 o
9 0 0 63.56 60.27 7.58 o
-10 1 0 13.06 20.47 4.93 o
-9 1 0 196.34 242.61 13.27 o
-8 1 0 23.94 24.18 7.22 o
-7 1 0 1024.54 953.77 37.53 o
-6 1 0 1398.07 1259.24 81.31 o
-5 1 0 94.61 96.03 7.74 o
-4 1 0 0.77 2.65 5.31 o
-3 1 0 7.28 3.22 2.95 o
-2 1 0 5.13 46.19 7.90 o
-1 1 0 517.18 843.84 69.75 o
0 1 0 17028.51 18197.10 759.68 o
1 1 0 2675.50 2700.39 91.67 o
2 1 0 90.37 78.86 5.36 o
3 1 0 1714.04 2157.36 114.86 o
4 1 0 430.92 298.72 19.71 o
5 1 0 1439.33 1186.91 72.78 o
7 1 0 354.70 350.13 12.79 o
8 1 0 47.04 42.92 5.22 o
9 1 0 0.64 0.00 5.69 o
-10 2 0 45.68 43.97 6.07 o
-9 2 0 465.74 505.23 16.85 o
-8 2 0 40.51 43.09 4.55 o
-7 2 0 1435.69 1399.63 43.83 o
-6 2 0 6076.99 5620.02 239.39 o
-5 2 0 2640.69 2760.86 139.50 o
-4 2 0 4608.39 5345.06 263.84 o
-3 2 0 358.15 474.40 29.89 o
-2 2 0 49.36 15.67 3.22 o
-1 2 0 417.93 558.63 22.18 o
0 2 0 5507.71 6268.81 197.02 o
1 2 0 116.74 195.57 19.90 o
2 2 0 1889.40 2117.51 77.74 o
3 2 0 59.42 169.45 13.65 o
4 2 0 1988.18 1904.89 104.63 o
5 2 0 3214.46 2367.75 110.31 o
7 2 0 718.21 715.71 20.83 o
8 2 0 123.66 135.47 8.03 o
9 2 0 51.95 55.73 6.82 o
-10 3 0 19.31 27.67 6.07 o
-9 3 0 6.70 10.09 4.80 o
-8 3 0 271.32 282.76 8.62 o
-7 3 0 9.91 4.78 5.68 o
-6 3 0 243.90 182.72 15.92 o
-5 3 0 6095.07 6396.64 309.71 o
-4 3 0 1296.48 1263.48 72.40 o
-3 3 0 12.33 24.26 7.20 o
-2 3 0 813.86 768.96 26.34 o
-1 3 0 989.53 944.21 31.76 o
0 3 0 848.72 938.80 36.72 o
1 3 0 96.12 95.78 7.24 o
2 3 0 0.69 0.39 3.34 o
3 3 0 886.02 907.52 53.83 o
4 3 0 504.46 489.77 26.91 o
5 3 0 566.14 404.86 28.05 o
6 3 0 0.85 0.76 4.26 o
7 3 0 103.81 94.09 12.32 o
8 3 0 124.00 146.84 14.59 o
-10 4 0 2.87 6.44 4.93 o
-9 4 0 68.97 66.80 6.63 o
-8 4 0 32.88 26.69 3.85 o
-7 4 0 56.73 39.97 6.72 o
-6 4 0 354.52 329.42 21.23 o
-5 4 0 2987.62 3015.98 159.97 o
-4 4 0 2057.61 2023.16 96.29 o
-3 4 0 674.17 656.57 43.97 o
-2 4 0 464.73 419.34 17.96 o
-1 4 0 1820.55 1913.98 71.97 o
0 4 0 3416.58 3996.12 131.88 o
1 4 0 1609.67 1686.88 61.79 o
2 4 0 4319.04 3962.55 173.62 o
3 4 0 167.06 80.74 9.86 o
4 4 0 215.15 155.80 14.03 o
6 4 0 724.38 763.64 21.05 o
7 4 0 9.25 8.50 5.69 o
8 4 0 192.83 214.56 12.51 o
-10 5 0 178.23 172.21 11.75 o
-9 5 0 70.38 83.07 6.19 o
-8 5 0 39.95 39.67 4.25 o
-7 5 0 49.04 66.53 7.58 o
-5 5 0 52.18 72.78 10.24 o
-4 5 0 125.93 126.99 12.13 o
-3 5 0 1812.25 1913.61 90.98 o
-2 5 0 1105.69 1275.88 45.03 o
-1 5 0 5598.06 6863.97 225.30 o
0 5 0 10343.10 12414.42 450.06 o
1 5 0 12512.51 13630.04 471.10 o
3 5 0 2380.07 1694.12 92.12 o
5 5 0 930.73 957.00 25.85 o
6 5 0 74.83 46.59 5.72 o
7 5 0 24.28 19.79 4.82 o
8 5 0 0.29 0.00 4.93 o
-10 6 0 30.23 41.25 4.55 o
-9 6 0 169.83 184.74 9.25 o
-8 6 0 77.21 76.62 7.55 o
-7 6 0 836.97 799.97 18.69 o
-5 6 0 822.26 835.21 32.79 o
-4 6 0 1898.02 1912.25 65.89 o
-3 6 0 170.92 165.66 11.75 o
-2 6 0 191.73 214.56 15.92 o
-1 6 0 242.20 276.92 10.19 o
0 6 0 618.33 575.19 22.11 o
1 6 0 279.89 261.19 17.82 o
2 6 0 2618.81 2243.41 110.31 o
4 6 0 953.38 988.07 26.01 o
5 6 0 129.63 98.33 6.69 o
6 6 0 242.33 262.41 10.95 o
7 6 0 1.29 0.00 3.88 o
-9 7 0 223.68 245.76 10.16 o
-8 7 0 43.42 44.45 4.29 o
-7 7 0 650.33 627.81 16.27 o
-6 7 0 1161.40 1153.55 29.47 o
-5 7 0 3848.14 3812.05 165.66 o
-4 7 0 2615.14 2565.96 83.06 o
-3 7 0 1316.50 1141.06 42.36 o
-2 7 0 3450.21 3545.17 116.14 o
-1 7 0 407.87 398.21 15.73 o
0 7 0 125.08 97.22 7.90 o
1 7 0 14.74 4.17 6.07 o
3 7 0 153.21 143.42 8.95 o
4 7 0 289.75 292.48 11.87 o
5 7 0 409.85 436.06 17.63 o
6 7 0 206.44 225.97 9.49 o
-9 8 0 58.66 54.02 7.77 o
-8 8 0 193.42 188.54 7.21 o
-7 8 0 68.02 63.76 4.99 o
-6 8 0 138.36 127.96 7.92 o
-5 8 0 648.89 641.96 25.40 o
-4 8 0 295.51 287.72 19.71 o
-3 8 0 1696.72 1730.13 76.95 o
-2 8 0 2760.29 2873.82 125.86 o
-1 8 0 983.54 970.66 68.80 o
0 8 0 469.26 436.85 38.48 o
2 8 0 92.47 89.60 10.61 o
3 8 0 161.08 156.24 7.99 o
4 8 0 37.51 43.31 6.14 o
5 8 0 72.86 70.86 13.40 o
6 8 0 9.38 7.66 3.15 o
-9 9 0 36.98 40.60 4.27 o
-8 9 0 8.40 7.77 4.16 o
-7 9 0 838.82 867.31 20.34 o
-6 9 0 150.04 141.50 6.90 o
-5 9 0 46.19 56.82 3.70 o
-4 9 0 577.09 601.21 14.96 o
-3 9 0 866.40 896.58 33.36 o
-2 9 0 887.99 920.83 28.95 o
-1 9 0 997.73 1029.97 52.31 o
0 9 0 492.23 477.79 18.02 o
1 9 0 389.87 378.08 12.30 o
2 9 0 568.94 573.65 14.74 o
3 9 0 713.49 743.43 17.59 o
4 9 0 583.97 624.95 22.73 o
5 9 0 48.29 45.27 11.18 o
-8 10 0 4.49 8.21 3.27 o
-7 10 0 228.84 222.85 9.64 o
-6 10 0 17.77 15.62 3.21 o
-5 10 0 145.95 148.55 6.82 o
-4 10 0 69.42 74.97 3.83 o
-3 10 0 1.13 4.98 2.85 o
-2 10 0 0.11 5.17 3.02 o
-1 10 0 407.14 416.85 10.71 o
0 10 0 184.88 175.03 6.73 o
1 10 0 274.74 267.78 9.74 o
2 10 0 684.11 694.63 21.90 o
3 10 0 750.90 815.24 24.71 o
4 10 0 815.73 866.21 47.57 o
-7 11 0 785.04 755.94 17.01 o
-6 11 0 376.04 388.84 10.57 o
-5 11 0 231.95 247.25 6.87 o
-4 11 0 951.54 973.00 21.97 o
-3 11 0 142.93 172.95 7.46 o
-2 11 0 379.99 407.58 12.64 o
-1 11 0 184.03 178.54 6.78 o
0 11 0 3.09 0.94 3.69 o
1 11 0 338.77 299.28 26.73 o
2 11 0 223.35 216.06 9.82 o
-6 12 0 238.48 257.03 10.14 o
-5 12 0 280.35 299.23 13.46 o
-4 12 0 265.90 297.16 9.71 o
-3 12 0 283.64 286.40 9.99 o
-2 12 0 803.28 738.78 18.53 o
-1 12 0 579.51 559.80 14.88 o
0 12 0 951.96 963.77 76.76 o
1 12 0 0.74 1.19 3.82 o
-3 13 0 199.11 208.82 7.33 o
-2 13 0 591.39 582.70 14.62 o
1 -13 1 2.59 0.87 3.45 o
2 -13 1 387.71 373.49 12.95 o
3 -13 1 277.30 268.56 10.90 o
4 -13 1 1.79 5.00 3.61 o
-2 -12 1 51.34 56.66 13.27 o
-1 -12 1 76.52 76.04 4.65 o
0 -12 1 174.82 180.65 6.85 o
1 -12 1 17.71 11.56 3.34 o
2 -12 1 110.95 138.68 6.96 o
3 -12 1 162.12 144.11 11.24 o
4 -12 1 41.12 44.62 3.56 o
5 -12 1 77.75 73.13 4.29 o
6 -12 1 156.66 161.99 5.89 o
-3 -11 1 158.72 154.21 10.05 o
-2 -11 1 426.86 427.89 12.01 o
-1 -11 1 333.97 270.14 9.83 o
0 -11 1 194.03 197.27 8.23 o
1 -11 1 68.58 62.41 3.90 o
2 -11 1 43.25 29.06 3.43 o
3 -11 1 0.05 2.96 2.90 o
4 -11 1 346.47 365.93 9.71 o
5 -11 1 0.94 0.73 2.86 o
6 -11 1 148.45 143.02 9.05 o
7 -11 1 146.69 156.20 6.20 o
-4 -10 1 58.56 55.59 5.49 o
-3 -10 1 125.25 149.43 7.77 o
-2 -10 1 1223.11 1182.90 27.97 o
-1 -10 1 1477.19 1407.46 29.00 o
0 -10 1 231.96 225.93 11.71 o
1 -10 1 35.54 41.08 4.16 o
2 -10 1 34.36 37.53 3.10 o
3 -10 1 38.08 41.60 3.54 o
4 -10 1 30.18 33.92 3.58 o
5 -10 1 118.65 107.58 10.51 o
6 -10 1 32.66 46.98 8.84 o
7 -10 1 1.95 2.42 3.34 o
8 -10 1 406.06 379.77 12.29 o
-5 -9 1 126.90 126.88 8.53 o
-4 -9 1 5.68 2.39 4.69 o
-3 -9 1 17.10 16.08 3.93 o
-2 -9 1 225.52 224.32 9.37 o
-1 -9 1 511.10 520.86 24.64 o
0 -9 1 6.11 6.77 6.45 o
1 -9 1 5.72 13.65 6.82 o
2 -9 1 0.64 0.76 6.07 o
3 -9 1 248.04 265.01 11.11 o
4 -9 1 1762.78 1846.46 40.49 o
5 -9 1 1025.77 986.61 23.73 o
6 -9 1 107.72 106.43 8.29 o
7 -9 1 13.60 11.79 3.78 o
8 -9 1 8.56 14.73 4.42 o
9 -9 1 83.68 77.61 5.45 o
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-5 -8 1 199.62 203.92 9.55 o
-4 -8 1 110.54 93.94 6.33 o
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-2 -8 1 3.21 7.90 6.18 o
0 -8 1 14.88 4.93 7.20 o
1 -8 1 1.68 6.46 6.25 o
2 -8 1 171.08 196.69 11.60 o
3 -8 1 1335.32 1376.11 49.81 o
4 -8 1 0.12 0.00 4.93 o
5 -8 1 76.95 67.15 10.42 o
6 -8 1 114.82 121.34 7.96 o
7 -8 1 4.18 6.24 3.64 o
8 -8 1 987.09 1002.53 28.24 o
9 -8 1 376.30 386.39 12.65 o
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-3 -7 1 459.69 418.89 52.69 o
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0 -7 1 122.07 165.69 11.37 o
1 -7 1 12.08 10.18 3.64 o
2 -7 1 209.91 228.49 12.79 o
3 -7 1 985.24 1053.86 35.72 o
4 -7 1 356.98 379.01 16.35 o
5 -7 1 342.85 365.44 22.74 o
6 -7 1 0.04 1.48 3.91 o
7 -7 1 1.64 1.24 3.44 o
8 -7 1 146.74 147.68 7.58 o
9 -7 1 108.57 105.46 6.74 o
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-5 -6 1 200.86 222.20 18.30 o
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-3 -6 1 1096.10 948.09 48.14 o
-2 -6 1 3401.97 3050.86 154.67 o
-1 -6 1 1066.60 969.31 32.97 o
0 -6 1 5846.01 6646.28 247.14 o
1 -6 1 598.64 776.41 29.89 o
2 -6 1 85.37 107.66 8.34 o
3 -6 1 493.72 480.30 26.91 o
4 -6 1 663.25 683.27 23.53 o
5 -6 1 27.65 27.29 7.20 o
7 -6 1 47.50 46.34 4.24 o
8 -6 1 6.72 7.82 4.23 o
9 -6 1 64.58 64.83 5.73 o
-8 -5 1 19.46 19.50 4.15 o
-7 -5 1 3.05 1.36 4.69 o
-6 -5 1 12.93 25.93 4.22 o
-5 -5 1 11.75 16.68 6.82 o
-4 -5 1 456.70 281.95 18.00 o
-3 -5 1 2356.40 1929.91 112.21 o
-2 -5 1 1531.01 1234.70 45.57 o
-1 -5 1 250.16 261.49 15.28 o
0 -5 1 5250.13 5736.83 193.40 o
1 -5 1 4176.00 4708.89 163.91 o
2 -5 1 2.94 17.44 7.20 o
3 -5 1 35.03 35.63 7.58 o
4 -5 1 186.29 152.77 10.24 o
5 -5 1 14.22 26.91 6.82 o
7 -5 1 115.01 120.48 12.35 o
8 -5 1 0.63 1.02 3.80 o
9 -5 1 48.32 43.69 5.37 o
-8 -4 1 464.14 542.23 16.29 o
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-6 -4 1 2456.29 2508.88 60.55 o
-4 -4 1 322.29 289.62 18.58 o
-3 -4 1 411.20 524.65 37.91 o
-2 -4 1 184.96 163.44 9.78 o
-1 -4 1 16.68 22.57 5.50 o
0 -4 1 350.22 357.86 15.28 o
1 -4 1 856.14 810.22 27.07 o
2 -4 1 1511.89 1791.16 114.86 o
3 -4 1 38.98 68.23 8.72 o
4 -4 1 402.19 512.14 33.36 o
5 -4 1 35.20 51.93 8.34 o
6 -4 1 172.57 173.62 14.03 o
7 -4 1 18.32 7.12 5.31 o
8 -4 1 115.61 101.80 6.69 o
9 -4 1 173.65 167.28 8.93 o
10 -4 1 5.55 7.20 4.55 o
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-8 -3 1 153.98 200.32 9.45 o
-7 -3 1 1582.52 1624.82 62.26 o
-6 -3 1 1627.99 1630.43 65.96 o
-5 -3 1 1425.77 983.72 51.18 o
-4 -3 1 286.41 216.46 18.58 o
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-1 -3 1 450.12 431.93 12.73 o
0 -3 1 681.69 601.82 17.69 o
1 -3 1 239.81 256.60 14.59 o
2 -3 1 1981.84 2139.74 54.41 o
3 -3 1 61.22 63.31 6.82 o
4 -3 1 90.75 85.29 9.10 o
5 -3 1 56.76 68.61 8.72 o
6 -3 1 324.36 343.22 17.37 o
7 -3 1 34.78 40.36 6.08 o
8 -3 1 120.98 132.41 16.77 o
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1 -2 1 158.83 165.28 3.41 o
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3 -2 1 937.96 798.35 35.63 o
4 -2 1 328.91 516.31 28.43 o
5 -2 1 322.32 295.14 13.71 o
6 -2 1 312.56 264.88 27.29 o
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8 -2 1 102.09 108.42 10.61 o
9 -2 1 22.74 20.09 6.07 o
-9 -1 1 40.44 41.58 5.09 o
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-5 -1 1 1343.83 1112.61 65.58 o
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-3 -1 1 2230.48 2105.43 72.78 o
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-1 -1 1 24934.07 26656.07 789.01 o
0 -1 1 2477.24 3029.25 183.48 o
1 -1 1 13511.15 15451.40 705.85 o
2 -1 1 8685.53 10004.37 487.12 o
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5 -1 1 14.57 25.34 4.91 o
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-10 0 1 108.87 118.27 8.72 o
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3 1 1 11.50 17.44 6.07 o
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-1 2 1 3161.40 3584.29 103.96 o
0 2 1 1553.92 1766.36 51.47 o
1 2 1 285.36 235.95 8.91 o
2 2 1 29.11 45.49 7.20 o
3 2 1 416.58 440.49 20.85 o
4 2 1 382.43 357.85 20.09 o
5 2 1 401.97 309.33 18.95 o
6 2 1 85.27 73.92 9.10 o
7 2 1 33.90 26.34 4.80 o
8 2 1 8.80 7.58 6.07 o
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-9 3 1 88.48 88.60 5.22 o
-8 3 1 12.50 6.39 3.89 o
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-5 3 1 698.99 740.73 45.11 o
-4 3 1 1849.74 1748.33 78.85 o
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-1 3 1 28867.40 37526.46 1309.43 o
0 3 1 1468.32 1516.05 54.55 o
1 3 1 1549.84 1726.91 77.74 o
2 3 1 4.49 24.64 5.69 o
3 3 1 917.88 783.18 44.73 o
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7 3 1 3.34 6.56 4.42 o
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