#------------------------------------------------------------------------------ #$Date: 2020-11-24 07:11:03 +0200 (Tue, 24 Nov 2020) $ #$Revision: 259226 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108715.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108715 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 28.1314 _cell_length_b 28.1314 _cell_length_c 4.0938 _exptl_crystal_F_000 1491.20 _reflns_d_resolution_high 0.7938 _cod_data_source_file dk5103C6H5N7.H2Oat200Ksup8.hkl _cod_data_source_block C6H5N7.H2Oat200K _shelx_title ' 1b in I41/a No88' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.37 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+3/4, x+1/4, z+1/4' '-x, -y+1/2, z' 'y+1/4, -x+1/4, z+1/4' 'x+1/2, y+1/2, z+1/2' '-y+5/4, x+3/4, z+3/4' '-x+1/2, -y+1, z+1/2' 'y+3/4, -x+3/4, z+3/4' '-x, -y, -z' 'y-3/4, -x-1/4, -z-1/4' 'x, y-1/2, -z' '-y-1/4, x-1/4, -z-1/4' '-x+1/2, -y+1/2, -z+1/2' 'y-1/4, -x+1/4, -z+1/4' 'x+1/2, y, -z+1/2' '-y+1/4, x+1/4, -z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 1114.60 952.00 8.99 o 2 2 0 790.35 1088.94 11.49 o -2 4 0 55910.05 51808.50 101.56 o 0 4 0 55227.89 52023.89 95.27 o 2 4 0 16889.40 16323.97 56.18 o 4 4 0 30189.13 25497.96 80.36 o -4 6 0 6605.47 5656.64 42.70 o -2 6 0 7348.47 7355.97 46.11 o 0 6 0 12189.35 10855.53 53.82 o 2 6 0 8469.51 8449.72 48.11 o 4 6 0 6064.86 6503.08 45.63 o 6 6 0 27060.47 25173.57 99.65 o -6 8 0 7583.96 7038.06 58.43 o -4 8 0 1717.85 1505.45 24.92 o -2 8 0 17995.49 15281.36 76.11 o 0 8 0 11495.98 9908.59 60.31 o 2 8 0 32319.49 27194.52 101.72 o 4 8 0 1571.01 1500.21 31.34 o 6 8 0 63.03 95.79 6.90 o 8 8 0 3642.23 3966.48 47.09 o -8 10 0 0.20 23.97 4.47 o -6 10 0 16927.65 16108.90 98.13 o -4 10 0 680.85 601.69 17.60 o -2 10 0 4940.74 4896.16 48.41 o 0 10 0 91.05 112.76 7.43 o 2 10 0 2247.75 2295.17 32.93 o 4 10 0 7799.72 7528.25 61.67 o 6 10 0 382.66 393.80 20.25 o 8 10 0 12542.82 12537.02 88.86 o 10 10 0 200.13 181.95 11.88 o -10 12 0 4000.43 4568.76 62.05 o -8 12 0 914.31 940.72 27.02 o -6 12 0 1954.07 1944.05 36.71 o -4 12 0 1611.77 1545.08 31.26 o -2 12 0 422.04 473.60 16.93 o 0 12 0 501.13 404.66 15.69 o 2 12 0 20682.43 20651.63 110.51 o 4 12 0 34560.40 32873.36 144.26 o 6 12 0 694.58 853.15 24.29 o 8 12 0 2799.40 3175.29 48.23 o 10 12 0 3853.37 3956.40 57.51 o 12 12 0 1290.59 1479.93 37.71 o -12 14 0 2335.51 2413.75 50.90 o -10 14 0 350.72 351.54 18.55 o -8 14 0 5971.53 6214.66 74.93 o -6 14 0 450.68 445.27 19.23 o -4 14 0 2831.80 3238.24 49.47 o -2 14 0 90.56 127.18 9.86 o 0 14 0 1164.57 1090.94 27.91 o 2 14 0 4689.86 4867.99 58.83 o 4 14 0 1130.98 990.74 27.44 o 6 14 0 39.32 102.37 9.25 o 8 14 0 13809.83 14592.53 113.25 o 10 14 0 274.89 314.95 17.53 o 12 14 0 583.84 664.17 26.67 o 14 14 0 14.07 15.03 4.79 o -14 16 0 3014.46 2806.52 43.07 o -12 16 0 52.23 49.28 8.05 o -10 16 0 2364.97 2210.83 50.07 o -8 16 0 508.84 560.70 24.40 o -6 16 0 703.91 878.74 29.13 o -4 16 0 80.26 54.17 7.28 o -2 16 0 2077.39 1972.43 41.52 o 0 16 0 13292.35 13675.86 109.25 o 2 16 0 726.82 884.47 28.02 o 4 16 0 2191.55 2446.88 46.66 o 6 16 0 312.34 360.02 18.69 o 8 16 0 1023.28 1052.48 32.75 o 10 16 0 412.88 354.64 19.98 o 12 16 0 51.77 55.66 8.43 o 14 16 0 117.40 96.60 11.61 o 16 16 0 293.70 301.36 10.35 o -16 18 0 596.84 627.32 17.46 o -14 18 0 576.76 621.75 13.23 o -12 18 0 140.42 124.53 6.49 o -10 18 0 4567.17 4656.24 76.94 o -8 18 0 12.28 12.18 4.46 o -6 18 0 21.28 49.96 7.91 o -4 18 0 11596.13 11098.76 110.52 o -2 18 0 678.61 677.15 26.53 o 0 18 0 5912.86 6141.23 79.40 o 2 18 0 1390.24 1632.42 40.82 o 4 18 0 62.11 90.92 10.02 o 6 18 0 3951.49 4207.72 67.86 o 8 18 0 447.61 385.19 21.28 o 10 18 0 0.05 -0.28 2.05 o 12 18 0 2.65 2.21 2.26 o 14 18 0 92.07 78.12 5.30 o 16 18 0 285.56 288.57 11.65 o 18 18 0 427.61 385.20 13.43 o -18 20 0 0.20 3.37 2.59 o -16 20 0 1551.78 1643.63 28.39 o -14 20 0 1861.63 1964.33 30.50 o -12 20 0 1590.20 1564.18 23.51 o -10 20 0 657.91 650.26 15.72 o -8 20 0 2483.93 2382.60 27.69 o -6 20 0 1259.69 1308.09 41.14 o -4 20 0 8262.50 8445.79 101.78 o -2 20 0 160.63 161.57 14.12 o 0 20 0 7121.93 7309.38 93.65 o 2 20 0 641.17 694.51 29.08 o 4 20 0 858.42 880.92 33.07 o 6 20 0 2581.33 2636.62 57.90 o 8 20 0 16.61 29.02 4.96 o 10 20 0 42.86 25.80 2.34 o 12 20 0 1.89 0.75 2.35 o 14 20 0 0.01 -2.66 2.66 o 16 20 0 761.54 745.39 18.98 o 18 20 0 293.82 318.70 12.23 o 20 20 0 1157.38 1074.25 21.76 o -20 22 0 84.86 89.15 6.23 o -18 22 0 4072.85 4144.70 42.15 o -16 22 0 518.61 478.32 15.20 o -14 22 0 240.27 247.53 11.01 o -12 22 0 1021.51 1037.16 22.08 o -10 22 0 655.98 641.29 17.41 o -8 22 0 1423.94 1381.95 42.68 o -6 22 0 615.96 545.15 13.38 o -4 22 0 627.90 623.55 12.32 o -2 22 0 3031.01 2994.82 23.50 o 0 22 0 425.51 469.97 9.35 o 2 22 0 37.13 41.59 4.05 o 4 22 0 266.98 234.25 8.91 o 6 22 0 2265.42 2121.01 26.55 o 8 22 0 197.44 215.74 8.69 o 10 22 0 2045.51 2117.76 31.19 o 12 22 0 25.90 27.45 4.16 o 14 22 0 10.64 11.37 2.99 o 16 22 0 1002.77 917.63 20.40 o 18 22 0 920.62 950.35 20.19 o 20 22 0 0.01 -2.07 2.20 o 22 22 0 504.40 443.13 12.26 o -22 24 0 832.88 844.95 14.95 o -20 24 0 23.55 28.85 3.54 o -18 24 0 308.96 330.37 11.33 o -16 24 0 2039.07 2017.60 28.88 o -14 24 0 360.42 346.44 12.59 o -12 24 0 1639.65 1585.68 26.87 o -10 24 0 638.11 664.60 17.61 o -8 24 0 4.30 6.37 2.56 o -6 24 0 1950.43 2098.77 31.07 o -4 24 0 2543.21 2398.34 33.47 o -2 24 0 3612.16 3394.52 27.80 o 0 24 0 132.82 112.30 5.18 o 2 24 0 1522.55 1475.90 18.34 o 4 24 0 1388.50 1297.11 28.63 o 6 24 0 516.46 568.65 16.49 o 8 24 0 825.56 808.04 19.70 o 10 24 0 472.36 458.97 14.59 o 12 24 0 51.59 50.18 5.14 o 14 24 0 445.91 393.73 13.36 o 16 24 0 172.33 177.82 8.80 o 18 24 0 181.31 196.16 8.78 o 20 24 0 578.39 580.56 13.73 o 22 24 0 4.83 9.49 2.09 o 24 24 0 127.09 120.75 4.92 o -24 26 0 20.03 29.21 2.02 o -22 26 0 2.06 1.12 1.09 o -20 26 0 2.01 -1.63 1.63 o -18 26 0 1141.62 1111.84 18.75 o -16 26 0 249.77 274.13 10.00 o -14 26 0 529.01 525.18 14.82 o -12 26 0 11.03 14.43 3.37 o -10 26 0 1210.34 1236.29 23.34 o -8 26 0 558.79 582.27 16.41 o -6 26 0 1289.43 1350.94 24.85 o -4 26 0 2545.43 2477.89 23.90 o -2 26 0 509.27 457.10 18.68 o 0 26 0 787.41 748.58 13.12 o 2 26 0 410.70 428.14 9.93 o 4 26 0 595.29 589.94 11.68 o 6 26 0 1154.04 1254.30 20.61 o 8 26 0 2109.35 2131.88 29.11 o 10 26 0 1019.64 1141.86 22.59 o 12 26 0 1407.76 1274.47 23.42 o 14 26 0 132.22 127.63 7.34 o 16 26 0 939.59 918.84 18.49 o 18 26 0 91.01 95.18 5.79 o 20 26 0 5.87 4.89 1.80 o 22 26 0 106.40 125.84 3.49 o 24 26 0 52.85 59.95 2.81 o -20 28 0 1.26 -0.99 0.99 o -18 28 0 2.95 2.66 1.56 o -16 28 0 277.48 295.57 9.32 o -14 28 0 249.67 285.28 9.69 o -12 28 0 324.28 284.91 10.24 o -10 28 0 146.86 156.03 7.94 o -8 28 0 61.33 68.65 5.46 o -6 28 0 51.40 50.48 4.96 o -4 28 0 145.45 150.26 8.11 o -2 28 0 34.55 19.65 2.57 o 0 28 0 452.28 460.72 12.59 o 2 28 0 23.21 19.10 2.41 o 4 28 0 1517.22 1624.47 41.94 o 6 28 0 595.23 530.27 10.63 o 8 28 0 2076.87 2058.40 20.45 o 10 28 0 284.02 320.25 7.97 o 12 28 0 279.79 278.48 7.15 o 14 28 0 256.62 302.70 9.60 o 16 28 0 0.57 0.80 1.10 o 18 28 0 4.95 1.80 0.84 o 20 28 0 156.86 163.13 3.66 o -18 30 0 82.44 66.42 3.17 o -16 30 0 301.30 367.54 8.59 o -14 30 0 164.83 183.00 6.84 o -12 30 0 10.71 11.56 2.36 o -10 30 0 39.06 22.02 2.90 o -8 30 0 362.90 338.22 10.83 o -6 30 0 518.67 635.63 15.04 o -4 30 0 34.72 32.28 3.83 o -2 30 0 1023.83 1050.05 19.75 o 0 30 0 726.44 812.55 17.49 o 2 30 0 6.73 2.83 2.62 o 4 30 0 160.43 162.84 5.48 o 6 30 0 829.38 796.05 19.55 o 8 30 0 2204.02 2232.25 21.07 o 10 30 0 59.90 73.15 4.74 o 12 30 0 1196.90 1133.85 24.62 o 14 30 0 42.87 30.64 2.36 o 16 30 0 0.39 1.21 0.65 o 18 30 0 131.85 119.12 4.09 o -14 32 0 22.79 26.60 2.14 o -12 32 0 14.39 19.92 2.21 o -10 32 0 204.33 229.99 7.18 o -8 32 0 66.32 44.79 3.59 o -6 32 0 195.86 171.58 6.81 o -4 32 0 15.26 6.52 2.02 o -2 32 0 427.79 491.32 12.00 o 0 32 0 0.01 4.48 1.99 o 2 32 0 169.52 183.84 7.44 o 4 32 0 531.28 628.73 13.43 o 6 32 0 161.51 152.54 6.43 o 8 32 0 359.53 397.34 9.73 o 10 32 0 154.76 145.34 4.85 o 12 32 0 0.31 0.30 1.11 o -10 34 0 9.70 10.24 1.35 o -8 34 0 586.11 588.96 9.41 o -6 34 0 171.23 163.82 5.23 o -4 34 0 469.69 354.94 8.03 o -2 34 0 49.51 56.92 3.42 o 0 34 0 93.17 67.36 3.78 o 2 34 0 0.45 1.72 1.13 o 4 34 0 87.17 86.68 4.12 o 6 34 0 77.23 73.08 3.63 o 8 34 0 72.25 76.99 3.42 o 0 1 1 21.77 23.90 1.83 o -1 2 1 872.55 790.68 10.50 o 1 2 1 3531.92 3536.03 16.11 o -2 3 1 6634.87 7424.23 26.85 o 0 3 1 8894.63 8567.61 33.74 o 2 3 1 38076.15 38324.68 152.07 o -3 4 1 18696.77 17684.25 52.00 o -1 4 1 17185.92 15412.86 48.46 o 1 4 1 27398.26 27062.75 53.42 o 3 4 1 3773.69 3310.27 14.75 o -4 5 1 19085.84 17877.71 55.94 o -2 5 1 2613.77 2408.62 14.34 o 0 5 1 65215.09 62201.72 151.36 o 2 5 1 31750.14 30748.61 76.33 o 4 5 1 1287.99 1066.44 18.65 o -5 6 1 146.88 182.75 8.79 o -3 6 1 9105.11 8354.97 29.55 o -1 6 1 59862.76 56479.31 82.71 o 1 6 1 11682.91 11220.36 31.26 o 3 6 1 35721.40 34365.20 72.79 o 5 6 1 13482.29 12820.86 71.94 o -6 7 1 669.29 630.77 11.83 o -4 7 1 1205.61 1243.91 12.33 o -2 7 1 18068.96 17280.95 64.66 o 0 7 1 10125.25 10121.42 31.83 o 2 7 1 264.94 268.74 6.43 o 4 7 1 5956.67 5660.72 25.88 o 6 7 1 255.16 231.39 10.58 o -7 8 1 2553.07 2576.33 25.92 o -5 8 1 516.19 507.79 11.12 o -3 8 1 2305.49 2337.19 14.52 o -1 8 1 1116.65 1116.87 11.26 o 1 8 1 7154.50 7034.74 46.31 o 3 8 1 363.09 318.76 7.71 o 5 8 1 465.66 545.42 8.88 o 7 8 1 4381.89 4186.38 48.30 o -8 9 1 2372.74 2196.77 38.28 o -6 9 1 352.45 338.87 9.52 o -4 9 1 4210.04 4321.91 20.38 o -2 9 1 76.41 56.90 3.13 o 0 9 1 8200.02 7941.65 114.70 o 2 9 1 132.59 196.84 6.49 o 4 9 1 870.33 768.60 10.80 o 6 9 1 2209.35 2095.57 18.88 o 8 9 1 0.13 0.62 2.04 o -9 10 1 659.54 550.47 20.73 o -7 10 1 484.24 565.04 13.27 o -5 10 1 196.99 291.81 12.65 o -3 10 1 1557.34 1387.46 14.56 o -1 10 1 5176.21 5135.41 34.90 o 1 10 1 1.81 2.21 1.31 o 3 10 1 680.94 607.54 12.06 o 5 10 1 1387.53 1254.49 19.67 o 7 10 1 299.59 279.92 7.51 o 9 10 1 1.17 -1.52 2.25 o -10 11 1 1681.11 1769.91 39.40 o -8 11 1 962.05 987.39 18.85 o -6 11 1 3296.44 3219.00 32.27 o -4 11 1 219.36 239.09 8.48 o -2 11 1 1170.48 1108.82 13.08 o 0 11 1 3991.25 4347.76 33.84 o 2 11 1 44.98 23.67 2.63 o 4 11 1 220.41 235.82 8.12 o 6 11 1 563.24 633.09 13.88 o 8 11 1 156.51 153.42 6.07 o 10 11 1 141.81 185.11 8.27 o -11 12 1 569.04 543.41 23.21 o -9 12 1 11.51 18.99 3.09 o -7 12 1 772.20 834.08 17.63 o -5 12 1 1361.18 1506.16 22.58 o -3 12 1 3053.81 3041.28 30.81 o -1 12 1 6906.93 7100.69 45.84 o 1 12 1 3710.08 3926.48 38.14 o 3 12 1 4996.57 5344.11 40.03 o 5 12 1 1506.62 1511.02 27.12 o 7 12 1 1018.47 1023.67 18.90 o 9 12 1 1574.45 1435.63 19.54 o 11 12 1 3162.28 3142.04 37.31 o -12 13 1 6.71 6.03 2.57 o -10 13 1 1383.14 1361.11 36.98 o -8 13 1 346.16 387.72 12.79 o -6 13 1 23.22 26.34 3.38 o -4 13 1 8994.34 9152.74 124.60 o -2 13 1 36.65 26.00 3.44 o 0 13 1 5844.68 6093.33 66.86 o 2 13 1 664.31 582.30 23.96 o 4 13 1 6111.72 6431.00 46.94 o 6 13 1 80.27 72.78 5.29 o 8 13 1 4267.65 4302.70 54.42 o 10 13 1 801.51 786.94 15.43 o 12 13 1 311.63 344.57 10.77 o -13 14 1 7.25 18.75 2.89 o -11 14 1 306.44 240.77 16.43 o -9 14 1 98.50 99.32 12.06 o -7 14 1 2688.70 2835.26 35.21 o -5 14 1 3445.79 3529.35 80.07 o -3 14 1 93.30 140.73 7.46 o -1 14 1 5846.86 5893.48 46.25 o 1 14 1 82.40 67.51 5.10 o 3 14 1 691.27 669.43 20.82 o 5 14 1 3154.50 3383.33 35.92 o 7 14 1 14.43 14.24 3.09 o 9 14 1 249.15 309.57 11.87 o 11 14 1 1905.23 1783.54 29.67 o 13 14 1 0.00 2.58 2.01 o -14 15 1 338.38 324.06 9.37 o -12 15 1 1952.11 2001.24 49.85 o -10 15 1 57.67 57.25 5.71 o -8 15 1 237.84 265.14 11.47 o -6 15 1 1798.03 1848.39 29.07 o -4 15 1 2991.47 2986.58 40.76 o -2 15 1 312.92 341.56 11.86 o 0 15 1 229.63 285.74 10.72 o 2 15 1 16.72 11.59 2.37 o 4 15 1 653.84 726.56 22.45 o 6 15 1 31.13 26.42 3.71 o 8 15 1 374.57 450.12 14.50 o 10 15 1 19.80 24.76 3.58 o 12 15 1 1253.76 1407.26 42.72 o 14 15 1 605.15 628.25 9.14 o -15 16 1 575.90 578.28 9.02 o -13 16 1 682.92 669.01 14.03 o -11 16 1 2.37 -2.93 2.93 o -9 16 1 66.23 49.42 5.39 o -7 16 1 782.14 825.93 20.72 o -5 16 1 744.53 747.54 18.97 o -3 16 1 745.68 770.82 18.75 o -1 16 1 442.03 560.10 15.64 o 1 16 1 720.18 729.18 17.82 o 3 16 1 1240.98 1462.62 25.39 o 5 16 1 2319.05 2580.31 34.10 o 7 16 1 1371.02 1443.85 33.86 o 9 16 1 1996.90 1987.08 32.02 o 11 16 1 72.02 82.47 10.53 o 13 16 1 750.06 820.98 12.49 o 15 16 1 1598.29 1605.92 19.95 o -16 17 1 378.91 438.99 7.11 o -14 17 1 103.67 116.44 4.50 o -12 17 1 12.03 8.89 1.77 o -10 17 1 305.28 319.27 13.96 o -8 17 1 0.80 7.59 2.23 o -6 17 1 47.76 45.57 5.10 o -4 17 1 382.35 429.10 14.73 o -2 17 1 865.82 815.50 21.11 o 0 17 1 20.33 33.24 4.22 o 2 17 1 74.32 86.24 6.53 o 4 17 1 5.77 12.33 2.68 o 6 17 1 75.87 70.16 6.02 o 8 17 1 0.60 6.38 3.64 o 10 17 1 2053.20 2237.87 54.60 o 12 17 1 643.34 621.98 11.02 o 14 17 1 10.62 11.22 2.17 o 16 17 1 672.52 667.83 10.07 o -17 18 1 1570.50 1505.10 24.67 o -15 18 1 129.87 140.81 4.87 o -13 18 1 0.00 -0.36 1.83 o -11 18 1 458.58 471.10 9.57 o -9 18 1 640.91 636.33 19.84 o -7 18 1 0.92 8.99 2.65 o -5 18 1 2236.37 2278.28 35.40 o -3 18 1 1929.19 1980.00 32.23 o -1 18 1 426.91 375.55 13.90 o 1 18 1 4504.90 4439.75 47.57 o 3 18 1 474.76 388.48 14.13 o 5 18 1 0.60 -3.32 3.32 o 7 18 1 42.49 34.34 6.53 o 9 18 1 253.99 275.50 19.54 o 11 18 1 593.42 577.29 10.78 o 13 18 1 44.75 45.38 3.22 o 15 18 1 30.13 26.71 3.23 o 17 18 1 696.48 715.53 10.40 o -18 19 1 644.11 617.36 9.61 o -16 19 1 1111.56 1061.31 11.04 o -14 19 1 128.43 150.64 4.90 o -12 19 1 23.15 17.88 1.80 o -10 19 1 102.02 105.68 4.33 o -8 19 1 29.62 31.98 2.20 o -6 19 1 632.50 625.45 19.57 o -4 19 1 452.27 485.15 16.76 o -2 19 1 93.38 87.09 7.07 o 0 19 1 8.05 7.54 2.41 o 2 19 1 1.97 -1.52 2.46 o 4 19 1 2264.10 2348.07 55.48 o 6 19 1 0.82 0.53 2.44 o 8 19 1 1723.51 1642.92 19.23 o 10 19 1 616.52 658.22 11.53 o 12 19 1 205.61 174.12 6.06 o 14 19 1 25.33 23.56 2.76 o 16 19 1 33.18 31.97 3.26 o 18 19 1 211.08 203.76 5.56 o -19 20 1 2.56 5.80 1.66 o -17 20 1 700.66 701.71 10.19 o -15 20 1 1307.42 1289.18 14.36 o -13 20 1 3067.70 3059.84 25.98 o -11 20 1 63.02 66.42 3.12 o -9 20 1 243.30 251.31 5.90 o -7 20 1 776.36 803.38 8.70 o -5 20 1 4.82 5.38 1.00 o -3 20 1 186.12 143.00 14.08 o -1 20 1 49.59 78.32 10.33 o 1 20 1 303.29 316.43 20.85 o 3 20 1 310.31 332.04 21.33 o 5 20 1 680.80 701.78 9.71 o 7 20 1 609.43 601.91 14.55 o 9 20 1 48.88 36.70 3.48 o 11 20 1 41.20 37.32 3.00 o 13 20 1 106.20 86.85 4.73 o 15 20 1 429.97 397.30 7.81 o 17 20 1 71.97 78.60 4.58 o 19 20 1 171.91 170.67 4.95 o -20 21 1 31.57 22.27 1.85 o -18 21 1 65.09 83.99 3.49 o -16 21 1 53.72 45.93 2.49 o -14 21 1 115.37 127.45 4.54 o -12 21 1 245.14 257.82 13.76 o -10 21 1 1920.04 1885.32 18.33 o -8 21 1 1903.91 1982.15 16.17 o -6 21 1 1322.90 1295.55 11.63 o -4 21 1 101.65 91.27 3.13 o -2 21 1 6.50 3.61 1.11 o 0 21 1 1977.22 1954.71 17.14 o 2 21 1 618.80 625.76 11.12 o 4 21 1 718.91 757.58 12.31 o 6 21 1 770.99 821.33 11.33 o 8 21 1 73.72 76.31 4.09 o 10 21 1 1997.22 1938.04 22.77 o 12 21 1 148.60 160.42 6.41 o 14 21 1 347.73 342.80 8.20 o 16 21 1 169.36 165.41 4.96 o 18 21 1 448.24 421.21 7.59 o 20 21 1 65.87 69.42 3.01 o -21 22 1 0.53 1.50 1.30 o -19 22 1 225.49 218.82 5.19 o -17 22 1 823.42 785.78 10.33 o -15 22 1 762.35 772.34 9.20 o -13 22 1 324.11 316.00 16.99 o -11 22 1 37.83 25.77 4.83 o -9 22 1 27.25 27.21 1.97 o -7 22 1 4.39 8.92 1.68 o -5 22 1 309.84 333.74 5.32 o -3 22 1 108.76 120.67 3.64 o -1 22 1 816.76 809.79 9.17 o 1 22 1 185.24 154.94 5.58 o 3 22 1 3338.17 3290.39 77.25 o 5 22 1 215.32 213.72 7.65 o 7 22 1 6.50 4.25 1.49 o 9 22 1 1622.54 1566.79 21.29 o 11 22 1 90.65 113.51 6.43 o 13 22 1 546.38 522.56 11.28 o 15 22 1 0.02 0.81 1.05 o 17 22 1 148.71 158.22 5.99 o 19 22 1 84.78 90.23 3.39 o 21 22 1 2.00 4.58 1.06 o -22 23 1 40.13 53.08 4.29 o -20 23 1 84.71 67.76 2.70 o -18 23 1 5.00 3.48 1.12 o -16 23 1 1.38 3.69 1.34 o -14 23 1 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