#------------------------------------------------------------------------------ #$Date: 2020-11-24 07:11:03 +0200 (Tue, 24 Nov 2020) $ #$Revision: 259226 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108716.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108716 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 28.1081 _cell_length_b 28.1081 _cell_length_c 4.0692 _exptl_crystal_F_000 1491.20 _reflns_d_resolution_high 0.7939 _cod_data_source_file dk5103C6H5N7.H2Oat150Ksup9.hkl _cod_data_source_block C6H5N7.H2Oat150K _shelx_title ' 1a in I41/a No88' _shelx_refln_list_code 4 _shelx_f_calc_maximum 260.85 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+3/4, x+1/4, z+1/4' '-x, -y+1/2, z' 'y+1/4, -x+1/4, z+1/4' 'x+1/2, y+1/2, z+1/2' '-y+5/4, x+3/4, z+3/4' '-x+1/2, -y+1, z+1/2' 'y+3/4, -x+3/4, z+3/4' '-x, -y, -z' 'y-3/4, -x-1/4, -z-1/4' 'x, y-1/2, -z' '-y-1/4, x-1/4, -z-1/4' '-x+1/2, -y+1/2, -z+1/2' 'y-1/4, -x+1/4, -z+1/4' 'x+1/2, y, -z+1/2' '-y+1/4, x+1/4, -z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 1183.31 968.48 12.05 o 2 2 0 791.57 1040.59 14.04 o -2 4 0 55381.12 50395.07 445.77 o 0 4 0 54431.23 50849.36 448.32 o 2 4 0 16173.88 16558.64 152.97 o 4 4 0 30623.90 27011.05 246.24 o -4 6 0 6863.18 6056.04 67.28 o -2 6 0 7386.49 7334.37 76.96 o 0 6 0 12596.39 11322.14 111.08 o 2 6 0 8656.68 9004.41 91.08 o 4 6 0 6272.49 6654.55 72.42 o 6 6 0 27336.68 25097.14 236.52 o -6 8 0 7953.93 7447.86 86.00 o -4 8 0 1893.58 1646.00 28.66 o -2 8 0 18644.59 15841.47 155.68 o 0 8 0 11570.37 10462.97 107.56 o 2 8 0 33037.65 29006.52 269.33 o 4 8 0 1445.68 1385.03 62.15 o 6 8 0 70.74 87.27 6.34 o 8 8 0 4183.44 4554.73 61.76 o -8 10 0 1.19 22.22 4.05 o -6 10 0 18333.54 17469.14 178.68 o -4 10 0 697.30 565.27 17.05 o -2 10 0 5132.10 5234.20 65.81 o 0 10 0 120.32 173.39 8.82 o 2 10 0 2371.67 2465.89 38.93 o 4 10 0 8103.06 7660.92 89.31 o 6 10 0 362.20 380.71 18.63 o 8 10 0 12945.09 12536.63 137.54 o 10 10 0 206.62 177.42 11.30 o -10 12 0 4196.66 4817.05 73.51 o -8 12 0 1129.86 1067.52 28.74 o -6 12 0 1935.15 1911.52 38.85 o -4 12 0 1813.55 1747.15 35.12 o -2 12 0 510.41 576.44 18.68 o 0 12 0 452.18 337.31 14.06 o 2 12 0 22776.16 22768.39 226.11 o 4 12 0 37448.20 36455.77 346.04 o 6 12 0 650.14 742.02 22.84 o 8 12 0 2975.43 3398.83 56.56 o 10 12 0 4259.39 4433.73 69.40 o 12 12 0 1330.86 1490.19 38.32 o -12 14 0 2520.42 2602.47 55.21 o -10 14 0 465.52 477.81 20.93 o -8 14 0 6787.86 6950.88 95.45 o -6 14 0 455.50 428.49 18.30 o -4 14 0 3452.90 3950.78 62.29 o -2 14 0 132.34 184.03 11.54 o 0 14 0 1153.95 1038.12 27.57 o 2 14 0 5074.95 5296.35 75.00 o 4 14 0 1300.49 1103.60 29.32 o 6 14 0 47.47 114.62 9.54 o 8 14 0 14782.82 15653.68 175.92 o 10 14 0 317.62 361.44 18.38 o 12 14 0 579.92 616.13 25.46 o 14 14 0 9.02 5.24 2.90 o -14 16 0 3758.30 3515.83 51.00 o -12 16 0 56.07 55.70 8.20 o -10 16 0 2777.16 2555.75 55.90 o -8 16 0 518.03 537.19 23.04 o -6 16 0 815.44 983.57 30.60 o -4 16 0 110.13 72.92 8.09 o -2 16 0 2336.22 2251.75 46.60 o 0 16 0 14677.22 14806.65 167.96 o 2 16 0 954.48 1140.98 31.71 o 4 16 0 2355.13 2571.29 50.97 o 6 16 0 404.96 456.04 20.57 o 8 16 0 1215.65 1280.99 36.41 o 10 16 0 438.86 370.06 20.10 o 12 16 0 61.43 75.84 9.55 o 14 16 0 136.73 111.56 12.27 o 16 16 0 297.99 298.02 10.07 o -16 18 0 787.24 810.03 20.04 o -14 18 0 654.50 662.66 13.60 o -12 18 0 198.23 180.81 10.52 o -10 18 0 5400.99 5587.70 93.67 o -8 18 0 13.71 16.66 4.78 o -6 18 0 37.00 65.33 8.63 o -4 18 0 13311.01 12976.14 158.45 o -2 18 0 567.22 556.01 23.53 o 0 18 0 6908.07 7191.32 102.93 o 2 18 0 1479.11 1783.53 43.72 o 4 18 0 120.92 182.72 13.82 o 6 18 0 4650.14 4871.30 82.36 o 8 18 0 554.31 490.71 23.81 o 10 18 0 0.07 0.52 3.11 o 12 18 0 2.49 4.22 2.13 o 14 18 0 132.89 104.77 6.03 o 16 18 0 461.08 420.63 14.00 o 18 18 0 558.82 501.33 15.10 o -18 20 0 0.57 2.64 3.08 o -16 20 0 2044.22 2025.89 34.62 o -14 20 0 2271.46 2283.54 36.71 o -12 20 0 1908.23 1776.37 26.63 o -10 20 0 873.29 845.06 18.27 o -8 20 0 2941.06 2781.27 34.03 o -6 20 0 1577.61 1539.89 44.94 o -4 20 0 9832.34 9732.54 134.46 o -2 20 0 164.44 170.14 14.06 o 0 20 0 7876.99 7871.67 114.89 o 2 20 0 893.95 913.95 32.96 o 4 20 0 855.62 857.14 32.59 o 6 20 0 3133.63 3097.12 66.52 o 8 20 0 23.43 35.57 6.64 o 10 20 0 94.67 59.97 6.66 o 12 20 0 8.72 7.76 2.36 o 14 20 0 1.48 -3.06 3.06 o 16 20 0 1064.28 1043.54 22.69 o 18 20 0 398.23 396.67 13.55 o 20 20 0 1466.20 1342.18 25.68 o -20 22 0 157.82 160.56 7.91 o -18 22 0 5878.49 5971.10 70.19 o -16 22 0 703.34 618.86 11.94 o -14 22 0 277.51 309.75 12.05 o -12 22 0 1173.48 1202.85 24.99 o -10 22 0 786.89 761.94 19.07 o -8 22 0 1464.15 1407.18 23.10 o -6 22 0 751.50 645.15 11.40 o -4 22 0 699.27 734.56 12.91 o -2 22 0 4001.94 3944.17 33.22 o 0 22 0 627.47 690.99 11.52 o 2 22 0 57.18 58.56 3.38 o 4 22 0 338.73 293.29 11.01 o 6 22 0 2783.83 2578.03 81.13 o 8 22 0 287.31 294.90 9.99 o 10 22 0 2668.20 2698.12 40.96 o 12 22 0 46.85 56.83 5.64 o 14 22 0 6.86 7.61 3.25 o 16 22 0 1436.49 1328.38 26.01 o 18 22 0 1467.33 1517.69 27.50 o 20 22 0 0.06 -1.69 2.48 o 22 22 0 675.02 604.14 14.61 o -22 24 0 1128.22 1225.38 20.24 o -20 24 0 34.48 42.95 4.17 o -18 24 0 458.19 485.16 13.63 o -16 24 0 2870.54 2673.32 39.03 o -14 24 0 355.93 340.23 12.45 o -12 24 0 2159.71 2070.50 34.33 o -10 24 0 863.97 841.42 20.28 o -8 24 0 8.66 11.09 3.01 o -6 24 0 2234.98 2322.39 37.24 o -4 24 0 3186.46 3042.55 44.96 o -2 24 0 4651.93 4439.82 51.95 o 0 24 0 132.10 99.08 4.87 o 2 24 0 1880.00 1757.30 39.22 o 4 24 0 2152.16 2086.58 47.99 o 6 24 0 709.87 759.94 19.44 o 8 24 0 986.80 1032.59 22.99 o 10 24 0 774.89 746.75 18.81 o 12 24 0 74.97 75.05 6.07 o 14 24 0 676.84 591.01 16.33 o 16 24 0 302.73 318.68 11.42 o 18 24 0 277.11 282.08 10.26 o 20 24 0 764.65 756.76 16.37 o 22 24 0 25.66 35.29 3.42 o 24 24 0 176.55 148.56 5.65 o -24 26 0 29.75 33.43 2.15 o -22 26 0 3.50 0.36 1.40 o -20 26 0 0.85 2.61 1.97 o -18 26 0 1547.63 1482.95 24.14 o -16 26 0 302.65 351.73 11.06 o -14 26 0 629.84 630.70 16.39 o -12 26 0 66.23 72.37 5.78 o -10 26 0 1749.89 1801.09 31.08 o -8 26 0 539.51 584.06 16.45 o -6 26 0 1809.20 1903.95 32.50 o -4 26 0 3380.84 3315.57 33.47 o -2 26 0 542.50 505.66 29.98 o 0 26 0 986.69 991.98 15.74 o 2 26 0 504.99 518.64 11.01 o 4 26 0 909.88 914.99 14.95 o 6 26 0 1743.98 1875.41 22.75 o 8 26 0 2764.65 2716.93 49.89 o 10 26 0 1519.79 1632.25 29.45 o 12 26 0 1656.58 1459.24 27.04 o 14 26 0 180.10 170.50 8.34 o 16 26 0 1281.96 1181.57 22.46 o 18 26 0 119.45 121.08 6.24 o 20 26 0 11.11 12.03 2.32 o 22 26 0 190.41 221.61 10.61 o -20 28 0 5.37 2.79 1.32 o -18 28 0 0.88 3.96 1.82 o -16 28 0 449.59 483.05 11.98 o -14 28 0 314.55 357.35 10.63 o -12 28 0 478.25 443.45 12.84 o -10 28 0 191.05 188.64 8.65 o -8 28 0 119.32 121.44 7.05 o -6 28 0 102.72 117.23 7.05 o -4 28 0 169.38 168.02 8.45 o -2 28 0 31.58 14.02 2.30 o 0 28 0 585.11 596.93 15.88 o 2 28 0 26.17 15.21 2.34 o 4 28 0 2155.29 2255.95 70.07 o 6 28 0 763.92 698.08 12.29 o 8 28 0 2889.14 2853.32 28.76 o 10 28 0 288.06 314.11 7.75 o 12 28 0 454.25 460.30 9.12 o 14 28 0 320.26 365.22 17.97 o 16 28 0 0.42 -0.18 1.33 o 18 28 0 5.97 2.55 1.04 o 20 28 0 236.99 241.10 12.04 o -18 30 0 184.61 154.17 4.75 o -16 30 0 541.32 605.02 11.64 o -14 30 0 260.23 309.72 8.72 o -12 30 0 31.39 29.95 3.23 o -10 30 0 57.52 40.53 3.87 o -8 30 0 461.53 437.00 12.25 o -6 30 0 782.40 889.72 18.73 o -4 30 0 45.72 45.96 4.22 o -2 30 0 1535.83 1526.21 26.08 o 0 30 0 966.05 1064.32 21.15 o 2 30 0 5.77 6.83 2.54 o 4 30 0 224.67 227.97 6.37 o 6 30 0 1146.41 1106.24 17.94 o 8 30 0 2915.25 2981.75 27.86 o 10 30 0 113.78 130.31 5.48 o 12 30 0 1575.30 1483.21 16.25 o 14 30 0 53.39 37.27 2.55 o 16 30 0 1.71 7.12 1.30 o 18 30 0 197.67 180.36 5.06 o -14 32 0 29.14 32.56 2.37 o -12 32 0 31.02 36.63 2.82 o -10 32 0 275.66 340.60 8.83 o -8 32 0 101.24 65.55 4.17 o -6 32 0 312.35 272.74 8.49 o -4 32 0 18.55 6.48 2.04 o -2 32 0 579.82 663.81 14.38 o 0 32 0 1.40 1.80 2.05 o 2 32 0 201.78 206.22 7.69 o 4 32 0 643.22 763.40 15.48 o 6 32 0 189.87 175.96 6.77 o 8 32 0 568.73 615.67 12.78 o 10 32 0 192.96 175.71 4.27 o 12 32 0 1.22 2.41 1.05 o -8 34 0 924.95 860.57 12.97 o -6 34 0 285.77 318.60 7.44 o -4 34 0 671.07 602.66 11.15 o -2 34 0 80.07 93.30 4.26 o 0 34 0 109.68 89.66 4.20 o 2 34 0 9.50 16.81 2.10 o 4 34 0 139.32 143.18 5.09 o 6 34 0 143.39 134.14 4.78 o 8 34 0 179.07 202.41 5.47 o 0 1 1 23.93 30.38 2.92 o -1 2 1 801.61 703.03 9.58 o 1 2 1 3485.82 3506.71 26.52 o -2 3 1 6499.12 7365.57 45.06 o 0 3 1 9309.21 9500.96 67.71 o 2 3 1 38674.17 39322.86 178.50 o -3 4 1 19816.56 18915.45 126.55 o -1 4 1 16090.80 14292.85 98.16 o 1 4 1 27910.14 28456.51 129.67 o 3 4 1 3140.74 2697.81 17.01 o -4 5 1 20034.79 18979.91 128.31 o -2 5 1 2497.39 2278.98 17.78 o 0 5 1 68045.32 65859.57 407.07 o 2 5 1 30950.46 30198.04 180.41 o 4 5 1 1579.41 1329.42 14.56 o -5 6 1 153.14 185.41 8.65 o -3 6 1 9945.06 9352.47 55.61 o -1 6 1 62801.57 60986.18 452.95 o 1 6 1 11641.81 11259.15 64.34 o 3 6 1 37706.86 36982.98 233.97 o 5 6 1 13662.88 12927.18 131.03 o -6 7 1 750.35 720.21 12.88 o -4 7 1 1090.85 1138.62 12.64 o -2 7 1 19137.78 18783.57 89.68 o 0 7 1 9820.19 9806.47 57.74 o 2 7 1 257.64 256.19 6.26 o 4 7 1 5851.11 5729.22 38.20 o 6 7 1 284.97 250.86 10.69 o -7 8 1 2720.36 2777.60 39.25 o -5 8 1 576.39 582.56 12.39 o -3 8 1 2386.40 2410.33 17.59 o -1 8 1 974.04 1025.90 13.88 o 1 8 1 7285.16 7160.05 55.65 o 3 8 1 443.23 390.85 8.54 o 5 8 1 574.12 663.80 9.97 o 7 8 1 4561.68 4319.43 59.82 o -8 9 1 2570.71 2410.32 43.29 o -6 9 1 341.09 336.70 9.32 o -4 9 1 4503.57 4676.37 33.77 o -2 9 1 46.22 29.65 1.77 o 0 9 1 9021.94 8935.57 68.37 o 2 9 1 72.46 129.48 5.12 o 4 9 1 869.19 775.74 11.10 o 6 9 1 2199.53 2095.75 26.50 o 8 9 1 0.24 0.37 2.42 o -9 10 1 732.47 625.26 21.49 o -7 10 1 486.54 595.31 21.27 o -5 10 1 182.47 257.42 8.30 o -3 10 1 1755.25 1604.20 13.81 o -1 10 1 5433.97 5478.62 48.11 o 1 10 1 3.89 2.53 1.28 o 3 10 1 656.74 540.95 11.49 o 5 10 1 1373.65 1216.62 15.42 o 7 10 1 344.20 320.27 7.94 o 9 10 1 0.00 0.94 1.36 o -10 11 1 1944.99 2020.90 43.90 o -8 11 1 988.34 1021.57 19.26 o -6 11 1 3310.97 3210.56 36.52 o -4 11 1 296.58 324.03 9.56 o -2 11 1 1359.76 1303.31 14.93 o 0 11 1 4164.49 4488.68 98.60 o 2 11 1 79.27 52.42 3.78 o 4 11 1 201.95 229.92 7.87 o 6 11 1 525.10 565.23 14.83 o 8 11 1 159.06 138.73 6.28 o 10 11 1 108.63 132.66 6.90 o -11 12 1 561.28 553.27 22.81 o -9 12 1 15.33 24.39 3.29 o -7 12 1 992.55 1073.39 20.17 o -5 12 1 1502.20 1682.32 24.90 o -3 12 1 3460.56 3508.75 38.25 o -1 12 1 7467.68 7627.44 65.16 o 1 12 1 4147.40 4406.44 95.02 o 3 12 1 5487.91 5911.77 83.39 o 5 12 1 1491.20 1493.68 27.27 o 7 12 1 1130.27 1185.68 20.81 o 9 12 1 1751.23 1554.92 20.99 o 11 12 1 3486.23 3426.07 34.98 o -12 13 1 5.03 2.34 1.84 o -10 13 1 1624.17 1591.06 40.39 o -8 13 1 283.84 310.00 11.04 o -6 13 1 14.93 22.54 3.19 o -4 13 1 9766.46 9989.75 83.60 o -2 13 1 50.69 42.78 4.02 o 0 13 1 6240.98 6565.31 59.89 o 2 13 1 799.83 690.81 15.05 o 4 13 1 6654.70 6730.79 61.84 o 6 13 1 93.78 86.86 5.61 o 8 13 1 4965.93 4802.39 51.49 o 10 13 1 915.82 903.95 16.45 o 12 13 1 322.22 369.61 10.87 o -13 14 1 15.34 23.98 3.02 o -11 14 1 405.85 366.53 19.65 o -9 14 1 138.59 120.61 7.41 o -7 14 1 3117.51 3214.95 40.75 o -5 14 1 3697.17 3842.84 44.25 o -3 14 1 124.50 161.82 7.61 o -1 14 1 6341.67 6428.25 142.83 o 1 14 1 66.80 100.21 50.18 o 3 14 1 761.16 748.74 31.34 o 5 14 1 3561.55 3818.86 43.43 o 7 14 1 42.55 48.55 4.55 o 9 14 1 270.40 336.55 12.11 o 11 14 1 2401.46 2313.21 35.62 o 13 14 1 2.51 0.39 2.41 o -14 15 1 421.58 422.84 8.36 o -12 15 1 2155.86 2050.26 71.12 o -10 15 1 80.06 89.30 6.82 o -8 15 1 235.85 247.38 10.65 o -6 15 1 2081.68 2138.24 49.07 o -4 15 1 3362.63 3330.97 41.27 o -2 15 1 360.14 388.62 12.34 o 0 15 1 266.29 324.61 19.79 o 2 15 1 21.66 15.90 2.66 o 4 15 1 627.13 700.44 16.78 o 6 15 1 43.32 41.57 4.25 o 8 15 1 426.95 494.98 14.94 o 10 15 1 8.06 15.85 5.52 o 12 15 1 1385.62 1563.93 45.53 o 14 15 1 659.36 669.17 12.98 o -15 16 1 661.38 613.35 12.03 o -13 16 1 877.97 838.04 16.03 o -11 16 1 3.81 -2.21 3.74 o -9 16 1 79.67 58.32 5.60 o -7 16 1 828.65 884.26 20.92 o -5 16 1 917.83 918.55 20.73 o -3 16 1 870.46 888.11 19.99 o -1 16 1 419.46 555.54 26.73 o 1 16 1 899.76 894.41 23.87 o 3 16 1 1291.68 1464.57 25.87 o 5 16 1 2570.66 2768.54 72.04 o 7 16 1 1574.58 1638.24 49.02 o 9 16 1 2284.90 2209.55 35.37 o 11 16 1 70.14 76.08 10.12 o 13 16 1 831.57 915.65 13.54 o 15 16 1 2091.87 2147.21 19.13 o -16 17 1 467.06 517.51 10.08 o -14 17 1 118.89 122.72 5.90 o -12 17 1 14.96 14.87 2.78 o -10 17 1 391.49 413.88 15.30 o -8 17 1 3.32 2.67 2.12 o -6 17 1 50.10 50.98 5.21 o -4 17 1 426.10 470.91 14.95 o -2 17 1 895.02 813.87 19.56 o 0 17 1 24.94 40.65 4.40 o 2 17 1 77.98 82.00 6.24 o 4 17 1 20.44 32.92 4.13 o 6 17 1 79.73 59.38 5.53 o 8 17 1 0.20 18.18 5.71 o 10 17 1 2512.45 2747.17 62.59 o 12 17 1 887.19 879.95 18.18 o 14 17 1 14.24 13.55 2.15 o 16 17 1 927.38 915.59 12.08 o -17 18 1 2084.77 2022.01 19.42 o -15 18 1 174.50 177.90 5.67 o -13 18 1 0.57 -1.91 2.09 o -11 18 1 514.25 520.42 13.30 o -9 18 1 744.04 731.91 20.65 o -7 18 1 1.57 11.93 3.01 o -5 18 1 2620.07 2563.64 38.93 o -3 18 1 2241.24 2347.87 36.54 o -1 18 1 538.28 490.00 20.35 o 1 18 1 5529.45 5425.26 60.26 o 3 18 1 620.54 531.67 28.60 o 5 18 1 0.02 1.28 3.19 o 7 18 1 51.89 48.43 8.22 o 9 18 1 305.42 345.79 21.42 o 11 18 1 760.57 717.33 12.08 o 13 18 1 40.20 41.41 3.14 o 15 18 1 42.67 42.19 8.50 o 17 18 1 961.68 979.39 12.60 o -18 19 1 848.17 837.83 11.39 o -16 19 1 1429.94 1393.33 13.36 o -14 19 1 141.01 170.85 5.13 o -12 19 1 29.99 24.13 3.30 o -10 19 1 125.04 135.26 4.72 o -8 19 1 40.67 41.69 2.30 o -6 19 1 796.01 778.47 21.29 o -4 19 1 608.97 661.59 19.14 o -2 19 1 110.03 96.72 7.23 o 0 19 1 0.08 6.18 3.00 o 2 19 1 3.73 7.99 4.06 o 4 19 1 2866.85 2978.65 64.90 o 6 19 1 0.90 3.20 3.47 o 8 19 1 2012.61 1961.43 30.25 o 10 19 1 684.45 727.05 12.32 o 12 19 1 297.46 269.26 7.38 o 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724.74 704.26 11.89 o 4 21 1 1029.63 1075.08 21.69 o 6 21 1 971.18 1027.90 12.60 o 8 21 1 68.44 63.99 3.80 o 10 21 1 2702.12 2665.46 55.91 o 12 21 1 171.49 192.18 6.82 o 14 21 1 446.71 458.89 20.74 o 16 21 1 214.60 215.82 5.59 o 18 21 1 546.28 506.37 8.37 o 20 21 1 101.18 106.28 3.70 o -21 22 1 0.05 0.92 1.07 o -19 22 1 270.56 271.68 6.46 o -17 22 1 1101.57 1061.69 12.55 o -15 22 1 930.37 949.65 10.49 o -13 22 1 408.00 383.79 12.93 o -11 22 1 69.62 49.03 3.56 o -9 22 1 48.09 44.25 2.45 o -7 22 1 15.01 26.09 2.06 o -5 22 1 358.91 395.19 5.91 o -3 22 1 160.80 190.66 4.43 o -1 22 1 834.93 841.74 9.53 o 1 22 1 197.43 163.04 4.79 o 3 22 1 4163.79 4187.75 35.67 o 5 22 1 262.65 265.38 7.91 o 7 22 1 7.34 7.56 1.86 o 9 22 1 2126.60 2142.45 30.58 o 11 22 1 88.12 102.61 5.22 o 13 22 1 712.32 692.71 13.22 o 15 22 1 0.34 2.41 1.44 o 17 22 1 219.30 232.27 5.61 o 19 22 1 123.08 128.06 3.94 o 21 22 1 1.22 3.90 1.41 o -22 23 1 50.43 80.17 4.98 o -20 23 1 103.04 88.81 3.03 o -18 23 1 3.86 2.90 1.40 o 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