#------------------------------------------------------------------------------ #$Date: 2020-11-24 07:13:08 +0200 (Tue, 24 Nov 2020) $ #$Revision: 259228 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108730.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108730 _cod_data_source_file dk5102293Ksup10.hkl _cod_data_source_block 293K loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 1 46453.80 67201.40 244.37 o 0 0 2 62692.60 83870.20 288.09 o 0 2 2 41374.50 47896.20 139.04 o 2 2 2 65814.30 75928.60 291.46 o 1 1 3 66027.50 73177.70 136.07 o 1 3 3 42808.00 44325.50 98.80 o 3 3 3 12007.50 13196.50 72.33 o 0 0 4 47869.90 51623.00 208.65 o 0 2 4 33514.90 32777.60 74.17 o 2 2 4 47880.90 47925.70 105.55 o 0 4 4 27150.00 26109.90 93.99 o 2 4 4 37560.10 37005.90 90.59 o 4 4 4 30465.30 29713.00 171.00 o 1 1 5 28800.20 28252.80 64.52 o 1 3 5 39301.30 36763.20 62.64 o 3 3 5 29219.10 28008.80 78.57 o 1 5 5 19249.30 18383.20 65.81 o 3 5 5 28435.60 27615.60 69.91 o 5 5 5 14037.70 13878.20 77.75 o 0 0 6 63825.50 60980.80 242.88 o 0 2 6 28901.30 26847.50 68.11 o 2 2 6 21947.30 21518.30 64.22 o 0 4 6 25594.90 23728.70 72.14 o 2 4 6 18867.10 18432.40 37.97 o 4 4 6 16416.30 16217.00 46.43 o 0 6 6 40115.90 35581.10 105.47 o 2 6 6 18158.00 17250.60 47.87 o 4 6 6 16871.70 16560.90 47.64 o 6 6 6 27938.00 27176.60 116.09 o 1 1 7 20892.60 20076.20 64.40 o 1 3 7 27437.60 24928.80 49.72 o 3 3 7 19266.70 18598.20 50.97 o 1 5 7 15004.50 14526.90 31.35 o 3 5 7 21049.20 20286.60 39.02 o 5 5 7 11374.80 11520.00 39.76 o 1 7 7 12613.20 12316.30 41.95 o 3 7 7 16477.60 16014.90 50.63 o 5 7 7 9764.82 9862.55 38.43 o 7 7 7 8763.29 8877.89 68.21 o 0 0 8 20099.00 18978.60 139.38 o 0 2 8 15678.10 14900.80 50.12 o 2 2 8 24831.80 22782.40 62.04 o 0 4 8 14000.10 13482.00 43.04 o 2 4 8 21522.20 20240.50 40.93 o 4 4 8 18706.80 18176.20 56.85 o 0 6 8 13661.10 13348.90 48.27 o 2 6 8 10810.30 10696.90 28.95 o 4 6 8 9932.58 10076.40 28.62 o 6 6 8 9947.51 10086.20 41.00 o 0 8 8 8565.44 8547.73 54.81 o 2 8 8 14207.00 14029.30 55.33 o 4 8 8 12750.30 12729.80 51.07 o 6 8 8 6546.54 6806.51 35.22 o 8 8 8 9094.98 9102.91 56.70 o 1 1 9 21010.30 19627.00 60.07 o 1 3 9 15819.10 15087.80 34.81 o 3 3 9 4709.48 4903.05 27.36 o 1 5 9 16814.30 16072.50 39.00 o 3 5 9 13254.00 12989.00 34.91 o 5 5 9 13844.70 13671.50 55.98 o 1 7 9 13314.70 13047.50 35.77 o 3 7 9 9749.68 9764.86 30.97 o 5 7 9 11054.50 11045.90 33.61 o 7 7 9 9152.57 9119.21 32.83 o 1 9 9 8634.41 8624.35 44.32 o 3 9 9 2867.09 2929.53 28.93 o 5 9 9 7648.62 7672.37 29.96 o 7 9 9 5926.39 6066.05 27.27 o 9 9 9 2099.30 2154.08 28.94 o 0 0 10 15953.70 15464.10 105.74 o 0 2 10 11304.70 10968.30 47.45 o 2 2 10 16332.70 15648.90 59.69 o 0 4 10 10181.20 10122.40 42.39 o 2 4 10 14222.40 13727.10 36.36 o 4 4 10 12375.60 12120.00 55.21 o 0 6 10 11615.60 11352.20 48.99 o 2 6 10 8371.62 8323.30 29.18 o 4 6 10 7670.00 7790.11 29.52 o 6 6 10 8816.09 8677.17 41.29 o 0 8 10 6955.09 6906.54 36.90 o 2 8 10 10259.30 10220.00 37.66 o 4 8 10 9175.95 9179.08 23.14 o 6 8 10 5512.88 5602.93 18.25 o 8 8 10 6997.05 7102.08 27.90 o 0 10 10 5538.55 5630.29 37.37 o 2 10 10 7332.07 7436.57 29.95 o 4 10 10 6525.83 6674.72 28.63 o 6 10 10 4522.08 4670.40 24.66 o 8 10 10 5303.83 5470.08 24.62 o 10 10 10 3958.13 4285.09 36.81 o 1 1 11 8994.58 8957.65 44.21 o 1 3 11 13839.60 13289.30 40.36 o 3 3 11 11137.80 10795.10 50.45 o 1 5 11 7301.23 7265.34 28.82 o 3 5 11 11630.00 11283.20 37.84 o 5 5 11 6082.11 6174.85 44.76 o 1 7 11 6392.54 6459.93 30.95 o 3 7 11 9369.82 9371.49 24.65 o 5 7 11 5344.03 5448.28 17.88 o 7 7 11 4861.98 4993.95 23.48 o 1 9 11 8065.89 8007.94 23.51 o 3 9 11 6729.92 6807.74 19.86 o 5 9 11 7049.66 7142.40 21.40 o 7 9 11 5888.34 6062.59 18.40 o 9 9 11 4502.80 4714.95 21.77 o 1 11 11 3968.88 4075.60 22.46 o 3 11 11 6218.35 6421.03 26.59 o 5 11 11 3501.27 3599.27 20.52 o 7 11 11 3176.47 3287.25 17.97 o 9 11 11 4232.19 4462.28 22.18 o 11 11 11 2332.69 2371.66 22.27 o 0 0 12 20312.30 18393.20 185.74 o 0 2 12 9398.69 9175.16 49.20 o 2 2 12 7483.17 7504.65 44.10 o 0 4 12 9052.33 8872.29 53.43 o 2 4 12 6986.16 6934.22 29.90 o 4 4 12 6504.48 6495.00 33.20 o 0 6 12 15225.60 14680.70 48.33 o 2 6 12 7239.93 7232.29 22.39 o 4 6 12 7039.80 7040.32 23.24 o 6 6 12 11708.10 11668.30 38.55 o 0 8 12 5960.12 5980.53 27.64 o 2 8 12 4965.88 5073.15 17.25 o 4 8 12 4738.53 4839.22 18.01 o 6 8 12 4823.10 4956.61 16.77 o 8 8 12 3549.58 3713.55 18.62 o 0 10 12 5554.88 5662.49 26.81 o 2 10 12 4267.80 4406.75 16.24 o 4 10 12 4029.36 4140.27 15.80 o 6 10 12 4566.57 4703.25 15.49 o 8 10 12 3186.91 3316.04 14.46 o 10 10 12 2768.72 2880.09 16.61 o 0 12 12 7376.45 7680.52 39.48 o 2 12 12 3895.32 4078.58 21.38 o 4 12 12 3847.44 3960.36 21.31 o 6 12 12 6010.75 6271.56 29.48 o 8 12 12 2873.67 2930.73 16.44 o 10 12 12 2787.90 2768.75 12.65 o 1 1 13 7013.08 7012.48 54.42 o 1 3 13 9186.72 9044.50 27.83 o 3 3 13 6453.19 6470.79 30.05 o 1 5 13 5761.78 5816.03 21.59 o 3 5 13 7800.42 7749.30 24.53 o 5 5 13 4831.08 4909.72 27.10 o 1 7 13 5383.71 5421.88 20.38 o 3 7 13 6698.06 6779.60 21.99 o 5 7 13 4515.52 4597.50 17.46 o 7 7 13 4320.92 4473.16 22.17 o 1 9 13 5768.21 5928.90 19.45 o 3 9 13 4258.90 4389.88 16.88 o 5 9 13 5056.58 5233.84 17.24 o 7 9 13 4456.53 4600.47 15.03 o 9 9 13 3045.59 3160.09 18.00 o 1 11 13 3351.87 3489.80 13.66 o 3 11 13 4493.74 4673.10 16.34 o 5 11 13 2944.40 3045.49 13.76 o 7 11 13 2796.45 2848.76 12.27 o 9 11 13 3197.85 3256.68 10.80 o 1 13 13 3074.34 3133.27 20.14 o 3 13 13 3570.71 3670.74 21.59 o 5 13 13 2683.72 2668.62 14.44 o 7 13 13 2627.14 2543.64 11.73 o 0 0 14 6338.61 6326.50 66.65 o 0 2 14 5205.14 5273.86 31.89 o 2 2 14 8318.93 8256.68 38.63 o 0 4 14 4969.79 5023.37 31.05 o 2 4 14 7615.09 7580.23 25.36 o 4 4 14 6957.39 6913.51 33.19 o 0 6 14 5083.10 5164.89 27.10 o 2 6 14 4251.71 4394.99 18.36 o 4 6 14 4089.47 4160.02 17.02 o 6 6 14 4175.21 4318.45 23.32 o 0 8 14 3675.58 3762.71 22.32 o 2 8 14 5821.47 5990.42 19.74 o 4 8 14 5417.04 5566.60 18.48 o 6 8 14 3115.59 3202.01 13.07 o 8 8 14 4273.52 4498.23 20.94 o 0 10 14 3311.19 3406.87 18.81 o 2 10 14 4667.16 4865.49 16.65 o 4 10 14 4316.23 4476.93 17.63 o 6 10 14 2842.54 2908.47 12.82 o 8 10 14 3557.10 3625.04 12.73 o 10 10 14 2905.49 2891.71 15.97 o 0 12 14 2975.48 3062.59 20.82 o 2 12 14 2614.68 2657.18 12.18 o 4 12 14 2547.05 2560.85 10.64 o 6 12 14 2565.03 2529.91 9.74 o 8 12 14 2057.98 2000.27 9.99 o 0 14 14 2109.87 2064.43 18.87 o 2 14 14 3088.60 3094.40 17.58 o 4 14 14 2931.38 3038.77 24.15 o 1 1 15 6696.36 6650.45 36.66 o 1 3 15 5446.54 5503.54 22.90 o 3 3 15 2099.67 2135.02 19.41 o 1 5 15 5879.10 5972.63 22.38 o 3 5 15 4977.05 5060.66 19.34 o 5 5 15 5225.37 5343.09 27.32 o 1 7 15 5032.07 5145.40 18.10 o 3 7 15 4009.49 4095.35 15.46 o 5 7 15 4472.06 4586.52 16.76 o 7 7 15 3927.88 4075.13 23.31 o 1 9 15 3756.53 3890.27 16.80 o 3 9 15 1678.07 1703.76 10.66 o 5 9 15 3499.27 3597.16 14.36 o 7 9 15 2903.23 2925.83 11.78 o 9 9 15 1396.15 1303.48 11.22 o 1 11 15 3642.62 3714.09 15.57 o 3 11 15 3228.08 3290.39 13.07 o 5 11 15 3326.51 3367.72 11.37 o 7 11 15 2908.71 2872.97 10.52 o 1 13 15 2851.12 2820.30 11.61 o 3 13 15 2296.28 2240.13 11.01 o 0 0 16 5498.69 5496.44 67.23 o 0 2 16 3997.47 4043.69 26.58 o 2 2 16 5328.51 5382.07 28.89 o 0 4 16 3758.44 3811.18 24.78 o 2 4 16 4840.46 4925.96 19.61 o 4 4 16 4388.12 4516.31 26.01 o 0 6 16 4533.69 4654.64 25.41 o 2 6 16 3379.40 3447.96 14.12 o 4 6 16 3196.99 3285.95 16.02 o 6 6 16 3801.54 3896.08 22.36 o 0 8 16 3033.83 3117.46 21.85 o 2 8 16 4022.43 4171.61 16.62 o 4 8 16 3710.49 3814.57 15.56 o 6 8 16 2626.18 2599.87 11.17 o 8 8 16 3132.87 3045.44 15.15 o 0 10 16 2603.01 2612.62 17.26 o 2 10 16 3148.50 3163.54 12.93 o 4 10 16 2887.21 2891.73 11.07 o 6 10 16 2280.92 2187.82 9.44 o 0 12 16 2776.98 2730.57 18.10 o 2 12 16 2211.63 2111.66 12.79 o 1 1 17 3198.56 3198.15 23.54 o 1 3 17 4676.46 4708.68 19.51 o 3 3 17 4015.83 4140.85 31.37 o 1 5 17 2849.84 2885.09 15.42 o 3 5 17 4223.27 4337.26 19.28 o 5 5 17 2568.93 2572.94 20.85 o 1 7 17 2646.26 2643.93 13.70 o 3 7 17 3640.07 3686.33 15.38 o 5 7 17 2375.34 2308.38 10.98 o 7 7 17 2242.08 2076.48 12.26 o 1 9 17 3320.53 3306.47 13.76 o 3 9 17 2932.47 2872.94 11.72 o 5 9 17 3045.00 2917.96 12.91 o 0 0 18 6010.12 5978.91 73.17 o 0 2 18 3287.98 3298.32 23.96 o 2 2 18 2851.84 2834.25 23.99 o 0 4 18 3255.12 3202.95 22.53 o 2 4 18 2755.55 2698.43 13.92 o 4 4 18 2651.81 2610.20 18.83 o 0 6 18 4969.28 4989.91 26.64 o 2 6 18 2819.46 2706.95 13.30 o 4 6 18 2795.68 2659.12 11.85 o 6 6 18 4157.19 4003.55 19.10 o 0 8 18 2482.58 2277.85 15.98 o 2 8 18 2230.72 2102.47 10.99 o 4 8 18 2173.11 2008.19 12.31 o 1 1 19 2672.84 2579.99 20.24 o 1 3 19 3190.81 3029.62 12.90 o 3 3 19 2385.26 2188.23 15.18 o 1 5 19 2362.43 2142.80 9.27 o 3 5 19 2875.52 2714.66 11.85 o 0 0 20 2354.16 2150.57 43.52 o 0 2 20 2066.80 1832.03 17.56 o 2 2 20 2916.69 2667.16 33.66 o loop_ _twin_refln_datum_id _twin_refln_individual_id _twin_refln_index_h _twin_refln_index_k _twin_refln_index_l _twin_refln_F_squared_calc _twin_refln_F_squared_meas _twin_refln_F_squared_sigma _twin_refln_include_status ? ? ? ? ? ? ? ? ?