#------------------------------------------------------------------------------ #$Date: 2021-01-26 07:40:26 +0200 (Tue, 26 Jan 2021) $ #$Revision: 261216 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108755.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108755 _cell_angle_alpha 90.000 _cell_angle_beta 111.589 _cell_angle_gamma 90.000 _cell_length_a 23.7449 _cell_length_b 5.0750 _cell_length_c 24.1740 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.9933 _cod_data_source_file ne5003NaOnPr_2HOnPrsup8.hkl _cod_data_source_block NaOnPr_2HOnPr _shelx_title ' MB12_0m_a.res in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.35 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25538.57 32455.95 2347.67 o 4 0 0 33.71 56.99 6.93 o 6 0 0 4978.48 6173.45 404.09 o 8 0 0 5934.06 6132.75 445.47 o 10 0 0 965.91 386.15 56.92 o 12 0 0 1769.50 1758.08 91.61 o 14 0 0 341.94 331.80 20.49 o 16 0 0 1.98 19.76 13.79 o 18 0 0 9.09 53.53 18.49 o 20 0 0 15.60 43.38 13.14 o 22 0 0 3.05 7.36 11.15 o 1 1 0 9.56 24.54 5.59 o 3 1 0 39258.86 42854.95 2173.84 o 5 1 0 18689.29 19693.77 896.47 o 7 1 0 3813.06 5072.50 196.49 o 9 1 0 183.30 174.34 16.97 o 11 1 0 499.68 361.74 11.34 o 13 1 0 76.21 91.01 6.63 o 15 1 0 109.12 60.43 8.70 o 17 1 0 3.79 11.09 10.50 o 19 1 0 5.72 22.06 11.94 o 21 1 0 0.00 1.86 9.64 o 0 2 0 2639.97 2823.38 207.27 o 2 2 0 162.54 122.23 18.43 o 4 2 0 1096.60 1075.96 47.76 o 6 2 0 40.19 71.83 5.93 o 8 2 0 755.38 781.13 22.92 o 10 2 0 1041.55 739.20 21.21 o 12 2 0 32.11 24.21 5.30 o 14 2 0 14.46 6.97 5.49 o 16 2 0 22.12 13.48 8.57 o 18 2 0 8.59 5.56 10.28 o 20 2 0 35.29 44.78 10.05 o 1 3 0 485.14 817.39 31.90 o 3 3 0 1087.76 1436.01 66.97 o 5 3 0 349.93 369.73 19.25 o 7 3 0 151.20 144.77 12.31 o 9 3 0 76.63 76.07 6.60 o 11 3 0 0.62 -3.47 6.10 o 13 3 0 79.21 65.31 7.69 o 15 3 0 113.26 127.69 9.16 o 17 3 0 16.70 9.70 8.49 o 2 4 0 0.02 14.69 14.96 o 4 4 0 28.64 15.19 7.04 o 6 4 0 4.37 10.56 6.10 o 8 4 0 12.34 19.54 6.94 o 10 4 0 0.01 -4.32 8.58 o 12 4 0 4.23 6.83 8.19 o -21 1 1 2.24 1.92 9.97 o -19 1 1 30.08 29.07 10.16 o -17 1 1 35.17 24.33 9.46 o -15 1 1 51.77 50.01 8.65 o -13 1 1 230.20 299.99 11.94 o -11 1 1 73.64 178.30 9.84 o -9 1 1 681.50 922.67 38.30 o -7 1 1 474.05 532.68 25.22 o -5 1 1 4116.64 3695.59 169.17 o -3 1 1 25.49 29.43 6.82 o -1 1 1 106.07 240.09 11.64 o 1 1 1 789.40 714.64 38.48 o 3 1 1 1205.40 1405.41 73.93 o 5 1 1 2312.16 2588.57 108.76 o 7 1 1 316.20 331.74 16.58 o 9 1 1 352.77 343.84 18.47 o 11 1 1 24.83 27.14 4.04 o 13 1 1 88.63 152.04 9.23 o 15 1 1 36.68 38.27 6.84 o 17 1 1 0.87 11.03 8.85 o 19 1 1 0.79 -9.57 10.74 o 21 1 1 0.93 18.95 11.24 o -20 2 1 3.56 31.20 9.82 o -18 2 1 0.38 -5.36 9.15 o -16 2 1 2.02 -2.48 7.60 o -14 2 1 56.82 41.29 5.94 o -12 2 1 35.95 35.16 5.21 o -10 2 1 83.32 96.68 5.82 o -8 2 1 10.73 12.32 4.25 o -6 2 1 0.03 -5.06 5.06 o -4 2 1 73.26 41.52 4.85 o -2 2 1 397.36 439.34 28.59 o 0 2 1 51.07 102.89 11.29 o 2 2 1 419.93 385.73 39.57 o 4 2 1 493.69 478.11 23.30 o 6 2 1 543.04 517.67 18.09 o 8 2 1 179.95 213.36 9.21 o 10 2 1 16.63 39.80 4.87 o 12 2 1 17.70 5.44 5.04 o 14 2 1 5.66 9.92 6.57 o 16 2 1 6.80 8.91 8.28 o 18 2 1 0.00 1.91 9.64 o -17 3 1 10.13 16.87 9.13 o -15 3 1 26.07 54.12 7.53 o -13 3 1 8.23 4.63 6.88 o -11 3 1 1.41 -4.08 5.94 o -9 3 1 1.63 22.58 6.22 o -7 3 1 79.33 70.72 5.54 o -5 3 1 114.47 92.40 6.87 o -3 3 1 79.62 86.68 6.15 o -1 3 1 133.95 104.54 7.76 o 1 3 1 417.85 615.51 39.90 o 3 3 1 400.04 559.19 27.91 o 5 3 1 440.72 442.22 19.47 o 7 3 1 105.35 128.24 8.70 o 9 3 1 14.25 1.23 5.47 o 11 3 1 64.80 65.14 7.50 o 13 3 1 109.44 153.65 9.73 o 15 3 1 99.92 103.76 9.69 o 17 3 1 19.60 -6.41 6.41 o -14 4 1 0.33 -7.84 20.98 o -12 4 1 7.45 -7.45 9.47 o -10 4 1 19.42 9.93 7.97 o -8 4 1 13.83 16.13 7.22 o -6 4 1 6.25 4.39 6.10 o -4 4 1 8.66 17.58 9.51 o 0 4 1 0.67 9.75 16.80 o 2 4 1 23.20 20.60 14.17 o 4 4 1 3.14 1.70 6.83 o 6 4 1 20.27 27.92 6.82 o 8 4 1 102.49 72.46 8.19 o 10 4 1 92.45 74.75 11.98 o 12 4 1 22.55 0.23 8.21 o -22 0 2 6.77 15.26 23.47 o -20 0 2 7.10 8.04 12.22 o -18 0 2 0.01 1.99 9.60 o -16 0 2 303.46 334.75 33.12 o -14 0 2 3353.69 3465.56 178.32 o -12 0 2 1514.43 1536.97 80.38 o -10 0 2 10.26 3.79 15.62 o -8 0 2 694.39 731.84 46.28 o -6 0 2 21603.13 27272.84 1970.05 o -4 0 2 1861.61 1537.75 91.71 o -2 0 2 37474.33 43526.30 3145.24 o 0 0 2 12185.59 10968.52 645.79 o 4 0 2 4827.84 4721.03 354.48 o 6 0 2 0.67 -3.60 7.07 o 8 0 2 6.30 13.58 14.08 o 10 0 2 1733.63 1447.61 87.85 o 12 0 2 556.14 447.15 25.94 o 14 0 2 92.16 51.39 11.82 o 16 0 2 159.43 282.54 26.57 o 18 0 2 15.44 6.96 13.50 o 20 0 2 1.60 28.84 11.18 o -21 1 2 17.83 24.67 9.01 o -19 1 2 13.73 28.18 10.03 o -17 1 2 14.32 28.87 9.67 o -15 1 2 46.55 17.16 8.51 o -13 1 2 3.36 3.13 4.76 o -11 1 2 866.48 861.31 25.76 o -9 1 2 4337.00 4191.25 163.15 o -7 1 2 7118.34 6346.54 244.46 o -5 1 2 291.87 351.96 21.52 o -3 1 2 14786.13 17129.96 873.97 o -1 1 2 3994.97 4293.33 227.84 o 1 1 2 876.86 726.94 39.11 o 3 1 2 3784.57 3894.56 200.11 o 5 1 2 394.11 398.56 18.59 o 7 1 2 365.01 274.91 16.45 o 9 1 2 13.15 35.79 6.94 o 11 1 2 0.04 -3.70 3.70 o 13 1 2 162.72 138.91 8.36 o 15 1 2 5.67 5.40 6.26 o 17 1 2 13.55 57.90 9.12 o 19 1 2 6.46 31.17 29.64 o -20 2 2 9.93 24.15 9.09 o -18 2 2 2.83 -0.89 8.13 o -16 2 2 0.03 1.04 6.35 o -14 2 2 3.33 5.06 5.70 o -12 2 2 99.16 70.11 5.96 o -10 2 2 279.27 344.06 11.26 o -8 2 2 95.28 85.36 5.08 o -6 2 2 1518.19 1891.01 81.00 o -4 2 2 2871.83 2892.75 150.57 o -2 2 2 62.00 51.84 10.32 o 0 2 2 231.48 330.17 21.83 o 2 2 2 430.24 597.79 33.29 o 4 2 2 2306.34 2262.47 105.61 o 6 2 2 5205.45 4677.79 144.53 o 8 2 2 2198.25 2067.78 64.88 o 10 2 2 221.32 206.52 8.85 o 12 2 2 8.80 2.48 5.47 o 14 2 2 4.89 -2.30 6.48 o 16 2 2 2.72 13.12 9.44 o 18 2 2 42.56 62.32 15.76 o -17 3 2 28.60 32.52 7.81 o -15 3 2 43.15 34.55 6.98 o -13 3 2 8.93 -6.30 6.42 o -11 3 2 102.70 156.75 8.26 o -9 3 2 157.98 160.93 7.68 o -7 3 2 70.79 112.73 6.44 o -5 3 2 166.00 163.69 7.94 o -3 3 2 20.75 5.92 4.62 o -1 3 2 1840.45 2728.18 114.99 o 1 3 2 3396.99 3880.08 172.30 o 3 3 2 920.57 964.62 37.18 o 5 3 2 32.94 36.62 5.65 o 7 3 2 20.26 11.93 7.70 o 9 3 2 117.88 75.41 6.88 o 11 3 2 165.26 216.74 14.85 o 13 3 2 195.36 184.89 10.38 o 15 3 2 39.20 36.71 7.58 o 17 3 2 1.85 -4.00 8.05 o -14 4 2 16.76 12.11 7.43 o -12 4 2 6.27 -6.42 8.04 o -10 4 2 2.00 0.08 7.33 o -8 4 2 14.36 10.03 7.03 o -6 4 2 40.11 55.52 10.95 o -4 4 2 13.60 35.12 10.98 o -2 4 2 48.54 140.26 29.93 o 0 4 2 138.92 198.64 34.04 o 2 4 2 42.44 45.41 10.82 o 4 4 2 36.49 38.14 8.17 o 6 4 2 65.74 53.67 7.20 o 8 4 2 2.67 10.16 6.96 o 10 4 2 24.42 23.18 9.03 o 12 4 2 15.81 -4.90 7.98 o -21 1 3 26.23 27.29 9.20 o -19 1 3 69.19 113.01 13.12 o -17 1 3 16.22 11.39 8.92 o -15 1 3 1.76 0.09 7.00 o -13 1 3 0.28 7.85 5.89 o -11 1 3 473.33 371.13 21.64 o -9 1 3 2139.81 1859.05 73.56 o -7 1 3 4204.06 3983.21 157.25 o -5 1 3 1900.20 2408.87 124.41 o -3 1 3 12635.98 12710.72 577.80 o -1 1 3 739.39 742.87 32.67 o 1 1 3 9.61 -4.32 4.32 o 3 1 3 3440.53 4094.25 210.38 o 5 1 3 2542.36 2193.30 92.51 o 7 1 3 1243.90 1055.26 46.43 o 9 1 3 0.36 -3.98 3.98 o 11 1 3 92.85 160.29 7.44 o 13 1 3 75.51 66.29 6.74 o 15 1 3 81.43 142.16 12.96 o 17 1 3 1.16 -3.74 7.99 o 19 1 3 0.69 22.04 11.70 o -20 2 3 5.10 6.30 8.85 o -18 2 3 29.25 8.03 8.57 o -16 2 3 116.13 142.29 8.77 o -14 2 3 59.86 61.32 6.28 o -12 2 3 155.16 129.98 6.83 o -10 2 3 314.45 394.55 15.22 o -8 2 3 149.54 142.31 6.19 o -6 2 3 491.28 411.51 19.95 o -4 2 3 75.13 106.54 9.38 o -2 2 3 1048.89 1484.01 64.07 o 0 2 3 3341.86 3552.77 163.59 o 2 2 3 1382.21 1877.71 88.29 o 4 2 3 1706.28 2008.87 94.70 o 6 2 3 124.26 125.45 6.56 o 8 2 3 16.06 22.85 4.32 o 10 2 3 26.51 32.15 5.36 o 12 2 3 109.99 139.34 7.92 o 14 2 3 0.46 1.66 6.92 o 16 2 3 0.87 6.83 9.90 o 18 2 3 0.02 -3.52 17.71 o -17 3 3 8.90 8.45 7.09 o -15 3 3 0.38 2.36 6.65 o -13 3 3 0.30 -5.00 6.27 o -11 3 3 15.76 38.60 5.77 o -9 3 3 56.34 65.84 6.48 o -7 3 3 37.43 63.86 5.30 o -5 3 3 6.32 3.24 3.67 o -3 3 3 391.33 436.05 17.19 o -1 3 3 1736.25 2842.56 127.60 o 1 3 3 1688.60 1887.60 69.84 o 3 3 3 268.88 392.11 20.67 o 5 3 3 77.38 30.62 5.65 o 7 3 3 9.32 27.11 6.08 o 9 3 3 170.92 154.32 9.29 o 11 3 3 129.14 127.45 8.75 o 13 3 3 112.60 102.80 8.70 o 15 3 3 21.78 10.00 7.04 o -14 4 3 1.89 2.97 7.64 o -12 4 3 8.59 3.75 8.01 o -10 4 3 7.05 -0.64 6.47 o -8 4 3 0.31 -0.31 6.43 o -6 4 3 40.61 58.80 8.57 o -4 4 3 167.92 301.70 43.86 o -2 4 3 170.96 256.90 18.17 o 0 4 3 62.63 90.02 11.52 o 2 4 3 0.36 1.06 9.12 o 4 4 3 132.54 144.03 11.93 o 6 4 3 203.71 205.16 14.47 o 8 4 3 212.77 163.13 13.95 o 10 4 3 66.56 37.00 9.21 o 12 4 3 2.29 -0.01 7.85 o -22 0 4 1.16 3.71 16.43 o -20 0 4 3.58 -1.24 14.00 o -18 0 4 186.27 272.76 27.06 o -16 0 4 866.83 523.98 33.85 o -14 0 4 1835.57 1774.18 92.63 o -12 0 4 0.56 7.38 6.96 o -10 0 4 1127.99 1478.28 157.28 o -8 0 4 28.95 13.66 9.81 o -6 0 4 259.19 185.74 24.97 o -4 0 4 1857.05 2688.53 206.86 o -2 0 4 218.71 185.55 15.04 o 0 0 4 5150.03 4789.73 346.29 o 2 0 4 12595.57 15729.33 925.88 o 4 0 4 346.30 422.70 24.04 o 6 0 4 435.86 361.95 26.13 o 8 0 4 67.94 150.23 28.76 o 10 0 4 345.29 362.88 21.69 o 12 0 4 536.01 577.22 32.24 o 14 0 4 796.36 825.06 51.93 o 16 0 4 78.26 59.07 13.23 o 18 0 4 3.04 18.00 24.65 o 20 0 4 3.57 18.78 12.32 o -21 1 4 44.53 65.17 10.61 o -19 1 4 5.39 26.28 10.54 o -17 1 4 16.81 29.15 7.91 o -15 1 4 2.27 20.23 5.69 o -13 1 4 0.30 -1.21 4.42 o -11 1 4 1025.06 888.31 27.32 o -9 1 4 601.58 683.48 29.96 o -7 1 4 124.60 124.29 10.34 o -5 1 4 976.21 813.23 39.27 o -3 1 4 262.95 304.49 18.71 o -1 1 4 45093.00 53409.15 2431.73 o 1 1 4 350.79 388.93 25.81 o 3 1 4 1781.38 1444.27 56.55 o 5 1 4 52.18 54.08 7.00 o 7 1 4 691.49 569.54 27.35 o 9 1 4 571.30 437.90 13.63 o 11 1 4 135.58 127.07 7.50 o 13 1 4 56.52 68.57 9.35 o 15 1 4 3.34 5.18 7.28 o 17 1 4 3.37 2.20 8.42 o 19 1 4 33.24 55.76 9.39 o -20 2 4 0.05 12.22 9.24 o -18 2 4 1.57 3.87 8.75 o -16 2 4 5.81 44.54 9.30 o -14 2 4 47.44 77.09 6.49 o -12 2 4 174.89 213.04 8.55 o -10 2 4 9.42 33.89 5.77 o -8 2 4 1915.58 1922.04 51.70 o -6 2 4 6282.15 6662.57 277.87 o -4 2 4 1799.80 1947.88 76.41 o -2 2 4 74.76 289.39 15.63 o 0 2 4 2.41 3.42 6.43 o 2 2 4 1050.65 1038.26 56.12 o 4 2 4 3995.19 4166.15 135.43 o 6 2 4 2539.62 2391.82 68.56 o 8 2 4 520.82 463.47 14.68 o 10 2 4 0.56 2.93 4.09 o 12 2 4 9.76 1.83 5.29 o 14 2 4 1.61 2.63 6.53 o 16 2 4 20.67 43.34 10.61 o 18 2 4 17.63 12.80 22.71 o -19 3 4 5.17 -1.17 17.02 o -17 3 4 21.79 -7.01 7.01 o -15 3 4 1.78 -6.58 6.58 o -13 3 4 97.19 112.95 8.07 o -11 3 4 139.28 161.56 8.66 o -9 3 4 38.63 28.02 4.74 o -7 3 4 0.08 3.80 4.18 o -5 3 4 77.38 97.26 5.82 o -3 3 4 1435.12 2212.59 86.02 o -1 3 4 2953.63 4149.56 172.14 o 1 3 4 560.37 643.78 25.43 o 3 3 4 19.16 13.05 5.00 o 5 3 4 27.12 32.99 6.02 o 7 3 4 41.73 37.35 6.78 o 9 3 4 91.74 140.68 9.38 o 11 3 4 162.11 177.22 11.64 o 13 3 4 48.93 53.70 7.33 o 15 3 4 0.98 0.53 6.51 o -14 4 4 17.04 18.06 7.58 o -12 4 4 3.90 -7.46 9.26 o -10 4 4 2.04 -6.16 7.67 o -8 4 4 23.74 26.10 6.16 o -6 4 4 0.44 2.89 8.87 o -4 4 4 156.41 225.84 27.36 o -2 4 4 213.86 347.78 22.65 o 0 4 4 79.13 67.41 11.11 o 2 4 4 22.02 12.80 10.25 o 4 4 4 0.31 28.36 8.16 o 6 4 4 11.03 24.60 8.27 o 8 4 4 34.60 27.90 8.91 o 10 4 4 33.16 9.76 8.56 o -21 1 5 3.33 38.46 9.78 o -19 1 5 18.92 33.16 8.62 o -17 1 5 8.96 37.67 7.93 o -15 1 5 32.54 63.70 6.95 o -13 1 5 239.74 227.78 9.14 o -11 1 5 447.87 413.96 18.26 o -9 1 5 3727.23 3547.40 149.05 o -7 1 5 2573.72 2855.74 120.02 o -5 1 5 858.50 925.26 37.45 o -3 1 5 55.11 61.88 6.24 o -1 1 5 4731.55 5124.83 234.47 o 1 1 5 14342.35 11611.92 527.26 o 3 1 5 1483.00 1368.51 63.81 o 5 1 5 64.96 78.77 9.86 o 7 1 5 278.13 197.33 9.63 o 9 1 5 1132.27 944.21 27.88 o 11 1 5 402.09 414.87 19.60 o 13 1 5 99.31 85.31 10.07 o 15 1 5 39.08 31.21 8.94 o 17 1 5 0.56 4.90 8.26 o 19 1 5 10.50 89.17 35.68 o -20 2 5 2.71 -4.89 9.29 o -18 2 5 13.79 45.95 20.04 o -16 2 5 44.63 76.74 7.23 o -14 2 5 62.06 81.66 6.22 o -12 2 5 230.30 282.36 9.85 o -10 2 5 563.00 502.88 14.68 o -8 2 5 85.81 111.83 5.74 o -6 2 5 347.38 249.34 10.19 o -4 2 5 2302.41 2722.92 119.53 o -2 2 5 2750.51 3075.32 158.66 o 0 2 5 382.03 442.62 34.29 o 2 2 5 21.68 11.61 6.09 o 4 2 5 290.80 292.12 10.71 o 6 2 5 562.70 489.77 15.41 o 8 2 5 126.75 186.90 7.95 o 10 2 5 23.11 11.04 4.79 o 12 2 5 15.94 9.25 5.44 o 14 2 5 43.39 33.19 6.96 o 16 2 5 29.07 19.86 12.12 o -19 3 5 3.83 -7.63 7.63 o -17 3 5 0.28 -7.50 7.73 o -15 3 5 39.72 35.39 7.43 o -13 3 5 92.20 109.65 10.12 o -11 3 5 76.94 99.10 8.47 o -9 3 5 36.42 33.95 5.14 o -7 3 5 70.23 202.02 41.06 o -5 3 5 287.57 279.85 14.62 o -3 3 5 825.39 1052.46 59.80 o -1 3 5 1129.82 1281.34 61.39 o 1 3 5 374.40 399.77 18.52 o 3 3 5 40.61 42.98 4.90 o 5 3 5 3.19 -5.22 6.16 o 7 3 5 9.57 8.31 6.87 o 9 3 5 23.59 17.97 8.16 o 11 3 5 45.25 58.97 9.33 o 13 3 5 5.24 6.80 8.48 o 15 3 5 0.01 -0.38 7.46 o -14 4 5 5.05 -2.17 7.19 o -12 4 5 0.13 -6.40 10.88 o -10 4 5 45.67 36.70 8.01 o -8 4 5 142.84 135.88 16.36 o -6 4 5 283.26 288.65 27.88 o -4 4 5 258.39 413.83 26.07 o -2 4 5 97.48 176.01 15.47 o 0 4 5 0.13 -7.05 10.30 o 2 4 5 179.71 153.25 16.79 o 4 4 5 226.34 245.62 16.65 o 6 4 5 168.83 192.77 22.23 o 8 4 5 64.34 59.95 12.28 o 10 4 5 6.37 -7.94 7.94 o -22 0 6 10.94 36.12 13.52 o -20 0 6 32.36 19.10 14.93 o -18 0 6 389.05 366.47 67.49 o -16 0 6 701.05 608.13 48.05 o -14 0 6 293.23 329.48 24.48 o -12 0 6 513.99 690.88 44.06 o -10 0 6 0.11 1.38 11.68 o -8 0 6 1050.48 928.80 57.78 o -6 0 6 13.18 21.79 8.23 o -4 0 6 11522.92 11124.61 805.24 o -2 0 6 39243.25 33544.19 2426.51 o 0 0 6 9308.28 8703.31 513.08 o 2 0 6 635.37 572.87 31.17 o 4 0 6 684.78 734.65 57.05 o 6 0 6 155.18 230.79 39.32 o 8 0 6 49.10 51.01 8.33 o 10 0 6 288.46 354.82 30.33 o 12 0 6 654.02 528.20 41.47 o 14 0 6 223.97 265.08 40.79 o 16 0 6 1.05 -11.74 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