#------------------------------------------------------------------------------ #$Date: 2021-01-28 07:58:45 +0200 (Thu, 28 Jan 2021) $ #$Revision: 261293 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108767.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108767 _cell_angle_alpha 90.000 _cell_angle_beta 129.087 _cell_angle_gamma 90.000 _cell_length_a 21.2210 _cell_length_b 10.3080 _cell_length_c 19.4134 _exptl_crystal_F_000 1824.00 _reflns_d_resolution_high 0.7972 _cod_data_source_file ra5090cis-HNSsup2.hkl _cod_data_source_block cis-HNS _shelx_title ' 2201911581lyz_0m_a.res in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 219.48 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12051.18 11100.46 542.41 o 4 0 0 10889.15 11366.91 702.04 o 6 0 0 37176.68 36227.31 2390.24 o 8 0 0 3883.01 4276.70 560.19 o 10 0 0 1913.76 2308.31 234.73 o 12 0 0 361.85 339.71 34.83 o 14 0 0 92.56 90.09 23.22 o 16 0 0 210.22 226.21 43.81 o 18 0 0 316.00 293.29 52.51 o 20 0 0 423.10 514.81 69.50 o 1 1 0 206.64 142.91 5.39 o 3 1 0 22417.20 19419.14 189.65 o 7 1 0 2994.08 3397.42 157.88 o 9 1 0 5366.88 5590.74 307.33 o 11 1 0 3706.30 3946.16 177.18 o 13 1 0 0.84 -0.32 7.89 o 15 1 0 861.29 790.62 46.52 o 17 1 0 535.54 573.35 42.24 o 19 1 0 0.00 1.62 29.91 o 0 2 0 9961.65 8384.19 258.34 o 2 2 0 9703.08 8614.75 221.34 o 4 2 0 265.03 128.92 10.60 o 6 2 0 105.95 191.68 15.17 o 8 2 0 10764.71 11876.82 467.81 o 10 2 0 8812.74 9300.90 433.96 o 12 2 0 159.39 166.80 17.02 o 14 2 0 3076.91 3353.46 80.27 o 16 2 0 362.28 406.51 29.84 o 18 2 0 0.06 4.10 17.16 o 20 2 0 41.69 68.68 45.82 o 1 3 0 26248.87 22432.54 171.54 o 3 3 0 24512.83 22482.26 410.79 o 5 3 0 16689.33 16839.72 712.63 o 7 3 0 17.83 50.29 12.29 o 9 3 0 3538.45 4076.91 108.33 o 11 3 0 2096.03 2360.03 58.77 o 13 3 0 0.06 -5.62 8.95 o 15 3 0 3278.79 3102.71 92.18 o 17 3 0 651.48 632.87 53.17 o 19 3 0 144.29 149.10 39.21 o 0 4 0 3421.69 2969.04 74.40 o 2 4 0 9817.40 9096.37 142.57 o 4 4 0 1529.89 1684.24 52.90 o 6 4 0 12299.02 13353.01 594.96 o 8 4 0 849.39 971.57 33.91 o 10 4 0 1527.65 1392.54 43.10 o 12 4 0 652.96 777.42 60.35 o 14 4 0 94.91 115.18 21.97 o 16 4 0 171.56 226.01 30.18 o 18 4 0 14.13 28.27 96.00 o 1 5 0 1306.98 981.81 34.41 o 3 5 0 3038.20 3017.61 57.76 o 5 5 0 11163.11 12529.21 540.72 o 7 5 0 221.68 276.26 35.25 o 9 5 0 1738.12 1683.59 81.93 o 11 5 0 28.83 17.20 13.36 o 13 5 0 15.35 44.68 10.50 o 15 5 0 57.51 66.29 18.05 o 17 5 0 610.25 501.05 69.47 o 19 5 0 59.89 102.27 62.97 o 0 6 0 251.76 281.71 40.44 o 2 6 0 419.68 344.62 31.63 o 4 6 0 11141.43 10784.08 404.12 o 6 6 0 2031.25 2263.61 141.26 o 8 6 0 8.22 6.91 8.15 o 10 6 0 11.67 24.99 7.30 o 12 6 0 12.25 18.25 10.55 o 14 6 0 1517.89 1293.57 56.76 o 16 6 0 502.27 393.38 43.73 o 18 6 0 6.05 -34.63 57.42 o 1 7 0 2751.80 2644.84 95.93 o 3 7 0 28.69 26.47 7.10 o 5 7 0 53.18 49.09 7.17 o 7 7 0 228.83 297.18 29.25 o 9 7 0 1964.16 2016.25 60.19 o 11 7 0 177.39 120.22 29.75 o 13 7 0 68.32 31.60 17.61 o 15 7 0 68.85 66.68 17.18 o 17 7 0 226.70 172.20 31.57 o 0 8 0 6.56 12.69 11.84 o 2 8 0 162.97 243.29 26.30 o 4 8 0 794.78 835.95 56.39 o 6 8 0 412.69 402.45 31.55 o 8 8 0 470.82 490.85 32.13 o 10 8 0 91.03 128.39 21.87 o 12 8 0 29.22 19.82 17.64 o 14 8 0 449.36 401.69 51.56 o 16 8 0 38.86 116.90 42.59 o 1 9 0 335.35 394.72 28.01 o 3 9 0 3.49 -4.18 6.74 o 5 9 0 20.63 49.22 14.64 o 7 9 0 164.65 167.30 25.82 o 9 9 0 1492.38 1446.58 59.06 o 11 9 0 45.78 -17.84 17.84 o 13 9 0 154.74 117.33 26.39 o 0 10 0 410.81 363.76 38.29 o 2 10 0 50.39 20.22 9.96 o 4 10 0 150.39 112.19 21.63 o 6 10 0 21.79 -1.15 16.01 o 8 10 0 57.50 -16.07 16.07 o 10 10 0 837.63 821.29 52.16 o 12 10 0 97.79 81.31 28.08 o 1 11 0 126.16 119.34 22.68 o 3 11 0 125.23 96.03 18.79 o 5 11 0 1477.18 1374.88 74.28 o 7 11 0 48.33 25.00 20.38 o 9 11 0 504.81 451.05 45.53 o 0 12 0 200.57 209.33 66.49 o 2 12 0 16.15 -12.80 12.80 o 4 12 0 919.58 980.30 86.91 o 6 12 0 294.44 245.65 45.29 o -21 1 1 724.68 628.53 33.93 o -19 1 1 320.43 297.89 33.27 o -17 1 1 1313.19 1376.25 53.67 o -15 1 1 67.41 75.77 16.38 o -13 1 1 370.12 402.76 34.90 o -11 1 1 7379.29 8091.35 265.30 o -9 1 1 5471.31 5846.75 251.50 o -7 1 1 31708.11 33236.17 1385.49 o -3 1 1 2260.26 2364.28 103.22 o -1 1 1 48.27 29.79 3.88 o 1 1 1 560.39 548.68 16.39 o 3 1 1 850.40 891.13 47.23 o 5 1 1 16999.10 16318.43 787.36 o 7 1 1 7174.35 8142.17 423.82 o 9 1 1 4208.87 4702.23 219.02 o 11 1 1 716.13 763.87 32.57 o 13 1 1 3.80 31.51 19.60 o 15 1 1 2317.57 2305.93 87.32 o 17 1 1 20.24 26.49 18.77 o 19 1 1 49.08 57.87 33.94 o -20 2 1 111.31 67.14 30.82 o -18 2 1 1189.41 1218.48 115.97 o -16 2 1 4604.73 4451.53 74.71 o -14 2 1 4736.50 4948.59 177.67 o -12 2 1 10276.36 11422.16 432.33 o -10 2 1 1619.18 1823.95 62.08 o -8 2 1 2933.36 2996.77 125.49 o -6 2 1 23817.98 24919.89 1095.52 o -4 2 1 9237.05 8865.23 343.99 o -2 2 1 1899.51 1758.43 73.62 o 0 2 1 3745.52 3778.81 243.49 o 4 2 1 2678.74 2641.28 89.07 o 6 2 1 1581.11 1503.79 63.19 o 8 2 1 3477.09 3396.02 104.71 o 10 2 1 572.30 722.89 30.79 o 12 2 1 2139.98 2182.80 90.97 o 14 2 1 965.19 969.43 38.54 o 16 2 1 340.85 370.76 41.67 o 18 2 1 18.30 45.47 19.54 o -19 3 1 523.22 369.73 59.50 o -17 3 1 643.54 598.18 62.80 o -15 3 1 7.90 5.19 14.46 o -13 3 1 1013.89 1072.35 60.18 o -11 3 1 1973.21 1928.24 111.06 o -9 3 1 7072.15 7209.91 343.77 o -7 3 1 2262.14 2701.34 161.81 o -5 3 1 11371.10 10960.17 420.29 o -3 3 1 48171.25 38063.97 363.33 o -1 3 1 1701.51 1704.89 112.34 o 1 3 1 21407.74 21885.06 1593.16 o 3 3 1 17159.37 16462.53 617.91 o 5 3 1 20333.57 20764.94 352.58 o 7 3 1 31.43 46.38 7.52 o 9 3 1 9107.20 9609.41 371.82 o 11 3 1 813.77 957.75 36.43 o 13 3 1 213.88 178.86 15.84 o 15 3 1 552.31 565.86 31.72 o 17 3 1 1287.65 1386.41 61.33 o 19 3 1 0.00 109.84 84.10 o -20 4 1 1156.99 1143.02 119.07 o -18 4 1 204.46 194.10 56.27 o -16 4 1 6.71 -9.23 12.65 o -14 4 1 143.42 56.57 22.67 o -12 4 1 56.41 94.33 10.08 o -10 4 1 6.62 6.63 5.42 o -8 4 1 1680.65 2012.65 91.21 o -6 4 1 420.50 425.45 28.92 o -4 4 1 661.68 582.03 30.96 o 0 4 1 71.21 49.14 7.36 o 2 4 1 2432.02 2370.35 115.31 o 4 4 1 14301.72 14710.72 500.06 o 6 4 1 376.41 488.26 20.18 o 8 4 1 1647.74 1772.18 75.45 o 10 4 1 356.59 352.14 20.49 o 12 4 1 1039.25 945.47 41.03 o 14 4 1 428.25 459.21 29.89 o 16 4 1 105.22 23.78 24.68 o 18 4 1 434.35 448.61 52.62 o -19 5 1 39.26 64.85 46.60 o -17 5 1 3868.94 3527.64 146.12 o -15 5 1 17.62 4.59 12.13 o -13 5 1 149.99 126.30 17.40 o -11 5 1 212.65 209.94 20.53 o -9 5 1 3.69 2.63 4.53 o -7 5 1 9169.97 11014.41 516.99 o -5 5 1 1123.66 1084.61 55.75 o -3 5 1 4726.27 4849.17 278.82 o -1 5 1 15678.26 16295.04 834.62 o 1 5 1 106.32 180.08 24.02 o 3 5 1 22741.88 22915.35 812.59 o 5 5 1 7.20 0.43 5.14 o 7 5 1 21.19 10.64 8.43 o 9 5 1 849.81 745.97 34.96 o 11 5 1 953.04 760.70 68.18 o 13 5 1 849.22 624.17 30.92 o 15 5 1 66.66 80.70 13.50 o 17 5 1 167.56 85.62 62.12 o -18 6 1 89.87 55.54 31.33 o -16 6 1 1367.94 1324.69 66.59 o -14 6 1 23.67 19.53 18.37 o -12 6 1 154.80 103.02 14.60 o -10 6 1 331.72 391.19 27.78 o -8 6 1 5506.45 6198.09 318.21 o -6 6 1 1234.94 1292.91 44.73 o -4 6 1 5936.10 5951.15 229.16 o -2 6 1 802.56 571.27 57.14 o 0 6 1 3479.67 4023.98 355.86 o 2 6 1 510.92 652.27 61.57 o 4 6 1 210.59 195.68 18.34 o 6 6 1 1662.44 1887.50 90.97 o 8 6 1 668.41 661.83 65.93 o 10 6 1 25.76 2.92 8.85 o 12 6 1 1404.98 1275.12 52.30 o 14 6 1 7.41 1.88 10.18 o 16 6 1 66.28 64.95 27.45 o -17 7 1 218.17 96.96 38.24 o -15 7 1 1204.13 1071.35 57.50 o -13 7 1 26.56 34.77 17.28 o -11 7 1 675.16 683.99 93.42 o -9 7 1 655.22 711.38 47.34 o -7 7 1 478.85 562.68 31.02 o -5 7 1 106.72 77.94 10.63 o -3 7 1 234.60 260.78 19.22 o -1 7 1 2628.41 2765.66 159.24 o 1 7 1 4270.03 4541.47 361.16 o 3 7 1 5449.31 5831.33 254.20 o 5 7 1 3530.77 3842.26 174.29 o 7 7 1 26.04 31.56 9.20 o 9 7 1 118.79 114.71 26.69 o 11 7 1 618.51 596.91 41.39 o 13 7 1 12.36 7.16 23.37 o 15 7 1 116.51 78.46 11.93 o -16 8 1 0.03 -10.27 46.99 o -14 8 1 1002.46 877.04 34.33 o -12 8 1 804.69 710.68 49.37 o -10 8 1 32.10 17.86 15.08 o -8 8 1 602.73 720.12 43.55 o -6 8 1 482.55 480.72 36.42 o -4 8 1 3842.74 3726.31 160.41 o -2 8 1 179.98 189.95 23.02 o 0 8 1 302.46 303.98 23.79 o 2 8 1 208.59 254.07 22.96 o 4 8 1 248.72 255.65 21.38 o 6 8 1 739.50 819.65 42.19 o 8 8 1 512.28 608.62 36.00 o 10 8 1 863.66 898.50 49.63 o 12 8 1 0.02 19.32 15.72 o 14 8 1 175.30 229.26 42.47 o -15 9 1 694.65 681.24 42.44 o -13 9 1 8.88 81.76 27.16 o -11 9 1 49.16 64.01 21.17 o -9 9 1 1228.03 1147.86 86.74 o -7 9 1 4.87 -1.95 9.91 o -5 9 1 186.57 170.66 24.97 o -3 9 1 776.16 765.99 51.80 o -1 9 1 1873.79 1920.72 135.17 o 1 9 1 29.29 17.24 11.41 o 3 9 1 9.52 3.88 7.56 o 5 9 1 634.09 553.20 32.53 o 7 9 1 1117.27 1040.37 45.92 o 9 9 1 37.99 32.11 14.43 o 11 9 1 279.33 187.05 31.02 o 13 9 1 49.08 49.03 28.45 o -12 10 1 308.43 176.31 59.00 o -10 10 1 62.66 77.00 19.66 o -8 10 1 277.50 299.50 35.01 o -6 10 1 256.65 299.04 16.13 o -4 10 1 249.33 215.71 20.31 o -2 10 1 534.29 584.18 32.10 o 0 10 1 0.71 -9.86 9.86 o 2 10 1 2265.20 2225.28 129.10 o 4 10 1 112.48 123.81 19.21 o 6 10 1 136.65 250.97 30.87 o 8 10 1 181.94 110.09 32.95 o 10 10 1 61.66 28.92 37.29 o 12 10 1 178.62 174.25 32.63 o -11 11 1 177.78 212.05 33.85 o -9 11 1 0.94 21.87 18.83 o -7 11 1 687.70 708.13 78.55 o -5 11 1 7.06 -7.12 20.24 o -3 11 1 5236.19 5743.83 359.73 o -1 11 1 314.89 496.93 40.85 o 1 11 1 4.00 10.17 11.38 o 3 11 1 1241.07 1337.62 75.73 o 5 11 1 1323.83 1172.22 72.18 o 7 11 1 181.19 165.14 30.00 o 9 11 1 382.51 410.08 46.60 o -8 12 1 309.61 292.43 46.36 o -6 12 1 1.24 -12.07 54.46 o -4 12 1 1.32 0.62 11.41 o -2 12 1 70.29 84.71 18.31 o 0 12 1 26.71 32.80 22.82 o 2 12 1 29.76 36.81 14.50 o 4 12 1 249.88 224.33 39.73 o 6 12 1 413.22 500.35 64.00 o -20 0 2 30.00 51.30 26.45 o -18 0 2 141.90 158.75 36.71 o -16 0 2 403.41 509.81 149.09 o -14 0 2 2765.34 2890.86 149.00 o -12 0 2 4262.99 4497.82 636.55 o -10 0 2 167.28 206.89 18.89 o -8 0 2 477.27 526.89 56.85 o -6 0 2 30047.85 32274.36 1444.28 o -2 0 2 2610.28 1951.77 106.41 o 0 0 2 136.14 100.56 6.94 o 4 0 2 3296.26 2853.24 93.06 o 6 0 2 4185.34 4461.44 395.40 o 8 0 2 11233.99 12505.37 696.23 o 10 0 2 206.06 282.45 29.35 o 12 0 2 5.75 21.24 25.39 o 14 0 2 999.08 1176.91 71.18 o 16 0 2 797.11 660.12 78.65 o 18 0 2 120.20 127.74 89.96 o -21 1 2 382.26 454.58 67.35 o -19 1 2 42.75 63.89 16.67 o -17 1 2 699.18 738.54 37.01 o -15 1 2 464.54 444.32 31.92 o -13 1 2 4182.26 4507.89 172.31 o -11 1 2 66.10 34.61 7.66 o -9 1 2 9666.78 11677.28 591.82 o -7 1 2 37098.69 40478.59 1317.64 o -3 1 2 14427.63 12608.74 364.70 o -1 1 2 3954.11 3368.78 71.68 o 1 1 2 11942.55 11223.42 354.89 o 3 1 2 906.48 984.12 40.25 o 5 1 2 20838.24 21049.68 1098.80 o 7 1 2 7640.11 8984.93 385.40 o 9 1 2 2541.40 3048.16 182.92 o 11 1 2 966.66 1099.41 77.47 o 13 1 2 658.78 653.51 40.31 o 15 1 2 432.44 342.26 33.80 o 17 1 2 9.67 3.88 51.25 o 19 1 2 0.00 -19.04 19.04 o -20 2 2 1100.58 774.17 88.22 o -18 2 2 2133.70 1970.25 93.63 o -16 2 2 730.74 759.74 49.54 o -14 2 2 428.20 424.48 34.80 o -12 2 2 7369.80 8080.58 461.39 o -10 2 2 2474.66 2810.35 159.37 o -8 2 2 3974.62 4206.95 152.91 o -6 2 2 144.25 153.60 7.55 o -4 2 2 1193.69 982.89 48.89 o -2 2 2 25762.69 22112.50 344.77 o 0 2 2 21620.94 19472.52 624.79 o 2 2 2 410.46 357.33 11.93 o 4 2 2 3645.89 3795.77 139.01 o 6 2 2 1174.65 1401.78 80.75 o 8 2 2 241.03 270.18 18.83 o 10 2 2 1742.02 1843.09 67.89 o 12 2 2 0.36 -7.05 13.70 o 14 2 2 425.76 475.50 34.28 o 16 2 2 700.39 687.75 45.76 o 18 2 2 25.34 8.44 18.74 o -21 3 2 63.95 34.15 41.86 o -19 3 2 537.55 440.70 49.95 o -17 3 2 0.00 15.36 17.67 o -15 3 2 2332.70 2316.42 80.76 o -13 3 2 1276.34 1373.33 91.88 o -11 3 2 3236.88 3838.34 258.63 o -9 3 2 5662.88 6338.84 298.78 o -7 3 2 3110.30 3643.96 150.66 o -5 3 2 9304.46 8384.77 335.08 o -3 3 2 2445.39 2140.21 132.20 o -1 3 2 31736.41 26972.38 219.95 o 3 3 2 25.99 50.82 6.44 o 5 3 2 438.99 400.00 22.51 o 7 3 2 3309.98 3728.02 146.75 o 9 3 2 41.21 64.58 9.08 o 11 3 2 54.63 33.18 8.41 o 13 3 2 8.02 10.49 9.19 o 15 3 2 1808.06 1743.49 62.98 o 17 3 2 60.24 43.40 21.02 o -20 4 2 20.58 43.96 32.27 o -18 4 2 2.44 3.99 36.37 o -16 4 2 748.77 585.99 45.97 o -14 4 2 162.93 102.49 18.29 o -12 4 2 2432.19 2564.55 163.91 o -10 4 2 5018.44 5354.84 265.65 o -8 4 2 14684.85 16226.43 684.15 o -6 4 2 994.29 961.29 65.35 o -4 4 2 2645.54 2289.68 92.18 o -2 4 2 3298.68 3104.53 162.63 o 0 4 2 14300.42 15094.89 537.76 o 2 4 2 1495.62 1340.91 39.02 o 4 4 2 8122.66 8073.90 134.31 o 6 4 2 5671.72 5610.72 113.70 o 8 4 2 257.43 269.96 16.18 o 10 4 2 10793.51 10838.24 378.34 o 12 4 2 449.79 483.48 33.25 o 14 4 2 7.08 18.32 12.04 o 16 4 2 116.60 95.41 28.03 o 18 4 2 271.55 172.15 41.80 o -19 5 2 620.24 527.70 70.20 o -17 5 2 506.85 409.40 45.76 o -15 5 2 61.29 12.24 14.50 o -13 5 2 57.59 32.81 12.31 o -11 5 2 1013.72 1089.26 44.45 o -9 5 2 1583.94 1581.61 64.55 o -7 5 2 4189.94 4287.59 191.24 o -5 5 2 135.47 136.15 13.55 o -3 5 2 856.93 935.72 30.31 o -1 5 2 9135.17 9926.52 593.71 o 1 5 2 2540.19 2661.61 160.18 o 3 5 2 17.00 35.12 8.84 o 5 5 2 3665.63 3843.88 108.37 o 7 5 2 20.38 29.37 8.68 o 9 5 2 986.79 1091.29 50.72 o 11 5 2 268.62 238.86 21.20 o 13 5 2 56.20 65.10 16.66 o 15 5 2 123.72 133.72 18.13 o 17 5 2 14.66 15.63 70.31 o -18 6 2 890.14 890.99 62.01 o -16 6 2 1420.29 1377.19 67.90 o -14 6 2 227.53 159.01 30.23 o -12 6 2 6.11 -0.35 11.06 o -10 6 2 2688.10 2966.28 98.89 o -8 6 2 103.58 74.95 10.37 o -6 6 2 9308.08 9413.71 320.71 o -4 6 2 2417.87 2434.08 113.38 o -2 6 2 7001.16 6897.54 362.84 o 0 6 2 2059.30 2315.83 136.54 o 2 6 2 3991.56 3850.29 130.11 o 4 6 2 74.67 47.14 14.77 o 6 6 2 51.56 50.93 11.10 o 8 6 2 303.13 401.41 28.95 o 10 6 2 46.93 30.23 15.93 o 12 6 2 8.08 49.19 23.05 o 14 6 2 55.47 31.33 21.20 o 16 6 2 297.83 215.79 57.16 o 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1988.46 98.59 o -20 2 22 619.87 761.64 52.41 o -18 2 22 68.25 47.88 20.63 o -16 2 22 929.82 930.88 51.02 o -14 2 22 13.06 23.23 18.20 o -12 2 22 455.49 452.76 37.11 o -10 2 22 3.27 3.82 22.65 o -8 2 22 108.08 41.72 32.80 o -21 3 22 79.21 52.71 23.17 o -19 3 22 231.44 223.28 38.32 o -17 3 22 39.40 108.90 22.99 o -15 3 22 23.38 16.52 15.53 o -13 3 22 356.19 416.04 53.55 o -11 3 22 5.62 2.45 21.40 o -9 3 22 642.06 580.67 57.10 o -20 4 22 3.13 35.56 23.03 o -18 4 22 213.34 185.40 27.93 o -16 4 22 371.07 463.34 38.71 o -14 4 22 325.32 383.85 33.83 o -12 4 22 1425.44 1545.64 80.40 o -10 4 22 0.37 -6.51 21.04 o -17 5 22 30.21 26.17 20.53 o -15 5 22 1147.22 1269.76 79.60 o -13 5 22 785.52 1021.02 83.62 o -21 1 23 0.72 10.49 20.62 o -19 1 23 24.05 39.68 24.92 o -17 1 23 1769.83 1972.07 78.73 o -15 1 23 157.49 139.76 41.11 o -13 1 23 46.41 20.05 19.19 o -11 1 23 71.91 89.70 21.31 o -20 2 23 3.70 21.40 22.53 o -18 2 23 31.40 75.44 25.67 o -16 2 23 130.89 123.85 24.75 o -14 2 23 415.77 458.25 45.56 o -12 2 23 0.51 -13.97 23.91 o -10 2 23 51.19 129.31 52.84 o -19 3 23 42.55 47.20 24.32 o -17 3 23 6.59 -19.52 20.40 o -15 3 23 835.54 1040.09 103.15 o -13 3 23 1539.56 1636.04 99.46 o -16 4 23 221.26 226.68 50.20 o -18 0 24 508.76 610.13 146.29 o -16 0 24 324.56 425.28 111.86 o -14 0 24 243.51 235.35 59.14 o -19 1 24 427.44 472.99 55.70 o -17 1 24 28.35 6.91 19.61 o -15 1 24 0.00 27.79 23.96 o -16 2 24 47.69 52.17 45.62 o