#------------------------------------------------------------------------------
#$Date: 2021-01-29 07:29:51 +0200 (Fri, 29 Jan 2021) $
#$Revision: 261305 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108771.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108771
_cell_angle_alpha                90.000
_cell_angle_beta                 108.512
_cell_angle_gamma                90.000
_cell_length_a                   6.7703
_cell_length_b                   11.8624
_cell_length_c                   6.7705
_exptl_crystal_F_000             768.00
_reflns_d_resolution_high        0.6253
_cod_data_source_file            ra5092Isup2.hkl
_cod_data_source_block           I
_shelx_title                     ' Cu2GeSe3_Cc in Cc #9'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            540.29
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
6 0 -10 27987.63 28927.86 1532.97 o
5 1 -10 3108.16 3066.63 183.86 o
4 2 -10 345.68 406.31 51.79 o
6 2 -10 210.28 236.92 35.28 o
5 3 -10 5.27 -4.14 42.91 o
4 4 -10 453.23 390.14 54.85 o
3 5 -10 829.11 782.83 72.06 o
5 5 -10 2406.10 2363.31 149.95 o
4 6 -10 10396.85 9786.24 533.96 o
3 1 -9 323.83 280.91 39.78 o
5 1 -9 135.98 133.07 26.26 o
7 1 -9 280.53 219.72 34.59 o
2 2 -9 4070.07 4304.63 242.75 o
4 2 -9 2487.62 2633.20 165.60 o
6 2 -9 397.87 447.45 77.22 o
3 3 -9 45143.70 45864.54 2358.02 o
5 3 -9 24689.52 24755.46 1873.19 o
7 3 -9 793.92 821.78 71.22 o
2 4 -9 4007.37 3887.86 231.89 o
4 4 -9 2946.01 3195.10 179.69 o
6 4 -9 408.15 477.51 37.16 o
1 5 -9 197.43 264.63 46.94 o
3 5 -9 321.28 280.21 47.51 o
5 5 -9 75.42 67.06 40.02 o
2 6 -9 18.16 47.60 41.67 o
4 6 -9 51.74 61.68 40.29 o
6 6 -9 17.96 11.31 44.98 o
1 7 -9 394.73 404.58 60.91 o
3 7 -9 270.94 236.25 47.64 o
5 7 -9 287.16 283.07 50.68 o
0 8 -9 896.06 982.04 86.87 o
2 8 -9 2945.49 2989.33 185.31 o
4 8 -9 1393.24 1418.97 102.67 o
1 9 -9 10376.57 10402.23 570.83 o
3 9 -9 28135.93 26324.55 1406.64 o
2 0 -8 41958.16 40108.44 2088.19 o
4 0 -8 1598.47 1553.98 92.00 o
6 0 -8 22073.00 22026.35 1191.47 o
8 0 -8 33408.23 34532.05 1827.85 o
1 1 -8 4659.32 4670.50 262.18 o
3 1 -8 468.55 457.12 39.45 o
5 1 -8 1884.53 1856.10 80.03 o
7 1 -8 2598.33 2863.11 119.39 o
0 2 -8 370.80 390.51 39.78 o
2 2 -8 189.72 202.08 19.89 o
4 2 -8 192.52 196.64 22.93 o
6 2 -8 297.65 313.79 30.37 o
8 2 -8 90.57 86.50 38.29 o
1 3 -8 21.15 29.39 28.42 o
3 3 -8 12.84 19.40 18.99 o
5 3 -8 0.67 -0.40 22.00 o
7 3 -8 11.01 1.87 27.27 o
0 4 -8 319.10 299.28 44.19 o
2 4 -8 249.43 217.06 36.32 o
4 4 -8 514.86 522.13 35.38 o
6 4 -8 431.55 438.63 34.44 o
8 4 -8 100.57 52.85 44.99 o
-1 5 -8 4286.25 4394.53 263.59 o
1 5 -8 3400.42 3666.68 200.31 o
3 5 -8 204.06 146.34 34.93 o
5 5 -8 1562.00 1703.74 73.88 o
0 6 -8 45459.56 48930.84 2458.45 o
2 6 -8 32524.71 31845.17 1615.53 o
6 6 -8 17164.85 16066.80 911.03 o
-1 7 -8 3291.02 3312.92 206.19 o
1 7 -8 4099.93 4370.35 242.92 o
3 7 -8 552.54 544.57 54.73 o
5 7 -8 1643.59 1532.29 106.67 o
7 7 -8 2769.69 2829.68 170.74 o
0 8 -8 295.36 298.00 49.57 o
2 8 -8 218.90 288.82 50.53 o
4 8 -8 19.19 24.42 35.87 o
-1 9 -8 33.44 34.49 47.88 o
1 9 -8 115.42 156.78 49.13 o
3 9 -8 71.96 58.37 45.81 o
0 10 -8 244.88 163.05 52.46 o
2 10 -8 354.40 305.92 57.87 o
4 10 -8 612.05 575.43 62.20 o
1 11 -8 1631.23 1633.49 119.10 o
3 11 -8 56.03 63.33 50.78 o
-1 1 -7 261.66 239.59 31.21 o
1 1 -7 281.92 303.26 19.89 o
3 1 -7 496.04 567.68 66.91 o
5 1 -7 239.66 281.52 23.79 o
7 1 -7 120.68 166.99 27.65 o
9 1 -7 145.91 220.56 53.14 o
0 2 -7 681.34 786.79 54.50 o
2 2 -7 1251.03 1192.78 54.67 o
4 2 -7 3330.49 3505.63 136.78 o
6 2 -7 777.32 821.47 45.38 o
8 2 -7 1133.28 1238.65 61.48 o
-1 3 -7 43803.34 44316.90 2116.59 o
1 3 -7 2734.38 3080.22 207.92 o
3 3 -7 38514.38 39486.33 2055.24 o
5 3 -7 72735.45 78927.78 2888.76 o
9 3 -7 902.54 881.27 77.20 o
-2 4 -7 4838.65 5358.54 278.03 o
0 4 -7 1069.23 1130.86 72.86 o
2 4 -7 1055.62 1204.69 52.43 o
4 4 -7 3988.35 4214.36 298.83 o
6 4 -7 1266.35 1310.15 83.56 o
8 4 -7 802.60 834.47 69.30 o
-1 5 -7 347.99 347.53 41.58 o
1 5 -7 104.98 118.83 30.50 o
3 5 -7 221.19 217.07 21.76 o
5 5 -7 213.38 200.86 24.33 o
7 5 -7 27.04 -21.52 38.49 o
-2 6 -7 72.68 78.65 36.29 o
0 6 -7 74.78 113.57 35.74 o
2 6 -7 8.53 14.21 29.94 o
4 6 -7 41.99 50.09 29.67 o
6 6 -7 55.80 -4.14 37.53 o
8 6 -7 7.71 2.21 44.15 o
-3 7 -7 231.29 242.98 45.84 o
-1 7 -7 243.77 305.42 43.49 o
1 7 -7 514.35 477.67 48.51 o
3 7 -7 587.93 588.00 55.44 o
7 7 -7 312.75 298.43 48.47 o
-2 8 -7 2845.79 3122.41 184.35 o
0 8 -7 161.85 163.43 40.72 o
2 8 -7 1253.16 1193.41 90.63 o
6 8 -7 355.86 403.31 49.72 o
8 8 -7 1024.53 916.72 75.56 o
-3 9 -7 28609.65 27094.37 1455.90 o
-1 9 -7 26874.31 26253.29 1314.55 o
1 9 -7 2158.26 2078.48 127.59 o
3 9 -7 21997.31 22321.89 1228.26 o
5 9 -7 42874.13 42304.44 2299.42 o
7 9 -7 17395.85 17190.36 866.79 o
-2 10 -7 3394.72 3394.99 206.63 o
0 10 -7 907.52 875.61 72.51 o
2 10 -7 754.94 642.17 64.87 o
4 10 -7 3255.51 3061.99 195.37 o
6 10 -7 1356.71 1284.80 93.94 o
-1 11 -7 317.70 415.80 55.24 o
1 11 -7 80.15 82.52 41.95 o
5 11 -7 148.07 162.73 44.17 o
0 12 -7 145.30 176.67 49.69 o
4 12 -7 79.81 98.94 51.33 o
1 13 -7 495.32 565.39 66.18 o
3 13 -7 437.79 337.49 61.20 o
0 0 -6 53030.57 51264.82 2850.11 o
2 0 -6 135701.22 151408.80 7929.57 o
4 0 -6 66665.99 68021.45 3410.32 o
8 0 -6 23599.00 28152.60 1395.23 o
-1 1 -6 1048.78 1095.28 47.74 o
1 1 -6 4985.87 5277.39 199.03 o
3 1 -6 2739.37 2764.14 112.21 o
5 1 -6 766.32 835.19 37.58 o
7 1 -6 3267.22 3351.69 180.37 o
9 1 -6 1752.11 1840.36 114.95 o
-2 2 -6 182.51 225.31 26.23 o
0 2 -6 249.46 251.34 16.48 o
2 2 -6 345.19 363.38 24.73 o
4 2 -6 132.36 146.43 26.92 o
6 2 -6 134.03 151.83 32.02 o
8 2 -6 89.85 105.57 42.50 o
-3 3 -6 25.80 28.28 23.45 o
-1 3 -6 8.61 10.07 19.73 o
1 3 -6 13.99 24.51 11.80 o
3 3 -6 27.78 29.37 13.12 o
5 3 -6 6.27 19.31 25.52 o
7 3 -6 4.96 -1.15 22.43 o
9 3 -6 14.53 56.56 44.84 o
-2 4 -6 208.86 193.16 30.10 o
0 4 -6 435.52 463.29 38.56 o
2 4 -6 363.28 370.84 23.57 o
4 4 -6 358.91 375.84 25.06 o
6 4 -6 466.77 498.89 32.39 o
8 4 -6 164.81 184.00 42.38 o
-3 5 -6 854.60 793.04 61.44 o
-1 5 -6 1689.04 1699.37 111.94 o
1 5 -6 4298.71 4356.89 250.19 o
3 5 -6 1679.14 1772.11 79.34 o
5 5 -6 892.46 933.12 44.70 o
7 5 -6 2535.58 2517.86 142.80 o
9 5 -6 940.58 1015.47 77.76 o
-6 6 -6 23506.30 21886.40 1173.16 o
-4 6 -6 28954.83 28454.90 1459.03 o
-2 6 -6 3990.00 3780.61 232.50 o
0 6 -6 38685.13 39803.59 2134.30 o
2 6 -6 98504.89 110015.64 5749.75 o
8 6 -6 18504.33 18026.25 997.17 o
-3 7 -6 1511.46 1456.87 97.21 o
-1 7 -6 373.82 410.31 39.79 o
1 7 -6 4132.73 4290.98 241.75 o
5 7 -6 423.01 439.12 45.60 o
7 7 -6 2757.67 2650.09 157.48 o
9 7 -6 2074.45 2140.34 129.95 o
-4 8 -6 381.77 409.40 51.11 o
-2 8 -6 202.92 243.94 37.97 o
0 8 -6 67.46 55.89 26.91 o
2 8 -6 257.43 207.00 35.63 o
4 8 -6 139.35 188.13 36.30 o
6 8 -6 1.38 -4.00 35.18 o
8 8 -6 29.67 28.15 39.46 o
-3 9 -6 139.05 169.21 40.99 o
-1 9 -6 43.96 9.38 31.73 o
1 9 -6 68.96 91.35 33.26 o
3 9 -6 142.02 165.91 39.61 o
5 9 -6 34.66 109.55 32.98 o
7 9 -6 25.96 15.18 41.80 o
-4 10 -6 179.14 230.52 51.90 o
-2 10 -6 284.58 271.07 43.91 o
0 10 -6 453.93 458.34 49.47 o
4 10 -6 567.68 542.56 59.03 o
6 10 -6 583.00 550.26 59.02 o
8 10 -6 175.75 183.31 48.03 o
-3 11 -6 270.56 249.22 51.92 o
3 11 -6 674.61 690.84 66.65 o
5 11 -6 686.73 753.99 66.23 o
7 11 -6 1449.14 1710.49 108.92 o
-2 12 -6 2476.79 2763.31 160.45 o
0 12 -6 16951.37 16195.33 927.99 o
2 12 -6 43092.65 42386.89 2205.02 o
4 12 -6 22593.75 24372.80 1261.82 o
6 12 -6 918.13 1008.05 77.76 o
-1 13 -6 146.19 118.84 48.17 o
3 13 -6 2103.89 2333.86 141.95 o
5 13 -6 222.41 236.62 48.59 o
2 14 -6 133.39 171.00 50.10 o
4 14 -6 148.44 159.83 52.72 o
-7 1 -5 324.73 323.56 66.01 o
-5 1 -5 182.72 167.45 44.17 o
-3 1 -5 151.04 157.37 20.43 o
-1 1 -5 303.55 315.88 17.42 o
1 1 -5 234.43 267.82 28.46 o
3 1 -5 372.75 390.61 21.35 o
5 1 -5 311.23 329.36 33.02 o
7 1 -5 69.91 78.44 29.05 o
9 1 -5 49.47 61.02 30.15 o
-6 2 -5 1347.89 1341.99 100.18 o
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0 2 -5 4214.81 4518.70 219.04 o
2 2 -5 254.50 245.33 15.14 o
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8 2 -5 33.91 21.43 47.32 o
10 2 -5 1744.03 1616.88 115.13 o
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4 4 -5 2506.09 2448.26 100.21 o
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10 4 -5 1228.31 1139.68 88.21 o
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3 5 -5 63.71 45.82 15.46 o
5 5 -5 88.54 92.14 17.38 o
7 5 -5 51.61 83.76 32.29 o
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0 6 -5 122.23 117.33 22.78 o
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6 6 -5 75.31 97.43 32.15 o
8 6 -5 46.79 69.27 36.84 o
-5 7 -5 117.33 60.70 26.84 o
-3 7 -5 226.05 207.62 23.09 o
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7 7 -5 143.48 143.00 35.33 o
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6 8 -5 706.96 632.77 56.43 o
8 8 -5 185.39 228.87 41.96 o
-5 9 -5 3893.61 4344.88 227.91 o
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3 9 -5 1685.36 1756.42 99.99 o
5 9 -5 30058.32 27609.37 1566.75 o
7 9 -5 41667.18 43022.92 2265.03 o
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1 11 -5 283.13 247.48 39.22 o
3 11 -5 67.38 104.32 35.74 o
5 11 -5 9.02 59.74 35.73 o
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-3 13 -5 232.88 289.23 52.46 o
1 13 -5 555.74 573.88 56.39 o
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3 1 -4 2553.00 2522.55 96.71 o
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