#------------------------------------------------------------------------------ #$Date: 2021-03-02 08:04:16 +0200 (Tue, 02 Mar 2021) $ #$Revision: 262343 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108774.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108774 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.2305 _cell_length_b 8.8992 _cell_length_c 8.7624 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.8056 _cod_data_source_file um5047Xylitol0_63GPasup4.hkl _cod_data_source_block Xylitol0_63GPa _shelx_title ' xyl066 in P212121 No19' _shelx_refln_list_code 4 _shelx_f_calc_maximum 57.05 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 263.90 255.51 11.80 o 4 0 0 210.05 240.23 2.36 o 6 0 0 503.75 523.98 4.96 o 8 0 0 16.97 15.33 1.35 o 2 1 0 845.87 816.77 4.68 o 3 1 0 52.98 48.50 0.65 o 4 1 0 740.37 736.99 2.76 o 5 1 0 92.58 93.40 1.01 o 6 1 0 48.06 43.97 0.98 o 7 1 0 437.86 435.49 4.12 o 8 1 0 114.48 106.94 3.09 o 9 1 0 3.90 2.98 1.00 o 10 1 0 102.02 120.58 4.63 o 3 2 0 2017.88 1968.71 11.33 o 4 2 0 11.82 10.81 0.53 o 5 2 0 73.40 66.51 1.93 o 6 2 0 63.83 67.20 2.13 o 7 2 0 755.17 780.74 8.07 o 8 2 0 67.72 72.69 2.67 o 9 2 0 4.09 1.59 1.11 o 2 0 1 259.29 250.77 1.46 o 3 0 1 23.54 23.52 0.39 o 4 0 1 466.93 490.73 2.85 o 5 0 1 96.52 93.19 1.04 o 6 0 1 527.25 532.38 3.22 o 7 0 1 439.84 419.88 4.33 o 8 0 1 69.60 69.34 2.10 o 9 0 1 40.12 46.38 2.35 o 10 0 1 108.96 121.45 4.66 o -9 1 1 2.24 2.86 1.51 o -8 1 1 8.61 10.05 0.97 o -7 1 1 199.11 193.48 5.50 o -6 1 1 246.94 240.27 2.90 o -5 1 1 98.77 91.47 1.33 o -4 1 1 784.28 790.39 4.52 o -3 1 1 3253.45 3072.60 8.68 o -2 1 1 341.95 352.74 2.47 o -1 1 1 541.03 508.98 6.31 o 1 1 1 539.70 521.10 4.42 o 2 1 1 341.64 351.57 4.13 o 3 1 1 3254.38 3074.77 9.24 o 4 1 1 783.79 798.14 3.61 o 5 1 1 98.73 94.57 1.35 o 6 1 1 246.85 239.79 2.37 o 7 1 1 199.34 194.38 3.25 o 8 1 1 8.62 8.32 0.88 o 9 1 1 2.25 2.09 1.14 o -9 2 1 6.99 7.77 2.02 o -8 2 1 10.51 10.49 1.70 o -7 2 1 30.95 33.52 1.67 o -6 2 1 125.04 131.85 2.58 o -5 2 1 373.63 382.61 4.56 o -4 2 1 428.24 430.87 3.93 o -3 2 1 2.00 1.93 0.31 o -2 2 1 238.17 233.11 2.97 o -1 2 1 1583.48 1455.47 9.64 o 0 2 1 574.20 577.29 7.46 o 1 2 1 1581.88 1409.27 23.07 o 2 2 1 238.20 237.81 2.32 o 3 2 1 1.96 1.66 0.22 o 4 2 1 428.17 418.23 4.77 o 5 2 1 373.84 377.21 3.87 o 6 2 1 125.19 128.14 2.55 o 7 2 1 31.09 32.73 2.38 o 8 2 1 10.57 10.74 1.62 o 9 2 1 7.02 11.82 2.83 o 10 2 1 40.14 44.40 5.22 o -8 3 1 30.06 32.31 4.07 o -7 3 1 460.16 485.44 13.40 o -6 3 1 12.88 10.73 2.24 o -5 3 1 287.51 286.41 8.77 o -4 3 1 76.19 78.89 4.10 o 3 3 1 117.40 108.36 3.32 o 4 3 1 76.09 75.64 2.10 o 5 3 1 287.57 283.51 4.79 o 6 3 1 13.04 13.48 1.15 o 7 3 1 460.27 462.68 13.06 o 8 3 1 30.17 29.85 3.79 o 2 0 2 496.47 446.73 5.18 o 3 0 2 1212.61 1228.23 5.73 o 4 0 2 451.20 445.11 6.70 o 5 0 2 152.13 142.94 1.92 o 6 0 2 84.51 84.32 1.63 o 7 0 2 7.55 8.83 0.71 o 8 0 2 12.38 11.18 1.18 o 9 0 2 69.32 71.39 3.34 o 10 0 2 30.23 34.89 4.60 o -9 1 2 21.06 22.20 3.76 o -8 1 2 14.18 14.30 1.37 o -7 1 2 319.34 315.03 4.48 o -6 1 2 504.95 511.47 7.62 o -5 1 2 287.46 282.80 2.86 o -4 1 2 27.02 25.89 0.77 o -3 1 2 837.62 884.29 7.89 o -2 1 2 1143.35 1111.19 9.10 o -1 1 2 579.97 598.29 3.74 o 0 1 2 1908.97 1798.09 7.07 o 1 1 2 580.26 604.41 5.50 o 2 1 2 1142.35 1127.81 4.86 o 3 1 2 837.94 891.25 4.78 o 4 1 2 26.87 25.22 0.71 o 5 1 2 287.29 283.63 2.88 o 6 1 2 505.18 498.91 3.98 o 7 1 2 319.56 312.18 4.38 o 8 1 2 14.19 14.19 1.33 o 9 1 2 21.11 23.29 3.61 o 10 1 2 10.22 9.39 3.48 o -9 2 2 22.96 24.88 3.86 o -8 2 2 11.21 12.23 1.50 o -7 2 2 79.83 73.66 2.90 o -6 2 2 199.90 196.29 2.65 o -5 2 2 118.58 112.64 1.68 o -4 2 2 482.49 468.20 2.98 o -3 2 2 9.67 13.60 0.89 o -2 2 2 25.33 25.90 0.68 o -1 2 2 726.34 753.70 3.56 o 0 2 2 1265.20 1201.61 5.89 o 1 2 2 726.31 756.98 5.89 o 2 2 2 25.32 26.97 0.68 o 3 2 2 9.73 12.23 0.60 o 4 2 2 482.08 470.12 3.57 o 5 2 2 118.41 114.54 1.70 o 6 2 2 200.34 208.41 2.74 o 7 2 2 79.86 74.57 2.15 o 8 2 2 11.25 9.38 1.37 o 9 2 2 23.03 29.54 3.98 o -9 3 2 5.65 7.34 2.39 o -8 3 2 52.64 50.52 3.28 o -7 3 2 121.65 121.57 4.66 o -6 3 2 93.50 98.62 3.83 o -5 3 2 10.97 12.45 1.16 o -4 3 2 192.29 191.00 3.17 o -3 3 2 303.36 339.06 4.92 o -2 3 2 654.95 660.28 4.58 o -1 3 2 784.40 836.53 6.06 o 0 3 2 340.89 361.28 4.77 o 1 3 2 785.49 828.96 4.13 o 2 3 2 655.06 650.88 7.37 o 3 3 2 303.24 340.69 3.83 o 4 3 2 192.26 194.04 2.36 o 5 3 2 10.88 11.03 0.75 o 6 3 2 93.67 94.12 3.65 o 7 3 2 121.65 115.12 9.79 o 8 3 2 52.64 46.61 2.98 o 9 3 2 5.64 6.87 2.46 o -7 4 2 15.46 13.93 2.74 o -6 4 2 72.15 73.66 5.01 o 3 4 2 3.14 3.26 0.78 o 4 4 2 95.65 91.08 3.96 o 5 4 2 8.15 7.64 1.22 o 6 4 2 72.02 65.85 6.31 o 7 4 2 15.55 13.99 2.61 o 4 0 3 1911.55 2020.94 38.01 o 5 0 3 32.07 34.70 1.55 o 6 0 3 629.05 613.96 6.79 o 7 0 3 0.18 1.80 0.79 o -9 1 3 4.71 2.80 1.93 o -8 1 3 46.33 49.71 2.70 o -7 1 3 55.07 60.37 3.04 o -6 1 3 154.17 155.90 3.91 o -5 1 3 8.35 7.71 0.78 o -4 1 3 378.44 390.48 5.98 o -3 1 3 159.21 169.56 2.04 o -2 1 3 892.98 903.27 7.91 o -1 1 3 404.68 385.91 5.86 o 1 1 3 405.24 372.45 15.61 o 2 1 3 892.71 889.84 10.35 o 3 1 3 159.00 170.63 2.43 o 4 1 3 378.36 380.35 3.40 o 5 1 3 8.41 8.75 0.83 o 6 1 3 154.47 160.05 3.90 o 7 1 3 55.11 58.28 2.63 o 8 1 3 46.17 49.98 2.63 o 9 1 3 4.71 3.45 2.18 o -9 2 3 10.94 12.59 3.17 o -8 2 3 22.70 23.02 1.99 o -7 2 3 11.76 12.28 1.07 o -6 2 3 181.94 177.26 3.55 o -5 2 3 31.21 32.46 1.17 o -4 2 3 6.73 6.82 0.55 o -3 2 3 797.33 846.28 5.23 o -2 2 3 652.35 667.39 3.59 o -1 2 3 1838.06 1837.73 6.69 o 0 2 3 359.80 351.56 2.00 o 1 2 3 1838.13 1841.10 10.62 o 2 2 3 652.62 666.11 3.82 o 3 2 3 797.39 848.57 7.70 o 4 2 3 6.77 7.66 0.52 o 5 2 3 31.29 31.33 1.03 o 6 2 3 182.25 177.20 3.20 o 7 2 3 11.64 9.67 0.95 o 8 2 3 22.73 25.05 2.50 o 9 2 3 11.00 9.50 2.10 o -9 3 3 3.97 4.52 1.89 o -8 3 3 111.90 108.80 7.32 o -7 3 3 154.28 155.06 3.28 o -6 3 3 17.16 16.16 1.13 o -5 3 3 29.90 29.45 1.06 o -4 3 3 17.26 16.53 0.76 o -3 3 3 595.73 585.66 3.59 o -2 3 3 33.45 32.18 0.82 o -1 3 3 1212.98 1174.19 4.52 o 0 3 3 2.32 1.54 0.30 o 1 3 3 1212.55 1171.89 8.56 o 2 3 3 33.55 31.33 0.76 o 3 3 3 596.30 582.23 4.12 o 4 3 3 17.28 17.25 0.78 o 5 3 3 29.86 29.66 1.04 o 6 3 3 17.18 14.99 1.08 o 7 3 3 154.38 155.66 3.31 o 8 3 3 111.78 113.79 4.72 o 9 3 3 3.98 1.27 1.83 o -8 4 3 13.80 12.71 2.81 o -7 4 3 12.41 13.53 1.82 o -6 4 3 192.85 200.20 5.84 o -5 4 3 258.72 265.17 5.88 o -4 4 3 581.54 550.84 5.87 o -3 4 3 0.21 0.91 0.44 o -2 4 3 14.29 15.36 0.78 o -1 4 3 177.81 206.07 3.05 o 0 4 3 284.87 323.08 3.33 o 1 4 3 178.01 203.25 2.72 o 2 4 3 14.20 14.00 0.72 o 3 4 3 0.21 -0.41 0.46 o 4 4 3 581.58 572.30 5.96 o 5 4 3 259.25 268.76 5.38 o 6 4 3 192.60 186.65 5.56 o 7 4 3 12.49 14.94 1.81 o 8 4 3 13.82 11.31 3.90 o 9 4 3 55.05 53.54 5.01 o -2 5 3 87.63 87.69 4.20 o 3 5 3 109.50 106.37 5.01 o 4 5 3 147.47 138.93 6.16 o 5 5 3 45.15 46.45 3.70 o 6 5 3 2.36 2.80 1.59 o -8 1 4 14.29 17.94 2.80 o -7 1 4 23.39 29.05 2.51 o -6 1 4 298.42 269.80 6.76 o -5 1 4 70.72 78.19 2.61 o -4 1 4 1109.42 1098.03 11.31 o 4 1 4 1110.31 1103.39 9.88 o 5 1 4 70.36 74.54 4.04 o 6 1 4 298.13 268.28 7.04 o 7 1 4 23.33 25.14 2.32 o -9 2 4 1.30 -1.85 1.85 o -8 2 4 2.32 3.19 1.27 o -7 2 4 45.73 43.22 2.43 o -6 2 4 181.26 174.91 5.58 o -5 2 4 131.50 142.07 3.46 o -4 2 4 59.53 59.86 1.70 o -3 2 4 34.13 32.62 0.95 o -2 2 4 18.32 19.58 0.80 o -1 2 4 205.59 213.49 2.65 o 0 2 4 6.59 6.75 0.41 o 1 2 4 205.69 209.41 1.97 o 2 2 4 18.35 20.48 0.73 o 3 2 4 34.14 30.78 0.93 o 4 2 4 59.59 55.96 1.47 o 5 2 4 131.61 136.13 4.75 o 6 2 4 181.38 169.32 4.29 o 7 2 4 45.60 43.52 2.46 o 8 2 4 2.34 4.85 1.49 o 9 2 4 1.33 3.36 1.38 o -8 3 4 12.64 11.90 1.64 o -7 3 4 30.44 35.56 2.54 o -6 3 4 123.62 122.03 3.77 o -5 3 4 251.65 239.79 3.54 o -4 3 4 165.02 158.29 2.32 o -3 3 4 653.62 662.23 4.92 o -2 3 4 154.91 151.64 1.91 o -1 3 4 1079.78 1159.19 9.27 o 0 3 4 28.57 28.54 0.66 o 1 3 4 1079.44 1135.67 11.23 o 2 3 4 155.33 149.20 1.81 o 3 3 4 653.62 657.31 4.16 o 4 3 4 165.37 161.86 2.34 o 5 3 4 252.15 238.80 3.03 o 6 3 4 123.44 124.27 2.97 o 7 3 4 30.29 32.99 1.90 o 8 3 4 12.69 10.72 1.57 o 9 3 4 2.67 -0.22 2.11 o -8 4 4 6.71 10.44 2.01 o -7 4 4 42.88 43.94 3.95 o -6 4 4 96.10 92.23 2.58 o -5 4 4 149.05 150.33 2.52 o -4 4 4 156.99 155.62 2.42 o -3 4 4 116.10 114.85 2.13 o -2 4 4 247.96 255.18 2.78 o -1 4 4 111.12 111.41 1.76 o 0 4 4 109.83 106.69 1.34 o 1 4 4 111.12 110.85 1.76 o 2 4 4 247.39 253.67 2.76 o 3 4 4 116.14 112.84 2.10 o 4 4 4 157.21 155.04 2.41 o 5 4 4 148.88 142.16 2.44 o 6 4 4 95.90 89.80 2.53 o 7 4 4 42.95 36.74 2.27 o 8 4 4 6.75 7.20 3.09 o -7 5 4 50.23 61.44 5.32 o -6 5 4 149.15 138.99 7.40 o -5 5 4 4.95 4.79 1.26 o -4 5 4 400.19 395.76 10.76 o -3 5 4 146.14 154.19 4.04 o -2 5 4 214.74 222.46 4.40 o -1 5 4 107.61 108.79 2.85 o 0 5 4 118.97 111.18 3.60 o 1 5 4 107.53 105.82 2.20 o 2 5 4 214.53 235.77 5.12 o 3 5 4 145.95 150.43 3.84 o 4 5 4 400.24 405.76 16.26 o 5 5 4 4.92 5.50 1.15 o 6 5 4 149.36 146.64 7.46 o 7 5 4 50.23 60.42 5.16 o 8 5 4 50.76 45.12 4.85 o -7 2 5 10.86 10.18 2.47 o -6 2 5 16.30 15.89 1.88 o -5 2 5 53.60 58.31 2.51 o -4 2 5 165.62 166.42 3.82 o -3 2 5 146.85 135.88 3.72 o 3 2 5 146.56 150.76 4.19 o 4 2 5 165.48 170.59 3.90 o 5 2 5 53.55 52.18 3.95 o 6 2 5 16.34 15.68 1.61 o 7 2 5 10.88 11.45 1.79 o -8 3 5 11.16 12.93 1.85 o -7 3 5 11.39 13.24 1.68 o -6 3 5 90.37 88.36 2.89 o -5 3 5 75.07 77.74 2.09 o -4 3 5 160.73 169.67 2.77 o -3 3 5 194.49 196.13 2.84 o -2 3 5 57.33 56.76 1.49 o -1 3 5 201.18 208.02 3.31 o 0 3 5 10.45 11.27 0.62 o 1 3 5 200.80 207.30 2.50 o 2 3 5 57.17 56.68 1.36 o 3 3 5 194.46 202.44 3.49 o 4 3 5 160.46 165.67 2.76 o 5 3 5 74.94 75.17 2.46 o 6 3 5 90.41 84.79 2.85 o 7 3 5 11.39 12.67 1.64 o 8 3 5 11.21 10.74 1.82 o -7 4 5 18.43 19.24 1.48 o -6 4 5 46.95 48.41 1.99 o -5 4 5 154.53 156.63 3.63 o -4 4 5 160.21 162.09 3.13 o -3 4 5 132.66 136.61 2.47 o -2 4 5 84.73 86.64 1.72 o -1 4 5 28.65 29.10 1.16 o 0 4 5 26.61 25.38 0.90 o 1 4 5 28.62 26.78 0.96 o 2 4 5 84.94 85.60 1.72 o 3 4 5 132.33 131.79 2.72 o 4 4 5 160.12 157.77 3.12 o 5 4 5 154.47 152.78 3.18 o 6 4 5 47.02 45.79 1.92 o 7 4 5 18.52 19.80 1.88 o 8 4 5 13.23 17.41 3.45 o -7 5 5 2.67 2.86 2.39 o -6 5 5 32.90 30.19 3.82 o -5 5 5 10.20 9.89 1.07 o -4 5 5 27.09 25.59 1.42 o -3 5 5 84.42 84.36 2.31 o -2 5 5 274.38 278.56 3.57 o -1 5 5 98.72 96.89 2.07 o 0 5 5 432.35 438.67 5.53 o 1 5 5 98.69 99.72 1.91 o 2 5 5 274.08 270.53 3.24 o 3 5 5 84.45 84.94 2.29 o 4 5 5 27.07 25.14 1.39 o 5 5 5 10.21 9.82 1.03 o 6 5 5 32.91 31.14 2.77 o 7 5 5 2.71 -0.16 1.83 o -6 6 5 59.57 63.31 5.41 o -5 6 5 67.67 67.41 3.72 o -4 6 5 102.09 109.01 4.96 o -3 6 5 16.50 17.60 3.96 o -2 6 5 150.54 151.10 3.44 o -1 6 5 54.50 54.63 2.09 o 0 6 5 21.51 21.20 1.39 o 1 6 5 54.66 53.60 2.47 o 2 6 5 150.58 145.03 5.88 o 3 6 5 16.58 15.13 1.81 o 4 6 5 102.38 99.84 4.31 o 5 6 5 67.73 64.55 5.19 o 6 6 5 59.51 56.31 5.04 o 7 6 5 6.20 3.02 2.02 o -7 3 6 0.99 4.85 2.15 o -6 3 6 13.63 12.31 1.83 o -5 3 6 300.59 288.10 5.74 o -4 3 6 75.57 73.05 3.64 o -3 3 6 101.27 104.04 3.84 o -2 3 6 102.31 96.24 3.49 o 2 3 6 102.25 105.52 4.04 o 3 3 6 101.14 98.70 8.85 o 4 3 6 75.50 66.86 4.93 o 5 3 6 300.64 287.46 7.38 o 6 3 6 13.64 14.28 1.88 o -7 4 6 44.88 48.83 3.60 o -6 4 6 1.99 3.11 2.07 o -5 4 6 11.77 10.19 1.45 o -4 4 6 2.92 2.32 1.10 o -3 4 6 111.87 118.08 3.25 o -2 4 6 331.82 337.24 4.34 o -1 4 6 59.83 62.01 2.13 o 0 4 6 9.11 7.11 0.94 o 1 4 6 59.79 59.83 1.65 o 2 4 6 331.87 339.57 3.71 o 3 4 6 112.00 115.39 2.72 o 4 4 6 2.94 2.06 0.71 o 5 4 6 11.79 11.09 1.38 o 6 4 6 1.94 3.24 1.82 o 7 4 6 44.86 44.73 3.47 o -6 5 6 26.55 26.39 1.91 o -5 5 6 2.13 2.72 0.86 o -4 5 6 56.97 53.88 2.07 o -3 5 6 101.99 101.14 2.63 o -2 5 6 53.07 56.45 1.61 o -1 5 6 53.98 51.16 2.03 o 0 5 6 22.43 22.22 1.41 o 1 5 6 54.15 50.36 1.77 o 2 5 6 52.98 58.69 1.64 o 3 5 6 101.90 101.09 2.67 o 4 5 6 57.10 55.52 2.11 o 5 5 6 2.16 3.32 0.87 o 6 5 6 26.54 29.10 2.66 o 7 5 6 8.58 11.44 3.26 o -5 6 6 14.55 20.27 4.90 o -4 6 6 49.63 51.22 2.34 o -3 6 6 78.78 77.71 2.77 o -2 6 6 56.63 56.84 2.06 o -1 6 6 90.17 87.10 2.85 o 0 6 6 1.09 1.03 0.89 o 1 6 6 89.89 85.31 2.80 o 2 6 6 56.58 59.19 2.36 o 3 6 6 78.70 77.93 2.78 o 4 6 6 49.69 50.73 2.37 o 5 6 6 14.58 13.44 2.02 o 6 6 6 9.33 13.53 3.30 o -6 5 7 11.67 13.15 2.09 o -5 5 7 32.81 35.06 2.42 o -4 5 7 93.57 103.84 3.87 o -3 5 7 0.79 0.30 0.86 o -2 5 7 220.80 213.93 5.03 o -1 5 7 68.63 70.12 2.88 o 0 5 7 19.27 19.84 1.91 o 1 5 7 68.61 73.19 3.11 o 2 5 7 221.28 211.33 3.83 o 3 5 7 0.81 -1.06 1.06 o 4 5 7 93.24 97.12 3.79 o 5 5 7 32.81 33.50 2.52 o 6 5 7 11.70 11.21 2.03 o -5 6 7 20.62 21.68 1.81 o -4 6 7 14.34 15.71 1.39 o -3 6 7 0.04 0.36 1.51 o -2 6 7 80.30 80.99 3.95 o -1 6 7 79.01 82.98 2.92 o 0 6 7 1.58 0.48 0.93 o 1 6 7 79.16 84.48 2.92 o 2 6 7 80.20 79.74 3.33 o 3 6 7 0.04 1.55 1.06 o 4 6 7 14.40 12.77 1.26 o 5 6 7 20.63 22.78 2.17 o -3 7 7 4.04 6.13 2.89 o -2 7 7 36.09 30.31 2.90 o -1 7 7 7.79 4.51 1.53 o 0 7 7 25.30 22.66 1.73 o 1 7 7 7.83 4.79 1.20 o 2 7 7 36.04 29.53 2.82 o 3 7 7 4.08 3.73 1.44 o 4 7 7 11.92 9.68 1.89 o -4 6 8 4.41 3.89 2.02 o -3 6 8 18.24 21.02 3.48 o -2 6 8 25.64 22.76 1.99 o -1 6 8 2.50 -1.14 1.50 o 0 6 8 31.93 32.36 2.27 o 1 6 8 2.45 3.48 4.24 o 2 6 8 25.63 26.77 4.26 o -2 7 8 3.13 4.63 2.11 o -1 7 8 9.88 8.18 1.49 o 0 7 8 1.87 1.67 1.41 o 1 7 8 9.84 16.00 2.35 o 2 7 8 3.11 3.61 2.18 o