#------------------------------------------------------------------------------ #$Date: 2021-03-11 08:03:05 +0200 (Thu, 11 Mar 2021) $ #$Revision: 262992 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/87/2108787.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108787 _cell_angle_alpha 90.000 _cell_angle_beta 110.894 _cell_angle_gamma 90.000 _cell_length_a 18.1614 _cell_length_b 22.1885 _cell_length_c 17.1716 _exptl_crystal_F_000 2824.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file aw5051Isup2.hkl _cod_data_source_block I _shelx_title ' OPTI in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 787.46 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 20130.07 21414.47 326.16 o 5 0 0 9373.90 9975.10 128.95 o 6 0 0 180190.64 189578.52 486.32 o 7 0 0 4067.96 4033.85 91.55 o 8 0 0 100875.09 100533.11 409.76 o 9 0 0 4705.00 4739.52 120.52 o 10 0 0 2739.66 2755.27 172.03 o 11 0 0 9830.31 10031.85 167.79 o 12 0 0 7589.31 7715.33 168.97 o 13 0 0 115.25 201.63 124.97 o 14 0 0 10303.53 10161.06 198.08 o 15 0 0 76.66 110.31 164.30 o 16 0 0 4910.15 4458.36 178.22 o 17 0 0 2198.14 2218.20 175.26 o 18 0 0 981.18 1017.73 197.54 o 19 0 0 2437.64 2464.98 191.95 o 20 0 0 1873.36 1715.78 200.59 o 21 0 0 0.04 117.29 216.51 o 4 1 0 137993.34 144535.39 814.22 o 5 1 0 5912.03 6274.44 91.57 o 6 1 0 33450.17 35268.45 302.73 o 7 1 0 764.53 677.00 61.14 o 8 1 0 14811.84 14578.60 98.32 o 9 1 0 3665.72 3814.56 72.09 o 10 1 0 51222.37 51052.07 242.93 o 11 1 0 66.44 157.63 87.73 o 12 1 0 20340.07 20013.89 147.28 o 13 1 0 646.64 722.42 101.46 o 14 1 0 53.72 4.96 120.81 o 15 1 0 1173.86 1264.34 115.67 o 16 1 0 7795.73 7644.82 170.83 o 17 1 0 210.26 256.76 123.09 o 18 1 0 9143.80 8918.55 156.16 o 19 1 0 84.23 169.89 125.98 o 20 1 0 298.80 244.63 141.52 o 21 1 0 588.35 508.62 154.36 o 3 2 0 1036.61 1037.88 99.07 o 4 2 0 703.30 741.98 81.40 o 5 2 0 624.77 907.48 92.95 o 6 2 0 81029.62 85937.37 489.31 o 7 2 0 5361.27 5668.58 94.42 o 8 2 0 33435.62 32143.22 276.87 o 9 2 0 467.73 495.45 71.14 o 10 2 0 527.32 563.47 75.37 o 11 2 0 1794.63 1728.18 84.02 o 12 2 0 14996.76 14989.41 202.55 o 13 2 0 446.25 493.29 101.45 o 14 2 0 1299.67 1395.71 108.90 o 15 2 0 466.34 456.43 104.77 o 16 2 0 6646.36 6417.18 138.88 o 17 2 0 2353.07 2127.46 124.87 o 18 2 0 460.05 551.16 127.87 o 19 2 0 145.15 160.73 135.46 o 20 2 0 2331.28 2277.64 155.55 o 21 2 0 33.91 131.08 182.43 o 3 3 0 2789.17 2901.86 56.46 o 4 3 0 43750.91 45073.36 254.25 o 5 3 0 5181.98 5316.90 141.95 o 6 3 0 4755.53 4911.89 85.47 o 7 3 0 11120.00 11759.08 117.58 o 8 3 0 2442.07 2026.02 87.21 o 9 3 0 1988.08 2507.55 100.17 o 10 3 0 33056.91 32366.38 162.32 o 11 3 0 353.73 285.68 77.69 o 12 3 0 19822.52 19749.83 136.23 o 13 3 0 300.85 384.92 97.77 o 14 3 0 183.70 285.88 103.36 o 15 3 0 27.87 68.85 126.89 o 16 3 0 5850.22 5754.01 138.30 o 17 3 0 247.40 214.69 118.44 o 18 3 0 7655.97 7710.34 155.86 o 19 3 0 610.85 554.79 131.26 o 20 3 0 731.24 616.10 148.18 o 21 3 0 517.09 522.45 148.51 o 2 4 0 23111.22 24498.48 242.18 o 3 4 0 133.40 171.82 56.78 o 4 4 0 5573.47 5671.60 73.77 o 5 4 0 193.75 139.27 78.94 o 6 4 0 25053.99 25730.01 311.03 o 7 4 0 178.80 207.35 82.13 o 8 4 0 10973.65 9950.76 121.57 o 9 4 0 1.51 -8.24 93.77 o 10 4 0 4338.61 4469.83 128.65 o 11 4 0 9.01 23.90 91.54 o 12 4 0 3958.93 3893.42 112.90 o 13 4 0 2896.71 2886.03 104.03 o 14 4 0 7107.79 7173.50 116.61 o 15 4 0 368.62 318.64 114.87 o 16 4 0 1535.15 1523.18 117.29 o 17 4 0 445.52 508.89 116.85 o 18 4 0 322.81 426.67 127.17 o 19 4 0 527.37 528.21 134.13 o 20 4 0 963.83 1126.27 147.46 o 21 4 0 2.21 39.25 271.97 o 1 5 0 1879.45 2022.95 52.02 o 2 5 0 43083.85 43912.54 120.73 o 3 5 0 2203.55 2233.33 63.71 o 4 5 0 5200.52 5109.40 75.49 o 5 5 0 2467.72 2421.75 72.28 o 6 5 0 27335.41 27888.74 126.85 o 7 5 0 189.65 127.89 84.29 o 8 5 0 2811.81 2924.39 97.84 o 9 5 0 976.32 1129.60 90.40 o 10 5 0 23773.01 23796.20 222.63 o 11 5 0 3.01 -36.24 173.45 o 12 5 0 1253.51 1198.28 120.90 o 13 5 0 819.24 803.77 110.76 o 14 5 0 3585.80 3526.71 106.35 o 15 5 0 1098.28 947.84 106.19 o 16 5 0 4143.05 4061.70 126.59 o 17 5 0 4.77 57.90 120.53 o 18 5 0 5118.12 5031.36 140.98 o 19 5 0 59.25 126.44 150.91 o 20 5 0 375.23 491.09 149.44 o 21 5 0 484.02 524.69 160.08 o 0 6 0 93253.88 98391.18 742.59 o 1 6 0 81.05 140.11 32.60 o 2 6 0 27992.88 29264.14 143.63 o 3 6 0 0.21 42.42 45.48 o 4 6 0 549.33 547.44 66.41 o 5 6 0 40.79 14.23 65.34 o 6 6 0 54314.52 56221.61 246.78 o 7 6 0 105.91 114.77 78.68 o 8 6 0 17649.14 17593.60 151.86 o 9 6 0 1003.85 991.82 91.28 o 10 6 0 1698.13 1618.39 100.10 o 11 6 0 1692.91 1649.48 124.31 o 12 6 0 3913.39 3719.14 122.03 o 13 6 0 2944.56 2878.99 141.97 o 14 6 0 3932.52 3913.18 129.10 o 15 6 0 1225.72 1004.55 102.24 o 16 6 0 1363.36 1408.73 116.72 o 17 6 0 683.94 609.99 122.68 o 18 6 0 116.63 163.35 133.62 o 19 6 0 135.29 141.60 149.63 o 20 6 0 1415.46 1289.21 147.82 o 21 6 0 1.66 147.89 232.75 o 1 7 0 1341.37 1420.75 37.00 o 2 7 0 22636.35 24006.51 100.21 o 3 7 0 643.52 687.10 43.45 o 4 7 0 19854.82 20000.93 95.99 o 5 7 0 732.02 744.60 66.75 o 6 7 0 1472.82 1390.27 71.23 o 7 7 0 6441.81 7002.30 101.42 o 8 7 0 4404.13 4040.27 98.99 o 9 7 0 911.59 947.35 102.04 o 10 7 0 19486.29 18734.52 167.92 o 11 7 0 342.40 271.19 117.14 o 12 7 0 9017.70 8832.71 150.18 o 13 7 0 1244.12 1211.54 130.80 o 14 7 0 1408.04 1273.95 140.00 o 15 7 0 624.82 594.81 117.65 o 16 7 0 3142.61 3069.87 115.17 o 17 7 0 0.70 22.80 112.25 o 18 7 0 4559.31 4295.85 146.99 o 19 7 0 9.67 60.08 131.03 o 20 7 0 47.88 214.06 189.56 o 21 7 0 15.50 78.02 169.97 o 0 8 0 60520.54 62392.97 409.20 o 1 8 0 634.78 650.42 34.78 o 2 8 0 7408.35 7439.44 45.40 o 3 8 0 394.96 398.95 41.10 o 4 8 0 120.39 74.31 40.72 o 5 8 0 1524.95 1688.49 70.48 o 6 8 0 12288.42 11662.83 96.25 o 7 8 0 1691.81 1719.24 84.77 o 8 8 0 11399.94 11405.08 114.43 o 9 8 0 340.34 302.17 106.43 o 10 8 0 110.88 89.49 98.54 o 11 8 0 152.89 124.56 114.05 o 12 8 0 3583.73 3654.72 137.17 o 13 8 0 35.84 53.30 153.08 o 14 8 0 135.78 169.02 138.89 o 15 8 0 815.87 722.65 125.50 o 16 8 0 2265.47 1904.57 131.16 o 17 8 0 233.15 251.15 121.13 o 18 8 0 295.31 306.63 114.73 o 19 8 0 31.29 35.74 177.63 o 20 8 0 594.06 534.05 146.92 o 1 9 0 3722.60 3921.80 39.65 o 2 9 0 25319.30 25816.83 78.02 o 3 9 0 429.33 442.84 36.66 o 4 9 0 6750.39 6383.62 51.74 o 5 9 0 379.68 316.92 55.98 o 6 9 0 1174.40 1109.74 72.44 o 7 9 0 1228.84 1250.29 76.27 o 8 9 0 1760.70 1815.65 90.99 o 9 9 0 151.26 176.63 102.32 o 10 9 0 7061.82 6920.18 208.29 o 11 9 0 63.24 50.12 104.56 o 12 9 0 4579.65 4455.24 135.61 o 13 9 0 315.20 360.66 135.92 o 14 9 0 130.26 102.45 154.16 o 15 9 0 12.30 5.68 168.46 o 16 9 0 1661.85 1657.43 122.25 o 17 9 0 23.45 7.10 169.66 o 18 9 0 2139.26 2038.91 123.59 o 19 9 0 0.54 36.43 169.56 o 20 9 0 401.37 354.85 147.93 o 0 10 0 43535.64 44161.75 195.70 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74.11 o 9 13 0 83.97 100.70 81.40 o 10 13 0 2097.10 2167.05 104.70 o 11 13 0 583.05 594.41 140.07 o 12 13 0 880.10 1003.78 127.66 o 13 13 0 59.04 104.71 127.95 o 14 13 0 23.72 65.20 166.01 o 16 13 0 280.66 273.83 158.41 o 17 13 0 0.25 19.63 195.84 o 18 13 0 403.78 458.94 164.98 o 19 13 0 13.02 82.32 182.78 o 0 14 0 1484.16 1449.97 60.69 o 1 14 0 38.65 39.35 40.88 o 2 14 0 392.86 344.55 41.46 o 3 14 0 213.80 182.98 43.05 o 4 14 0 885.63 870.74 48.70 o 5 14 0 53.87 41.79 52.04 o 6 14 0 673.56 682.92 57.82 o 7 14 0 2.95 26.42 65.76 o 8 14 0 99.50 102.77 77.13 o 9 14 0 12.64 78.26 89.72 o 10 14 0 17.96 63.50 103.57 o 11 14 0 102.16 92.89 103.20 o 12 14 0 0.14 66.72 170.55 o 13 14 0 36.80 71.52 183.84 o 14 14 0 41.61 77.36 256.41 o 15 14 0 1.20 88.39 174.84 o 16 14 0 0.35 86.95 156.63 o 17 14 0 136.07 165.07 221.32 o 18 14 0 1.63 -14.41 295.36 o 1 15 0 963.00 985.23 45.53 o 2 15 0 329.00 338.62 44.31 o 3 15 0 0.04 23.30 55.11 o 4 15 0 420.41 411.73 48.32 o 5 15 0 690.81 666.10 51.07 o 6 15 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19 0 877.21 751.46 82.69 o 6 19 0 334.58 275.74 80.09 o 7 19 0 1103.88 1030.79 109.56 o 8 19 0 82.24 53.76 109.56 o 9 19 0 43.21 142.70 135.56 o 10 19 0 156.71 170.81 112.23 o 11 19 0 21.73 14.89 118.17 o 12 19 0 2.46 91.76 140.23 o 13 19 0 322.80 199.98 155.53 o 14 19 0 5.84 67.36 167.75 o 15 19 0 1.84 89.08 163.46 o 16 19 0 29.88 90.34 188.50 o 0 20 0 1926.48 1901.26 114.74 o 1 20 0 509.05 511.78 80.35 o 2 20 0 1541.58 1411.28 98.64 o 3 20 0 318.37 333.18 95.02 o 4 20 0 379.00 331.10 96.78 o 5 20 0 267.05 202.35 94.09 o 6 20 0 494.30 588.41 98.15 o 7 20 0 71.20 83.66 172.24 o 8 20 0 504.63 557.44 126.45 o 9 20 0 428.63 441.24 135.71 o 10 20 0 209.42 228.66 145.43 o 11 20 0 714.95 511.96 149.37 o 12 20 0 11.88 58.51 154.58 o 13 20 0 102.87 131.21 151.87 o 14 20 0 21.65 -1.63 264.83 o 15 20 0 81.69 201.92 170.05 o 1 21 0 40.21 21.31 114.13 o 2 21 0 2179.95 1999.84 117.94 o 3 21 0 110.53 101.24 110.57 o 4 21 0 101.32 169.04 118.16 o 5 21 0 295.45 295.33 117.43 o 6 21 0 725.19 633.17 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