#------------------------------------------------------------------------------ #$Date: 2021-09-22 04:44:10 +0300 (Wed, 22 Sep 2021) $ #$Revision: 269238 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/10/88/2108858.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108858 loop_ _publ_author_name 'Gaydamaka, Anna A.' 'Arkhipov, Sergey G.' 'Boldyreva, Elena V.' _publ_section_title ; A new guaninate hydrate K^+^·C~5~H~4~N~5~O^{-^}·H~2~O: crystal structure from 100 to 300K in a comparison with 2Na^+^·C~5~H~3~N~5~O^2{-^}·7H~2~O ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first ; ; _journal_paper_doi 10.1107/S205252062100754X _journal_volume 77 _journal_year 2021 _chemical_formula_moiety 'C10 H12 K2 N10 O4' _chemical_formula_sum 'C10 H12 K2 N10 O4' _chemical_formula_weight 414.50 _chemical_name_common potassium{2-amino-6-oxo-1-hydro-purine-7(9)-ide/2-amino-6-oxo-7-hydro-purine-1(3)-ide}monohydrate _chemical_name_systematic potassium{2-amino-6-oxo-1-hydro-purine-7(9)-ide/2-amino-6-oxo-7-hydro-purine-1(3)-ide}monohydrate _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary direct _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 129.598(12) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 36.534(3) _cell_length_b 3.84179(16) _cell_length_c 28.656(2) _cell_measurement_reflns_used 7917 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 29.0600 _cell_measurement_theta_min 2.8410 _cell_volume 3099.1(6) _computing_cell_refinement 'CrysAlisPro (Rigaku Oxford Diffraction,2018)' _computing_data_collection 'CrysAlisPro (Rigaku Oxford Diffraction,2018)' _computing_data_reduction 'CrysAlisPro (Rigaku Oxford Diffraction,2018)' _computing_molecular_graphics 'Mercury (Macrae et al., 2020), Vesta(Momma,2011)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT-2018/3 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.357 _diffrn_detector_type Ruby _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.940 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Ruby, Gemini ultra' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0673 _diffrn_reflns_av_unetI/netI 0.0577 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.940 _diffrn_reflns_limit_h_max 50 _diffrn_reflns_limit_h_min -49 _diffrn_reflns_limit_k_max 5 _diffrn_reflns_limit_k_min -5 _diffrn_reflns_limit_l_max 39 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_number 26051 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.940 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.643 _diffrn_reflns_theta_min 2.230 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.658 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.74339 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.777 _exptl_crystal_description needle _exptl_crystal_F_000 1696 _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.03 _refine_diff_density_max 0.443 _refine_diff_density_min -0.395 _refine_diff_density_rms 0.082 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.913 _refine_ls_hydrogen_treatment refxyz _refine_ls_matrix_type full _refine_ls_number_parameters 271 _refine_ls_number_reflns 4123 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 0.913 _refine_ls_R_factor_all 0.0632 _refine_ls_R_factor_gt 0.0374 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0522P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0837 _refine_ls_wR_factor_ref 0.0891 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2877 _reflns_number_total 4123 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file xk5085sup1.cif _cod_data_source_block 150K _cod_original_cell_volume 3099.1(5) _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 2108858 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _oxdiff_exptl_absorpt_empirical_full_min 0.848 _oxdiff_exptl_absorpt_empirical_full_max 1.291 _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _shelx_res_file ; TITL 150K in C2/c 150K.res created by SHELXL-2018/3 at 15:34:33 on 01-Jul-2021 REM C2/c (#15 with fixed user cell (not necessary: std = user cell)!) CELL 0.71073 36.534144 3.841793 28.655934 90.0000 129.5976 90.0000 ZERR 8.00 0.002644 0.000157 0.002183 0.0000 0.0119 0.0000 LATT 7 SYMM -x, y,-z+1/2 SFAC C H N O K UNIT 80.00 96.00 80.00 32.00 16.00 L.S. 10 ACTA BOND CONF TEMP -123 BOND $H EQIV $1 x+1/2, -y+1/2, z+1/2 EQIV $2 -x+1/2, -y+1.5, -z+1 EQIV $3 x, y-1, z HTAB O2w N9a HTAB N7a O3w HTAB O3w N7b HTAB N2a N3b_$1 HTAB N1b O1a_$2 HTAB O3w N7b_$3 LIST 6 FMAP 2 PLAN 20 DANG H12 H11 1.52 0.005 SADI H11 O3w O3w H12 SADI H5 O2w O2w H6 MORE 3 WGHT 0.052200 FVAR 0.50422 K1 5 0.492949 0.145925 0.922203 11.00000 0.01811 0.02147 = 0.01893 -0.00296 0.01271 -0.00423 C8A 1 0.331386 0.048123 0.794319 11.00000 0.01931 0.04043 = 0.01990 0.00339 0.01294 0.00752 H1 2 0.310985 0.115661 0.805245 11.00000 -1.20000 C4A 1 0.386685 -0.147070 0.795924 11.00000 0.01332 0.02060 = 0.01269 -0.00057 0.00714 -0.00098 C5A 1 0.350462 -0.041681 0.737276 11.00000 0.01075 0.02026 = 0.01428 0.00001 0.00687 -0.00002 C6A 1 0.355668 -0.067238 0.692583 11.00000 0.01063 0.01364 = 0.01310 -0.00032 0.00510 -0.00281 C2A 1 0.430196 -0.307866 0.770462 11.00000 0.01096 0.01360 = 0.01382 -0.00093 0.00650 -0.00228 N9A 3 0.374383 -0.089903 0.831754 11.00000 0.01718 0.03678 = 0.01577 0.00309 0.01091 0.00658 N7A 3 0.315201 0.084546 0.737400 11.00000 0.01257 0.03068 = 0.01460 0.00417 0.00664 0.00651 H2 2 0.288080 0.156862 0.707333 11.00000 -1.20000 N1A 3 0.397061 -0.213537 0.711978 11.00000 0.01166 0.01912 = 0.01186 0.00052 0.00682 -0.00087 N3A 3 0.428767 -0.283588 0.815495 11.00000 0.01098 0.02185 = 0.01156 0.00064 0.00560 0.00088 N2A 3 0.471692 -0.427812 0.784412 11.00000 0.01198 0.02444 = 0.01094 0.00148 0.00624 0.00388 H3 2 0.491078 -0.532226 0.820740 11.00000 -1.20000 H4 2 0.467830 -0.533906 0.756185 11.00000 -1.20000 O1A 4 0.325260 0.034808 0.638022 11.00000 0.01300 0.02111 = 0.01218 0.00236 0.00497 0.00073 O2W 4 0.452716 -0.345574 0.945844 11.00000 0.01364 0.02950 = 0.01477 0.00526 0.00837 0.00044 H5 2 0.427237 -0.297915 0.913461 11.00000 -1.20000 H6 2 0.445016 -0.437868 0.963420 11.00000 -1.20000 K2 5 0.262424 0.524267 0.571264 11.00000 0.01360 0.01889 = 0.01590 0.00181 0.00738 0.00080 C8B 1 0.119683 0.739883 0.542166 11.00000 0.01801 0.01983 = 0.01566 0.00154 0.01112 -0.00113 H7 2 0.121453 0.639740 0.572153 11.00000 -1.20000 C4B 1 0.091104 0.999350 0.460126 11.00000 0.01196 0.01512 = 0.01142 -0.00368 0.00683 -0.00194 C5B 1 0.139233 0.935581 0.491700 11.00000 0.01057 0.01549 = 0.01104 -0.00039 0.00522 0.00050 C6B 1 0.160936 1.047821 0.467761 11.00000 0.01142 0.01456 = 0.01280 -0.00373 0.00640 -0.00160 C2B 1 0.082077 1.270964 0.383855 11.00000 0.01050 0.01429 = 0.01170 -0.00463 0.00633 -0.00145 N7B 3 0.157768 0.769682 0.545558 11.00000 0.01430 0.01939 = 0.01227 0.00127 0.00674 0.00024 N9B 3 0.078210 0.870972 0.491878 11.00000 0.01528 0.01686 = 0.01492 0.00078 0.01025 -0.00116 N3B 3 0.061401 1.168280 0.405731 11.00000 0.00999 0.01617 = 0.01095 -0.00197 0.00601 -0.00127 N1B 3 0.129202 1.212281 0.412166 11.00000 0.01032 0.01785 = 0.01258 0.00065 0.00795 -0.00089 H8 2 0.139928 1.294062 0.395425 11.00000 -1.20000 N2B 3 0.056806 1.431210 0.329528 11.00000 0.00971 0.02265 = 0.01516 0.00547 0.00827 0.00299 H9 2 0.031957 1.522929 0.317324 11.00000 -1.20000 H10 2 0.072422 1.539794 0.319647 11.00000 -1.20000 O1B 4 0.203517 1.018791 0.490365 11.00000 0.00812 0.02448 = 0.01533 0.00231 0.00580 0.00239 O3W 4 0.225305 0.296347 0.631282 11.00000 0.01679 0.02451 = 0.02321 0.00210 0.00347 0.00346 H11 2 0.205773 0.485102 0.607907 11.00000 -1.20000 H12 2 0.209665 0.091547 0.611771 11.00000 -1.20000 HKLF 4 REM 150K in C2/c REM wR2 = 0.0891, GooF = S = 0.913, Restrained GooF = 0.913 for all data REM R1 = 0.0374 for 2877 Fo > 4sig(Fo) and 0.0632 for all 4123 data REM 271 parameters refined using 3 restraints END WGHT 0.0514 0.0000 REM Highest difference peak 0.443, deepest hole -0.395, 1-sigma level 0.082 Q1 1 0.3767 -0.0079 0.7693 11.00000 0.05 0.44 Q2 1 0.1169 1.0016 0.4796 11.00000 0.05 0.41 Q3 1 0.1443 0.8805 0.4715 11.00000 0.05 0.40 Q4 1 0.2203 0.9416 0.5209 11.00000 0.05 0.35 Q5 1 0.2497 0.7980 0.5605 11.00000 0.05 0.35 Q6 1 0.1483 0.8812 0.5173 11.00000 0.05 0.34 Q7 1 0.5176 0.0329 0.9591 11.00000 0.05 0.33 Q8 1 0.3634 -0.1391 0.7606 11.00000 0.05 0.33 Q9 1 0.0624 1.0040 0.4196 11.00000 0.05 0.32 Q10 1 0.3286 -0.0209 0.7282 11.00000 0.05 0.32 Q11 1 0.0411 1.0719 0.3793 11.00000 0.05 0.31 Q12 1 0.0655 1.2441 0.3918 11.00000 0.05 0.31 Q13 1 0.0610 1.2334 0.4206 11.00000 0.05 0.31 Q14 1 0.0617 0.8386 0.4968 11.00000 0.05 0.30 Q15 1 0.2937 0.5426 0.6090 11.00000 0.05 0.30 Q16 1 0.1438 0.6001 0.5390 11.00000 0.05 0.29 Q17 1 0.4461 -0.3894 0.7689 11.00000 0.05 0.29 Q18 1 0.5015 0.3132 0.9494 11.00000 0.05 0.28 Q19 1 0.2644 0.3318 0.5911 11.00000 0.05 0.28 Q20 1 0.1073 1.2198 0.3988 11.00000 0.05 0.28 ; _shelx_res_checksum 71600 _shelx_hkl_file ; 0 0 3-2.18066 26.0760 2 0 0 -3 2.80416 14.8078 6 0 0 3 13.2858 21.1046 1 0 0 3 0.35620 14.6026 6 0 0 4 3405.69 49.1435 6 0 0 4 3497.36 63.4485 1 0 0 4 3504.48 70.0383 2 0 0 -4 3568.63 61.4552 3 0 0 -4 3424.08 48.9727 6 0 0 -5-6.88319 29.8113 3 0 0 -5-5.79847 24.0810 6 0 0 5-9.65703 42.1986 2 0 0 5 9.93850 34.8212 1 0 0 -5-3.20936 37.1188 7 0 0 5-5.81288 23.0009 6 0 0 -5 1.57690 28.5580 1 0 0 6 5714.97 75.6193 6 0 0 -6 5365.12 96.9385 7 0 0 6 5558.92 95.8264 1 0 0 6 5734.20 106.381 2 0 0 -6 5585.24 74.9194 6 0 0 -6 5768.87 94.0558 1 0 0 -6 5985.65 94.0644 3 0 0 -7 1.38019 32.0113 1 0 0 7-4.96368 52.2181 2 0 0 -7-4.40947 33.3957 3 0 0 -7 5.83244 45.7349 7 0 0 7-6.37310 26.9927 6 0 0 -7 2.83076 28.2165 6 0 0 7-2.67374 41.3765 1 0 0 -8 8987.36 141.666 7 0 0 8 9363.47 138.708 1 0 0 8 9047.61 150.793 2 0 0 8 9242.40 109.606 6 0 0 -8 9383.68 136.227 1 0 0 -8 9282.16 131.701 3 0 0 -8 8993.83 141.095 2 0 0 -8 9034.43 108.075 6 0 0 -9 1.59623 51.3082 7 0 0 9 8.92601 28.9872 6 0 0 -9 5.42094 44.7336 2 0 0 -9-3.30474 34.8553 1 0 0 -9 2.44508 30.2730 3 0 0 -9 7.13715 31.9770 6 0 0 9 61.2894 44.1766 1 0 0 9 5.44860 56.4833 2 0 0 -10 799.010 64.7599 2 0 0 -10 717.638 66.8382 7 0 0 -10 816.392 53.8002 3 0 0 -10 847.264 58.1710 1 0 0 -10 743.656 46.0769 6 0 0 10 775.961 44.3772 6 0 0 10 842.991 75.4035 2 0 0 10 752.629 60.8210 1 0 0 -11 2.07720 37.4626 3 0 0 -11 13.3834 33.8121 6 0 0 -11-2.64523 38.5102 1 0 0 -11 10.5298 52.5905 7 0 0 11 5.90861 44.3957 1 0 0 11-3.43234 61.1475 2 0 0 -11-7.47518 49.1908 2 0 0 11 25.7497 26.8561 6 0 0 -12 1086.45 77.5892 7 0 0 -12 1095.57 76.1648 2 0 0 12 1027.97 69.6446 1 0 0 -12 1027.66 54.5702 6 0 0 -12 1052.56 64.7064 3 0 0 12 947.295 50.5142 6 0 0 12 1012.11 85.6027 2 0 0 -12 1095.52 68.2403 1 0 0 -13-4.24348 34.9407 6 0 0 13-18.4631 27.8088 6 0 0 13 38.4506 62.1141 2 0 0 -13 24.1873 53.3550 7 0 0 13-20.0907 44.1431 1 0 0 -13-2.04735 49.3169 2 0 0 -13 17.7616 35.8353 3 0 0 -13-16.0108 40.6790 1 0 0 14 4749.96 107.912 6 0 0 -14 4603.09 140.989 2 0 0 -14 4954.92 142.283 7 0 0 14 4500.65 129.660 1 0 0 -14 4701.24 106.674 6 0 0 14 4792.58 153.237 2 0 0 -14 4876.13 134.284 1 0 0 -15 1.35357 35.6256 6 0 0 -15 7.33512 52.0337 2 0 0 15 3.10409 65.4073 2 0 0 -15 12.1855 43.3263 1 0 0 -15 6.41771 39.3282 3 0 0 15 17.7108 31.0925 6 0 0 -15-13.1980 57.5804 7 0 0 -16 634.267 65.5403 1 0 0 -16 613.748 53.7547 6 0 0 -16 662.227 77.2385 2 0 0 16 651.882 51.2757 6 0 0 -16 650.402 75.6642 7 0 0 16 655.380 88.6854 2 0 0 -16 746.401 66.5145 3 0 0 -17 34.1441 36.5246 6 0 0 17 0.80052 29.1954 6 0 0 -17 4.18168 44.3992 3 0 0 17 44.0282 71.2361 2 0 0 -17 7.81714 58.3393 7 0 0 -17-20.5127 58.5899 2 0 0 -17-14.2413 45.9453 1 0 0 -18 430.753 52.7229 6 0 0 18-6.47700 30.9764 6 0 0 -18 431.812 64.9191 1 0 0 -18 476.491 63.7348 3 0 0 -18 445.003 74.6328 7 0 0 18 421.129 87.1521 2 0 0 19 15.6815 37.6168 6 0 0 -19-5.28535 60.3765 7 0 0 19-14.3533 74.5406 2 0 0 -19 1.92402 46.2066 3 0 0 20 1139.39 115.496 2 0 0 -20 1218.18 101.429 7 0 0 20 1051.97 70.5733 6 0 0 21 3.77436 41.4055 6 0 0 21 50.8346 80.8247 2 0 0 -21 29.0340 65.8906 7 0 0 22 127.667 43.4904 6 0 0 22 132.674 85.6241 2 0 0 -22 128.922 68.5133 7 0 0 -23 35.7009 71.6801 7 0 0 23 50.2278 86.8032 2 0 0 -24 1571.78 120.937 7 0 0 24 1651.77 142.559 2 0 0 25-26.6525 97.8899 2 0 0 -25 16.0380 74.2831 7 0 0 26 707.559 122.264 2 0 0 -26 581.663 93.8298 7 0 0 27-45.6487 104.019 2 0 0 -27 4.37075 73.1974 7 0 0 -28 411.051 100.945 7 0 0 28 341.755 116.621 2 0 0 -29 5.37714 81.8266 7 0 -2 0 1319.06 77.5942 1 0 2 0 1353.43 52.6426 2 0 2 0 1286.59 79.4621 6 0 -2 0 1349.22 76.8955 6 0 2 -1 1036.08 72.6684 6 0 2 1 933.862 35.5543 4 0 2 1 1013.27 53.5595 2 0 2 1 993.892 73.7762 6 0 -2 -1 1016.42 70.0149 6 0 -2 -1 975.709 39.7647 5 0 -2 1 924.806 75.3333 1 0 -2 -1 1004.34 75.4082 1 0 -2 1 914.286 68.6567 6 0 2 2 87.0291 45.9025 6 0 -2 -2 80.0746 44.3394 6 0 2 2 123.989 44.1167 2 0 2 -2 92.3683 58.3793 6 0 -2 -2 127.469 50.8444 1 0 2 -2 104.913 16.5579 5 0 -2 2 128.115 52.9931 1 0 -2 -2 109.213 28.3651 5 0 2 2 58.1092 20.0481 4 0 2 -2-3.09088 32.7512 1 0 -2 2 75.8527 47.1007 6 0 -2 -3 1641.89 87.4077 7 0 -2 -3 1613.36 79.1781 6 0 -2 3 1656.60 87.0771 1 0 2 -3 1248.52 35.4910 5 0 2 3 1410.39 41.5388 4 0 2 3 1572.83 78.3220 6 0 -2 -3 1515.21 56.4668 5 0 2 3 1594.47 72.2274 2 0 2 -3 1641.23 88.1668 6 0 2 4 1781.11 48.1162 4 0 -2 -4 1779.37 90.7977 7 0 -2 -4 1669.93 64.4429 5 0 2 4 1875.05 79.7657 6 0 2 -4 2044.25 97.6555 6 0 2 -4 1425.51 36.3004 2 0 -2 -4 1928.56 83.6779 6 0 2 4 824.123 57.7459 7 0 2 4 1901.25 81.7740 2 0 -2 4 1724.31 91.1464 1 0 2 5 3358.58 106.136 7 0 2 -5 2739.60 49.8522 2 0 -2 5 3251.48 115.958 1 0 2 5 3266.76 98.9099 6 0 2 5 3124.40 100.548 2 0 -2 -5 3159.01 69.0973 4 0 -2 -5 3113.31 113.043 7 0 2 -5 3440.57 120.812 6 0 -2 6 786.576 71.9702 1 0 2 6 802.642 55.8765 6 0 2 -6 739.037 33.3282 2 0 2 6 816.258 72.0831 2 0 -2 -6 782.467 43.4984 4 0 2 -6 843.068 73.2207 6 0 -2 -6 881.238 75.1486 7 0 -2 6 5.99060 33.5162 6 0 2 6 736.761 61.4253 7 0 2 -7 7.28173 23.2742 2 0 -2 7 14.2791 38.1568 6 0 -2 -7-12.6188 52.8158 7 0 -2 -7 2.10816 28.3307 4 0 -2 -7-1.27671 42.0421 8 0 2 7 45.7430 41.0440 7 0 2 -7 6.46846 37.2792 1 0 2 7-27.1454 53.4670 2 0 2 -7-8.50494 54.2780 6 0 2 7 42.7501 33.1132 6 0 -2 7 3.75438 47.4439 1 0 2 -8-6.26609 51.0613 6 0 -2 -8 10.8623 29.8294 4 0 2 8-2.78821 31.1201 6 0 -2 -8 14.1489 43.2761 8 0 -2 -8 7.42637 52.4626 7 0 -2 8 1.40655 43.0353 6 0 2 -8 11.1754 25.2635 2 0 2 8-3.69808 59.1528 2 0 -2 8 20.1771 53.8407 1 0 2 8-15.8024 40.2474 7 0 2 -8-11.6839 41.7424 1 0 2 -9 300.559 34.1779 2 0 -2 -9 344.508 53.5928 8 0 -2 -9 356.127 64.7644 7 0 -2 -9 351.320 42.7863 4 0 2 -9 360.951 57.6490 1 0 2 9 329.800 42.4356 6 0 2 9 317.849 51.5899 7 0 2 -9 380.592 65.8027 6 0 -2 9 272.446 54.1649 6 0 2 9 318.404 67.8529 2 0 -2 9 350.932 64.6100 1 0 2 -10 248.686 60.6957 6 0 -2 -10 187.714 59.6254 7 0 2 10 311.005 52.4876 7 0 -2 10 316.296 61.1852 1 0 2 -10 232.753 55.0902 1 0 -2 -10 348.976 52.8689 8 0 2 10 323.717 72.2277 2 0 2 10 288.642 40.5330 6 0 2 -10 301.842 37.5812 2 0 -2 -10 280.617 44.4413 4 0 -2 10 301.345 56.5705 6 0 -2 -11 2193.24 95.8370 8 0 2 11 2011.02 94.1645 7 0 -2 11 1766.02 69.1138 3 0 2 -11 2298.55 111.113 1 0 2 11 2297.08 122.327 2 0 -2 11 2117.38 102.548 6 0 -2 11 2015.89 104.045 1 0 2 -11 1739.42 67.9059 2 0 2 11 1979.90 77.1430 6 0 -2 -11 2017.62 85.0462 4 0 2 -11 2153.85 107.267 6 0 -2 -11 2039.79 103.663 7 0 -2 -12 1285.22 91.3829 7 0 2 12 1284.18 82.3438 7 0 2 12 1381.32 67.4156 6 0 -2 -12 1339.32 77.4447 4 0 2 -12 1335.01 94.5674 1 0 -2 12 1241.61 88.7548 6 0 -2 -12 1431.86 80.4451 8 0 2 -12 1236.26 93.3060 6 0 2 12 1257.33 103.890 2 0 -2 12 1200.16 62.0322 3 0 2 -12 1313.63 64.9253 2 0 -2 12 1352.23 91.6760 1 0 -2 -13 122.861 46.1734 8 0 2 13 139.649 76.7853 2 0 -2 -13 100.519 59.2818 7 0 2 -13 145.981 58.3502 6 0 -2 -13 149.144 46.7412 4 0 -2 13 100.312 49.3343 6 0 2 13 134.958 34.0602 6 0 2 -13 131.333 42.7040 2 0 -2 13 163.785 60.5997 1 0 2 13 95.7732 50.7757 7 0 -2 13 148.747 39.2789 3 0 -2 -14 1071.44 73.7947 8 0 -2 14 925.868 55.6952 8 0 2 14 1238.08 112.218 2 0 -2 -14 1079.41 90.5707 7 0 2 -14 1102.83 68.9218 2 0 2 -14 1051.92 86.4715 6 0 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129.068 7 2 -2 -7 5242.96 141.319 7 2 2 -7 5066.06 145.113 6 -2 2 7 5383.09 138.821 2 2 2 -7 4604.89 51.3390 2 -2 2 7 4933.07 121.031 6 2 -2 -6-31.2476 41.6495 8 -2 -2 6 18.8325 51.5010 1 2 2 -6 22.4721 49.3754 6 -2 2 6 22.5305 54.7091 2 2 -2 -6 8.77106 52.9302 7 -2 2 6 3.25465 34.4300 7 2 2 -6-6.39744 32.6257 1 2 -2 -6 29.3734 22.5021 4 -2 2 6 11.1444 37.3604 6 2 2 -5 1756.17 91.4115 6 -2 -2 5 1541.25 88.6756 1 2 -2 -5 1747.64 92.3797 7 -2 2 5 1619.28 80.0583 6 -2 2 5 1741.19 84.3623 2 2 -2 -5 1850.12 86.9114 8 2 -2 -4 600.843 69.2370 7 -2 2 4 587.665 62.3013 2 2 -2 -4 610.015 38.9028 5 -2 2 4 606.533 61.0030 6 2 -2 -4 654.461 58.7215 6 2 2 -4 723.320 72.0380 6 2 2 -4 612.867 34.3601 5 -2 -2 4 595.969 67.8400 1 2 2 -4-14.4266 37.4519 1 -2 -2 4 657.477 63.2944 6 2 -2 -3 1224.48 42.3128 5 2 2 -3 1255.45 42.4592 5 -2 2 3 1427.84 81.8502 6 2 -2 -3 1333.39 84.6854 7 2 2 -3 1403.26 82.2374 6 -2 -2 3 1201.73 76.1945 6 2 -2 -3 1283.79 81.4498 1 -2 -2 3 1338.40 80.7240 1 2 -2 -3 1415.43 76.4373 6 -2 2 2 2910.69 41.7561 4 2 -2 -2 4409.20 123.289 6 2 -2 -2 4115.82 57.5705 5 -2 2 2 4412.37 123.126 6 2 2 -2 3814.73 67.9852 5 2 -2 -2 4339.38 125.849 1 2 2 -2 4291.10 125.940 6 2 2 -2 3690.01 53.1470 2 -2 -2 2 4247.57 119.691 6 -2 -2 2 4452.86 123.837 1 -2 2 1 1003.79 73.9301 6 -2 -2 1 917.496 66.3575 6 2 -2 -1 916.389 69.5008 6 2 2 -1 891.589 43.7588 4 2 -2 -1 1012.20 72.5416 1 2 2 -1 996.837 69.4129 6 -2 -2 1 819.943 72.0612 1 2 2 -1 911.191 39.2719 2 2 2 0 7529.02 152.979 6 -2 -2 0 7151.40 148.366 6 2 -2 0 7698.29 158.940 6 2 2 0 6801.52 97.8300 4 -2 -2 0 7628.60 154.437 1 2 2 0 6895.07 97.3757 2 -2 2 0 7409.66 158.975 6 2 -2 0 7406.15 161.116 1 -2 -2 0 7062.41 101.766 5 2 2 1 922.600 64.2726 6 -2 2 -1 854.697 76.4754 6 2 -2 1 901.641 72.8222 1 2 2 1 837.210 39.9513 4 -2 -2 -1 876.026 47.1963 5 2 2 1-41.9600 35.6162 7 2 2 1 809.129 51.3956 2 -2 -2 -1 809.962 70.1781 1 -2 -2 -1 867.278 63.8895 6 -2 -2 -2 61.2372 42.5622 6 2 2 2 60.3500 24.2600 4 -2 2 -2 67.3749 52.9817 6 2 2 2 8.38007 34.6987 7 2 2 2 79.9899 42.6870 2 2 -2 2 66.3404 52.8594 1 2 2 2 60.6280 41.1012 6 -2 -2 -2 52.6760 33.8120 5 -2 -2 -2 55.7618 47.0110 1 -2 -2 -3 1223.33 69.3591 6 2 2 3 1181.03 65.8399 6 2 2 3 386.015 48.2235 7 -2 2 -3 1435.41 85.4314 6 -2 -2 -3 1360.57 82.3167 7 2 -2 3 1402.93 85.9036 1 2 2 3 1333.64 69.1860 2 2 2 3 1251.97 47.8391 4 -2 -2 -3 1263.82 61.4962 5 -2 2 -4 77.0115 26.5887 2 -2 -2 -4 72.6928 55.5318 7 -2 2 -4 85.5326 54.0333 6 2 2 4 123.681 27.4317 4 2 2 4 73.1181 48.2706 2 -2 -2 -4 99.1481 41.2938 5 -2 -2 -4 106.118 40.4359 6 -2 -2 -4 124.580 32.9610 4 2 2 4 132.703 37.6365 6 2 2 4 68.3585 41.7112 7 2 -2 4 88.0193 55.1835 1 2 2 5 22.8498 32.4374 6 2 2 5 50.1633 26.9752 4 -2 -2 -5 41.6243 52.8237 7 -2 2 -5 87.6338 55.9347 6 2 2 5 45.0070 40.1077 7 2 -2 5 67.0905 52.7914 1 2 -2 5-0.84302 36.0271 6 -2 -2 -5 36.8934 31.2904 4 -2 -2 -5 43.2997 42.0428 5 -2 2 -5 7.70835 26.0580 2 2 2 5 55.8989 50.3576 2 -2 2 -6 8739.03 183.664 6 2 -2 6 8621.87 181.156 6 -2 -2 -6 8183.14 172.434 7 2 2 6 8147.35 162.048 7 2 2 6 8336.72 166.933 2 2 2 6 8185.02 130.721 4 2 -2 6 8724.76 184.085 1 2 2 6 7574.96 137.620 6 -2 -2 -6 7966.21 130.516 4 -2 2 -6 9246.76 189.081 1 -2 2 -6 7492.46 107.709 2 -2 2 -7 1177.11 52.8805 2 -2 -2 -7 1327.47 84.9821 7 2 2 7 1099.21 59.6557 6 -2 -2 -7 1213.60 62.0642 4 2 2 7 1179.94 86.6928 2 2 -2 7 1285.48 83.4146 1 -2 2 -7 1264.18 87.9218 6 -2 2 -7 1389.45 86.3849 1 2 2 7 1252.45 73.8293 7 2 -2 7 1228.75 78.8828 6 -2 -2 -8 6916.52 164.375 7 -2 -2 -8 6811.61 137.107 4 2 2 8 6735.12 152.249 7 2 -2 8 5672.76 129.029 8 2 -2 8 6439.19 169.407 1 -2 2 -8 6630.46 169.000 6 2 -2 8 7025.08 169.453 6 -2 2 -8 7279.80 175.805 1 2 2 8 6899.92 172.878 2 2 2 8 6536.33 126.162 6 -2 2 -8 6285.32 110.588 2 2 2 9 139.403 45.8262 7 2 2 9 154.799 67.6864 2 -2 -2 -9 159.798 44.8067 8 -2 -2 -9 115.038 55.3328 7 2 2 9 114.497 32.8238 6 2 -2 9 203.693 59.0722 1 2 -2 9 180.979 51.6784 6 -2 2 -9 187.959 51.6544 1 2 -2 9 149.759 40.1394 8 -2 2 -9 149.520 36.6872 2 -2 -2 -9 198.496 44.2035 4 -2 2 -9 176.953 55.4566 6 2 -2 10 31.0317 32.9440 8 2 -2 10 22.8500 49.6806 1 -2 -2 -10 51.0692 53.4342 7 2 -2 10 20.2067 43.8288 6 -2 -2 -10 41.1854 39.9775 4 2 2 10 63.4506 41.2447 7 -2 2 -10 15.6101 54.9440 6 -2 2 -10 22.0122 33.9497 2 -2 -2 -10 69.7427 43.7113 8 -2 2 -10 36.2571 51.1439 1 2 2 10 30.4997 28.7109 6 2 2 10 51.1578 69.7029 2 -2 -2 -11 317.061 52.9190 4 2 -2 11 278.869 44.3528 3 2 2 11 286.791 79.1332 2 -2 2 -11 264.940 45.1687 2 -2 2 -11 368.431 62.5930 1 -2 2 -11 246.374 59.5293 6 2 -2 11 281.214 40.3785 8 -2 -2 -11 281.490 62.5697 7 2 -2 11 267.408 59.0842 6 2 -2 11 373.032 63.4885 1 2 2 11 345.677 54.7075 7 -2 -2 -11 335.837 53.6425 8 2 2 11 275.844 37.4612 6 -2 2 -12 1859.93 107.751 6 2 -2 12 1882.54 80.2874 3 2 -2 12 2087.81 105.618 6 2 -2 12 1747.00 73.0362 8 2 2 12 2110.57 101.130 7 2 2 12 2030.08 122.847 2 -2 -2 -12 2169.18 97.5025 4 -2 2 -12 1873.25 82.2419 2 2 -2 12 2126.30 111.531 1 2 2 12 1854.10 71.8597 6 -2 -2 -12 1938.66 105.520 7 -2 -2 -12 2069.61 94.7522 8 2 2 13 186.507 35.3556 6 2 -2 13 179.466 43.7340 3 -2 2 -13 277.270 61.9995 6 -2 -2 -13 278.021 52.0217 8 -2 -2 -13 186.948 65.1535 7 2 2 13 222.944 79.1691 2 2 -2 13 210.244 65.7792 1 2 -2 13 157.877 35.9059 8 -2 -2 -13 246.861 53.5379 4 -2 2 -13 252.682 48.7594 2 -2 -2 -14 2000.10 112.177 7 2 -2 14 1591.42 67.8175 8 -2 2 -14 1621.42 105.223 6 -2 -2 -14 1922.73 101.020 4 -2 2 -14 1738.39 87.1025 2 -2 -2 -14 1930.31 93.2798 8 2 2 14 1814.42 70.4582 6 2 2 14 1852.40 134.243 2 2 -2 14 1881.01 109.968 1 2 -2 14 1779.96 82.8711 3 -2 -2 -15-23.0974 61.9105 7 -2 -2 -15 14.0697 49.9890 4 -2 2 -15 41.0640 52.7271 6 2 2 15 14.7153 23.7528 6 2 -2 15 18.8483 54.7631 1 2 2 15 35.2370 29.0823 6 2 -2 15 25.7317 42.8674 3 -2 -2 -15 24.4341 44.3793 8 2 -2 15 25.2866 28.4053 8 -2 2 -15 28.8489 44.4247 2 2 2 15 38.9978 84.5542 2 -2 2 -16 1218.58 84.6930 2 -2 -2 -16 1259.85 99.7759 7 2 2 16 1155.35 59.6277 6 2 -2 16 887.521 49.8086 8 -2 -2 -16 1211.52 78.3031 8 2 -2 16 1259.96 77.8910 3 -2 2 -16 1053.82 92.7994 6 2 -2 16 1190.17 96.9443 1 2 2 16 1209.57 59.5545 6 -2 -2 -16 1245.78 91.5159 4 2 2 16 1410.48 128.145 2 -2 -2 -17-0.41305 43.2319 8 -2 2 -17 41.4156 60.0326 6 2 -2 17-8.89177 48.5371 2 2 2 17 46.2142 94.4993 2 2 -2 17 18.9426 45.3750 3 -2 -2 -17-19.2203 64.5855 7 2 2 17 26.3113 25.7432 6 2 -2 17 10.2117 24.4951 8 2 -2 17 23.7372 63.1567 1 2 -2 17 6.75391 22.7761 8 2 2 17 37.9501 28.7600 6 -2 2 -17-32.1291 54.5527 2 2 -2 18 417.244 31.6598 8 -2 -2 -18 811.453 93.4622 7 2 -2 18 942.052 80.9082 2 2 2 18 823.755 124.976 2 -2 2 -18 958.721 85.1731 2 2 -2 18 898.936 91.2123 1 -2 -2 -18 923.200 71.7689 8 -2 2 -18 962.369 88.2391 6 2 2 18 918.224 54.3516 6 2 -2 19 25.0395 54.0385 2 -2 2 -19 56.8958 58.4447 6 2 2 19 45.3850 28.5266 6 2 -2 19 38.0758 62.6989 1 -2 -2 -19 65.6449 65.2755 7 2 2 19 29.0161 96.9221 2 2 2 20 82.6671 103.842 2 2 -2 20 145.855 61.3932 2 -2 2 -20 134.332 66.9307 6 -2 -2 -20 216.480 75.8007 7 2 -2 20 186.393 74.9071 1 2 -2 21 53.7501 71.0244 1 2 -2 21 98.1925 62.1777 2 -2 -2 -21 103.519 73.8186 7 2 2 21 162.158 108.663 2 -2 2 -21 65.8463 57.9479 6 -2 -2 -22 1063.98 112.103 7 2 2 22 944.333 144.064 2 -2 2 -22 712.118 86.0565 6 2 -2 22 755.855 90.1579 2 2 -2 22 861.016 103.565 1 2 2 23 137.956 110.137 2 2 -2 23 99.8939 62.9453 2 -2 -2 -23 101.610 77.2817 7 2 -2 23 85.8313 69.7181 1 -2 2 -23 101.179 64.6862 6 2 -2 24 139.584 62.2671 2 2 2 24 191.134 123.446 2 -2 -2 -24 113.447 86.7004 7 -2 2 -24 81.6255 61.3618 6 2 -2 24 102.447 74.0350 1 -2 2 -25-8.51493 60.6652 6 2 -2 25-22.0294 76.0274 1 -2 -2 -25 7.97122 82.1324 7 2 -2 25 8.02296 70.6664 2 -2 2 -26 289.541 94.5250 7 2 -2 26 185.224 77.8166 2 -2 2 -26 237.464 75.6292 6 -2 -2 -26 508.744 100.747 7 -2 4 20 169.939 109.030 2 -2 4 19 94.0500 100.657 2 -2 4 18 145.062 104.521 2 2 4 -17 465.099 101.558 6 -2 4 17 293.202 105.848 2 2 -4 -17 446.897 104.626 7 2 -4 -16 372.346 100.145 7 2 4 -16 559.955 107.033 6 -2 -4 16 450.544 98.7890 1 -2 4 16 332.899 103.360 2 -2 4 16 431.665 69.1854 6 2 -4 -15 135.702 90.7722 7 -2 4 15 81.0107 47.7149 6 2 4 -15 67.1106 80.9586 6 -2 4 15 111.565 97.5469 2 -2 -4 15 139.182 83.2844 1 2 4 -14 1675.88 140.716 6 -2 -4 14 1607.48 136.758 1 2 -4 -14 1668.71 142.513 7 -2 4 14 1136.43 125.157 2 -2 4 14 1311.68 100.449 6 2 -4 -13 1053.19 116.322 1 -2 4 13 920.512 116.985 2 -2 -4 13 1151.51 118.427 1 -2 4 13 1037.24 93.4473 6 2 4 -13 1499.79 136.276 6 2 -4 -13 1326.69 128.368 7 2 -4 -12 355.125 95.3572 1 -2 4 12 311.970 83.0408 2 -2 4 12 347.376 69.2055 6 2 -4 -12 544.900 98.7442 7 2 4 -12 474.078 97.8160 6 -2 -4 12 454.039 93.5050 1 -2 -4 11 1074.60 112.616 1 -2 4 11 963.848 91.9209 6 -2 4 11 817.872 98.5211 2 2 -4 -11 879.247 106.973 1 2 4 -11 1130.40 117.905 6 2 -4 -10-4.95300 74.4214 1 -2 4 10 9.59219 67.5841 2 -2 -4 10 17.1937 69.5136 1 -2 4 10-68.5642 54.7170 6 2 4 -10 54.1213 76.7042 6 -2 4 9 52.3629 60.5223 6 -2 4 9 49.5805 60.6223 2 2 -4 -9 0.13583 70.5296 1 -2 -4 9 23.6379 72.8876 1 2 4 -9 31.4039 73.5248 6 -2 4 8 1023.28 99.1350 6 -2 -4 8 926.059 108.479 1 2 4 -8 1168.73 119.785 6 -2 4 8 778.322 85.3566 2 2 -4 -8 1060.26 110.382 1 2 -4 -7 42.0270 75.1116 1 -2 -4 7 61.9548 75.6827 1 2 4 -7 52.6684 68.9452 6 -2 4 7 58.7172 57.7874 6 -2 4 7 64.0506 56.8974 2 -2 4 6 603.438 70.3090 2 2 -4 -6 788.330 102.881 1 -2 4 6 800.028 93.0171 6 -2 -4 6 902.467 102.490 1 2 4 -6 933.073 104.882 6 -2 4 5 346.068 57.1545 2 2 4 -5 527.234 91.3434 6 -2 -4 5 446.428 83.3661 1 2 4 -5 125.714 38.5898 4 2 -4 -5 374.216 91.9977 1 -2 4 5 445.929 80.5232 6 2 -4 -4 34.7684 76.3490 1 -2 4 4 66.4611 64.8400 6 -2 4 4 3.51159 45.4433 2 2 4 -4 20.4207 76.6336 6 -2 -4 4 49.7422 71.3723 1 2 4 -4-2.73051 30.5504 4 2 4 -3 972.535 107.042 6 2 4 -3 389.353 39.9440 4 -2 -4 3 985.544 106.949 1 -2 4 3 634.117 57.3133 2 2 -4 -3 1097.01 113.029 1 -2 4 3 976.585 102.371 6 -2 4 2 2122.82 134.128 6 -2 -4 2 1923.83 134.544 1 2 4 -2 2153.26 134.045 6 -2 4 2 1417.39 66.9268 2 2 -4 -2 2092.71 140.459 1 -2 -4 1 19.6807 73.8139 1 -2 4 1 4.09909 32.4269 2 -2 4 1 31.6689 69.6089 6 2 4 -1 0.71154 65.8992 6 2 -4 -1 24.7364 76.2714 1 2 -4 0 2294.90 145.495 1 -2 4 0 2292.12 143.972 6 2 4 0 2705.78 143.793 6 -2 -4 0 2265.86 143.573 1 2 4 1 711.798 90.7035 6 -2 4 -1 661.967 101.207 6 -2 -4 -1 539.260 91.9982 1 2 -4 1 679.883 99.8431 1 2 4 2 410.898 77.5665 6 -2 4 -2 571.518 93.6153 6 2 -4 2 316.777 83.4202 1 -2 -4 -2 382.295 81.3491 1 2 4 2 246.912 46.1770 2 -2 4 -3 565.900 97.1862 6 2 4 3 292.164 52.9531 2 2 -4 3 482.691 91.7253 1 2 4 3 497.801 77.3282 6 -2 -4 -3 453.796 83.9901 1 2 -4 4 130.107 70.4809 1 -2 -4 -4 56.2824 67.0724 1 2 4 4 46.2153 48.1023 2 2 4 4 100.273 61.2244 6 -2 4 -4 53.8995 73.3695 6 -2 -4 -5 36.3776 69.8863 1 2 -4 5 73.5941 71.3141 1 -2 4 -5 66.9475 69.6668 6 2 4 5 66.3857 50.2522 2 2 4 5 21.8183 58.4387 6 -2 -4 -6 668.008 97.5029 1 2 4 6 704.862 84.3496 6 2 -4 6 780.440 105.909 1 2 4 6 541.272 70.3866 2 -2 4 -6 655.300 105.433 6 2 4 7 47.5352 58.2717 2 2 4 7 23.7149 52.1859 6 -2 -4 -7 103.673 47.7220 5 2 -4 7 65.4815 72.2769 1 -2 -4 -7 22.3098 76.0268 1 -2 4 -7 32.2898 72.9181 6 -2 -4 -8 140.526 72.6822 1 -2 -4 -8 230.809 53.4898 5 2 4 8 203.450 68.0448 2 2 4 8 202.178 60.0769 6 -2 4 -8 197.074 89.5370 6 2 -4 8 222.876 76.1379 1 2 4 9 70.1470 67.0371 2 -2 4 -9 173.528 82.9902 6 2 -4 9 75.8865 73.5513 1 2 4 9 81.4031 51.6838 6 -2 -4 -9 67.2611 49.7409 5 -2 -4 -9 15.3836 72.0800 1 2 4 10 5.02200 70.2033 2 2 -4 10 35.2542 69.1258 1 -2 -4 -10 19.7135 76.9746 1 -2 -4 -10 10.8522 50.5393 5 2 4 10-11.2373 46.9661 6 -2 4 -10 44.8993 81.1564 6 -2 4 -11 130.509 85.2239 6 -2 -4 -11 124.466 75.0747 1 2 4 11 42.9433 75.7531 2 2 4 11 160.292 54.5770 6 2 -4 11 124.526 81.8878 1 -2 -4 -11 177.538 62.6711 5 2 4 12 801.250 103.645 2 -2 -4 -12 895.011 115.909 7 -2 4 -12 958.107 119.848 6 -2 -4 -12 849.237 88.7937 5 2 -4 12 721.566 106.896 1 2 4 12 729.032 78.4010 6 -2 -4 -12 723.026 104.422 1 -2 -4 -13 29.6743 82.5898 1 2 4 13 112.351 88.2231 2 -2 -4 -13 103.981 83.8104 7 2 -4 13 63.0430 75.8339 1 2 4 13 101.511 49.5897 6 -2 4 -13 146.590 91.0772 6 -2 -4 -14 989.041 118.641 1 2 4 14 1106.54 123.721 2 -2 -4 -14 1300.65 131.561 7 -2 4 -14 1304.71 135.116 6 2 -4 14 1298.89 125.605 1 -2 -4 -15-6.85340 85.5268 7 2 4 15-0.44951 93.0374 2 -2 4 -15 4.60304 82.8948 6 2 4 16 73.1333 85.3653 2 -2 -4 -16-40.4210 83.3188 7 2 4 17 592.032 127.675 2 2 4 18 18.1740 101.740 2 2 4 19 67.4671 105.727 2 -3 -1 31 90.2500 97.5215 2 -3 -1 30 62.3870 94.5674 2 3 1 -30 111.898 83.3801 7 3 -1 -30 105.559 84.7997 7 -3 -1 29-85.5897 93.0273 2 3 -1 -29 48.3304 76.5692 7 3 1 -29 76.8496 79.7356 7 3 1 -29 101.330 57.6091 6 -3 1 28 358.452 120.974 2 -3 -1 28 435.774 101.299 2 3 1 -28 313.331 69.7053 6 3 1 -28 393.886 93.7966 7 3 -1 -28 293.462 86.4001 7 3 1 -27 57.7718 55.8274 6 -3 -1 27 182.223 87.7126 2 3 -1 -27 15.8670 75.7394 7 3 1 -27 1.21514 74.8784 7 -3 1 27 40.0619 106.838 2 -3 -1 26 2401.44 146.844 1 3 1 -26 2164.25 145.435 7 -3 1 26 2005.85 166.358 2 3 -1 -26 2312.86 145.523 7 -3 -1 26 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828.673 52.7413 4 -6 -2 -3 832.411 70.3631 7 -6 2 -3 755.076 51.5021 2 -6 2 -3 882.011 74.8403 6 6 2 3 631.694 54.1248 7 6 -2 3 73.1330 36.9370 8 6 -2 3 866.383 71.2198 6 6 2 3 795.760 52.4323 6 -6 -2 -3 864.024 54.8893 6 -6 2 -3 766.042 49.4721 4 -6 -2 -3 790.202 58.9840 2 -6 2 -3 969.724 74.2398 1 -6 -2 -3 802.855 66.6906 5 6 -2 3 812.017 73.3534 1 -6 -2 -4 225.015 55.2512 5 6 2 4 279.942 47.8793 7 -6 -2 -4 248.115 56.0709 7 -6 2 -4 267.359 57.5856 6 6 -2 4 35.5876 35.8707 8 6 2 4 238.301 39.1329 4 6 -2 4 232.949 49.7549 6 -6 -2 -4 252.957 40.0712 6 -6 -2 -4 236.267 43.4415 4 6 2 4 265.280 57.3721 2 -6 2 -4 240.131 40.3913 4 -6 -2 -4 260.191 49.4958 2 6 -2 4 207.997 57.7323 1 6 2 4 200.804 35.2643 6 -6 2 -4 195.176 40.1576 2 -6 2 -4 217.260 50.9795 1 -6 -2 -5 171.535 43.3006 4 6 2 5 149.043 43.1072 7 6 -2 5 169.348 57.2593 1 -6 -2 -5-8.74849 39.9815 2 6 2 5 207.975 39.4255 4 6 -2 5 52.5320 35.1279 8 -6 -2 -5 125.331 53.7342 7 6 2 5 175.381 59.3238 2 6 -2 5 216.462 53.3032 6 -6 -2 -5 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53.4417 1 9 1 -4 1545.11 57.3160 6 -9 -1 3 2048.15 78.2733 5 -9 1 3 1960.48 55.6687 4 -9 -1 3 2051.68 63.5657 2 9 -1 -3 2067.94 68.7373 8 -9 1 3 1944.45 72.3125 8 -9 1 3 2057.52 80.4025 6 9 1 -3 1941.32 75.4437 4 9 1 -3 2003.38 72.3739 5 9 -1 -3 2029.97 57.7371 4 9 -1 -3 1916.22 51.1729 5 -9 -1 3 1994.99 60.6964 6 9 -1 -3 1960.92 72.3870 1 -9 -1 3 2093.57 65.3736 3 9 1 -3 2043.97 53.1349 1 9 -1 -3 2028.53 64.0327 7 9 1 -3 2020.68 59.0974 6 -9 1 3 2035.74 64.2262 7 -9 -1 3 2080.87 55.9262 1 -9 1 2 5690.87 86.1049 5 -9 -1 2 5477.76 119.464 5 -9 1 2 5883.60 97.6422 4 9 1 -2 5906.06 118.313 5 9 -1 -2 5669.52 104.509 8 -9 -1 2 5679.29 88.7776 6 -9 -1 2 6002.88 107.730 3 -9 -1 2 5842.81 103.106 2 9 1 -2 5877.13 117.153 4 -9 -1 2 5697.90 118.097 4 9 1 -2 5603.92 84.6409 6 9 -1 -2 5515.50 82.9377 5 9 -1 -2 5742.57 95.6822 4 -9 1 2 5582.27 96.2440 7 9 1 -2 5549.47 90.2838 7 9 -1 -2 5688.81 108.573 1 -9 1 2 5931.32 119.975 6 -9 1 2 5716.44 106.604 8 -9 -1 2 5725.96 82.0138 1 -9 1 1 2729.90 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374.177 51.8553 4 10 4 -2 485.378 75.1459 6 -10 4 2 568.388 103.061 6 10 4 -1 190.464 63.7962 6 10 -4 -1 277.042 90.0078 1 -10 -4 1 169.830 74.6552 1 10 4 -1 123.538 43.2654 4 -10 4 1 162.881 78.5279 6 -10 -4 0 349.367 81.6641 1 10 4 0 262.330 46.3861 4 10 4 0 447.976 69.3296 6 10 -4 0 455.887 89.6104 1 -10 4 0 335.633 94.7065 6 -10 -4 -1 148.492 72.1096 1 10 -4 1 127.607 68.8288 1 10 4 1 109.439 40.9190 4 -10 4 -1 195.094 83.9006 6 10 4 1 148.542 54.1399 6 10 -4 2 72.2940 77.9368 1 -10 4 -2 39.7735 82.3048 6 10 4 2 21.4710 51.8085 6 -10 -4 -2 36.7124 68.7867 1 10 -4 3 2604.22 158.527 1 -10 -4 -3 2962.54 136.364 5 -10 4 -3 3038.44 176.814 6 10 4 3 2909.87 134.173 6 -10 -4 -3 2515.87 145.120 1 -10 -4 -4 270.693 72.7326 5 -10 4 -4 315.388 92.3753 6 10 4 4 244.539 61.7112 2 10 -4 4 258.386 83.5477 1 -10 -4 -4 238.523 78.4182 1 10 4 4 273.869 60.4473 6 10 -4 5 134.367 81.8374 1 -10 -4 -5 124.598 72.1213 1 -10 -4 -5 275.455 67.3118 5 10 4 5 111.285 60.5197 2 -10 4 -5 251.515 94.3991 6 10 4 5 116.920 51.0556 6 -10 -4 -6 2337.41 133.156 5 10 -4 6 1938.47 141.570 1 -10 4 -6 1933.76 152.424 6 10 4 6 2283.94 115.061 6 10 4 6 1878.15 117.323 2 -10 -4 -6 1576.04 124.149 1 -10 -4 -7 92.4934 67.9443 1 -10 -4 -7 64.8518 71.1039 5 10 4 7 153.285 69.9217 2 -10 4 -7 149.337 86.5404 6 10 -4 7 116.604 74.9837 1 -10 -4 -8 51.2646 67.2274 1 -10 -4 -8-5.82971 71.1440 5 10 4 8 34.8252 73.0804 2 -10 4 -8 78.0434 82.3804 6 10 -4 8 45.3243 77.7163 1 10 -4 9 674.954 103.879 1 -10 -4 -9 545.073 89.8375 1 10 4 9 758.411 97.7079 2 -10 -4 -9 880.735 106.936 5 -10 4 -9 768.822 115.810 6 -10 -4 -10 370.591 84.0406 1 10 -4 10 503.283 96.8547 1 -10 -4 -10 621.737 97.5030 5 10 4 10 382.394 85.9278 2 -10 4 -10 447.517 107.108 6 -10 -4 -11 22.4598 73.5060 1 10 4 11-27.5841 80.4376 2 -10 -4 -11-2.36862 78.2172 5 -10 -4 -12 674.849 102.419 5 10 4 12 424.748 108.286 2 -10 -4 -13 141.622 77.9231 5 10 4 13 60.8238 93.2666 2 -11 -1 34 821.962 133.955 2 -11 -1 33 223.068 98.6208 2 -11 -1 32 194.448 98.7034 2 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27.3065 7 -16 0 -7-10.1919 30.0088 1 16 0 7 43.5975 69.6749 2 -16 0 -8 17.0508 59.2525 5 16 0 8 21.3061 56.2921 3 -16 0 -8 33.1448 16.1728 6 -16 0 -8 35.4138 22.6716 8 -16 0 -8 21.6000 27.4011 7 -16 0 -8 37.9949 35.9383 1 16 0 8 45.3673 70.8315 2 -16 0 -9 4.11222 15.2209 6 -16 0 -9 21.9391 63.7902 5 -16 0 -9 3.66644 32.5417 7 -16 0 -9-6.98057 20.0678 8 -16 0 -9 6.46505 35.2466 1 16 0 9-16.2217 73.9648 2 -16 0 -10 3817.71 117.674 1 -16 0 -10 3835.87 60.0579 8 -16 0 -10 3702.59 165.009 5 -16 0 -10 3777.95 109.545 7 16 0 10 3867.73 169.074 2 -16 0 -11 11.8976 37.3072 7 -16 0 -11-13.3311 39.1105 1 16 0 11 69.3974 83.8869 2 -16 0 -12 11849.1 219.807 1 -16 0 -12 12505.8 205.754 7 16 0 12 13033.0 304.314 2 -16 0 -13 1.00379 43.1827 7 16 0 13 42.5441 90.1844 2 -16 0 -14 69.0430 46.3787 7 16 0 14 31.4721 87.0417 2 -16 0 -15-16.0777 47.9442 7 16 0 15-12.9902 88.8388 2 -16 0 -16 211.529 57.3192 7 16 0 16 207.225 100.553 2 16 0 17-34.4614 96.5737 2 16 0 18 720.931 122.586 2 16 2 -32-33.0258 76.6435 6 16 2 -31 465.697 89.5848 6 -16 -2 31 520.031 96.0209 1 -16 2 31 196.233 113.147 2 16 -2 -31 573.944 104.736 7 -16 -2 30 211.711 83.0064 1 16 2 -30 51.1465 70.3966 6 -16 2 30 124.137 98.1357 2 16 -2 -30 146.127 83.0269 7 -16 -2 30 64.6062 57.5754 2 16 2 -29 18.9928 70.5782 6 -16 2 29 77.8530 100.306 2 -16 -2 29 33.4972 71.2681 1 -16 -2 29 50.4198 52.5963 2 16 -2 -29 20.3055 82.2533 7 16 2 -28 139.451 73.2415 6 -16 -2 28 31.8581 44.4711 8 -16 -2 28 105.816 74.9358 1 -16 2 28 45.4966 95.0379 2 -16 -2 28 84.6651 55.6799 2 16 -2 -28 147.817 83.8296 7 16 -2 -27 6.83708 81.9872 7 16 2 -27 17.3712 62.5064 6 -16 -2 27-6.60003 42.6647 8 -16 -2 27 2.52850 50.0171 2 -16 -2 27 2.85609 70.6062 1 -16 2 27 19.4199 90.1299 2 16 2 -26 1334.35 112.654 6 -16 -2 26 1286.39 88.9015 8 -16 2 26 1028.04 124.785 2 -16 -2 26 1221.62 88.7546 2 -16 -2 26 1395.51 114.046 1 16 -2 -26 1360.91 124.574 7 16 2 -25 1365.27 114.759 6 -16 2 25 1265.75 129.203 2 -16 -2 25 1273.09 86.9702 2 16 -2 -25 1479.38 120.175 7 -16 -2 25 1402.39 116.406 1 -16 -2 25 1549.54 94.9025 8 16 2 -24 270.399 74.5316 6 -16 2 24 364.383 96.8456 2 -16 -2 24 263.650 56.9327 8 -16 -2 24 359.435 57.2486 2 16 -2 -24 417.818 88.5729 7 -16 -2 24 366.320 78.2095 1 16 2 -23 93.6186 60.4197 6 -16 2 23 48.8467 88.0384 2 -16 -2 23 64.6976 45.2104 8 -16 -2 23 61.2367 43.7541 2 -16 -2 23 39.5050 66.1880 1 16 -2 -23 48.1988 68.6724 7 -16 -2 22 2009.71 121.175 1 -16 2 22 1569.40 127.519 2 -16 -2 22 1676.83 84.0172 2 -16 2 22 1815.27 113.615 8 16 -2 -22 2122.87 126.735 7 -16 -2 22 1771.36 102.403 8 16 2 -22 1779.61 113.051 6 16 2 -21 105.038 61.1838 6 -16 2 21 92.7210 85.2122 2 -16 2 21 85.3236 56.4422 8 -16 -2 21 139.548 62.7945 1 -16 -2 21 78.7744 39.2755 2 16 -2 -21 92.6280 62.8587 7 -16 -2 21 60.0853 48.3108 8 16 2 -20 23.6137 58.3905 6 -16 -2 20 4.69658 45.7490 8 -16 -2 20 13.0718 35.4637 2 -16 2 20 48.1555 55.0432 8 16 -2 -20 68.2505 62.1235 7 -16 -2 20 10.5194 59.8673 1 -16 -2 19 2749.95 87.5596 2 -16 -2 19 3317.29 133.232 8 -16 2 19 3348.55 137.481 8 16 -2 -19 3764.70 148.333 7 -16 -2 19 3398.06 136.094 1 16 2 -19 3670.72 143.959 6 -16 -2 18 828.624 53.4356 2 -16 -2 18 1000.75 83.4290 8 -16 2 18 994.668 88.4985 8 16 -2 -18 1032.39 92.5701 7 -16 -2 18 1125.82 87.2586 1 16 2 -18 1068.92 88.1265 6 16 2 -17 3298.43 131.479 1 -16 -2 17 2406.95 74.6872 2 16 -2 -17 3031.10 130.914 7 -16 2 17 2653.81 124.827 8 -16 -2 17 2833.95 122.619 1 -16 -2 17 2671.34 120.814 8 16 2 -17 2978.80 126.892 6 16 2 -16 933.130 76.1317 1 -16 -2 16 836.983 48.3780 2 16 -2 -16 848.657 80.0581 8 -16 2 16 816.630 84.3704 8 16 -2 -16 995.875 85.3868 7 -16 -2 16 788.290 80.7124 8 -16 -2 16 804.616 77.8059 1 16 2 -16 933.365 81.6320 6 16 2 -15 108.831 53.3481 6 -16 -2 15 85.4482 62.4279 8 -16 2 15 107.212 56.5342 8 16 -2 -15 100.248 52.0590 8 16 2 -15 100.333 42.6138 1 -16 2 15 96.4956 49.0256 7 16 -2 -15 129.833 58.5910 7 -16 -2 15 83.9877 51.6150 1 -16 -2 15 110.394 58.1663 6 16 2 -14 36.0753 50.7375 6 16 -2 -14 25.8796 46.1781 8 -16 2 14 13.4837 57.4648 8 16 -2 -14 40.6846 32.8204 4 16 2 -14 29.7821 41.4478 1 16 -2 -14 44.3708 54.0048 7 -16 -2 14 29.8368 46.0317 1 -16 2 14 23.4910 46.4838 7 -16 -2 14 38.9224 47.9321 6 16 2 -13 938.004 75.3945 5 -16 2 13 879.264 81.1359 8 16 -2 -13 717.787 41.8237 4 -16 2 13 849.204 71.0256 7 16 -2 -13 734.821 73.4636 7 -16 -2 13 764.564 67.6071 1 16 -2 -13 761.826 74.4573 8 -16 2 13 856.721 80.0814 6 -16 -2 13 851.932 78.5641 6 16 2 -13 1008.01 72.4259 1 16 2 -13 749.164 74.0548 6 16 2 -12 1997.93 98.3977 5 16 -2 -12 1535.16 51.1217 4 16 -2 -12 1841.01 96.4929 8 -16 2 12 1924.02 102.519 8 -16 2 12 1901.74 92.1715 7 -16 -2 12 1763.20 87.2804 1 16 -2 -12 1921.73 98.6524 7 -16 2 12 1881.52 104.415 6 -16 -2 12 1869.29 99.4389 6 16 2 -12 2071.07 94.9366 1 16 2 -12 1654.58 90.0886 6 16 2 -11 2239.66 100.806 5 16 -2 -11 1554.81 50.0429 4 -16 -2 11 1698.01 54.7635 2 -16 2 11 1845.19 89.9148 7 -16 -2 11 1932.94 89.4923 1 16 -2 -11 2031.46 99.2903 7 16 -2 -11 1928.27 97.2324 8 -16 2 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100.378 5 -21 3 2 742.273 103.658 6 21 -3 -2 711.124 83.9049 1 21 3 -2 714.632 56.3326 6 21 3 -1 189.519 37.5918 6 -21 -3 1 151.728 84.6556 5 -21 -3 1 158.334 48.2257 1 21 -3 -1 234.946 65.9110 1 21 3 -1 265.423 62.6758 4 -21 3 1 236.679 82.4358 6 21 -3 0 1232.82 101.992 1 -21 -3 0 1326.50 129.880 5 21 3 0 1265.92 99.9686 4 -21 3 0 1362.67 119.255 6 -21 -3 0 1027.75 71.0118 1 21 3 0 1452.05 66.0784 6 -21 -3 -1 420.891 97.6268 5 -21 -3 -1 245.323 50.5267 1 21 3 1 353.423 72.8980 4 21 -3 1 290.677 68.5279 1 -21 3 -1 458.274 93.0648 6 -21 -3 -2 64.9628 82.2917 5 21 3 2 38.7582 57.9681 4 21 -3 2 49.9618 54.4755 1 -21 3 -2 14.5204 79.2831 6 -21 -3 -3 61.2051 82.1598 5 21 3 3 76.0732 62.5190 4 -21 3 -3 71.9208 70.6108 6 21 -3 3 101.412 60.6937 1 21 3 4 394.734 76.8182 4 -21 -3 -4 428.601 101.739 5 -21 3 -4 457.427 95.0415 6 21 -3 4 386.939 69.7630 1 21 -3 5 18.3824 57.4003 1 -21 -3 -5-1.34848 95.1981 5 21 3 5-40.8704 58.3250 4 21 -3 5-20.5290 67.2794 3 -21 3 -5-12.5170 72.6875 6 -21 -3 -6 638.203 110.557 5 21 -3 6 610.945 86.7327 1 21 3 6 688.271 89.7605 4 21 -3 6 503.164 90.7385 3 -21 3 -6 581.848 99.3466 6 -21 -3 -7 72.9927 87.2144 5 21 -3 7 191.238 62.5401 1 21 -3 7 103.400 66.1133 3 -21 3 -7 56.1362 79.6210 6 -21 -3 -8-40.0585 87.4179 5 21 -3 8 23.4241 53.8678 1 21 -3 8-11.3095 70.5404 3 -21 3 -8 57.0308 73.2976 6 -21 -3 -9-20.5846 69.9035 8 -21 -3 -9-3.83069 102.500 5 21 -3 9-16.7625 59.5164 1 21 -3 9-11.4278 69.3966 3 -21 3 -9-0.14557 80.4853 6 21 -3 10 398.997 73.3712 1 21 3 10 501.445 112.331 2 21 -3 10 435.248 86.4663 3 -21 3 -10 467.431 98.2228 6 21 -3 11 53.6163 65.6714 1 21 -3 11 129.270 77.6602 3 -22 0 37-19.0557 98.3337 2 -22 0 36 250.589 105.926 2 -22 0 35 37.8070 94.2626 2 22 0 -35-36.3386 88.4216 7 -22 0 34 899.752 123.766 2 22 0 -34 1771.64 144.797 7 -22 0 33-27.5851 89.5611 2 -22 0 33 21.9723 42.6570 8 22 0 -33 0.14483 78.2950 7 -22 0 32 952.681 120.335 2 -22 0 32 1161.92 85.5429 8 22 0 -32 1531.10 129.140 7 -22 0 31-6.03509 83.6786 2 -22 0 31 17.3299 45.7669 8 22 0 -31-12.7803 77.9888 7 -22 0 30 124.620 82.2071 2 -22 0 30 166.625 51.3963 8 22 0 -30 67.2572 74.6157 7 -22 0 29 9.62198 77.8842 2 -22 0 29-6.40834 44.9146 8 22 0 -29-47.3206 72.3767 7 -22 0 28 1017.79 106.792 2 -22 0 28 1596.99 97.3142 8 22 0 -28 1607.57 122.963 7 -22 0 27 2.56435 76.8272 2 22 0 -27-28.4789 49.1875 8 -22 0 27 26.0180 48.6294 8 22 0 -27-18.9351 68.2374 7 -22 0 26 448.274 65.8511 8 22 0 -26 603.019 88.1966 7 22 0 -26 533.406 71.0026 8 22 0 -25 20.7119 49.9087 8 -22 0 25 12.1847 48.2026 8 22 0 -25-11.9449 64.9841 7 22 0 -24 333.913 61.9944 8 -22 0 24 241.340 57.6030 8 22 0 -24 254.007 70.6403 7 22 0 -23-23.9401 51.6466 8 22 0 -23-0.33898 58.4883 7 -22 0 23-28.5878 50.8466 8 22 0 -22 25.8088 50.4146 8 -22 0 22-3.97902 52.3885 8 22 0 -22 1.98426 59.9893 7 22 0 -22 5.63563 44.4493 1 22 0 -21 27.8488 49.5452 8 -22 0 21-12.5343 54.9701 8 22 0 -21-0.07419 52.7477 7 22 0 -21-1.05937 40.0420 1 -22 0 20 3052.85 116.025 6 22 0 -20 3427.25 118.377 1 22 0 -20 3647.94 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134.546 39.2057 6 -22 -2 9 149.828 69.8488 8 22 -2 -9 132.774 39.8288 5 -22 2 9 144.135 62.2641 8 22 2 -9 97.3362 61.7971 4 -22 2 9 162.728 48.9999 7 -22 -2 9 145.801 36.0564 1 -22 -2 9 55.6390 42.5986 2 22 2 -9 117.705 37.5894 7 22 -2 -9 94.5100 39.3087 4 -22 2 9 120.403 61.0442 6 -22 -2 9 161.582 43.9045 3 -22 -2 9 104.807 45.4528 6 22 -2 -8 39.4905 44.1652 1 22 2 -8 37.5917 34.8959 6 -22 -2 8 89.9978 68.1223 8 22 -2 -8 37.0073 37.8298 5 -22 2 8 48.7925 56.9973 8 -22 -2 8 47.9918 31.1508 1 22 2 -8 19.5396 60.1128 4 -22 2 8 80.8567 44.6569 7 -22 -2 8 34.2512 48.1731 2 22 2 -8 0.30362 29.4128 7 22 -2 -8 62.9466 41.2801 4 -22 2 8 29.0343 60.4338 6 -22 -2 8 110.267 45.8650 3 -22 -2 8 74.9454 42.3202 6 22 2 -7 36.0287 34.8243 6 22 -2 -7 16.1702 41.2154 1 -22 -2 7 45.5978 64.4292 5 -22 -2 7-7.65226 64.7595 8 -22 2 7 5.04449 55.9474 8 -22 2 7 10.8001 33.1478 4 -22 -2 7 13.0147 28.5638 1 22 2 -7 0.45434 56.2885 4 -22 -2 7 18.5735 48.3914 2 -22 2 7 22.0194 43.3667 7 22 2 -7 5.76993 26.5732 7 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6 -23 -1 7 274.831 56.8296 2 23 -1 -7 335.039 39.7281 1 -23 1 6 1801.16 100.750 5 -23 -1 6 1856.78 113.170 5 -23 -1 6 2020.09 111.107 8 23 -1 -6 2107.64 104.240 8 23 1 -6 2113.53 109.064 5 -23 1 6 2270.58 106.646 8 -23 -1 6 1895.80 109.911 4 -23 -1 6 2015.25 103.385 2 -23 1 6 1893.16 101.639 4 23 1 -6 1979.80 111.001 4 -23 1 6 1815.77 55.6615 7 23 1 -6 2079.26 43.6654 7 23 -1 -6 1893.01 96.8601 4 23 -1 -6 2020.55 95.0092 5 -23 1 6 1875.78 91.9094 6 23 1 -6 2132.16 103.802 3 -23 -1 6 2107.70 74.9910 6 23 -1 -6 1913.92 73.3759 1 -23 -1 5 38.8965 29.7838 6 23 1 -5 43.9169 53.0588 3 -23 1 5 32.6856 53.0110 5 -23 -1 5 56.7619 61.5141 8 -23 -1 5 41.8486 62.3871 5 23 -1 -5 26.7955 48.1280 8 23 -1 -5 17.8912 29.2071 1 -23 1 5 26.2651 53.2216 8 -23 -1 5 10.4312 47.2247 4 -23 1 5 46.3059 50.9452 4 23 1 -5 41.0679 14.4411 7 -23 1 5 35.8847 25.5524 7 23 1 -5 55.0804 58.7163 4 23 -1 -5 14.6934 54.9701 4 -23 -1 5 15.0205 52.4540 2 -23 1 5 48.9542 48.5498 6 -23 -1 4 57.3247 28.0607 6 23 1 -4 29.0850 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239.527 104.036 4 40 0 -32 182.568 64.9992 7 -40 0 31 54.2260 81.8234 8 40 0 -31-0.55033 97.7653 4 40 0 -31 30.6346 50.7980 7 -40 0 30 105.815 83.1775 8 40 0 -30 118.413 98.3876 4 40 0 -30 116.280 51.3586 7 -40 0 29 31.3501 81.2307 8 40 0 -29 8.97219 88.6776 4 40 0 -29 1.96130 49.6329 7 -40 0 28-4.61376 89.5151 8 40 0 -28-34.6235 85.9416 4 40 0 -28 9.33098 45.3671 7 -40 0 27 6.28230 86.2079 8 40 0 -27-16.2621 90.6808 4 40 0 -27-26.5345 45.1220 7 -40 0 26 2429.73 162.515 8 40 0 -26 2113.76 159.278 4 40 0 -26 2396.97 110.201 7 -40 0 25 88.9798 85.3445 8 40 0 -25-25.8410 84.8173 4 40 0 -25 32.3343 37.2681 7 -40 0 24 788.140 116.451 8 40 0 -24 586.969 60.5208 7 40 0 -24 620.531 105.241 4 -40 0 23 37.5058 80.2357 8 40 0 -23 10.2399 85.5805 4 40 0 -23-8.99097 34.4238 7 -40 0 22 189.781 92.0365 8 40 0 -22 155.918 91.4828 4 -40 0 21 54.4285 85.4403 8 40 0 -21-2.69690 81.3311 4 40 0 -21-15.5523 57.2920 3 -40 0 20 75.1623 87.6392 8 40 0 -20 5.95824 86.6281 4 40 0 -20-3.84987 61.0046 3 -40 0 19 28.0105 80.1074 8 40 0 -19-13.0964 82.2943 4 40 0 -19-9.56715 59.5869 3 -40 0 18 418.324 93.7406 8 40 0 -18 393.410 96.3232 4 40 0 -18 341.769 79.8723 3 -40 0 17 53.3430 79.9950 8 40 0 -17 26.4017 83.2591 4 40 0 -17-11.8498 65.8931 3 -40 0 16 580.721 104.472 8 40 0 -16 560.374 99.4662 4 40 0 -16 605.461 94.6155 3 -40 0 15-18.2074 85.7624 8 40 0 -15 27.2814 83.7293 4 40 0 -15-19.0074 70.1323 3 -40 0 14 58.4586 90.2299 8 40 0 -14 133.035 79.1245 4 40 0 -14 51.6413 78.5161 3 -40 0 13-7.75335 78.0469 8 40 0 -13-16.8017 83.8904 4 40 0 -13 22.9123 70.4898 3 -40 0 12 992.377 118.530 8 40 0 -12 1030.82 120.804 4 40 0 -12 913.890 111.540 3 -40 0 11-26.7064 81.4002 8 40 0 -11-1.42530 83.4750 4 -40 0 11 43.3959 55.8980 6 40 0 -11 13.1697 72.8921 3 -40 0 10 482.301 97.5206 8 40 0 -10 486.069 105.400 4 40 0 -10 614.359 106.106 3 -40 0 9 25.4866 80.6242 8 40 0 -9-40.8422 81.5263 4 40 0 -9 48.8678 81.4680 3 40 0 -8 486.163 102.058 3 -40 0 8 429.212 93.7079 8 40 0 -8 552.819 104.832 4 40 0 -7 69.1583 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73.4840 4 -40 2 12 41.9278 73.4349 6 -40 -2 11-37.4986 98.1938 8 -40 2 11 15.0203 77.2442 8 40 -2 -11 34.2922 73.5160 4 -40 2 11 30.0962 73.2893 6 -40 -2 10 166.285 93.5177 8 -40 2 10 238.470 82.5611 8 40 -2 -10 242.298 78.6825 4 -40 2 10 202.242 81.2050 6 -40 -2 9 81.1663 85.7939 8 -40 2 9 48.9093 69.5360 8 40 -2 -9-29.1245 78.2559 4 -40 2 9 11.2718 75.0341 6 -40 -2 8 65.6258 88.9114 8 -40 2 8 60.6103 73.7702 8 -40 2 8 132.052 76.7386 6 -40 -2 7 326.907 104.721 8 -40 2 7 232.669 76.5163 8 -40 -2 6 387.192 98.9943 8 41 1 -37-17.2728 73.0677 7 41 -1 -36-8.07573 96.3964 4 41 1 -36-24.4279 70.5654 7 41 -1 -36 37.3051 73.4248 7 -41 -1 35-6.69386 84.3659 8 41 -1 -35 16.4693 93.7925 4 41 1 -35-41.2469 64.4213 7 41 -1 -35 39.5455 67.4301 7 -41 -1 34 423.822 103.246 8 41 -1 -34 333.805 105.543 4 41 1 -34 327.184 79.0244 7 41 -1 -34 307.010 81.6783 7 -41 -1 33 95.7763 90.4178 8 -41 1 33 71.0042 86.2241 8 41 -1 -33 123.320 98.0646 4 41 1 -33 115.237 60.3870 7 41 -1 -33 211.638 70.1759 7 -41 -1 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418.342 89.7296 8 41 -1 -7 577.690 108.035 4 -41 -1 6 37.6193 83.3924 8 41 -3 -24 199.336 81.5659 1 41 -3 -23 44.8705 83.4016 1 41 -3 -22 181.791 76.8733 1 41 -3 -21 161.937 74.6733 1 41 -3 -20 28.9797 77.2949 1 41 -3 -19 6.71557 71.1822 1 42 0 -37 48.0057 71.5191 7 42 0 -36 982.440 110.862 7 42 0 -35-2.48986 65.6185 7 -42 0 34 183.837 86.5218 8 42 0 -34 277.389 115.836 4 42 0 -34 196.176 69.8267 7 -42 0 33 15.0169 83.9813 8 42 0 -33-14.7175 103.275 4 42 0 -33-28.6748 55.5782 7 -42 0 32 260.939 93.4919 8 42 0 -32 290.406 114.536 4 42 0 -32 227.875 63.1745 7 -42 0 31-19.4849 79.3360 8 42 0 -31-3.19351 106.869 4 42 0 -31-7.28831 52.4935 7 -42 0 30 752.148 109.369 8 42 0 -30 546.854 118.033 4 42 0 -30 733.412 78.2957 7 -42 0 29-8.35185 87.1471 8 42 0 -29-69.7556 93.1342 4 42 0 -29-13.5886 47.0740 7 -42 0 28 866.262 126.663 8 42 0 -28 955.466 132.109 4 42 0 -28 1189.74 89.5508 7 -42 0 27-10.7327 85.8848 8 42 0 -27-13.2007 94.9672 4 42 0 -27-13.9093 43.4968 7 -42 0 26 370.064 100.575 8 42 0 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8 -42 2 20-114.729 87.3891 8 42 2 -20-35.9552 92.3205 4 42 -2 -20-52.3974 69.9163 4 -42 2 20 27.6478 77.0936 6 -42 -2 19 199.425 106.854 8 -42 2 19 303.181 95.8720 8 42 2 -19 110.653 85.3856 4 42 -2 -19 290.772 80.1010 4 -42 2 19 214.983 84.9028 6 -42 -2 18 527.250 118.019 8 -42 2 18 572.578 115.642 8 42 -2 -18 523.580 90.1269 4 -42 2 18 721.283 110.078 6 -42 -2 17 37.9324 94.5687 8 -42 2 17 21.1858 89.7977 8 42 -2 -17 11.8549 70.5811 4 -42 2 17-1.05878 78.6624 6 -42 -2 16 29.3492 99.9994 8 -42 2 16-7.64644 88.2195 8 42 -2 -16-12.4366 67.3700 4 -42 2 16-35.9184 79.4110 6 -42 -2 15 76.1547 96.5999 8 -42 2 15 73.0994 89.3018 8 42 -2 -15 157.382 72.8366 4 -42 2 15 123.394 79.3552 6 -42 -2 14 274.936 99.0012 8 -42 2 14 254.957 91.9349 8 42 -2 -14 432.454 87.1448 4 -42 2 14 422.158 92.7083 6 -42 2 13 426.488 96.1266 8 42 -2 -13 429.597 89.9922 4 -42 2 13 293.851 89.4995 6 -42 2 12 32.8530 82.4523 8 42 -2 -12 96.2064 80.3307 4 -42 2 12 77.4503 80.0810 6 -42 2 11 3.81419 84.6580 8 42 -2 -11 26.9163 74.5234 4 -42 2 11-5.30285 74.6896 6 -42 2 10 274.996 85.8551 8 42 -2 -10 388.473 90.8074 4 -42 2 9 52.2880 69.9315 8 43 -1 -36 163.057 103.769 4 43 1 -36 379.231 78.8689 7 43 -1 -36 248.002 79.7765 7 43 -1 -35 32.1669 97.6819 4 43 1 -35-28.7151 69.4579 7 43 -1 -35 66.3681 75.8329 7 43 -1 -34-15.5710 91.8538 4 43 1 -34 40.1986 65.9913 7 43 -1 -34 108.224 67.9652 7 43 -1 -33 365.457 107.205 4 43 1 -33 437.595 71.8279 7 43 -1 -33 494.941 82.5398 7 43 -1 -32 466.923 120.101 4 43 1 -32 449.851 73.0586 7 43 -1 -32 551.214 83.0013 7 -43 -1 31 390.027 112.218 8 43 -1 -31 325.633 113.150 4 43 -1 -31 418.969 71.6699 7 -43 -1 30 272.445 106.561 8 -43 1 30 236.572 99.6531 8 43 1 -30 65.4028 107.552 4 43 -1 -30 171.034 107.589 4 43 -1 -30 163.305 58.4203 7 -43 -1 29-17.1389 90.3719 8 -43 1 29 23.0122 86.0625 8 43 1 -29 105.573 100.146 4 43 -1 -29-20.6422 89.0282 4 -43 -1 28 80.9436 94.7259 8 -43 1 28 169.199 90.9641 8 43 1 -28 48.5601 103.049 4 43 -1 -28 51.5549 90.4084 4 -43 -1 27 265.177 107.379 8 -43 1 27 301.226 104.750 8 43 1 -27 235.348 117.024 4 43 -1 -27 338.024 102.990 4 -43 -1 26 155.951 94.1742 8 -43 1 26 154.111 94.0857 8 43 1 -26 124.014 103.953 4 43 -1 -26 154.780 96.6472 4 -43 -1 25 208.645 108.901 8 -43 1 25 257.250 93.8267 8 43 1 -25 189.404 100.151 4 43 -1 -25 231.551 99.7587 4 43 1 -25 179.752 55.6783 3 -43 -1 24 1450.28 145.531 8 -43 1 24 1700.13 150.800 8 43 1 -24 1277.48 144.016 4 43 -1 -24 1438.15 142.134 4 43 1 -24 1259.79 93.8674 3 -43 -1 23 222.745 102.871 8 -43 1 23 225.525 107.703 8 43 1 -23 57.7715 93.8128 4 43 -1 -23 96.1142 88.8649 4 43 1 -23 111.750 51.1353 3 -43 -1 22 665.728 117.018 8 -43 1 22 547.168 117.576 8 43 1 -22 552.655 113.640 4 43 -1 -22 670.768 118.614 4 43 1 -22 564.153 74.3814 3 43 1 -21 173.046 59.5692 3 -43 -1 21 264.477 96.0979 8 -43 1 21 214.206 100.736 8 43 1 -21 170.532 100.282 4 43 -1 -21 218.549 95.1333 4 43 1 -20 518.284 78.1223 3 -43 -1 20 557.079 110.413 8 -43 1 20 507.455 110.329 8 43 1 -20 406.913 107.309 4 43 -1 -20 489.286 102.007 4 43 1 -19 336.207 72.1236 3 -43 -1 19 191.315 96.9939 8 -43 1 19 258.623 97.4870 8 43 1 -19 76.8663 88.8337 4 43 -1 -19 72.0493 86.0613 4 43 1 -18 259.296 71.5752 3 -43 -1 18 415.525 110.355 8 -43 1 18 266.278 96.9256 8 43 1 -18 296.523 100.225 4 43 -1 -18 377.018 95.4756 4 43 1 -17 39.1747 63.5000 3 -43 -1 17 108.308 96.4792 8 -43 1 17 12.0663 82.6208 8 43 1 -17 42.3220 92.2291 4 43 -1 -17 69.2387 83.0263 4 -43 1 17 44.3551 74.1594 6 43 -1 -17 68.2838 83.7765 3 43 1 -16 365.746 79.1181 3 -43 -1 16 349.078 104.136 8 -43 1 16 551.999 108.563 8 43 1 -16 403.757 106.564 4 43 -1 -16 406.959 101.173 4 -43 1 16 464.274 85.7912 6 43 -1 -16 448.801 102.169 3 43 1 -15 180.818 73.2829 3 -43 -1 15 272.520 96.7120 8 -43 1 15 228.495 96.6916 8 43 1 -15 271.926 98.2120 4 43 -1 -15 208.076 91.6678 4 -43 1 15 216.936 76.3921 6 43 -1 -15 207.875 95.7774 3 43 1 -14 12.8039 72.8533 3 -43 -1 14 86.3601 92.2476 8 -43 1 14 18.4676 80.5740 8 43 1 -14 40.1560 87.3204 4 43 -1 -14-23.8775 83.6700 4 -43 1 14-25.6747 66.1263 6 43 -1 -14 49.2849 88.3166 3 43 1 -13 440.965 93.6177 3 -43 -1 13 436.878 115.120 8 -43 1 13 407.612 96.3748 8 43 -1 -13 541.170 107.674 4 -43 1 13 557.650 88.9267 6 43 -1 -13 440.123 105.556 3 43 1 -12 541.314 96.5728 3 -43 -1 12 529.597 110.893 8 -43 1 12 612.041 105.991 8 43 -1 -12 563.927 109.825 4 43 1 -11 83.4021 77.5023 3 -43 -1 11 122.138 90.2297 8 -43 1 11 106.823 80.6804 8 43 -1 -11 21.6647 88.1401 4 43 1 -10 376.783 102.952 3 -43 -1 10 404.676 109.483 8 -43 1 10 358.496 93.1106 8 43 -1 -10 410.667 104.554 4 -43 -1 9 75.3750 82.0041 8 -43 1 9 97.2738 78.1376 8 -43 -1 8 7.02748 84.7870 8 -43 1 8 197.944 79.0343 8 -43 -1 7 299.642 98.0043 8 44 0 -36 126.544 71.1896 7 44 0 -35-9.89669 67.7254 7 44 0 -34 0.73579 61.7399 7 44 0 -33 33.6059 101.362 4 44 0 -33 11.3283 59.8321 7 44 0 -32 133.668 105.929 4 -44 0 31 22.1548 83.6854 8 44 0 -31 17.6760 99.0604 4 -44 0 30 7.82468 89.9423 8 44 0 -30-29.4429 98.2319 4 -44 0 29-3.46740 99.8890 8 44 0 -29-44.4567 93.2482 4 -44 0 28 21.5976 88.1271 8 44 0 -28 119.298 92.5331 4 -44 0 27-72.9714 99.1564 8 44 0 -27 52.4015 95.6776 4 -44 0 26 9.99273 88.5329 8 44 0 -26 38.0277 93.8446 4 44 0 -26 26.9269 51.0716 3 -44 0 25 49.7551 96.5711 8 44 0 -25 15.8924 96.1571 4 44 0 -25 50.9984 55.7019 3 -44 0 24-13.9390 87.8635 8 44 0 -24 54.6806 90.1990 4 44 0 -24-7.53937 57.1555 3 -44 0 23 89.4120 86.3968 8 44 0 -23 18.8898 88.7688 4 44 0 -23 0.38617 59.9188 3 -44 0 22 174.309 100.807 8 44 0 -22 140.515 88.9479 4 44 0 -22 65.4518 63.9004 3 -44 0 21-56.1904 94.2813 8 44 0 -21-28.1215 88.2225 4 44 0 -21 14.7613 63.9249 3 -44 0 20 382.075 110.437 8 44 0 -20 358.391 107.253 4 44 0 -20 305.769 83.8043 3 -44 0 19-38.7633 91.9273 8 44 0 -19-4.78105 93.2475 4 44 0 -19 28.2604 74.9715 3 -44 0 18-40.2323 96.9233 8 44 0 -18 9.59682 84.2635 4 44 0 -18 4.97288 71.5123 3 -44 0 17 54.9746 88.1734 8 44 0 -17 37.1937 84.7781 4 44 0 -17 13.4613 81.3949 3 -44 0 16 25.8495 88.1741 8 44 0 -16 23.9467 89.1662 4 44 0 -16-2.91409 80.9131 3 -44 0 15-65.8390 97.1364 8 44 0 -15-33.5793 93.8751 4 44 0 -15 11.3316 73.7681 3 -44 0 14 167.237 90.2023 8 44 0 -14 213.109 91.1495 4 44 0 -14 262.252 89.6862 3 -44 0 13-23.9928 95.9913 8 44 0 -13-40.3848 89.1379 4 44 0 -13-39.2909 83.4642 3 -44 0 12 1306.89 134.234 8 44 0 -12 1363.03 140.137 3 -44 0 11 61.6847 82.9553 8 -44 0 10 337.911 94.5975 8 -44 0 9-3.92733 80.4647 8 -44 0 8 62.3116 78.0393 8 -44 2 22-8.81791 81.8095 6 -44 2 21 184.147 93.7980 6 -44 2 20 355.676 97.6654 6 -44 2 19 22.9435 76.3357 6 -44 2 18 68.3045 78.1385 6 -44 2 17-9.21139 77.3558 6 -44 2 16 228.020 82.9958 6 44 -2 -15 489.411 92.4359 4 -44 2 15 547.500 102.047 6 44 -2 -14 264.250 81.7254 4 -44 2 14 218.635 87.1197 6 -44 2 13 16.1062 80.8304 6 45 -1 -35 100.753 100.062 4 45 -1 -34-43.0686 95.9117 4 45 -1 -33 652.998 121.624 4 45 -1 -32 146.610 101.708 4 45 -1 -31 29.0821 93.7388 4 45 -1 -30 112.580 94.9636 4 45 -1 -29 3.75195 95.0161 4 45 -1 -28 568.994 112.088 4 45 -1 -27 78.3170 86.5484 4 45 1 -26 152.925 93.0091 4 45 -1 -26 152.206 99.4734 4 -45 1 25 257.943 99.2460 8 45 1 -25 237.862 99.3283 4 45 -1 -25 78.8160 96.5241 4 45 1 -24 53.8019 50.5353 3 -45 -1 24 99.9294 102.077 8 -45 1 24 131.385 94.4268 8 45 1 -24-22.1015 99.2818 4 45 -1 -24 11.5734 94.5485 4 45 1 -23 51.8774 51.3781 3 -45 -1 23 73.2234 88.2214 8 -45 1 23 105.107 93.5704 8 45 1 -23 37.0244 98.0962 4 45 -1 -23 4.91035 89.1533 4 45 1 -22 19.2441 53.0611 3 -45 -1 22 92.1548 98.8831 8 -45 1 22 7.61304 87.0728 8 45 1 -22-21.8554 94.5786 4 45 -1 -22 33.4478 85.9794 4 45 1 -21 82.7837 55.9590 3 -45 -1 21 73.4812 102.651 8 -45 1 21 89.8008 92.3544 8 45 1 -21 94.6191 92.6129 4 45 -1 -21 119.236 87.9415 4 45 1 -20 237.084 68.1801 3 -45 -1 20 292.198 107.881 8 -45 1 20 195.308 95.1230 8 45 1 -20 234.985 95.0293 4 45 -1 -20 268.803 98.1878 4 45 1 -19-2.59174 56.7615 3 -45 -1 19 62.9527 96.9411 8 -45 1 19 36.0437 95.1594 8 45 -1 -19 149.740 93.7606 4 45 -1 -19 29.8429 86.5783 3 45 1 -18 5.08067 58.0501 3 -45 -1 18-1.66936 102.334 8 -45 1 18 4.16999 96.0952 8 45 -1 -18 52.3968 87.4389 4 -45 1 18 8.76587 66.8219 6 45 -1 -18 17.2659 86.0361 3 45 1 -17 89.9980 65.4840 3 -45 -1 17 75.0091 94.8448 8 -45 1 17 139.530 93.8625 8 45 -1 -17 80.2678 80.7084 4 -45 1 17 78.1208 72.8240 6 45 -1 -17 42.2539 92.8324 3 45 1 -16 68.9002 73.2488 3 -45 -1 16 124.958 98.0740 8 -45 1 16 150.148 99.9995 8 45 -1 -16 161.685 90.2981 4 -45 1 16 81.7021 68.7020 6 45 1 -15 33.8873 77.3725 3 -45 -1 15-29.6225 95.6758 8 -45 1 15 123.572 81.4147 8 45 -1 -15-7.11356 88.8012 4 -45 1 15 83.5337 80.6415 6 45 1 -14 434.325 95.8336 3 -45 -1 14 557.684 120.086 8 -45 1 14 524.266 111.915 8 45 -1 -14 548.618 115.798 4 45 1 -13-30.4355 80.6541 3 -45 -1 13 92.5862 93.5258 8 -45 1 13 107.114 92.4424 8 45 -1 -13 9.82271 93.0370 4 -45 -1 12 266.046 95.9303 8 -45 1 12 177.248 88.4476 8 -45 -1 11 232.337 96.7517 8 -45 1 11 182.237 83.5660 8 -45 -1 10 442.163 102.526 8 46 0 -31 122.898 98.7410 4 46 0 -30 241.037 107.554 4 46 0 -29-33.9441 105.846 4 46 0 -29 27.8085 54.0433 3 46 0 -28 276.777 111.173 4 46 0 -28 263.872 69.4401 3 46 0 -27-10.5488 102.193 4 46 0 -27 48.0564 54.1847 3 46 0 -26 158.399 100.801 4 46 0 -26 99.3637 58.6129 3 -46 0 25 8.76739 95.5461 8 46 0 -25-18.2746 92.4252 4 46 0 -25 14.8858 58.5144 3 -46 0 24 408.443 105.976 8 46 0 -24 491.278 113.631 4 46 0 -24 471.237 81.7713 3 -46 0 23 12.4130 99.1893 8 46 0 -23 35.7738 95.3622 4 46 0 -23-1.11938 63.7558 3 -46 0 22 649.053 118.142 8 46 0 -22 514.099 116.781 4 46 0 -22 427.455 83.5531 3 -46 0 21 52.5135 98.9860 8 46 0 -21 10.9152 96.8892 4 46 0 -21-21.0744 73.2983 3 -46 0 20 129.117 97.9491 8 46 0 -20 104.668 92.8383 4 46 0 -20 127.442 73.8722 3 -46 0 19 5.99787 92.7320 8 46 0 -19-22.2794 90.2654 4 46 0 -19 39.8301 77.5200 3 -46 0 18 143.377 94.1432 8 46 0 -18 80.0440 90.8221 4 46 0 -18 102.394 78.9459 3 -46 0 17-58.1307 99.5982 8 46 0 -17-33.2952 94.0570 4 46 0 -17 3.57145 72.8707 3 -46 0 16 145.080 97.2100 8 46 0 -16 4.16226 76.2487 3 -46 0 15-40.8822 88.4911 8 46 0 -15-128.331 92.2398 3 -46 0 14 147.032 95.9428 8 -46 0 13 6.65112 91.4114 8 -46 0 12 232.495 98.6696 8 -46 0 11-4.24855 89.0717 8 47 -1 -33 126.662 93.1214 4 47 -1 -32 253.800 105.381 4 47 -1 -31 61.0791 97.4865 4 47 -1 -30 288.533 97.5797 4 47 -1 -29 123.476 100.230 4 47 -1 -28 58.1850 93.0769 4 47 -1 -27 140.269 87.3537 4 47 -1 -26 40.0445 90.5912 4 47 -1 -25 254.487 104.359 4 47 -1 -24 1288.06 145.330 4 47 1 -23 172.787 61.4651 3 47 -1 -23 321.217 106.591 4 47 1 -22 80.8156 62.4893 3 47 -1 -22 63.3290 91.1975 4 47 1 -21 471.883 82.1442 3 47 -1 -21 444.641 107.732 4 47 1 -20 50.8520 62.3003 3 47 -1 -20 66.2847 91.1513 4 -47 1 20 60.8849 72.1935 6 47 1 -19 158.076 68.2270 3 47 -1 -19 325.610 110.867 4 -47 1 19 181.548 83.3004 6 47 1 -18 526.151 95.8160 3 47 -1 -18 530.458 119.971 4 -47 1 18 508.414 91.4443 6 47 1 -17 24.7442 78.3357 3 47 -1 -17-15.9668 91.9205 4 -47 1 17 24.3339 74.0442 6 47 1 -16 104.798 78.7874 3 48 0 -28 94.4394 63.0052 3 48 0 -27-57.1074 64.0256 3 48 0 -26 40.2561 61.3782 3 48 0 -25 4.46332 67.4135 3 48 0 -24 58.8173 65.1922 3 48 0 -23 72.9705 67.4360 3 48 0 -22-19.5525 67.9877 3 48 0 -21 111.896 79.2026 3 48 0 -20 1857.92 149.635 3 48 0 -19-33.5906 80.4119 3 49 -1 -30-21.7025 91.7891 4 49 -1 -29 298.274 107.322 4 49 -1 -28-16.8353 101.011 4 49 -1 -27 0.19463 104.572 4 49 -1 -26 149.608 111.291 4 49 -1 -25 231.656 107.562 4 49 -1 -24-19.0102 102.387 4 49 -1 -23 214.487 113.581 4 -49 1 21 336.460 88.8524 6 50 0 -27-14.1708 71.0933 3 50 0 -26 35.9324 77.3124 3 50 0 -25-24.0921 77.3255 3 50 0 -24-42.6654 77.6384 3 50 0 -23 65.5688 78.0263 3 0 0 0 0.00 0.00 0 TITL 150K in C2/c REM C2/c (#15 with fixed user cell (not necessary: std = user cell)!) CELL 0.71073 36.534144 3.841793 28.655934 90.0000 129.5976 90.0000 ZERR 8.00 0.002644 0.000157 0.002183 0.0000 0.0119 0.0000 LATT 7 SYMM -x, y,-z+1/2 SFAC C H N O K UNIT 80.00 96.00 80.00 32.00 16.00 TREF HKLF 4 END ; _shelx_hkl_checksum 56552 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group K1 K 0.49295(2) 0.14592(12) 0.92220(2) 0.01886(11) Uani 1 1 d . . . . . C8A C 0.33139(7) 0.0481(6) 0.79432(9) 0.0262(5) Uani 1 1 d . . . . . H1 H 0.3110(8) 0.116(6) 0.8052(10) 0.031 Uiso 1 1 d . U . . . C4A C 0.38668(6) -0.1471(5) 0.79592(8) 0.0164(4) Uani 1 1 d . . . . . C5A C 0.35046(6) -0.0417(5) 0.73728(8) 0.0159(4) Uani 1 1 d . . . . . C6A C 0.35567(6) -0.0672(5) 0.69258(8) 0.0142(4) Uani 1 1 d . . . . . C2A C 0.43020(6) -0.3079(5) 0.77046(8) 0.0138(4) Uani 1 1 d . . . . . N9A N 0.37438(5) -0.0899(5) 0.83175(7) 0.0229(4) Uani 1 1 d . . . . . N7A N 0.31520(6) 0.0845(5) 0.73740(7) 0.0207(4) Uani 1 1 d . . . . . H2 H 0.2881(8) 0.157(6) 0.7073(10) 0.025 Uiso 1 1 d . U . . . N1A N 0.39706(5) -0.2135(4) 0.71198(7) 0.0147(3) Uani 1 1 d . . . . . N3A N 0.42877(5) -0.2836(4) 0.81550(7) 0.0159(3) Uani 1 1 d . . . . . N2A N 0.47169(5) -0.4278(4) 0.78441(8) 0.0166(3) Uani 1 1 d . . . . . H3 H 0.4911(7) -0.532(6) 0.8207(10) 0.020 Uiso 1 1 d . U . . . H4 H 0.4678(7) -0.534(6) 0.7562(10) 0.020 Uiso 1 1 d . U . . . O1A O 0.32526(4) 0.0348(4) 0.63802(6) 0.0176(3) Uani 1 1 d . . . . . O2W O 0.45272(5) -0.3456(4) 0.94584(6) 0.0198(3) Uani 1 1 d D . . . . H5 H 0.4272(6) -0.298(6) 0.9135(8) 0.024 Uiso 1 1 d D U . . . H6 H 0.4450(8) -0.438(6) 0.9634(10) 0.024 Uiso 1 1 d D U . . . K2 K 0.26242(2) 0.52427(11) 0.57126(2) 0.01757(11) Uani 1 1 d . . . . . C8B C 0.11968(6) 0.7399(5) 0.54217(9) 0.0176(4) Uani 1 1 d . . . . . H7 H 0.1215(7) 0.640(6) 0.5722(10) 0.021 Uiso 1 1 d . U . . . C4B C 0.09110(6) 0.9993(5) 0.46013(8) 0.0133(4) Uani 1 1 d . . . . . C5B C 0.13923(6) 0.9356(5) 0.49170(8) 0.0136(4) Uani 1 1 d . . . . . C6B C 0.16094(6) 1.0478(5) 0.46776(8) 0.0139(4) Uani 1 1 d . . . . . C2B C 0.08208(6) 1.2710(5) 0.38386(8) 0.0127(4) Uani 1 1 d . . . . . N7B N 0.15777(5) 0.7697(4) 0.54556(7) 0.0166(3) Uani 1 1 d . . . . . N9B N 0.07821(5) 0.8710(4) 0.49188(7) 0.0152(3) Uani 1 1 d . . . . . N3B N 0.06140(5) 1.1683(4) 0.40573(6) 0.0128(3) Uani 1 1 d . . . . . N1B N 0.12920(5) 1.2123(4) 0.41217(7) 0.0131(3) Uani 1 1 d . . . . . H8 H 0.1399(7) 1.294(6) 0.3954(9) 0.016 Uiso 1 1 d . U . . . N2B N 0.05681(5) 1.4312(5) 0.32953(7) 0.0156(3) Uani 1 1 d . . . . . H9 H 0.0320(8) 1.523(6) 0.3173(10) 0.019 Uiso 1 1 d . U . . . H10 H 0.0724(7) 1.540(6) 0.3196(9) 0.019 Uiso 1 1 d . U . . . O1B O 0.20352(4) 1.0188(4) 0.49036(6) 0.0172(3) Uani 1 1 d . . . . . O3W O 0.22530(5) 0.2963(4) 0.63128(6) 0.0281(4) Uani 1 1 d D . . . . H11 H 0.2058(8) 0.485(4) 0.6079(10) 0.034 Uiso 1 1 d D U . . . H12 H 0.2097(8) 0.092(3) 0.6118(10) 0.034 Uiso 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 K1 0.0181(2) 0.0215(2) 0.0189(2) -0.00296(17) 0.01271(18) -0.00423(16) C8A 0.0193(10) 0.0404(14) 0.0199(11) 0.0034(9) 0.0129(9) 0.0075(9) C4A 0.0133(8) 0.0206(10) 0.0127(9) -0.0006(8) 0.0071(7) -0.0010(7) C5A 0.0108(8) 0.0203(10) 0.0143(9) 0.0000(7) 0.0069(8) 0.0000(7) C6A 0.0106(8) 0.0136(10) 0.0131(9) -0.0003(7) 0.0051(8) -0.0028(6) C2A 0.0110(8) 0.0136(10) 0.0138(9) -0.0009(7) 0.0065(7) -0.0023(7) N9A 0.0172(8) 0.0368(11) 0.0158(8) 0.0031(7) 0.0109(7) 0.0066(7) N7A 0.0126(8) 0.0307(11) 0.0146(8) 0.0042(7) 0.0066(7) 0.0065(7) N1A 0.0117(7) 0.0191(9) 0.0119(7) 0.0005(6) 0.0068(6) -0.0009(6) N3A 0.0110(7) 0.0219(9) 0.0116(8) 0.0006(6) 0.0056(6) 0.0009(6) N2A 0.0120(7) 0.0244(10) 0.0109(8) 0.0015(7) 0.0062(7) 0.0039(6) O1A 0.0130(6) 0.0211(8) 0.0122(7) 0.0024(5) 0.0050(5) 0.0007(5) O2W 0.0136(6) 0.0295(8) 0.0148(7) 0.0053(6) 0.0084(6) 0.0004(6) K2 0.01360(19) 0.0189(2) 0.0159(2) 0.00181(16) 0.00738(17) 0.00080(15) C8B 0.0180(9) 0.0198(11) 0.0157(10) 0.0015(8) 0.0111(8) -0.0011(7) C4B 0.0120(8) 0.0151(9) 0.0114(9) -0.0037(7) 0.0068(7) -0.0019(7) C5B 0.0106(8) 0.0155(10) 0.0110(9) -0.0004(7) 0.0052(7) 0.0005(7) C6B 0.0114(8) 0.0146(10) 0.0128(9) -0.0037(7) 0.0064(8) -0.0016(7) C2B 0.0105(8) 0.0143(9) 0.0117(9) -0.0046(7) 0.0063(7) -0.0015(7) N7B 0.0143(7) 0.0194(9) 0.0123(8) 0.0013(6) 0.0067(6) 0.0002(6) N9B 0.0153(7) 0.0169(9) 0.0149(8) 0.0008(6) 0.0102(7) -0.0012(6) N3B 0.0100(7) 0.0162(8) 0.0109(7) -0.0020(6) 0.0060(6) -0.0013(6) N1B 0.0103(7) 0.0178(9) 0.0126(8) 0.0006(6) 0.0079(6) -0.0009(6) N2B 0.0097(7) 0.0226(10) 0.0152(8) 0.0055(6) 0.0083(7) 0.0030(6) O1B 0.0081(6) 0.0245(8) 0.0153(7) 0.0023(5) 0.0058(5) 0.0024(5) O3W 0.0168(7) 0.0245(9) 0.0232(8) 0.0021(6) 0.0035(6) 0.0035(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2W K1 O2W 88.49(4) . 1_565 ? O2W K1 N3A 70.56(5) . . ? O2W K1 N3A 117.33(4) 1_565 . ? O2W K1 N3B 149.65(5) . 8_566 ? O2W K1 N3B 120.65(5) 1_565 8_566 ? N3A K1 N3B 99.73(5) . 8_566 ? O2W K1 N9B 138.51(4) . 8_566 ? O2W K1 N9B 83.69(4) 1_565 8_566 ? N3A K1 N9B 147.34(5) . 8_566 ? N3B K1 N9B 47.90(4) 8_566 8_566 ? O2W K1 O2W 83.91(4) . 5_657 ? O2W K1 O2W 63.05(5) 1_565 5_657 ? N3A K1 O2W 154.32(5) . 5_657 ? N3B K1 O2W 101.07(4) 8_566 5_657 ? N9B K1 O2W 56.29(4) 8_566 5_657 ? O2W K1 N9B 82.91(4) . 8_556 ? O2W K1 N9B 139.54(4) 1_565 8_556 ? N3A K1 N9B 96.84(5) . 8_556 ? N3B K1 N9B 69.46(4) 8_566 8_556 ? N9B K1 N9B 77.32(4) 8_566 8_556 ? O2W K1 N9B 76.72(4) 5_657 8_556 ? O2W K1 N3A 121.43(4) . 1_565 ? O2W K1 N3A 64.99(4) 1_565 1_565 ? N3A K1 N3A 77.16(4) . 1_565 ? N3B K1 N3A 82.02(4) 8_566 1_565 ? N9B K1 N3A 91.67(4) 8_566 1_565 ? O2W K1 N3A 120.56(4) 5_657 1_565 ? N9B K1 N3A 149.54(4) 8_556 1_565 ? O2W K1 C4B 147.80(4) . 8_566 ? O2W K1 C4B 105.18(5) 1_565 8_566 ? N3A K1 C4B 123.99(5) . 8_566 ? N3B K1 C4B 24.38(4) 8_566 8_566 ? N9B K1 C4B 24.22(4) 8_566 8_566 ? O2W K1 C4B 77.04(4) 5_657 8_566 ? N9B K1 C4B 67.67(4) 8_556 8_566 ? N3A K1 C4B 90.70(5) 1_565 8_566 ? O2W K1 C4A 66.70(4) . . ? O2W K1 C4A 94.00(5) 1_565 . ? N3A K1 C4A 23.34(4) . . ? N3B K1 C4A 115.15(4) 8_566 . ? N9B K1 C4A 154.31(5) 8_566 . ? O2W K1 C4A 143.63(4) 5_657 . ? N9B K1 C4A 117.96(5) 8_556 . ? N3A K1 C4A 64.57(5) 1_565 . ? C4B K1 C4A 138.67(5) 8_566 . ? O2W K1 N9A 52.43(4) . . ? O2W K1 N9A 76.26(4) 1_565 . ? N3A K1 N9A 43.76(4) . . ? N3B K1 N9A 137.41(4) 8_566 . ? N9B K1 N9A 157.28(5) 8_566 . ? O2W K1 N9A 120.67(4) 5_657 . ? N9B K1 N9A 125.15(5) 8_556 . ? N3A K1 N9A 70.32(4) 1_565 . ? C4B K1 N9A 158.62(4) 8_566 . ? C4A K1 N9A 23.12(4) . . ? O2W K1 K1 46.24(3) . 1_545 ? O2W K1 K1 134.73(3) 1_565 1_545 ? N3A K1 K1 55.37(3) . 1_545 ? N3B K1 K1 104.18(3) 8_566 1_545 ? N9B K1 K1 127.71(3) 8_566 1_545 ? O2W K1 K1 104.60(3) 5_657 1_545 ? N9B K1 K1 50.40(3) 8_556 1_545 ? N3A K1 K1 132.53(3) 1_565 1_545 ? C4B K1 K1 114.34(3) 8_566 1_545 ? C4A K1 K1 70.63(4) . 1_545 ? N9A K1 K1 74.83(3) . 1_545 ? O2W K1 H5 16.7(4) . . ? O2W K1 H5 83.9(5) 1_565 . ? N3A K1 H5 59.5(4) . . ? N3B K1 H5 154.5(5) 8_566 . ? N9B K1 H5 152.4(4) 8_566 . ? O2W K1 H5 96.1(4) 5_657 . ? N9B K1 H5 96.8(4) 8_556 . ? N3A K1 H5 105.2(4) 1_565 . ? C4B K1 H5 164.0(4) 8_566 . ? C4A K1 H5 51.3(4) . . ? N9A K1 H5 35.7(4) . . ? K1 K1 H5 52.8(5) 1_545 . ? N9A C8A N7A 113.76(19) . . ? N9A C8A H1 125.5(13) . . ? N7A C8A H1 120.7(13) . . ? N3A C4A N9A 125.05(16) . . ? N3A C4A C5A 124.69(17) . . ? N9A C4A C5A 110.25(16) . . ? N3A C4A K1 57.64(9) . . ? N9A C4A K1 81.21(10) . . ? C5A C4A K1 139.31(14) . . ? C4A C5A N7A 105.81(17) . . ? C4A C5A C6A 120.32(16) . . ? N7A C5A C6A 133.84(17) . . ? O1A C6A N1A 120.23(17) . . ? O1A C6A C5A 125.17(16) . . ? N1A C6A C5A 114.61(16) . . ? O1A C6A K2 49.48(9) . 1_545 ? N1A C6A K2 111.37(12) . 1_545 ? C5A C6A K2 109.90(11) . 1_545 ? N3A C2A N1A 128.95(16) . . ? N3A C2A N2A 117.34(16) . . ? N1A C2A N2A 113.61(17) . . ? C8A N9A C4A 104.04(16) . . ? C8A N9A K1 140.73(15) . . ? C4A N9A K1 75.67(10) . . ? C8A N7A C5A 106.14(16) . . ? C8A N7A H2 126.6(15) . . ? C5A N7A H2 127.1(15) . . ? C2A N1A C6A 120.24(16) . . ? C2A N3A C4A 111.12(15) . . ? C2A N3A K1 123.91(11) . . ? C4A N3A K1 99.02(12) . . ? C2A N3A K1 114.61(11) . 1_545 ? C4A N3A K1 126.64(12) . 1_545 ? K1 N3A K1 77.16(4) . 1_545 ? C2A N2A H3 113.3(14) . . ? C2A N2A H4 114.1(14) . . ? H3 N2A H4 115(2) . . ? C6A O1A K2 142.26(12) . . ? C6A O1A K2 109.36(11) . 1_545 ? K2 O1A K2 92.91(4) . 1_545 ? K1 O2W K1 88.49(4) . 1_545 ? K1 O2W K1 96.09(4) . 5_657 ? K1 O2W K1 116.95(5) 1_545 5_657 ? K1 O2W H5 88.1(16) . . ? K1 O2W H5 106.2(16) 1_545 . ? K1 O2W H5 136.7(16) 5_657 . ? K1 O2W H6 157.6(18) . . ? K1 O2W H6 107.2(18) 1_545 . ? K1 O2W H6 62.7(17) 5_657 . ? H5 O2W H6 102(2) . . ? O1A K2 O1A 92.92(4) . 1_565 ? O1A K2 O1B 169.11(4) . . ? O1A K2 O1B 87.08(4) 1_565 . ? O1A K2 O1B 87.65(4) . 1_545 ? O1A K2 O1B 169.22(4) 1_565 1_545 ? O1B K2 O1B 90.34(4) . 1_545 ? O1A K2 O1B 83.15(4) . 7_566 ? O1A K2 O1B 88.28(4) 1_565 7_566 ? O1B K2 O1B 85.97(4) . 7_566 ? O1B K2 O1B 81.10(4) 1_545 7_566 ? O1A K2 O3W 82.79(4) . . ? O1A K2 O3W 107.88(4) 1_565 . ? O1B K2 O3W 107.58(4) . . ? O1B K2 O3W 82.87(4) 1_545 . ? O1B K2 O3W 159.05(5) 7_566 . ? O1A K2 C6A 74.84(5) . 1_565 ? O1A K2 C6A 21.16(4) 1_565 1_565 ? O1B K2 C6A 106.92(5) . 1_565 ? O1B K2 C6A 162.48(4) 1_545 1_565 ? O1B K2 C6A 96.83(4) 7_566 1_565 ? O3W K2 C6A 94.39(4) . 1_565 ? O1A K2 C6B 102.03(5) . 1_545 ? O1A K2 C6B 164.91(4) 1_565 1_545 ? O1B K2 C6B 78.63(5) . 1_545 ? O1B K2 C6B 19.21(4) 1_545 1_545 ? O1B K2 C6B 95.44(4) 7_566 1_545 ? O3W K2 C6B 72.48(4) . 1_545 ? C6A K2 C6B 166.85(5) 1_565 1_545 ? O1A K2 K2 44.15(3) . 1_545 ? O1A K2 K2 137.06(3) 1_565 1_545 ? O1B K2 K2 134.86(3) . 1_545 ? O1B K2 K2 44.52(3) 1_545 1_545 ? O1B K2 K2 86.53(3) 7_566 1_545 ? O3W K2 K2 72.56(3) . 1_545 ? C6A K2 K2 118.16(3) 1_565 1_545 ? C6B K2 K2 57.92(3) 1_545 1_545 ? O1A K2 K2 135.85(3) . 1_565 ? O1A K2 K2 42.94(3) 1_565 1_565 ? O1B K2 K2 45.14(3) . 1_565 ? O1B K2 K2 135.48(3) 1_545 1_565 ? O1B K2 K2 93.46(3) 7_566 1_565 ? O3W K2 K2 107.44(3) . 1_565 ? C6A K2 K2 61.84(3) 1_565 1_565 ? C6B K2 K2 122.08(3) 1_545 1_565 ? K2 K2 K2 180.0 1_545 1_565 ? O1A K2 K2 125.70(4) . 7_566 ? O1A K2 K2 86.84(3) 1_565 7_566 ? O1B K2 K2 43.42(3) . 7_566 ? O1B K2 K2 84.11(3) 1_545 7_566 ? O1B K2 K2 42.55(3) 7_566 7_566 ? O3W K2 K2 148.02(3) . 7_566 ? C6A K2 K2 106.22(4) 1_565 7_566 ? C6B K2 K2 86.08(4) 1_545 7_566 ? K2 K2 K2 115.882(13) 1_545 7_566 ? K2 K2 K2 64.116(13) 1_565 7_566 ? O1A K2 K2 83.94(3) . 7_556 ? O1A K2 K2 128.68(3) 1_565 7_556 ? O1B K2 K2 87.57(3) . 7_556 ? O1B K2 K2 40.68(3) 1_545 7_556 ? O1B K2 K2 40.42(3) 7_566 7_556 ? O3W K2 K2 122.32(4) . 7_556 ? C6A K2 K2 134.78(4) 1_565 7_556 ? C6B K2 K2 56.14(3) 1_545 7_556 ? K2 K2 K2 59.479(12) 1_545 7_556 ? K2 K2 K2 120.519(12) 1_565 7_556 ? K2 K2 K2 56.403(13) 7_566 7_556 ? O1A K2 H11 101.3(3) . . ? O1A K2 H11 105.5(4) 1_565 . ? O1B K2 H11 89.1(3) . . ? O1B K2 H11 84.9(4) 1_545 . ? O1B K2 H11 165.1(5) 7_566 . ? O3W K2 H11 18.6(3) . . ? C6A K2 H11 98.0(5) 1_565 . ? C6B K2 H11 69.8(5) 1_545 . ? K2 K2 H11 87.0(3) 1_545 . ? K2 K2 H11 93.0(3) 1_565 . ? K2 K2 H11 131.0(3) 7_566 . ? K2 K2 H11 125.4(4) 7_556 . ? N7B C8B N9B 116.83(18) . . ? N7B C8B H7 121.7(13) . . ? N9B C8B H7 121.4(13) . . ? N9B C4B N3B 125.05(15) . . ? N9B C4B C5B 109.54(16) . . ? N3B C4B C5B 125.40(17) . . ? N9B C4B K1 66.59(9) . 8_465 ? N3B C4B K1 61.54(9) . 8_465 ? C5B C4B K1 160.25(13) . 8_465 ? N7B C5B C4B 108.85(16) . . ? N7B C5B C6B 131.14(15) . . ? C4B C5B C6B 119.97(16) . . ? O1B C6B N1B 119.19(17) . . ? O1B C6B C5B 128.40(17) . . ? N1B C6B C5B 112.41(15) . . ? O1B C6B K2 45.70(9) . 1_565 ? N1B C6B K2 113.54(12) . 1_565 ? C5B C6B K2 112.01(11) . 1_565 ? N3B C2B N2B 120.60(15) . . ? N3B C2B N1B 123.64(16) . . ? N2B C2B N1B 115.70(17) . . ? C8B N7B C5B 102.22(14) . . ? C8B N9B C4B 102.54(15) . . ? C8B N9B K1 155.32(13) . 8_465 ? C4B N9B K1 89.20(10) . 8_465 ? C8B N9B K1 115.31(12) . 8_455 ? C4B N9B K1 115.77(11) . 8_455 ? K1 N9B K1 77.31(4) 8_465 8_455 ? C2B N3B C4B 113.99(14) . . ? C2B N3B K1 144.92(12) . 8_465 ? C4B N3B K1 94.07(10) . 8_465 ? C2B N1B C6B 124.56(16) . . ? C2B N1B H8 117.4(13) . . ? C6B N1B H8 117.9(13) . . ? C2B N2B H9 116.6(16) . . ? C2B N2B H10 118.5(13) . . ? H9 N2B H10 115(2) . . ? C6B O1B K2 123.76(12) . . ? C6B O1B K2 115.09(12) . 1_565 ? K2 O1B K2 90.34(4) . 1_565 ? C6B O1B K2 126.68(12) . 7_566 ? K2 O1B K2 94.03(4) . 7_566 ? K2 O1B K2 98.90(4) 1_565 7_566 ? K2 O3W H11 77.0(15) . . ? K2 O3W H12 103.9(16) . . ? H11 O3W H12 109.4(16) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag K1 O2W 2.7302(15) . ? K1 O2W 2.7758(16) 1_565 ? K1 N3A 2.9036(17) . ? K1 N3B 2.9140(15) 8_566 ? K1 N9B 3.0341(17) 8_566 ? K1 O2W 3.0428(15) 5_657 ? K1 N9B 3.1152(16) 8_556 ? K1 N3A 3.2421(16) 1_565 ? K1 C4B 3.3061(18) 8_566 ? K1 C4A 3.395(2) . ? K1 N9A 3.4627(18) . ? K1 K1 3.84178(16) 1_545 ? K1 H5 2.82(2) . ? C8A N9A 1.323(3) . ? C8A N7A 1.342(3) . ? C8A H1 1.01(2) . ? C4A N3A 1.362(2) . ? C4A N9A 1.376(2) . ? C4A C5A 1.380(3) . ? C5A N7A 1.379(2) . ? C5A C6A 1.413(3) . ? C6A O1A 1.272(2) . ? C6A N1A 1.357(2) . ? C6A K2 3.3251(19) 1_545 ? C2A N3A 1.328(2) . ? C2A N1A 1.349(2) . ? C2A N2A 1.378(2) . ? N7A H2 0.84(2) . ? N2A H3 0.90(2) . ? N2A H4 0.83(2) . ? O1A K2 2.6205(13) . ? O1A K2 2.6792(14) 1_545 ? O2W H5 0.812(17) . ? O2W H6 0.799(18) . ? K2 O1B 2.6936(14) . ? K2 O1B 2.7234(14) 1_545 ? K2 O1B 2.7378(14) 7_566 ? K2 O3W 2.9218(17) . ? K2 C6B 3.4462(18) 1_545 ? K2 K2 3.84179(15) 1_545 ? K2 K2 3.84180(16) 1_565 ? K2 K2 3.9732(9) 7_566 ? K2 K2 4.1496(9) 7_556 ? K2 H11 2.86(2) . ? C8B N7B 1.336(2) . ? C8B N9B 1.357(2) . ? C8B H7 0.91(2) . ? C4B N9B 1.356(2) . ? C4B N3B 1.368(2) . ? C4B C5B 1.394(2) . ? C5B N7B 1.384(2) . ? C5B C6B 1.407(3) . ? C6B O1B 1.252(2) . ? C6B N1B 1.388(2) . ? C2B N3B 1.313(2) . ? C2B N2B 1.350(2) . ? C2B N1B 1.376(2) . ? N1B H8 0.85(2) . ? N2B H9 0.82(2) . ? N2B H10 0.89(2) . ? O3W H11 0.935(13) . ? O3W H12 0.922(13) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag O2W H5 N9A 0.812(17) 2.021(18) 2.814(2) 165(2) . yes N7A H2 O3W 0.84(2) 1.98(2) 2.822(2) 174(2) . yes O3W H11 N7B 0.935(13) 1.862(16) 2.775(2) 165(2) . yes N2A H3 N3B 0.90(2) 2.20(2) 3.026(2) 153.1(19) 8_556 yes N1B H8 O1A 0.85(2) 2.13(2) 2.972(2) 172.9(19) 7_566 yes O3W H12 N7B 0.922(13) 2.034(17) 2.914(2) 158.9(19) 1_545 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N3A C4A C5A N7A -178.93(19) . . . . ? N9A C4A C5A N7A 0.3(2) . . . . ? K1 C4A C5A N7A -100.1(2) . . . . ? N3A C4A C5A C6A -0.8(3) . . . . ? N9A C4A C5A C6A 178.36(18) . . . . ? K1 C4A C5A C6A 78.0(3) . . . . ? C4A C5A C6A O1A -177.15(18) . . . . ? N7A C5A C6A O1A 0.3(4) . . . . ? C4A C5A C6A N1A 2.7(3) . . . . ? N7A C5A C6A N1A -179.8(2) . . . . ? C4A C5A C6A K2 129.03(16) . . . 1_545 ? N7A C5A C6A K2 -53.5(3) . . . 1_545 ? N7A C8A N9A C4A -0.1(3) . . . . ? N7A C8A N9A K1 84.3(3) . . . . ? N3A C4A N9A C8A 179.1(2) . . . . ? C5A C4A N9A C8A -0.1(2) . . . . ? K1 C4A N9A C8A 139.44(16) . . . . ? N3A C4A N9A K1 39.65(18) . . . . ? C5A C4A N9A K1 -139.53(16) . . . . ? N9A C8A N7A C5A 0.3(3) . . . . ? C4A C5A N7A C8A -0.3(2) . . . . ? C6A C5A N7A C8A -178.0(2) . . . . ? N3A C2A N1A C6A 1.0(3) . . . . ? N2A C2A N1A C6A -175.31(16) . . . . ? O1A C6A N1A C2A 177.10(17) . . . . ? C5A C6A N1A C2A -2.8(3) . . . . ? K2 C6A N1A C2A -128.31(15) 1_545 . . . ? N1A C2A N3A C4A 1.0(3) . . . . ? N2A C2A N3A C4A 177.19(17) . . . . ? N1A C2A N3A K1 -116.49(18) . . . . ? N2A C2A N3A K1 59.7(2) . . . . ? N1A C2A N3A K1 152.74(16) . . . 1_545 ? N2A C2A N3A K1 -31.1(2) . . . 1_545 ? N9A C4A N3A C2A 179.89(19) . . . . ? C5A C4A N3A C2A -1.0(3) . . . . ? K1 C4A N3A C2A -131.82(17) . . . . ? N9A C4A N3A K1 -48.3(2) . . . . ? C5A C4A N3A K1 130.78(18) . . . . ? N9A C4A N3A K1 32.4(3) . . . 1_545 ? C5A C4A N3A K1 -148.56(16) . . . 1_545 ? K1 C4A N3A K1 80.66(11) . . . 1_545 ? N1A C6A O1A K2 -143.91(15) . . . . ? C5A C6A O1A K2 35.9(3) . . . . ? K2 C6A O1A K2 122.8(2) 1_545 . . . ? N1A C6A O1A K2 93.26(17) . . . 1_545 ? C5A C6A O1A K2 -86.88(19) . . . 1_545 ? N9B C4B C5B N7B -1.4(2) . . . . ? N3B C4B C5B N7B 178.03(17) . . . . ? K1 C4B C5B N7B 73.6(4) 8_465 . . . ? N9B C4B C5B C6B -179.54(17) . . . . ? N3B C4B C5B C6B -0.1(3) . . . . ? K1 C4B C5B C6B -104.6(4) 8_465 . . . ? N7B C5B C6B O1B 0.8(3) . . . . ? C4B C5B C6B O1B 178.49(19) . . . . ? N7B C5B C6B N1B -178.57(18) . . . . ? C4B C5B C6B N1B -0.9(3) . . . . ? N7B C5B C6B K2 -49.3(2) . . . 1_565 ? C4B C5B C6B K2 128.35(15) . . . 1_565 ? N9B C8B N7B C5B -0.4(2) . . . . ? C4B C5B N7B C8B 1.1(2) . . . . ? C6B C5B N7B C8B 178.9(2) . . . . ? N7B C8B N9B C4B -0.4(2) . . . . ? N7B C8B N9B K1 -117.1(3) . . . 8_465 ? N7B C8B N9B K1 126.30(15) . . . 8_455 ? N3B C4B N9B C8B -178.36(18) . . . . ? C5B C4B N9B C8B 1.1(2) . . . . ? K1 C4B N9B C8B -158.10(14) 8_465 . . . ? N3B C4B N9B K1 -20.26(19) . . . 8_465 ? C5B C4B N9B K1 159.17(14) . . . 8_465 ? N3B C4B N9B K1 55.2(2) . . . 8_455 ? C5B C4B N9B K1 -125.35(13) . . . 8_455 ? K1 C4B N9B K1 75.48(7) 8_465 . . 8_455 ? N2B C2B N3B C4B 177.83(17) . . . . ? N1B C2B N3B C4B 0.8(3) . . . . ? N2B C2B N3B K1 -41.9(3) . . . 8_465 ? N1B C2B N3B K1 141.02(16) . . . 8_465 ? N9B C4B N3B C2B 179.58(18) . . . . ? C5B C4B N3B C2B 0.2(3) . . . . ? K1 C4B N3B C2B 158.39(17) 8_465 . . . ? N9B C4B N3B K1 21.19(19) . . . 8_465 ? C5B C4B N3B K1 -158.15(17) . . . 8_465 ? N3B C2B N1B C6B -2.0(3) . . . . ? N2B C2B N1B C6B -179.18(17) . . . . ? O1B C6B N1B C2B -177.54(17) . . . . ? C5B C6B N1B C2B 1.9(3) . . . . ? K2 C6B N1B C2B -126.54(15) 1_565 . . . ? N1B C6B O1B K2 -155.89(12) . . . . ? C5B C6B O1B K2 24.8(3) . . . . ? K2 C6B O1B K2 108.72(14) 1_565 . . . ? N1B C6B O1B K2 95.40(17) . . . 1_565 ? C5B C6B O1B K2 -84.0(2) . . . 1_565 ? N1B C6B O1B K2 -28.8(2) . . . 7_566 ? C5B C6B O1B K2 151.86(15) . . . 7_566 ? K2 C6B O1B K2 -124.17(16) 1_565 . . 7_566 ? _cod_database_fobs_code 2108858