#------------------------------------------------------------------------------ #$Date: 2021-09-22 04:44:10 +0300 (Wed, 22 Sep 2021) $ #$Revision: 269238 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/88/2108862.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108862 _cell_angle_alpha 90.000 _cell_angle_beta 101.608 _cell_angle_gamma 90.000 _cell_length_a 10.5290 _cell_length_b 11.6677 _cell_length_c 11.1762 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.7200 _cod_data_source_file xk5085GuaNa_100Ksup7.hkl _cod_data_source_block GuaNa_100K _shelx_title ' GuaNa_100K in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.01 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 498.21 443.36 4.73 o 2 0 0 5097.20 5190.59 13.82 o 3 0 0 475.81 511.06 5.70 o 4 0 0 704.53 700.80 11.91 o 5 0 0 4328.06 4304.59 159.00 o 6 0 0 1932.41 2103.62 52.83 o 7 0 0 266.99 249.47 1.81 o 8 0 0 191.73 175.29 1.81 o 9 0 0 3.82 12.59 8.13 o 10 0 0 689.66 545.03 285.87 o 11 0 0 5.93 13.34 10.34 o 12 0 0 66.11 39.26 23.26 o 13 0 0 26.88 16.74 14.26 o 14 0 0 201.21 210.43 117.44 o 1 1 0 200.89 181.97 1.61 o 2 1 0 3239.30 3229.80 19.49 o 3 1 0 4.12 5.73 1.33 o 4 1 0 78.06 53.01 1.66 o 5 1 0 715.22 788.29 10.66 o 6 1 0 51.58 79.41 1.77 o 7 1 0 12.46 12.11 0.90 o 8 1 0 28.12 30.32 1.47 o 9 1 0 173.52 171.34 53.12 o 10 1 0 319.83 297.29 90.83 o 11 1 0 451.28 407.66 124.42 o 12 1 0 42.36 41.91 14.00 o 13 1 0 5.37 1.41 2.47 o 14 1 0 19.53 9.99 3.71 o 0 2 0 42.44 48.59 1.00 o 1 2 0 241.80 254.86 0.63 o 2 2 0 108.19 135.85 1.53 o 3 2 0 203.72 202.10 4.00 o 4 2 0 731.06 593.78 7.61 o 5 2 0 4535.66 4503.46 33.05 o 6 2 0 506.71 548.91 3.23 o 7 2 0 4.21 6.97 1.18 o 8 2 0 55.12 50.10 1.61 o 9 2 0 339.61 330.33 100.48 o 10 2 0 1436.92 1418.59 25.63 o 11 2 0 134.53 118.81 38.12 o 12 2 0 103.67 93.50 30.06 o 13 2 0 155.14 141.32 45.75 o 14 2 0 112.96 109.73 35.66 o 1 3 0 384.95 395.63 2.50 o 2 3 0 2310.16 2488.65 19.81 o 3 3 0 5148.76 5392.04 36.68 o 4 3 0 1.26 2.83 0.51 o 5 3 0 933.85 907.68 12.78 o 6 3 0 2657.03 2715.17 16.22 o 7 3 0 383.18 361.80 5.79 o 8 3 0 2.77 1.98 0.91 o 9 3 0 400.56 362.40 110.17 o 10 3 0 1.34 0.07 1.25 o 11 3 0 291.06 311.22 95.35 o 12 3 0 0.35 -1.96 1.96 o 13 3 0 7.96 5.37 2.31 o 14 3 0 47.83 36.90 14.01 o 0 4 0 61.24 61.04 0.80 o 1 4 0 841.19 746.30 10.68 o 2 4 0 4190.19 4094.59 17.07 o 3 4 0 528.10 571.74 5.73 o 4 4 0 884.10 859.53 12.31 o 5 4 0 1188.86 1286.29 10.15 o 6 4 0 822.82 832.24 6.45 o 7 4 0 287.29 303.39 2.72 o 8 4 0 216.29 215.14 3.40 o 9 4 0 52.08 48.98 2.82 o 10 4 0 36.72 28.42 9.06 o 11 4 0 484.32 480.59 145.64 o 12 4 0 506.98 479.69 7.03 o 13 4 0 342.67 334.57 104.51 o 1 5 0 25.28 24.64 1.59 o 2 5 0 5050.86 4575.83 15.19 o 3 5 0 8900.46 8547.39 42.34 o 4 5 0 2413.98 2429.84 28.71 o 5 5 0 1565.18 1598.44 4.36 o 6 5 0 112.94 118.50 2.13 o 7 5 0 422.43 428.63 2.53 o 8 5 0 20.83 24.84 2.31 o 9 5 0 5.30 4.56 1.89 o 10 5 0 105.31 93.89 30.77 o 11 5 0 46.09 54.14 5.04 o 12 5 0 0.06 -1.86 2.11 o 13 5 0 34.67 29.82 12.23 o 0 6 0 1027.17 957.11 2.67 o 1 6 0 2628.84 2445.20 25.08 o 2 6 0 1148.61 1198.65 11.48 o 3 6 0 704.18 735.76 3.11 o 4 6 0 579.80 587.65 6.63 o 5 6 0 161.68 157.34 1.10 o 6 6 0 182.14 163.93 1.42 o 7 6 0 674.45 641.60 4.03 o 8 6 0 635.98 630.83 6.82 o 9 6 0 210.31 212.45 2.67 o 10 6 0 71.71 71.27 1.66 o 11 6 0 140.38 152.01 6.53 o 12 6 0 520.63 589.74 15.07 o 13 6 0 32.76 31.05 4.31 o 1 7 0 1518.96 1628.39 18.85 o 2 7 0 78.75 58.37 0.87 o 3 7 0 479.73 554.80 5.23 o 4 7 0 1425.79 1457.08 2.96 o 5 7 0 84.98 66.55 2.67 o 6 7 0 467.98 470.80 4.78 o 7 7 0 83.08 82.00 2.46 o 8 7 0 1584.36 1582.09 5.07 o 9 7 0 146.55 168.59 2.91 o 10 7 0 11.54 7.90 1.59 o 11 7 0 20.97 23.40 1.91 o 12 7 0 120.25 126.10 5.63 o 0 8 0 360.07 333.69 2.09 o 1 8 0 741.66 767.61 8.87 o 2 8 0 1210.77 1234.05 8.80 o 3 8 0 3152.55 3113.49 26.79 o 4 8 0 1267.24 1218.73 12.58 o 5 8 0 18.38 23.26 1.41 o 6 8 0 344.33 316.97 6.79 o 7 8 0 0.64 2.10 1.16 o 8 8 0 393.83 401.29 7.08 o 9 8 0 0.49 -0.65 1.45 o 10 8 0 51.13 53.48 2.91 o 11 8 0 23.40 19.25 2.76 o 12 8 0 16.29 20.13 2.38 o 1 9 0 341.09 329.77 5.58 o 2 9 0 310.74 273.98 3.72 o 3 9 0 34.53 43.60 2.88 o 4 9 0 229.00 215.73 1.47 o 5 9 0 46.12 47.14 1.30 o 6 9 0 3.75 3.90 1.12 o 7 9 0 4.47 5.26 1.28 o 8 9 0 0.00 0.37 1.38 o 9 9 0 73.78 80.10 2.51 o 10 9 0 66.22 73.46 4.03 o 11 9 0 272.14 309.76 4.91 o 0 10 0 28.51 92.55 39.61 o 1 10 0 3103.97 3102.79 25.75 o 2 10 0 1301.89 1257.72 17.04 o 3 10 0 174.29 172.37 2.32 o 4 10 0 398.67 371.53 1.88 o 5 10 0 9.55 5.55 1.22 o 6 10 0 958.57 926.34 7.51 o 7 10 0 54.47 58.70 4.15 o 8 10 0 1.26 1.21 1.54 o 9 10 0 4.10 4.53 1.89 o 10 10 0 266.93 280.27 9.81 o 11 10 0 133.46 146.23 3.12 o 1 11 0 489.10 461.47 4.38 o 2 11 0 33.78 36.01 1.65 o 3 11 0 1.19 3.79 1.29 o 4 11 0 593.88 573.33 12.35 o 5 11 0 1604.25 1546.83 23.02 o 6 11 0 744.23 732.75 13.12 o 7 11 0 8.84 12.48 2.34 o 8 11 0 46.72 40.32 1.82 o 9 11 0 151.10 173.43 4.34 o 10 11 0 55.98 53.14 2.18 o 0 12 0 0.83 0.64 2.10 o 1 12 0 106.67 101.15 3.10 o 2 12 0 131.74 127.65 1.76 o 3 12 0 61.38 58.25 1.92 o 4 12 0 327.34 351.40 5.20 o 5 12 0 103.58 103.11 3.86 o 6 12 0 37.12 39.89 1.87 o 7 12 0 234.86 242.59 5.31 o 8 12 0 146.95 135.55 4.34 o 9 12 0 520.17 539.67 9.46 o 1 13 0 7.60 11.96 1.68 o 2 13 0 4.82 2.12 1.72 o 3 13 0 3.96 7.47 1.77 o 4 13 0 143.59 151.45 6.92 o 5 13 0 2.80 6.81 1.88 o 6 13 0 211.11 195.51 5.84 o 7 13 0 281.04 270.68 13.68 o 8 13 0 67.55 55.61 3.14 o 0 14 0 379.85 382.22 5.89 o 1 14 0 94.39 96.36 2.99 o 2 14 0 382.99 406.78 12.69 o 3 14 0 122.83 125.44 2.34 o 4 14 0 107.26 90.39 2.84 o 5 14 0 81.90 89.08 2.47 o 6 14 0 11.81 11.04 2.30 o 7 14 0 39.37 39.14 5.13 o 1 15 0 648.32 650.23 16.45 o 2 15 0 198.33 187.39 6.98 o 3 15 0 142.34 165.73 9.12 o 4 15 0 30.17 28.47 3.72 o 5 15 0 0.23 1.24 2.58 o 0 16 0 0.21 -3.99 3.99 o 1 16 0 37.26 41.71 4.84 o 2 16 0 84.37 95.26 3.45 o -14 1 1 102.99 102.36 36.34 o -13 1 1 1.80 -2.11 2.11 o -12 1 1 29.16 27.88 11.51 o -11 1 1 266.49 204.40 63.48 o -10 1 1 7.15 17.18 7.14 o -9 1 1 1324.35 1224.00 6.03 o -8 1 1 275.01 295.07 1.54 o -7 1 1 47.82 54.13 0.98 o -6 1 1 3292.27 3586.09 23.77 o -5 1 1 938.90 811.73 8.62 o -4 1 1 6486.52 6420.52 13.35 o -3 1 1 11.57 18.59 0.82 o -2 1 1 586.37 560.79 5.89 o -1 1 1 133.73 117.48 2.02 o 0 1 1 207.92 256.64 7.81 o 1 1 1 4880.75 4894.88 18.75 o 2 1 1 2.65 4.05 0.58 o 3 1 1 534.22 550.25 9.32 o 4 1 1 2644.05 2807.58 7.73 o 5 1 1 520.57 480.31 3.42 o 6 1 1 33.50 47.97 1.12 o 7 1 1 433.80 417.05 4.61 o 8 1 1 363.69 337.29 7.81 o 9 1 1 17.18 14.03 5.62 o 10 1 1 1.43 2.32 1.61 o 11 1 1 1512.20 1483.06 14.22 o 12 1 1 114.78 98.52 32.78 o 13 1 1 10.48 5.54 3.13 o 14 1 1 298.80 294.53 93.43 o -14 2 1 208.29 244.13 4.98 o -13 2 1 3.26 2.56 2.16 o -12 2 1 219.76 202.76 61.49 o -11 2 1 153.30 123.74 39.87 o -10 2 1 202.97 194.47 61.03 o -9 2 1 1858.38 1757.66 20.55 o -8 2 1 781.58 824.60 7.15 o -7 2 1 135.02 127.04 3.18 o -6 2 1 195.36 224.84 2.30 o -5 2 1 1549.28 1436.72 11.54 o -4 2 1 10855.65 10839.91 32.18 o -3 2 1 152.84 153.60 1.74 o -2 2 1 1121.71 1190.67 7.63 o -1 2 1 1509.58 1601.11 7.01 o 0 2 1 2299.97 2459.81 10.93 o 1 2 1 412.56 397.81 3.21 o 2 2 1 1095.99 997.13 6.33 o 3 2 1 1912.46 1872.09 12.72 o 4 2 1 152.11 165.21 4.13 o 5 2 1 516.58 565.43 8.60 o 6 2 1 45.26 38.99 0.73 o 7 2 1 220.77 215.83 5.61 o 8 2 1 501.85 495.91 9.81 o 9 2 1 825.98 747.99 196.95 o 10 2 1 120.73 115.88 36.74 o 11 2 1 138.29 129.11 40.58 o 12 2 1 81.53 78.50 26.28 o 13 2 1 5.31 0.59 2.18 o -14 3 1 125.71 122.28 41.23 o -13 3 1 0.09 0.10 2.17 o -12 3 1 14.77 9.06 4.69 o -11 3 1 29.35 19.03 7.97 o -10 3 1 912.66 874.37 262.21 o -9 3 1 140.29 140.58 4.70 o -8 3 1 16.87 18.99 1.42 o -7 3 1 1263.42 1161.99 10.99 o -6 3 1 56.60 81.18 0.89 o -5 3 1 863.89 898.15 2.88 o -4 3 1 981.80 1055.43 11.08 o -3 3 1 2624.87 2663.89 18.99 o -2 3 1 1259.79 1326.69 8.13 o -1 3 1 1591.02 1649.54 14.23 o 0 3 1 561.77 573.22 9.60 o 1 3 1 1683.58 1716.45 12.20 o 2 3 1 2356.56 2458.11 9.27 o 3 3 1 3038.17 3319.66 16.63 o 4 3 1 3.24 1.60 0.45 o 5 3 1 171.97 128.81 1.06 o 6 3 1 808.86 801.96 13.88 o 7 3 1 812.85 825.65 8.05 o 8 3 1 18.02 18.33 0.99 o 9 3 1 251.37 249.05 77.11 o 10 3 1 398.16 310.10 93.26 o 11 3 1 265.13 265.82 81.86 o 12 3 1 3.55 0.07 1.81 o 13 3 1 112.12 105.48 33.53 o -14 4 1 0.11 1.64 2.72 o -13 4 1 1.93 5.86 7.68 o -12 4 1 0.29 8.38 2.08 o -11 4 1 73.72 63.55 20.50 o -10 4 1 60.57 47.71 15.48 o -9 4 1 166.36 148.39 4.63 o -8 4 1 306.81 270.97 2.49 o -7 4 1 357.01 326.88 4.20 o -6 4 1 281.38 292.21 3.53 o -5 4 1 24.72 14.26 1.16 o -4 4 1 1623.99 1799.31 17.13 o -3 4 1 1131.33 951.22 5.18 o -2 4 1 2701.12 2804.98 10.20 o -1 4 1 1406.90 1408.72 11.09 o 0 4 1 7330.58 7046.96 36.83 o 1 4 1 1102.00 1172.41 14.99 o 2 4 1 289.35 257.72 4.26 o 3 4 1 1154.36 1220.75 14.37 o 4 4 1 16.28 16.07 1.55 o 5 4 1 499.92 466.01 2.61 o 6 4 1 164.58 163.08 1.90 o 7 4 1 265.92 241.91 3.41 o 8 4 1 910.82 808.32 4.27 o 9 4 1 263.95 218.00 67.42 o 10 4 1 4.27 0.55 1.30 o 11 4 1 6.01 3.69 1.65 o 12 4 1 0.28 0.53 1.85 o 13 4 1 336.77 335.52 100.64 o -13 5 1 112.39 105.81 34.55 o -12 5 1 427.63 452.47 136.39 o -11 5 1 104.38 98.14 5.41 o -10 5 1 195.37 175.52 3.43 o -9 5 1 759.32 711.94 6.19 o -8 5 1 66.43 62.31 1.46 o -7 5 1 27.67 24.63 1.21 o -6 5 1 88.07 101.45 1.19 o -5 5 1 378.63 383.20 3.00 o -4 5 1 716.18 754.75 3.90 o -3 5 1 3576.81 3614.72 21.63 o -2 5 1 602.24 755.18 3.60 o -1 5 1 2098.14 2119.29 12.69 o 0 5 1 7845.96 8020.72 62.50 o 1 5 1 392.11 434.36 6.52 o 2 5 1 775.47 900.61 8.44 o 3 5 1 508.31 516.89 3.16 o 4 5 1 163.79 163.43 0.88 o 5 5 1 67.88 72.50 0.79 o 6 5 1 507.70 531.13 2.70 o 7 5 1 5987.90 5576.57 25.06 o 8 5 1 1847.81 1808.67 3.61 o 9 5 1 241.10 237.21 72.11 o 10 5 1 98.88 87.46 27.90 o 11 5 1 40.36 44.20 14.19 o 12 5 1 24.53 37.22 12.92 o 13 5 1 224.77 268.49 4.98 o -13 6 1 71.75 90.68 3.70 o -12 6 1 4.83 10.31 2.15 o -11 6 1 228.71 225.72 6.45 o -10 6 1 75.84 70.99 3.89 o -9 6 1 113.71 126.71 1.81 o -8 6 1 2270.38 2199.40 24.30 o -7 6 1 1964.70 1901.21 5.31 o -6 6 1 1207.94 1234.44 12.49 o -5 6 1 2733.98 2704.66 16.02 o -4 6 1 103.84 102.35 3.83 o -3 6 1 2024.95 2019.05 12.01 o -2 6 1 622.12 587.58 10.09 o -1 6 1 2584.87 2451.32 10.14 o 0 6 1 1476.29 1496.76 23.03 o 1 6 1 2708.74 2686.55 4.72 o 2 6 1 1778.76 1772.32 8.15 o 3 6 1 3279.17 3510.81 17.07 o 4 6 1 144.54 130.13 1.46 o 5 6 1 420.68 437.19 4.43 o 6 6 1 644.09 618.82 4.95 o 7 6 1 713.50 710.74 7.24 o 8 6 1 1.04 1.96 1.11 o 9 6 1 899.72 878.19 12.26 o 10 6 1 0.06 1.84 1.41 o 11 6 1 0.24 0.55 2.01 o 12 6 1 84.26 96.05 4.16 o 13 6 1 54.42 54.04 6.22 o -13 7 1 13.33 9.06 3.44 o -12 7 1 320.78 342.19 3.28 o -11 7 1 76.95 81.59 2.69 o -10 7 1 35.80 40.73 2.82 o -9 7 1 77.63 75.13 2.20 o -8 7 1 1345.84 1346.64 14.76 o -7 7 1 600.02 571.53 5.23 o -6 7 1 143.54 146.29 1.78 o -5 7 1 6.29 11.67 1.95 o -4 7 1 161.59 156.26 2.44 o -3 7 1 619.22 608.74 14.52 o -2 7 1 16.04 30.44 0.84 o -1 7 1 65.90 62.55 1.07 o 0 7 1 51.99 69.50 1.10 o 1 7 1 140.21 139.71 1.37 o 2 7 1 107.13 119.53 2.05 o 3 7 1 302.84 282.29 3.70 o 4 7 1 276.26 286.91 2.35 o 5 7 1 765.59 770.58 6.90 o 6 7 1 550.45 533.57 3.26 o 7 7 1 53.39 50.75 1.06 o 8 7 1 222.28 205.90 3.62 o 9 7 1 340.34 327.48 9.54 o 10 7 1 5.44 7.83 1.51 o 11 7 1 76.32 78.48 2.69 o 12 7 1 387.03 389.44 13.67 o -12 8 1 32.95 45.36 3.27 o -11 8 1 10.37 13.75 2.10 o -10 8 1 46.73 49.16 1.95 o -9 8 1 626.10 627.97 4.64 o -8 8 1 294.76 277.72 2.15 o -7 8 1 648.12 623.64 10.18 o -6 8 1 32.25 32.70 1.18 o -5 8 1 179.88 184.83 1.42 o -4 8 1 76.37 79.68 1.98 o -3 8 1 720.32 677.28 12.21 o -2 8 1 644.42 657.13 7.37 o -1 8 1 22.49 19.07 1.16 o 0 8 1 50.56 39.84 0.92 o 1 8 1 838.29 795.08 5.40 o 2 8 1 404.87 402.46 10.03 o 3 8 1 4.67 4.74 0.82 o 4 8 1 578.17 599.61 7.91 o 5 8 1 21.08 18.98 1.26 o 6 8 1 1.07 2.12 0.93 o 7 8 1 15.33 13.53 1.05 o 8 8 1 68.14 69.98 1.82 o 9 8 1 1.23 1.95 1.33 o 10 8 1 186.34 194.49 6.29 o 11 8 1 165.48 161.31 5.97 o 12 8 1 190.94 201.97 4.65 o -12 9 1 25.06 27.21 3.17 o -11 9 1 0.75 -2.58 2.83 o -10 9 1 0.46 -1.00 1.96 o -9 9 1 33.07 39.42 2.10 o -8 9 1 328.04 302.32 5.20 o -7 9 1 5.36 3.05 1.34 o -6 9 1 405.83 384.15 1.98 o -5 9 1 0.03 1.59 1.13 o -4 9 1 324.38 318.31 3.23 o -3 9 1 657.36 637.70 10.03 o -2 9 1 1512.35 1418.78 22.75 o -1 9 1 97.89 92.25 1.88 o 0 9 1 286.14 277.65 2.64 o 1 9 1 99.16 100.58 2.64 o 2 9 1 126.34 120.30 2.89 o 3 9 1 635.38 587.97 3.82 o 4 9 1 342.67 317.82 9.16 o 5 9 1 20.74 24.30 1.44 o 6 9 1 44.20 51.20 3.01 o 7 9 1 100.31 94.66 2.26 o 8 9 1 229.07 230.48 6.06 o 9 9 1 430.35 432.71 14.38 o 10 9 1 69.50 80.10 4.56 o 11 9 1 8.78 9.17 2.00 o -11 10 1 371.22 374.04 5.64 o -10 10 1 2.76 5.66 2.48 o -9 10 1 12.45 17.56 1.89 o -8 10 1 32.90 37.55 1.74 o -7 10 1 25.45 21.09 1.53 o -6 10 1 21.84 22.02 1.66 o -5 10 1 277.42 254.99 5.27 o -4 10 1 97.81 91.72 2.47 o -3 10 1 544.98 542.56 6.44 o -2 10 1 195.72 201.60 3.03 o -1 10 1 0.05 1.47 1.11 o 0 10 1 109.12 101.47 2.98 o 1 10 1 14.73 16.28 1.11 o 2 10 1 137.88 134.95 1.50 o 3 10 1 35.67 35.93 1.24 o 4 10 1 23.56 21.03 1.13 o 5 10 1 745.84 793.94 19.32 o 6 10 1 468.88 451.94 5.56 o 7 10 1 3.99 4.03 1.26 o 8 10 1 11.40 6.53 1.46 o 9 10 1 545.04 587.87 12.73 o 10 10 1 95.01 75.45 2.59 o 11 10 1 335.99 289.22 5.90 o -10 11 1 382.46 409.54 8.32 o -9 11 1 9.93 13.40 2.96 o -8 11 1 23.97 29.42 1.92 o -7 11 1 471.77 443.20 4.68 o -6 11 1 25.77 32.25 1.64 o -5 11 1 901.17 870.43 15.69 o -4 11 1 5.05 8.98 1.38 o -3 11 1 148.26 133.94 2.67 o -2 11 1 888.88 823.23 13.48 o -1 11 1 2.09 6.64 1.27 o 0 11 1 1728.34 1618.22 21.31 o 1 11 1 32.59 33.06 1.34 o 2 11 1 964.36 961.82 13.46 o 3 11 1 139.89 139.15 3.46 o 4 11 1 658.97 618.05 4.78 o 5 11 1 161.21 181.70 4.84 o 6 11 1 44.01 35.65 1.43 o 7 11 1 0.02 0.64 1.45 o 8 11 1 1.28 1.47 2.22 o 9 11 1 97.02 95.97 1.73 o 10 11 1 297.47 322.93 14.55 o -9 12 1 5.41 7.22 2.56 o -8 12 1 26.36 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