#------------------------------------------------------------------------------ #$Date: 2022-01-01 06:16:20 +0200 (Sat, 01 Jan 2022) $ #$Revision: 271664 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/89/2108903.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108903 _cell_angle_alpha 95.557 _cell_angle_beta 98.352 _cell_angle_gamma 98.065 _cell_length_a 6.2055 _cell_length_b 7.8091 _cell_length_c 10.7762 _exptl_crystal_F_000 368.00 _reflns_d_resolution_high 0.7340 _cod_data_source_file yh5016NaRh-2sup5.hkl _cod_data_source_block NaRh-2 _shelx_title ' z476 in P-1; 295K; Xcalibur' _shelx_refln_list_code 4 _shelx_f_calc_maximum 117.25 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 24.22 20.74 2.59 o 2 0 0 2857.49 2912.86 67.53 o 3 0 0 471.27 478.18 16.57 o 4 0 0 3938.44 4075.76 91.48 o 5 0 0 26.12 36.94 7.12 o 6 0 0 609.34 652.09 49.23 o 7 0 0 263.61 275.78 35.21 o -7 1 0 1019.25 1036.42 69.68 o -6 1 0 1041.55 1038.15 63.76 o -5 1 0 1623.30 1669.25 78.65 o -4 1 0 1197.03 1221.41 39.73 o -3 1 0 1260.54 1296.80 46.80 o -2 1 0 1102.84 1158.60 29.99 o -1 1 0 4916.53 4976.48 90.10 o 0 1 0 1143.28 1179.31 17.77 o 1 1 0 6275.31 6362.99 114.36 o 2 1 0 269.78 308.39 14.14 o 3 1 0 4844.36 4594.52 133.68 o 4 1 0 516.01 534.76 25.48 o 5 1 0 2904.41 2969.88 114.29 o 6 1 0 0.33 1.11 6.66 o 7 1 0 1329.61 1251.62 78.78 o -7 2 0 796.14 703.19 57.12 o -6 2 0 579.67 657.24 49.33 o -5 2 0 106.05 118.17 18.56 o -4 2 0 830.35 839.19 39.13 o -3 2 0 1978.62 2069.39 67.16 o -2 2 0 10089.69 9990.97 181.17 o -1 2 0 4987.13 5015.42 95.28 o 0 2 0 13498.72 11548.56 273.16 o 1 2 0 3722.39 3891.71 78.12 o 2 2 0 1848.25 1847.77 46.69 o 3 2 0 1384.21 1357.31 65.73 o 4 2 0 927.21 1026.85 38.33 o 5 2 0 206.00 176.44 23.08 o 6 2 0 374.49 435.84 41.70 o 7 2 0 24.86 7.93 7.48 o -7 3 0 69.72 91.10 20.31 o -6 3 0 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