#------------------------------------------------------------------------------ #$Date: 2022-04-07 04:45:56 +0300 (Thu, 07 Apr 2022) $ #$Revision: 274414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/89/2108959.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108959 _cell_angle_alpha 90.000(5) _cell_angle_beta 111.747(7) _cell_angle_gamma 90.000(5) _cell_length_a 20.7891(16) _cell_length_b 3.8267(2) _cell_length_c 25.145(2) _exptl_crystal_F_000 872 _reflns_d_resolution_high 0.8930 _cod_data_source_file aw5065295Ksup2.hkl _cod_data_source_block 295K _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 351.38 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 11074.20 10954.50 61.30 o 6 0 0 3945.38 3901.50 55.87 o 8 0 0 822.22 819.69 48.55 o 10 0 0 712.85 807.19 51.66 o 12 0 0 599.67 626.22 54.77 o 14 0 0 1258.93 1336.24 64.17 o 16 0 0 115.79 102.59 58.43 < 18 0 0 129.75 178.10 154.25 < 1 1 0 234.90 232.14 31.53 o 2 1 0 4364.71 4258.62 23.79 o 3 1 0 156.06 131.93 18.85 o 4 1 0 4349.97 4402.20 34.16 o 5 1 0 0.54 18.11 33.49 < 6 1 0 241.10 253.85 28.00 o 7 1 0 281.77 333.39 29.89 o 8 1 0 179.75 116.99 30.56 o 9 1 0 176.24 220.12 32.14 o 10 1 0 992.93 952.78 39.16 o 11 1 0 4993.37 5390.35 59.77 o 12 1 0 262.41 278.68 37.75 o 13 1 0 317.16 376.57 40.32 o 14 1 0 334.98 274.71 41.35 o 15 1 0 53.43 85.57 41.90 < 16 1 0 225.05 195.67 44.40 o 17 1 0 18.62 34.28 67.76 < 0 2 0 1111.01 1314.83 63.80 o 1 2 0 27.45 27.63 34.77 < 2 2 0 2677.55 2655.89 30.50 o 3 2 0 402.73 414.27 17.08 o 4 2 0 272.87 323.08 19.82 o 5 2 0 1115.09 1102.52 25.56 o 6 2 0 16.72 15.74 28.36 < 7 2 0 1122.72 1143.20 29.28 o 8 2 0 133.77 145.04 26.47 o 9 2 0 28.71 42.70 27.39 < 10 2 0 18.44 38.73 39.40 < 11 2 0 212.22 256.11 32.45 o 12 2 0 692.31 686.11 37.02 o 13 2 0 20.09 57.58 40.13 < 14 2 0 460.44 436.77 37.63 o 15 2 0 384.65 395.42 39.83 o 16 2 0 9.62 53.86 57.70 < 17 2 0 58.29 93.08 78.44 < 18 2 0 236.49 184.51 132.84 < 1 3 0 10.66 32.45 43.67 < 2 3 0 3.67 27.87 57.88 < 3 3 0 25.12 47.15 37.69 < 4 3 0 1194.66 1099.22 50.81 o 5 3 0 351.89 362.24 25.50 o 6 3 0 142.95 137.78 22.87 o 7 3 0 14.29 41.11 23.18 < 8 3 0 1.92 21.59 34.40 < 9 3 0 172.94 155.35 27.69 o 10 3 0 48.02 58.74 31.17 < 11 3 0 0.12 33.79 94.05 < 12 3 0 159.63 149.74 46.48 o 13 3 0 28.66 114.30 88.81 < 14 3 0 14.60 74.53 89.42 < 15 3 0 0.05 59.16 97.16 < 7 4 0 84.67 82.52 146.51 < -17 0 1 555.91 536.92 65.08 o -15 0 1 2.26 43.24 70.94 < -13 0 1 1616.05 1905.68 66.06 o -11 0 1 537.14 670.80 55.38 o -9 0 1 9.25 47.39 55.93 < -7 0 1 762.23 736.86 49.34 o -5 0 1 12748.20 12273.30 74.35 o 3 0 1 714.67 679.22 37.02 o 5 0 1 1690.31 1673.17 45.26 o 7 0 1 137.64 108.51 42.45 < 9 0 1 29242.50 30318.00 141.38 o 11 0 1 1136.62 1219.99 53.55 o 13 0 1 2666.51 2717.74 69.53 o 15 0 1 184.85 231.71 60.75 o 17 0 1 85.98 67.15 86.67 < -19 1 1 3.71 9.33 138.39 < -18 1 1 20.39 46.42 135.34 < -17 1 1 419.29 449.22 53.74 o -16 1 1 7.22 26.17 60.93 < -15 1 1 732.39 751.86 45.74 o -14 1 1 4.71 44.65 52.88 < -13 1 1 290.04 339.37 38.43 o -12 1 1 342.21 346.14 38.18 o -11 1 1 643.17 658.18 38.18 o -10 1 1 66.70 87.89 34.52 < -9 1 1 742.00 704.96 35.80 o -8 1 1 229.86 236.53 31.90 o -7 1 1 286.22 258.61 30.07 o -6 1 1 1384.94 1380.46 32.45 o -5 1 1 830.44 842.50 26.47 o -4 1 1 2834.97 2719.33 28.73 o -3 1 1 3730.88 3555.73 28.12 o -2 1 1 128664.00 123468.00 103.99 o -1 1 1 3301.13 3244.72 49.95 o 0 1 1 2057.86 2050.17 34.10 o 1 1 1 7243.85 7117.19 24.28 o 2 1 1 661.60 683.37 18.30 o 3 1 1 10365.90 9992.85 39.22 o 4 1 1 1161.78 1148.08 26.17 o 5 1 1 429.99 455.01 25.25 o 6 1 1 1092.82 1092.21 29.09 o 7 1 1 374.21 355.65 29.95 o 8 1 1 78.66 125.71 30.44 o 9 1 1 13.00 32.57 36.05 < 10 1 1 103.77 113.57 32.27 o 11 1 1 468.88 465.87 37.33 o 12 1 1 147.90 159.01 36.78 o 13 1 1 186.43 218.60 40.19 o 14 1 1 201.40 197.31 40.74 o 15 1 1 404.74 368.52 43.24 o 16 1 1 521.04 498.50 46.72 o 17 1 1 377.89 420.61 90.03 o 18 1 1 475.54 329.30 149.92 < -18 2 1 47.45 26.41 121.93 < -17 2 1 165.13 111.43 64.10 < -16 2 1 355.70 329.73 41.72 o -15 2 1 1.53 55.26 51.30 < -14 2 1 162.84 171.21 35.99 o -13 2 1 733.84 763.21 38.06 o -12 2 1 3.94 29.89 46.90 < -11 2 1 4.51 65.20 33.18 < -10 2 1 18.18 28.85 39.58 < -9 2 1 11.69 26.35 30.92 < -8 2 1 31.14 40.38 25.50 < -7 2 1 975.58 972.11 27.87 o -6 2 1 3352.03 3380.80 33.91 o -5 2 1 1835.66 1841.21 27.14 o -4 2 1 491.18 497.28 21.35 o -3 2 1 933.22 919.11 25.25 o -2 2 1 3421.05 3387.88 32.69 o -1 2 1 1684.26 1598.94 46.72 o 0 2 1 22.13 48.43 35.62 < 1 2 1 440.39 420.43 33.00 o 2 2 1 2109.54 2123.85 28.73 o 3 2 1 108.32 109.54 17.69 o 4 2 1 1691.99 1659.08 24.82 o 5 2 1 8.33 24.09 33.12 < 6 2 1 8.96 30.44 30.25 < 7 2 1 1422.22 1448.53 31.53 o 8 2 1 103.36 103.57 27.26 o 9 2 1 80.96 105.15 28.48 o 10 2 1 62.19 89.48 30.01 < 11 2 1 30.14 47.51 37.63 < 12 2 1 19.04 40.01 38.00 < 13 2 1 185.72 267.52 36.84 o 14 2 1 0.25 35.32 44.83 < 15 2 1 49.58 62.58 40.07 < 16 2 1 73.21 65.20 49.47 < -15 3 1 1.00 47.76 93.75 < -14 3 1 401.94 403.23 80.63 o -13 3 1 2.33 37.75 127.23 < -12 3 1 122.32 124.30 50.87 < -11 3 1 16.47 22.69 51.97 < -10 3 1 69.22 71.00 31.05 < -9 3 1 239.72 224.27 29.22 o -8 3 1 205.14 177.31 25.43 o -7 3 1 61.03 61.18 21.65 < -6 3 1 31.64 33.61 19.58 < -5 3 1 44.02 38.61 21.53 < -4 3 1 296.65 255.20 43.79 o -3 3 1 204.40 210.91 40.99 o -2 3 1 15.01 32.81 36.78 < -1 3 1 17.46 12.56 40.19 < 0 3 1 192.63 219.94 37.57 o 1 3 1 27.51 35.99 39.83 < 2 3 1 24.24 43.06 37.08 < 3 3 1 35.26 45.62 41.78 < 4 3 1 140.62 123.88 25.68 o 5 3 1 559.23 556.81 22.26 o 6 3 1 2.24 38.06 33.36 < 7 3 1 47.82 47.15 22.93 < 8 3 1 19.07 27.20 24.15 < 9 3 1 13.64 48.18 29.70 < 10 3 1 8.55 24.64 44.22 < 11 3 1 58.28 67.28 42.76 < 12 3 1 138.56 106.62 64.65 < 13 3 1 20.84 44.71 72.52 < 14 3 1 70.12 66.36 90.76 < -6 4 1 19.52 83.87 134.37 < -18 0 2 379.63 267.03 92.89 < -16 0 2 92.37 92.59 54.71 < -14 0 2 492.81 440.01 54.77 o -12 0 2 360.26 267.21 51.42 o -10 0 2 112.29 75.02 45.50 < -8 0 2 100.67 81.00 47.94 < -6 0 2 586.86 482.70 45.20 o -4 0 2 46956.90 44833.20 120.89 o 4 0 2 748.88 678.86 42.15 o 6 0 2 55.56 23.97 54.71 < 8 0 2 3584.18 3683.14 63.19 o 10 0 2 20.42 38.00 47.21 < 12 0 2 808.62 762.78 55.63 o 14 0 2 2072.92 2056.45 68.13 o 16 0 2 1020.37 924.23 76.06 o -19 1 2 137.48 230.25 138.21 < -18 1 2 140.74 59.96 85.94 < -17 1 2 176.74 159.44 44.10 o -16 1 2 595.07 598.47 45.01 o -15 1 2 350.53 362.30 41.84 o -14 1 2 356.45 336.26 38.85 o -13 1 2 73.67 71.36 38.00 < -12 1 2 176.90 210.91 34.77 o -11 1 2 184.12 189.75 33.18 o -10 1 2 463.79 473.73 33.12 o -9 1 2 162.22 88.50 30.31 < -8 1 2 3174.33 3143.60 41.17 o -7 1 2 179.43 126.13 27.26 o -6 1 2 447.40 429.45 28.18 o -5 1 2 287.28 186.82 26.65 o -4 1 2 27463.40 25916.10 68.56 o -3 1 2 391.75 352.42 27.63 o -2 1 2 16551.20 15859.20 47.57 o -1 1 2 82.04 146.38 26.65 o 0 1 2 1128.03 1196.26 17.99 o 1 1 2 108.57 122.96 16.83 o 2 1 2 3219.49 3103.71 26.04 o 3 1 2 1.45 84.05 21.77 o 4 1 2 8.94 33.97 30.56 < 5 1 2 701.05 727.16 28.24 o 6 1 2 143.97 94.17 26.59 o 7 1 2 8769.26 9213.41 57.46 o 8 1 2 0.09 26.04 51.30 < 9 1 2 195.85 262.27 32.63 o 10 1 2 1940.49 1945.08 41.90 o 11 1 2 385.81 440.01 36.05 o 12 1 2 1125.53 1178.09 41.90 o 13 1 2 114.96 118.57 37.57 o 14 1 2 127.72 111.68 40.50 < 15 1 2 16.31 74.59 56.05 < 16 1 2 79.42 82.95 51.17 < 17 1 2 210.68 92.59 137.66 < -18 2 2 2.73 55.32 113.45 < -17 2 2 202.80 219.82 51.54 o -16 2 2 164.27 179.87 40.26 o -15 2 2 27.97 113.88 42.51 < -14 2 2 166.25 150.23 34.64 o -13 2 2 95.47 70.02 33.42 < -12 2 2 202.52 226.59 32.63 o -11 2 2 80.78 74.35 31.29 < -10 2 2 3.06 59.22 34.40 < -9 2 2 402.71 377.30 27.87 o -8 2 2 642.80 631.95 27.39 o -7 2 2 580.15 600.05 25.80 o -6 2 2 587.18 529.12 23.91 o -5 2 2 15.36 24.58 23.60 < -4 2 2 12559.70 12222.50 46.66 o -3 2 2 691.21 684.96 29.83 o -2 2 2 6.23 9.76 20.98 < -1 2 2 990.77 1011.64 43.31 o 0 2 2 390.23 410.12 36.23 o 1 2 2 123.82 131.68 20.19 o 2 2 2 2665.29 2605.45 23.54 o 3 2 2 307.98 322.17 19.15 o 4 2 2 299.89 293.62 20.43 o 5 2 2 1074.05 1005.54 26.23 o 6 2 2 95.84 135.16 24.70 o 7 2 2 956.08 999.92 29.83 o 8 2 2 374.11 415.24 28.73 o 9 2 2 0.69 47.82 35.44 < 10 2 2 131.50 159.50 30.07 o 11 2 2 0.38 22.14 40.80 < 12 2 2 37.70 46.96 34.34 < 13 2 2 6.61 30.01 45.81 < 14 2 2 6.10 45.07 45.07 < 15 2 2 26.66 57.15 49.16 < 16 2 2 151.29 159.07 62.82 < 18 2 2 69.64 93.20 127.05 < -15 3 2 95.68 112.47 76.30 < -14 3 2 7.31 39.58 96.31 < -13 3 2 124.71 116.07 62.76 < -12 3 2 49.56 57.15 71.30 < -11 3 2 49.59 44.77 42.70 < -10 3 2 37.52 29.52 34.52 < -9 3 2 132.69 128.82 28.48 o -8 3 2 93.21 110.34 26.90 o -7 3 2 364.42 389.38 24.34 o -6 3 2 2.90 6.47 64.47 < -5 3 2 955.06 958.76 38.36 o -4 3 2 34.58 89.78 53.37 < -3 3 2 252.26 264.71 53.37 o -2 3 2 11.57 19.40 36.78 < -1 3 2 25.61 16.65 35.62 < 0 3 2 22.91 47.09 39.34 < 1 3 2 174.77 211.16 37.45 o 2 3 2 2.08 45.74 80.45 < 3 3 2 25.60 45.07 36.17 < 4 3 2 7.19 22.02 38.43 < 5 3 2 323.53 351.20 21.29 o 6 3 2 10.05 32.45 23.24 < 7 3 2 15.14 33.36 23.67 < 8 3 2 38.25 32.57 24.03 < 9 3 2 49.86 55.32 27.26 < 10 3 2 156.50 165.54 34.40 o 11 3 2 5.28 48.67 54.16 < 12 3 2 76.61 71.42 92.53 < 13 3 2 16.72 54.83 75.94 < 14 3 2 91.64 90.03 92.53 < -7 4 2 331.31 412.86 155.72 < -6 4 2 57.74 69.78 136.26 < -5 4 2 90.17 243.49 128.02 < -19 0 3 1039.27 1009.87 169.13 o -17 0 3 167.85 158.83 59.96 < -15 0 3 0.18 29.76 65.08 < -13 0 3 545.45 577.85 56.54 o -11 0 3 976.86 1294.34 60.44 o -9 0 3 935.68 1042.80 51.91 o -7 0 3 5.44 52.94 48.67 < -5 0 3 3898.94 3718.28 55.02 o 3 0 3 3339.05 3298.46 58.19 o 5 0 3 1882.38 1865.42 54.41 o 7 0 3 47.85 12.14 55.38 < 9 0 3 103.98 151.08 50.62 < 11 0 3 58.69 39.10 54.28 < 13 0 3 1117.47 1088.12 66.42 o 15 0 3 1427.46 1324.84 71.06 o -18 1 3 273.42 264.22 68.56 o -17 1 3 27.63 53.92 49.22 < -16 1 3 120.60 95.03 40.68 < -15 1 3 4.93 27.51 48.43 < -14 1 3 28.43 34.64 41.54 < -13 1 3 220.42 240.74 35.99 o -12 1 3 141.45 192.07 35.07 o -11 1 3 657.07 672.27 35.80 o -10 1 3 52.48 35.56 34.46 < -9 1 3 1803.92 1746.73 38.12 o -8 1 3 0.22 27.63 36.23 < -7 1 3 2033.70 2004.91 35.50 o -6 1 3 2943.82 2949.15 35.68 o -5 1 3 171.15 182.80 25.56 o -4 1 3 393.71 645.55 34.52 o -3 1 3 692.74 681.30 25.98 o -2 1 3 892.28 862.26 33.73 o -1 1 3 3627.77 3495.53 35.99 o 0 1 3 1689.33 1691.71 22.45 o 1 1 3 126.05 129.06 19.82 o 2 1 3 122.91 135.71 21.04 o 3 1 3 2686.65 2610.09 30.01 o 4 1 3 0.65 24.58 32.51 < 5 1 3 9415.22 9142.66 52.27 o 6 1 3 219.79 239.15 29.34 o 7 1 3 2263.82 2278.22 37.27 o 8 1 3 5.23 20.86 39.71 < 9 1 3 216.32 214.82 32.75 o 10 1 3 7.67 46.42 40.87 < 11 1 3 901.65 891.23 39.58 o 12 1 3 77.55 60.63 37.21 < 13 1 3 367.11 352.97 39.65 o 14 1 3 458.56 438.24 41.48 o 15 1 3 66.00 106.49 42.76 < 16 1 3 151.05 100.46 67.34 < 17 1 3 582.90 360.84 151.45 < -18 2 3 48.34 90.88 77.58 < -17 2 3 46.77 47.39 52.70 < -16 2 3 377.00 361.93 41.05 o -15 2 3 88.16 100.15 36.96 < -14 2 3 681.91 663.42 38.49 o -13 2 3 20.47 41.60 37.75 < -12 2 3 402.10 419.21 34.10 o -11 2 3 20.42 79.11 40.01 < -10 2 3 203.04 194.26 28.91 o -9 2 3 0.38 19.27 35.74 < -8 2 3 942.93 903.13 29.09 o -7 2 3 241.36 238.54 25.98 o -6 2 3 5653.74 5275.25 47.64 o -5 2 3 56.24 56.97 21.71 < -4 2 3 4037.16 4032.58 34.77 o -3 2 3 76.86 106.86 26.04 o -2 2 3 600.75 633.97 28.30 o -1 2 3 1592.84 1514.22 28.97 o 0 2 3 294.81 258.61 20.01 o 1 2 3 279.23 294.78 18.24 o 2 2 3 154.38 162.85 17.32 o 3 2 3 54.03 70.69 18.85 o 4 2 3 98.96 69.11 19.94 o 5 2 3 1215.21 1282.51 26.78 o 6 2 3 387.90 382.92 26.47 o 7 2 3 220.08 244.89 27.02 o 8 2 3 146.05 160.47 28.18 o 9 2 3 628.31 616.22 32.33 o 10 2 3 178.76 227.69 31.78 o 11 2 3 103.41 66.36 32.39 < 12 2 3 605.57 583.10 36.90 o 13 2 3 395.59 361.93 37.39 o 14 2 3 306.14 346.75 40.26 o 15 2 3 105.19 151.51 41.96 o 16 2 3 66.94 86.98 68.07 < 17 2 3 62.14 51.36 127.78 < -16 3 3 22.18 33.06 109.61 < -15 3 3 171.25 244.34 80.57 o -14 3 3 91.03 70.26 72.28 < -13 3 3 62.99 58.43 68.56 < -12 3 3 1.46 15.55 82.04 < -11 3 3 21.10 59.96 44.40 < -10 3 3 804.44 804.44 36.60 o -9 3 3 191.51 184.44 27.87 o -8 3 3 314.39 260.99 25.86 o -7 3 3 0.07 16.29 31.78 < -6 3 3 3745.21 3694.31 58.80 o -5 3 3 183.54 193.23 29.64 o -4 3 3 24.54 50.62 22.51 < -3 3 3 306.39 263.37 54.53 o -2 3 3 2.23 14.39 68.37 < -1 3 3 19.47 26.23 43.55 < 0 3 3 418.11 428.90 42.27 o 1 3 3 0.10 31.35 54.16 < 2 3 3 188.86 197.56 34.77 o 3 3 3 25.58 20.07 47.15 < 4 3 3 28.36 34.03 21.35 < 5 3 3 0.44 23.42 22.57 < 6 3 3 127.35 164.99 23.97 o 7 3 3 0.22 32.33 38.43 < 8 3 3 96.52 94.91 25.74 o 9 3 3 2.13 30.44 36.35 < 10 3 3 6.51 18.05 45.38 < 11 3 3 36.29 23.79 61.73 < 12 3 3 64.25 147.42 75.33 < 13 3 3 85.23 153.21 78.99 < -7 4 3 163.21 174.62 152.67 < -6 4 3 134.78 216.04 138.94 < -5 4 3 51.98 31.84 130.40 < -4 4 3 53.42 80.94 118.21 < -18 0 4 883.87 845.25 84.72 o -16 0 4 19.66 71.18 72.70 < -14 0 4 92.70 147.30 53.25 < -12 0 4 1158.11 1125.69 57.03 o -10 0 4 934.08 923.87 51.66 o -8 0 4 3355.03 3266.32 64.35 o -6 0 4 842.21 819.69 50.38 o -4 0 4 9940.78 9461.78 64.53 o 0 0 4 91.90 98.26 49.22 < 2 0 4 125.47 69.23 42.76 < 4 0 4 513.38 484.17 45.56 o 6 0 4 79.78 149.62 48.55 o 8 0 4 1653.68 1694.40 59.71 o 10 0 4 2885.61 2952.81 70.26 o 12 0 4 109.51 99.91 59.83 < 14 0 4 757.31 695.45 63.07 o 16 0 4 210.04 155.29 83.50 < -20 1 4 5.66 33.97 131.56 < -19 1 4 24.07 45.81 131.38 < -18 1 4 173.65 145.84 59.96 < -17 1 4 183.10 191.88 41.48 o -16 1 4 699.77 669.77 42.21 o -15 1 4 149.29 138.58 37.39 o -14 1 4 17.25 27.87 41.23 < -13 1 4 341.81 244.16 36.41 o -12 1 4 405.12 377.98 34.40 o -11 1 4 778.66 780.41 35.44 o -10 1 4 33.46 29.03 31.35 < -9 1 4 507.86 555.41 33.42 o -8 1 4 1396.44 1541.24 35.68 o -7 1 4 117.70 83.32 28.79 < -6 1 4 75.06 69.17 28.48 < -5 1 4 1219.82 1178.94 32.02 o -4 1 4 8398.39 8265.76 48.98 o -3 1 4 1791.34 1703.73 39.34 o -2 1 4 10110.20 9926.61 49.04 o -1 1 4 78.26 84.11 25.13 o 0 1 4 3609.32 3469.24 31.47 o 1 1 4 628.47 619.21 24.76 o 2 1 4 58.73 33.06 23.85 < 3 1 4 383.99 366.51 25.07 o 4 1 4 984.64 961.32 29.70 o 5 1 4 29.79 67.46 28.85 < 6 1 4 432.41 466.05 31.47 o 7 1 4 212.92 233.36 30.07 o 8 1 4 432.61 452.33 32.39 o 9 1 4 112.57 72.52 35.32 < 10 1 4 988.65 976.20 38.91 o 11 1 4 0.02 36.41 48.98 < 12 1 4 2448.29 2453.27 49.83 o 13 1 4 55.01 71.18 39.95 < 14 1 4 25.31 79.23 54.77 < 15 1 4 77.42 176.58 43.31 o 16 1 4 806.40 727.10 84.17 o -18 2 4 13.15 92.95 115.46 < -17 2 4 80.01 83.32 52.33 < -16 2 4 4.95 52.15 46.60 < -15 2 4 764.11 744.91 40.32 o -14 2 4 18.52 21.29 40.74 < -13 2 4 158.93 207.44 33.73 o -12 2 4 479.77 483.43 32.94 o -11 2 4 15.63 30.80 31.78 < -10 2 4 71.77 79.23 28.54 < -9 2 4 848.38 823.65 32.14 o -8 2 4 2527.43 2437.72 39.77 o -7 2 4 29.20 27.75 35.19 < -6 2 4 506.75 439.15 27.39 o -5 2 4 798.07 792.49 27.20 o -4 2 4 47.98 55.93 24.28 < -3 2 4 882.97 893.61 23.06 o -2 2 4 47.95 50.81 18.66 < -1 2 4 52.03 74.47 18.11 o 0 2 4 301.66 289.11 18.97 o 1 2 4 70.45 36.60 17.63 < 2 2 4 285.15 283.31 20.31 o 3 2 4 2169.19 2178.38 28.42 o 4 2 4 61.36 48.55 21.96 < 5 2 4 1147.74 1137.77 27.63 o 6 2 4 141.22 133.76 25.62 o 7 2 4 100.07 98.99 27.14 o 8 2 4 626.98 668.24 30.50 o 9 2 4 41.58 44.65 31.47 < 10 2 4 874.68 889.59 35.44 o 11 2 4 135.20 126.44 32.27 o 12 2 4 84.27 83.26 37.57 < 13 2 4 164.31 119.49 35.44 o 14 2 4 668.78 583.46 42.51 o 15 2 4 67.97 114.24 68.86 < 16 2 4 66.81 88.01 89.54 < -16 3 4 2.63 10.86 150.59 < -15 3 4 121.98 199.51 81.37 < -14 3 4 180.37 176.94 78.01 < -13 3 4 265.45 268.01 58.92 o -12 3 4 277.21 305.15 47.57 o -11 3 4 261.20 263.92 40.80 o -10 3 4 730.08 717.16 34.71 o -9 3 4 2.45 34.22 62.70 < -8 3 4 209.34 178.16 27.14 o -7 3 4 62.70 56.30 25.86 < -6 3 4 1718.32 1658.90 49.16 o -5 3 4 53.52 70.75 30.62 < -4 3 4 359.03 366.45 25.98 o -3 3 4 241.85 255.99 56.11 o -2 3 4 0.02 38.06 52.09 < -1 3 4 71.66 73.25 51.84 < 0 3 4 377.97 366.39 43.00 o 1 3 4 6.33 23.30 54.04 < 2 3 4 4.53 22.38 24.70 < 3 3 4 1665.21 1703.48 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492.40 46.29 o -16 2 5 55.64 113.75 44.95 < -15 2 5 129.74 134.73 36.17 o -14 2 5 2047.16 1999.30 43.43 o -13 2 5 215.29 187.37 33.30 o -12 2 5 62.88 113.08 34.64 o -11 2 5 0.29 27.93 38.67 < -10 2 5 11.16 25.50 32.45 < -9 2 5 8.26 29.34 29.70 < -8 2 5 555.60 511.12 32.69 o -7 2 5 681.69 708.44 31.05 o -6 2 5 3781.01 3826.24 41.41 o -5 2 5 188.24 183.22 30.25 o -4 2 5 1654.04 1582.53 33.42 o -3 2 5 1252.62 1285.19 28.54 o -2 2 5 16.62 25.19 23.42 < -1 2 5 11.84 9.39 20.25 < 0 2 5 439.81 440.07 23.42 o 1 2 5 1446.66 1478.91 26.35 o 2 2 5 62.43 64.53 20.98 o 3 2 5 218.60 196.52 22.20 o 4 2 5 24.38 28.42 24.03 < 5 2 5 80.98 101.13 24.28 o 6 2 5 108.29 102.65 26.53 o 7 2 5 29.47 25.50 29.70 < 8 2 5 2.32 32.45 36.90 < 9 2 5 884.29 929.97 34.89 o 10 2 5 361.28 406.52 33.36 o 11 2 5 190.32 148.82 34.03 o 12 2 5 164.26 244.34 35.01 o 13 2 5 418.83 425.06 39.52 o 14 2 5 290.42 195.36 40.80 o 15 2 5 411.36 448.12 66.24 o 16 2 5 168.22 192.19 93.99 < -16 3 5 122.69 139.92 86.12 < -15 3 5 153.08 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875.62 30.86 o 2 1 6 179.28 217.68 27.08 o 3 1 6 693.15 675.62 30.19 o 4 1 6 43.25 39.28 33.91 < 5 1 6 253.29 292.58 32.81 o 6 1 6 1923.34 1959.96 40.62 o 7 1 6 0.51 39.10 47.70 < 8 1 6 994.30 1036.22 38.36 o 9 1 6 215.84 205.85 35.01 o 10 1 6 244.01 220.49 36.29 o 11 1 6 129.25 86.49 36.23 < 12 1 6 212.59 183.59 39.04 o 13 1 6 19.17 47.82 45.56 < 14 1 6 597.09 602.19 45.26 o 15 1 6 36.51 8.36 106.56 < -18 2 6 115.57 133.57 75.14 < -17 2 6 182.30 181.39 45.68 o -16 2 6 4.28 59.83 56.17 < -15 2 6 1604.65 1472.44 49.83 o -14 2 6 134.01 126.87 36.29 o -13 2 6 66.70 90.39 35.19 < -12 2 6 913.57 940.52 35.50 o -11 2 6 0.48 6.65 37.75 < -10 2 6 94.99 101.55 33.30 o -9 2 6 228.41 223.05 31.11 o -8 2 6 1534.25 1531.54 37.33 o -7 2 6 188.18 172.98 30.37 o -6 2 6 340.28 280.08 33.55 o -5 2 6 1635.73 1655.05 39.71 o -4 2 6 641.85 644.21 28.73 o -3 2 6 808.48 841.40 30.01 o -2 2 6 154.90 234.82 22.26 o -1 2 6 913.75 877.51 25.74 o 0 2 6 260.25 255.99 23.42 o 1 2 6 14.44 23.12 23.60 < 2 2 6 66.12 92.89 24.21 o 3 2 6 32.58 69.04 23.91 < 4 2 6 98.37 86.12 26.04 o 5 2 6 39.36 38.43 26.11 < 6 2 6 199.18 185.97 28.18 o 7 2 6 397.00 379.74 30.86 o 8 2 6 409.70 405.30 33.12 o 9 2 6 17.20 39.04 35.99 < 10 2 6 89.48 80.45 32.63 < 11 2 6 114.65 137.24 33.67 o 12 2 6 0.92 43.31 45.99 < 13 2 6 10.23 20.92 65.20 < 14 2 6 0.73 39.10 56.91 < 15 2 6 13.83 125.28 130.77 < -16 3 6 4.41 80.21 101.74 < -15 3 6 8.94 37.88 92.40 < -14 3 6 209.08 232.02 68.43 o -13 3 6 287.35 270.81 52.64 o -12 3 6 82.64 67.76 46.96 < -11 3 6 23.95 60.14 53.67 < -10 3 6 816.36 820.60 43.61 o -9 3 6 303.62 327.17 31.90 o -8 3 6 232.17 235.80 29.83 o -7 3 6 190.75 187.80 25.01 o -6 3 6 118.99 147.73 21.90 o -5 3 6 439.08 451.90 39.95 o -4 3 6 394.53 413.78 37.15 o -3 3 6 159.78 166.39 26.59 o -2 3 6 2.89 10.19 32.33 < -1 3 6 952.89 962.72 31.66 o 0 3 6 11.33 23.12 35.80 < 1 3 6 46.73 60.75 18.18 o 2 3 6 65.39 67.52 22.99 < 3 3 6 24.53 42.09 23.48 < 4 3 6 17.14 37.69 26.23 < 5 3 6 0.49 15.74 51.48 < 6 3 6 106.95 126.93 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162.82 174.87 24.40 o -5 3 7 65.14 94.48 28.97 o -4 3 7 734.01 720.82 37.57 o -3 3 7 0.06 17.81 59.53 < -2 3 7 96.88 74.17 28.42 < -1 3 7 276.83 281.06 32.51 o 0 3 7 0.14 16.65 28.97 < 1 3 7 4.26 17.75 27.87 < 2 3 7 26.29 31.35 25.19 < 3 3 7 3.87 17.51 28.48 < 4 3 7 85.92 66.73 24.40 < 5 3 7 121.07 99.54 25.86 o 6 3 7 97.94 84.54 29.89 < 7 3 7 149.32 134.18 30.80 o 8 3 7 28.21 52.33 42.63 < 9 3 7 80.30 76.97 39.58 < 10 3 7 59.85 89.97 55.32 < 11 3 7 96.62 91.06 136.50 < -6 4 7 19.09 0.06 150.59 < -20 0 8 186.79 207.56 152.85 < -18 0 8 3944.99 3994.03 89.29 o -16 0 8 2837.09 2875.90 76.30 o -14 0 8 1821.14 1910.07 69.04 o -12 0 8 20.69 99.05 58.74 < -10 0 8 712.38 562.85 54.04 o -8 0 8 74.53 54.16 43.98 < -6 0 8 20.40 40.93 47.03 < -4 0 8 2877.57 2826.80 64.35 o -2 0 8 137.91 114.73 49.95 < 0 0 8 5.93 14.39 69.96 < 2 0 8 71.72 90.64 46.78 < 4 0 8 283.94 204.63 50.69 o 6 0 8 56.00 52.15 53.61 < 8 0 8 35.06 97.53 59.83 < 10 0 8 174.43 180.97 58.74 o 12 0 8 73.43 151.39 59.77 < 14 0 8 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341.75 39.95 o -2 1 10 718.70 707.52 37.69 o -1 1 10 617.98 631.53 35.13 o 0 1 10 10.78 43.31 35.80 < 1 1 10 4188.17 4276.61 53.55 o 2 1 10 206.94 201.83 36.05 o 3 1 10 512.43 590.72 36.53 o 4 1 10 808.47 809.93 37.88 o 5 1 10 23.36 42.21 38.24 < 6 1 10 1813.79 1811.08 45.20 o 7 1 10 20.63 28.61 49.65 < 8 1 10 91.84 84.41 37.88 < 9 1 10 338.66 269.47 39.40 o 10 1 10 85.48 90.70 39.65 < 11 1 10 347.32 367.67 41.72 o 12 1 10 131.18 189.81 52.52 o -18 2 10 58.96 121.25 144.98 < -17 2 10 398.06 411.34 58.43 o -16 2 10 59.39 78.01 41.72 < -15 2 10 21.84 49.59 45.26 < -14 2 10 14.26 49.10 43.49 < -13 2 10 1485.34 1431.76 42.76 o -12 2 10 50.72 47.33 37.88 < -11 2 10 67.73 103.02 36.11 < -10 2 10 4.76 28.79 45.01 < -9 2 10 135.63 220.55 38.24 o -8 2 10 487.40 510.76 38.91 o -7 2 10 86.20 101.68 37.51 < -6 2 10 15.57 28.42 53.00 < -5 2 10 1298.88 1292.57 34.46 o -4 2 10 573.01 523.14 29.70 o -3 2 10 160.47 183.22 27.57 o -2 2 10 125.99 124.91 29.46 o -1 2 10 210.34 175.78 30.44 o 0 2 10 3.54 33.42 42.51 < 1 2 10 667.12 635.18 32.88 o 2 2 10 447.28 468.73 32.75 o 3 2 10 188.29 200.12 31.96 o 4 2 10 4.84 31.17 33.73 < 5 2 10 150.16 170.11 34.28 o 6 2 10 18.71 28.67 36.84 < 7 2 10 362.34 355.47 37.33 o 8 2 10 3.37 28.24 50.93 < 9 2 10 587.78 563.34 40.13 o 10 2 10 596.43 571.45 39.83 o 11 2 10 302.44 320.70 39.65 o 12 2 10 266.17 278.43 58.92 o -16 3 10 65.53 66.79 100.82 < -15 3 10 63.02 95.88 68.19 < -14 3 10 375.74 349.13 69.11 o -13 3 10 232.47 206.40 65.08 o -12 3 10 2.18 12.87 86.49 < -11 3 10 3.28 62.64 63.86 < -10 3 10 9.12 49.34 64.10 < -9 3 10 18.81 54.89 59.59 < -8 3 10 38.60 69.84 46.54 < -7 3 10 7.08 48.37 33.73 < -6 3 10 109.13 135.77 28.30 o -5 3 10 107.62 149.98 27.45 o -4 3 10 77.93 91.55 23.67 o -3 3 10 249.97 277.46 26.29 o -2 3 10 88.19 115.76 26.96 o -1 3 10 78.38 60.99 23.91 < 0 3 10 15.83 30.19 28.91 < 1 3 10 12.95 51.23 34.89 < 2 3 10 12.50 46.90 40.19 < 3 3 10 698.18 704.35 31.35 o 4 3 10 9.29 34.58 40.99 < 5 3 10 103.14 98.32 34.89 < 6 3 10 182.39 178.83 45.32 o 7 3 10 40.94 64.71 54.96 < 8 3 10 268.12 266.42 60.63 o 9 3 10 64.68 55.87 98.75 < -2 4 10 27.72 16.83 146.87 < -21 0 11 1244.89 1383.45 184.69 o -19 0 11 0.69 106.62 143.70 < -17 0 11 606.24 695.08 65.87 o -15 0 11 598.34 1194.62 69.35 o -13 0 11 28.18 31.11 58.13 < -11 0 11 4580.82 5178.64 78.74 o -9 0 11 7600.23 7778.97 92.22 o -7 0 11 4622.46 4525.16 75.94 o -5 0 11 325.56 346.87 50.01 o -3 0 11 583.00 577.24 61.36 o -1 0 11 8928.48 10083.10 93.56 o 1 0 11 4043.63 4358.77 80.76 o 3 0 11 2.56 35.01 73.19 < 5 0 11 1308.05 1339.48 61.30 o 7 0 11 6.18 196.76 52.76 o 9 0 11 1672.92 1583.75 73.80 o 11 0 11 3409.29 3375.07 89.54 o -21 1 11 238.69 178.04 96.80 < -20 1 11 443.36 353.09 77.40 o -19 1 11 1013.15 1065.25 86.06 o -18 1 11 466.08 474.22 54.04 o -17 1 11 4.08 29.15 61.36 < -16 1 11 232.24 199.69 42.33 o -15 1 11 991.02 908.62 45.14 o -14 1 11 117.58 149.19 36.47 o -13 1 11 485.03 433.05 36.29 o -12 1 11 1233.93 1262.07 40.19 o -11 1 11 320.31 395.36 35.68 o -10 1 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11 19.53 36.47 33.67 < 2 3 11 25.88 39.22 35.13 < 3 3 11 120.81 98.99 34.77 < 4 3 11 331.13 353.76 37.15 o 5 3 11 15.27 34.58 43.24 < 6 3 11 60.17 89.36 50.01 < 7 3 11 72.93 92.95 91.06 < 8 3 11 263.36 236.59 98.75 < 9 3 11 65.93 60.75 138.82 < -20 0 12 253.10 328.45 109.67 < -18 0 12 410.13 333.63 73.74 o -16 0 12 25.40 37.08 95.45 < -14 0 12 73.95 87.10 52.52 < -12 0 12 874.47 1008.71 56.11 o -10 0 12 488.52 502.65 55.26 o -8 0 12 2094.43 2015.65 69.41 o -6 0 12 33.15 92.28 51.23 < -4 0 12 803.18 1402.60 67.95 o -2 0 12 8229.23 9151.08 100.64 o 0 0 12 398.49 345.77 51.17 o 2 0 12 759.63 694.23 56.66 o 4 0 12 2508.34 2469.62 70.39 o 6 0 12 1385.17 1362.04 65.99 o 8 0 12 11406.80 11215.10 117.29 o 10 0 12 2151.52 2064.38 73.25 o -21 1 12 137.43 227.20 97.53 < -20 1 12 764.38 858.72 84.96 o -19 1 12 3.86 18.36 87.04 < -18 1 12 479.68 392.49 59.53 o -17 1 12 165.20 36.90 49.28 < -16 1 12 26.55 48.98 37.82 < -15 1 12 4.24 37.75 41.41 < -14 1 12 114.11 95.45 36.53 < -13 1 12 1850.39 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