#------------------------------------------------------------------------------
#$Date: 2022-06-02 05:14:52 +0300 (Thu, 02 Jun 2022) $
#$Revision: 275738 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/89/2108983.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108983
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   10.2003
_cell_length_b                   10.2003
_cell_length_c                   29.4078
_exptl_crystal_F_000             1866.00
_reflns_d_resolution_high        0.7998
_cod_data_source_file            yh5018lav147_K3CoNH36IrOx32sup4.hkl
_cod_data_source_block           lav147_K3CoNH36IrOx32
_shelx_title                     ' lav147_a.res in R-3'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            689.87
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 2 0 331443.53 332869.19 3682.42 o
0 3 0 199851.34 201348.28 2649.01 o
-2 4 0 191951.55 192326.00 2940.35 o
-4 5 0 284217.06 291001.53 3957.34 o
-1 5 0 285722.00 293978.03 4112.10 o
-3 6 0 191353.73 192256.66 2660.67 o
0 6 0 231653.62 239672.39 3667.30 o
-5 7 0 211738.25 211669.14 2950.09 o
-2 7 0 117643.20 117134.35 1743.19 o
-7 8 0 124810.47 128446.43 2152.02 o
-4 8 0 122884.52 123587.23 1920.69 o
-1 8 0 103299.31 106337.13 1757.40 o
-6 9 0 80601.05 79733.03 1503.34 o
-3 9 0 71579.10 71504.37 1354.44 o
0 9 0 48557.45 51773.51 953.81 o
-8 10 0 70521.62 71309.34 1682.13 o
-5 10 0 56749.43 57791.53 1314.68 o
-2 10 0 72163.62 73303.81 1823.84 o
-10 11 0 52919.45 53465.48 1388.45 o
-7 11 0 54149.71 54421.29 1235.18 o
-4 11 0 93792.46 92600.48 2240.89 o
-1 11 0 34383.87 37108.22 1051.99 o
-9 12 0 41537.94 41219.21 1149.14 o
-6 12 0 59866.51 58211.66 1577.28 o
-3 12 0 55666.21 55456.80 1841.26 o
0 2 1 15234.03 14902.63 207.43 o
-5 3 1 15.52 0.00 45.18 o
-2 3 1 6235.50 5382.64 109.04 o
1 3 1 1546.33 1868.32 84.42 o
-7 4 1 4340.82 4461.55 162.48 o
-4 4 1 3504.98 3922.43 131.38 o
-1 4 1 18252.47 18251.31 280.89 o
2 4 1 23.91 40.50 47.13 o
-9 5 1 2190.24 2351.42 151.50 o
-6 5 1 1579.20 1891.58 119.16 o
-3 5 1 1973.01 2515.49 134.52 o
0 5 1 119.69 216.91 59.71 o
3 5 1 1051.39 1090.12 139.38 o
-11 6 1 721.21 840.15 207.06 o
-8 6 1 1435.57 1425.40 144.54 o
-5 6 1 2784.54 3004.71 134.04 o
-2 6 1 4169.22 3920.46 131.40 o
1 6 1 35.74 103.21 78.30 o
4 6 1 3.19 71.20 146.71 o
-10 7 1 15.56 153.61 149.86 o
-7 7 1 63.28 100.84 83.09 o
-4 7 1 1515.08 1963.37 125.42 o
-1 7 1 565.29 822.70 95.19 o
2 7 1 192.21 296.76 89.73 o
5 7 1 37.14 167.99 177.43 o
-12 8 1 292.09 0.00 204.63 o
-9 8 1 1087.15 1269.24 136.46 o
-6 8 1 0.91 0.00 54.77 o
-3 8 1 716.23 725.30 89.16 o
0 8 1 235.19 353.47 96.97 o
3 8 1 168.55 288.89 209.83 o
-11 9 1 93.98 464.71 252.24 o
-8 9 1 244.24 299.71 82.03 o
-5 9 1 176.61 21.46 78.38 o
-2 9 1 554.38 762.26 116.55 o
1 9 1 576.06 613.66 168.95 o
-10 10 1 0.30 270.26 155.77 o
-7 10 1 5259.06 5799.48 341.67 o
-4 10 1 224.72 366.50 190.96 o
-1 10 1 98.15 377.33 170.65 o
-9 11 1 167.43 654.84 160.72 o
-6 11 1 6.43 120.16 168.75 o
-3 11 1 2662.33 2952.92 339.45 o
0 11 1 1153.91 1053.97 234.89 o
-8 12 1 51.61 0.00 157.64 o
-5 12 1 138.49 303.88 216.06 o
0 1 2 148763.09 154487.34 2121.61 o
-2 2 2 44326.91 42663.60 590.12 o
1 2 2 114441.20 117202.11 1620.16 o
-4 3 2 103271.84 104872.47 1312.71 o
-1 3 2 54525.62 52824.88 843.56 o
2 3 2 97101.65 101205.91 1539.23 o
-6 4 2 12723.97 12706.19 262.71 o
-3 4 2 61746.78 63303.76 920.62 o
0 4 2 65564.69 65845.88 881.18 o
3 4 2 64033.94 64257.68 981.13 o
-8 5 2 32912.30 32034.16 546.16 o
-5 5 2 64687.11 66464.41 1025.60 o
-2 5 2 22360.04 21258.74 364.32 o
1 5 2 47711.00 50418.72 798.18 o
4 5 2 45500.99 43651.75 1268.81 o
-10 6 2 25335.22 25569.05 828.76 o
-7 6 2 23594.46 24666.22 516.26 o
-4 6 2 136023.58 139535.84 1971.22 o
-1 6 2 64122.23 63666.45 1004.44 o
2 6 2 54031.24 53262.04 1164.18 o
5 6 2 20704.15 20095.69 717.11 o
-12 7 2 18764.58 19466.07 769.30 o
-9 7 2 33018.05 33618.57 740.04 o
-6 7 2 85118.30 84165.03 1193.02 o
-3 7 2 28935.96 28158.41 513.49 o
0 7 2 47984.82 49154.15 876.54 o
3 7 2 20864.19 20842.76 621.18 o
-11 8 2 31847.77 30879.59 1150.96 o
-8 8 2 24849.84 25280.29 531.64 o
-5 8 2 49108.69 49649.05 867.42 o
-2 8 2 37177.73 36400.93 663.20 o
1 8 2 10548.49 11041.51 335.86 o
4 8 2 14657.49 15292.68 630.80 o
-10 9 2 14672.20 14922.58 416.20 o
-7 9 2 13399.50 13311.98 353.83 o
-4 9 2 31022.52 30956.58 717.98 o
-1 9 2 24366.93 25137.02 621.74 o
2 9 2 27073.63 26771.48 761.42 o
-9 10 2 41031.86 39279.06 829.14 o
-6 10 2 12713.10 13385.55 451.03 o
-3 10 2 31831.59 31435.24 961.30 o
0 10 2 14593.48 15649.10 625.34 o
-11 11 2 13365.92 13243.09 985.03 o
-8 11 2 20280.35 19860.20 620.63 o
-5 11 2 26346.52 27618.33 909.48 o
-2 11 2 25585.75 25274.32 1387.73 o
-7 12 2 19320.27 18792.41 661.70 o
-4 12 2 21478.41 22428.79 844.61 o
1 1 3 2189.00 2057.64 59.51 o
-1 2 3 29955.23 29267.05 338.96 o
2 2 3 14390.00 14654.05 253.79 o
-3 3 3 24337.40 25556.08 457.23 o
0 3 3 33455.34 35054.99 613.61 o
3 3 3 3353.64 3110.45 124.52 o
-5 4 3 5203.96 5063.73 142.48 o
-2 4 3 2151.87 2748.08 97.06 o
1 4 3 13705.35 14239.73 271.00 o
4 4 3 8232.99 7725.10 230.99 o
-7 5 3 1833.04 2062.80 119.39 o
-4 5 3 7389.03 7185.79 175.35 o
-1 5 3 6895.63 7116.11 182.07 o
2 5 3 1500.00 1579.67 101.74 o
5 5 3 3435.82 3610.44 284.34 o
-9 6 3 2207.38 2321.84 168.11 o
-6 6 3 18136.77 18859.51 469.81 o
-3 6 3 607.07 662.05 68.07 o
0 6 3 5652.34 5941.59 209.18 o
3 6 3 1944.78 2391.98 189.93 o
6 6 3 3269.50 2781.50 347.13 o
-11 7 3 2352.45 2423.22 311.35 o
-8 7 3 6103.63 6074.00 343.66 o
-5 7 3 23966.18 24696.67 460.40 o
-2 7 3 8864.89 9256.87 255.60 o
1 7 3 14058.93 13894.64 349.75 o
4 7 3 1572.51 1875.55 240.61 o
-10 8 3 568.13 510.38 111.58 o
-7 8 3 2790.84 3067.58 157.84 o
-4 8 3 5062.71 4902.85 190.04 o
-1 8 3 12338.32 12412.73 357.30 o
2 8 3 237.77 3.98 149.14 o
-12 9 3 2737.62 2935.23 332.77 o
-9 9 3 2863.94 3202.72 169.04 o
-6 9 3 376.76 486.75 101.40 o
-3 9 3 1858.28 2071.23 160.58 o
0 9 3 581.50 549.54 163.31 o
3 9 3 3137.46 3431.03 383.05 o
-11 10 3 1246.41 920.07 315.19 o
-8 10 3 1421.73 1673.89 153.61 o
-5 10 3 1013.40 912.92 194.88 o
-2 10 3 436.59 863.25 218.69 o
1 10 3 2586.88 2478.74 429.33 o
-10 11 3 2508.28 2369.28 225.95 o
-7 11 3 6128.81 6503.15 565.06 o
-4 11 3 3231.10 3758.20 366.69 o
-1 11 3 1752.44 2148.34 331.11 o
-9 12 3 65.07 440.81 176.47 o
-6 12 3 3709.56 4587.08 405.49 o
-3 12 3 772.52 815.56 636.95 o
-3 2 4 316078.72 327069.81 3740.30 o
0 2 4 121173.33 119486.99 1433.57 o
-5 3 4 206971.62 213508.16 2831.78 o
-2 3 4 130497.52 133068.88 1598.93 o
1 3 4 99253.51 98647.02 1253.89 o
-7 4 4 31235.39 31023.54 545.21 o
-4 4 4 111277.02 113471.23 1733.01 o
-1 4 4 26507.88 24522.56 402.43 o
2 4 4 152967.73 154464.03 2323.14 o
-9 5 4 23833.25 24408.01 522.48 o
-6 5 4 94956.98 93228.02 1583.84 o
-3 5 4 97829.52 98246.59 1352.35 o
0 5 4 143697.41 145964.17 2575.84 o
3 5 4 77066.55 77021.09 1414.40 o
-11 6 4 49052.46 48470.16 1058.24 o
-8 6 4 51395.95 50767.91 923.02 o
-5 6 4 139800.50 143787.39 1906.62 o
-2 6 4 72046.20 71636.24 1100.25 o
1 6 4 123853.30 126343.31 1729.78 o
4 6 4 46600.77 47315.11 1088.83 o
-10 7 4 49447.28 48321.41 1187.86 o
-7 7 4 84109.86 87854.99 1317.57 o
-4 7 4 93935.72 95225.26 1357.67 o
-1 7 4 115991.24 117969.22 1775.59 o
2 7 4 50283.86 48736.90 1310.20 o
5 7 4 33244.75 34208.73 1115.53 o
-12 8 4 28470.23 29180.01 982.37 o
-9 8 4 57686.03 56616.59 1064.97 o
-6 8 4 70819.20 71531.93 1048.19 o
-3 8 4 92360.52 89865.61 1392.16 o
0 8 4 17712.62 17558.14 469.20 o
3 8 4 34463.09 35165.08 915.38 o
-11 9 4 35216.42 34864.77 807.69 o
-8 9 4 49130.02 49692.66 895.11 o
-5 9 4 69055.24 69947.18 1354.38 o
-2 9 4 46345.02 46846.72 974.21 o
1 9 4 41356.46 43517.75 1044.80 o
-10 10 4 26047.10 28144.77 1076.09 o
-7 10 4 15414.71 15755.53 425.68 o
-4 10 4 47958.55 49000.09 1318.55 o
-1 10 4 28619.61 30140.90 2135.79 o
-9 11 4 38435.88 39649.91 962.43 o
-6 11 4 27936.63 28377.77 812.91 o
-3 11 4 29586.67 32556.80 1034.94 o
-8 12 4 19712.13 20690.75 692.02 o
-5 12 4 32032.91 34850.09 1110.60 o
-2 2 5 11951.66 12807.47 189.52 o
1 2 5 90993.46 94942.64 1260.15 o
-4 3 5 955.59 953.16 65.70 o
-1 3 5 6392.20 6823.64 169.81 o
2 3 5 168.36 82.75 54.12 o
-6 4 5 1519.94 1723.21 101.05 o
-3 4 5 116.95 160.80 50.13 o
0 4 5 659.44 922.99 76.77 o
3 4 5 847.10 988.87 97.68 o
-8 5 5 818.18 863.17 94.18 o
-5 5 5 4061.37 4122.54 259.07 o
-2 5 5 1131.52 1156.68 91.24 o
1 5 5 190.83 298.92 72.11 o
4 5 5 482.42 307.51 82.59 o
-10 6 5 79.78 45.99 151.26 o
-7 6 5 360.02 466.24 78.69 o
-4 6 5 241.45 184.53 64.54 o
-1 6 5 29.61 34.37 43.84 o
2 6 5 2306.96 2316.63 147.42 o
5 6 5 120.82 0.00 155.58 o
-12 7 5 1.89 78.79 205.43 o
-9 7 5 457.24 449.61 97.78 o
-6 7 5 411.69 322.36 72.94 o
-3 7 5 3268.00 3039.39 144.06 o
0 7 5 2649.88 3109.79 192.69 o
3 7 5 2367.38 2161.52 242.80 o
-11 8 5 2850.84 3512.58 338.38 o
-8 8 5 61.46 195.99 150.25 o
-5 8 5 677.72 845.97 102.77 o
-2 8 5 47.22 138.25 74.13 o
1 8 5 1107.51 1310.73 199.24 o
4 8 5 427.78 55.40 191.64 o
-10 9 5 1967.79 2167.97 308.84 o
-7 9 5 623.26 812.43 105.67 o
-4 9 5 553.08 758.81 143.22 o
-1 9 5 801.48 811.00 173.61 o
2 9 5 386.85 405.36 205.43 o
-9 10 5 257.39 0.00 194.85 o
-6 10 5 33.52 53.31 148.70 o
-3 10 5 252.03 463.21 206.74 o
0 10 5 116.30 0.00 205.38 o
-8 11 5 83.99 184.84 143.02 o
-5 11 5 189.79 553.63 223.76 o
-2 11 5 2.14 37.97 257.83 o
-7 12 5 614.43 611.14 203.68 o
-4 12 5 14.19 0.00 195.64 o
0 0 6 251002.42 217701.62 4707.47 o
1 1 6 150401.00 150962.95 1907.75 o
-1 2 6 15547.84 14275.89 223.33 o
2 2 6 97828.83 102377.23 1364.68 o
-3 3 6 51337.57 52908.07 783.25 o
0 3 6 26295.34 25229.78 410.60 o
3 3 6 40035.12 38892.15 677.32 o
-5 4 6 80938.22 81657.07 1119.77 o
-2 4 6 64652.43 64069.15 875.42 o
1 4 6 36757.07 34249.29 567.67 o
4 4 6 31853.88 30816.02 566.29 o
-7 5 6 30183.52 28557.89 515.17 o
-4 5 6 54797.38 58139.70 825.94 o
-1 5 6 45565.56 44318.15 733.03 o
2 5 6 47741.05 45634.57 707.46 o
5 5 6 39109.12 38384.76 936.32 o
-9 6 6 11799.97 11663.02 341.06 o
-6 6 6 39572.57 41566.27 829.53 o
-3 6 6 61404.76 62489.07 885.47 o
0 6 6 60414.21 60277.38 1623.70 o
3 6 6 41595.29 42167.48 979.42 o
6 6 6 13057.72 13355.36 592.96 o
-11 7 6 24036.58 23905.13 1202.04 o
-8 7 6 21220.08 21737.05 625.56 o
-5 7 6 42201.48 43099.68 652.76 o
-2 7 6 42206.21 44536.61 758.43 o
1 7 6 16399.84 16202.16 390.28 o
4 7 6 19105.56 19091.45 626.50 o
-10 8 6 27916.88 27492.85 769.57 o
-7 8 6 34375.64 35235.43 620.80 o
-4 8 6 36697.50 36211.71 657.29 o
-1 8 6 32357.01 32403.44 677.78 o
2 8 6 28551.98 28774.52 788.87 o
-12 9 6 14200.85 14975.55 810.52 o
-9 9 6 33045.77 33401.68 878.64 o
-6 9 6 21554.27 21480.93 462.60 o
-3 9 6 42556.11 42647.13 1029.88 o
0 9 6 9525.02 9705.85 512.56 o
3 9 6 12272.37 12995.57 697.85 o
-11 10 6 11736.93 11880.98 746.74 o
-8 10 6 27832.10 28393.37 612.38 o
-5 10 6 9610.53 9613.60 495.91 o
-2 10 6 25502.61 26829.72 884.86 o
1 10 6 12883.09 13044.28 694.02 o
-10 11 6 19476.72 19028.47 882.12 o
-7 11 6 11035.21 11825.28 505.51 o
-4 11 6 18319.40 18556.58 728.94 o
-1 11 6 13129.55 13379.27 701.65 o
-9 12 6 16286.59 16813.26 681.23 o
-6 12 6 23402.19 23859.77 862.93 o
-3 12 6 20523.42 20012.71 966.36 o
-3 2 7 21247.42 21278.76 327.62 o
0 2 7 2999.68 3216.92 122.78 o
-5 3 7 15938.46 17204.48 334.93 o
-2 3 7 31860.50 33736.18 470.30 o
1 3 7 276.71 235.85 60.23 o
-7 4 7 793.57 952.18 100.07 o
-4 4 7 1050.46 1648.53 115.43 o
-1 4 7 216.03 254.18 64.26 o
2 4 7 229.20 319.47 73.18 o
-9 5 7 185.31 307.02 114.27 o
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-3 5 7 529.94 648.11 81.04 o
0 5 7 900.97 1112.65 93.58 o
3 5 7 191.60 511.02 85.60 o
-11 6 7 2276.54 2020.42 245.88 o
-8 6 7 42.27 0.00 61.90 o
-5 6 7 2026.28 1804.91 107.26 o
-2 6 7 4008.92 3959.83 173.32 o
1 6 7 63.61 143.64 113.10 o
4 6 7 311.73 306.33 159.86 o
-10 7 7 112.65 0.00 157.17 o
-7 7 7 862.82 965.66 163.17 o
-4 7 7 204.82 406.11 76.79 o
-1 7 7 718.75 752.48 93.29 o
2 7 7 4078.61 3816.60 312.55 o
5 7 7 54.71 0.00 173.02 o
-12 8 7 246.70 25.12 185.54 o
-9 8 7 2147.23 2247.12 241.52 o
-6 8 7 2599.14 2761.37 143.65 o
-3 8 7 955.80 1133.13 111.21 o
0 8 7 323.95 259.38 125.27 o
3 8 7 292.55 318.84 176.30 o
-11 9 7 831.19 722.56 237.29 o
-8 9 7 285.85 387.96 167.91 o
-5 9 7 47.84 138.50 57.44 o
-2 9 7 2804.46 2749.23 343.66 o
1 9 7 1924.91 1939.82 283.29 o
-10 10 7 300.35 113.50 228.00 o
-7 10 7 436.79 504.58 98.44 o
-4 10 7 142.34 158.84 191.49 o
-1 10 7 572.74 266.57 228.74 o
-9 11 7 137.99 0.00 210.47 o
-6 11 7 1077.22 1164.80 246.79 o
-3 11 7 152.91 372.43 217.32 o
-8 12 7 762.69 755.04 188.47 o
-5 12 7 1228.95 1043.83 322.74 o
0 1 8 304327.50 310253.47 4131.44 o
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1 2 8 475919.38 467216.69 7314.17 o
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2 3 8 246737.55 245569.22 3183.15 o
-6 4 8 132139.47 131762.28 1872.44 o
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0 4 8 244145.78 236083.91 3059.12 o
3 4 8 130062.84 126512.39 1997.81 o
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-5 5 8 147831.08 142171.42 2319.02 o
-2 5 8 121036.02 119311.76 1803.14 o
1 5 8 140609.95 135270.66 1833.99 o
4 5 8 94269.04 93058.65 1753.07 o
-10 6 8 67452.34 64681.79 1238.24 o
-7 6 8 101816.52 102493.25 1974.79 o
-4 6 8 151907.28 154675.08 2296.71 o
-1 6 8 130499.32 128492.38 1788.08 o
2 6 8 89485.59 85541.15 1601.35 o
5 6 8 65669.75 65947.13 1454.99 o
-12 7 8 32298.28 31873.51 1041.90 o
-9 7 8 76048.16 78320.60 1836.67 o
-6 7 8 106705.36 108963.85 1534.79 o
-3 7 8 175486.73 170017.98 2788.81 o
0 7 8 118258.53 116525.18 1886.18 o
3 7 8 89271.51 88336.14 1811.35 o
-11 8 8 65129.67 63339.16 1389.01 o
-8 8 8 127425.06 127729.12 2442.63 o
-5 8 8 130272.05 130107.45 1822.84 o
-2 8 8 144234.69 134805.75 2282.93 o
1 8 8 55362.22 55140.40 1237.75 o
4 8 8 46931.29 47550.15 1313.62 o
-10 9 8 62469.46 63819.60 1604.58 o
-7 9 8 55115.03 55152.98 995.82 o
-4 9 8 133764.80 134179.20 3007.34 o
-1 9 8 51433.59 53843.07 1434.75 o
2 9 8 53753.62 52042.16 1595.41 o
-9 10 8 61479.04 59782.30 1418.73 o
-6 10 8 48057.34 48522.86 1370.40 o
-3 10 8 61694.11 61823.20 1605.41 o
0 10 8 45496.83 45430.64 1284.70 o
-8 11 8 44113.00 45097.06 1236.66 o
-5 11 8 40429.31 40089.98 1183.68 o
-2 11 8 43273.26 43867.75 1584.92 o
-7 12 8 49059.60 48593.31 1373.68 o
-4 12 8 35782.75 35014.36 1322.73 o
1 1 9 37486.03 36942.05 543.45 o
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