#------------------------------------------------------------------------------ #$Date: 2022-10-28 17:35:29 +0300 (Fri, 28 Oct 2022) $ #$Revision: 278858 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/90/2109072.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2109072 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 5.8522(8) _cell_length_b 8.236(3) _cell_length_c 5.867(5) _exptl_crystal_F_000 712 _reflns_d_resolution_high 0.8463 _cod_data_source_file dk5080Isup2.hkl _cod_data_source_block I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 490.76 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_ssg_id 'x1, x2, x3, x4' '-x1, -x2+1/2, x3, x4+1/2' '-x1, x2+1/2, -x3, -x4' 'x1, -x2, -x3, -x4+1/2' '-x1, -x2, -x3, -x4' 'x1, x2+1/2, -x3, -x4+1/2' 'x1, -x2+1/2, x3, x4' '-x1, x2, x3, x4+1/2' 'x1+1/2, x2+1/2, x3+1/2, x4' '-x1+1/2, -x2, x3+1/2, x4+1/2' '-x1+1/2, x2, -x3+1/2, -x4' 'x1+1/2, -x2+1/2, -x3+1/2, -x4+1/2' '-x1+1/2, -x2+1/2, -x3+1/2, -x4' 'x1+1/2, x2, -x3+1/2, -x4+1/2' 'x1+1/2, -x2, x3+1/2, x4' '-x1+1/2, x2+1/2, x3+1/2, x4+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 0 2 0.21 0.55 0.14 < 0 0 2 -2 1.03 1.31 0.14 o 0 0 2 0 226351.00 240843.00 3471.64 o 0 0 2 2 0.80 1.45 0.35 o 0 0 4 -2 5.95 6.99 0.69 o 0 0 4 0 178118.00 181704.00 2610.97 o 0 0 4 2 0.52 2.01 0.55 < 0 0 6 -2 6.53 8.16 1.04 o 0 0 6 0 76680.60 88427.80 1273.95 o 0 0 6 2 0.07 0.35 0.42 < 0 1 1 -2 0.06 0.07 0.07 < 0 1 1 0 17.77 33.04 0.55 o 0 1 1 2 0.41 0.62 0.14 o 0 1 3 -2 1.68 2.35 0.28 o 0 1 3 0 86.26 110.07 2.15 o 0 1 3 2 1.38 2.98 0.55 o 0 1 5 -2 3.76 4.36 0.48 o 0 1 5 0 18.92 11.97 0.83 o 0 1 5 2 0.75 1.45 0.42 < 0 2 0 2 0.01 0.35 0.07 o 0 2 2 -2 0.76 1.25 0.14 o 0 2 2 0 3031.16 4406.07 58.28 o 0 2 2 2 0.01 0.21 0.14 < 0 2 4 -2 0.87 0.97 0.28 < 0 2 4 0 3537.72 3979.96 47.75 o 0 2 4 2 0.45 0.48 0.28 < 0 2 6 -2 2.43 2.08 0.42 o 0 2 6 0 3026.77 3337.90 41.76 o 0 2 6 2 1.26 2.28 0.62 < 0 3 1 -2 0.35 0.55 0.14 < 0 3 1 0 363.94 287.02 2.81 o 0 3 1 2 0.37 0.48 0.14 < 0 3 3 -2 2.57 3.18 0.35 o 0 3 3 0 99.18 120.40 3.33 o 0 3 3 2 0.13 0.28 0.21 < 0 3 5 -2 2.88 3.32 0.48 o 0 3 5 0 30.34 47.00 1.94 o 0 3 5 2 0.93 1.18 0.35 < 0 4 0 2 0.03 0.21 0.14 < 0 4 2 -2 0.57 0.55 0.07 o 0 4 2 0 148351.00 142197.00 1444.49 o 0 4 2 2 0.20 0.28 0.21 < 0 4 4 -2 6.09 6.92 0.55 o 0 4 4 0 120344.00 153146.00 1826.90 o 0 4 4 2 0.30 0.07 0.42 < 0 4 6 -2 4.27 4.29 0.83 o 0 4 6 0 57049.30 65864.80 944.90 o 0 5 1 -2 0.05 0.00 0.07 < 0 5 1 0 202.89 224.09 4.31 o 0 5 1 2 0.03 0.07 0.21 < 0 5 3 -2 1.26 1.18 0.21 o 0 5 3 2 0.93 1.04 0.48 < 0 5 5 -2 2.34 2.35 0.62 < 0 5 5 0 83.74 121.93 4.23 o 0 5 5 2 0.07 -0.07 0.35 < 0 6 0 2 0.10 0.07 0.07 < 0 6 2 -2 1.27 0.55 0.28 < 0 6 2 0 600.19 588.71 10.43 o 0 6 2 2 0.16 0.42 0.35 < 0 6 4 -2 0.34 0.14 0.35 < 0 6 4 0 4249.94 4473.28 68.04 o 0 6 4 2 0.93 1.52 0.76 < 1 0 1 -3 15.05 18.29 0.35 o 1 0 1 -2 0.54 1.45 0.14 o 1 0 1 -1 1061.92 890.09 6.91 o 1 0 1 0 736.27 635.97 5.64 o 1 0 1 1 973.80 867.51 9.67 o 1 0 1 2 0.49 0.97 0.21 o 1 0 1 3 25.94 29.92 1.11 o 1 0 3 -3 0.99 0.62 0.21 < 1 0 3 -2 0.01 0.14 0.28 < 1 0 3 -1 455.93 472.64 9.26 o 1 0 3 0 1440.32 2052.06 27.48 o 1 0 3 1 348.24 456.50 6.91 o 1 0 3 2 0.02 0.48 0.28 < 1 0 3 3 0.45 0.35 0.35 < 1 0 5 -3 11.28 12.53 0.83 o 1 0 5 -2 0.51 0.48 0.28 < 1 0 5 0 3866.41 3150.46 49.96 o 1 0 5 1 238.12 279.28 4.65 o 1 0 5 2 0.11 0.48 0.35 < 1 0 5 3 9.83 8.23 0.69 o 1 1 0 1 0.96 1.59 0.07 o 1 1 0 2 0.22 0.21 0.07 < 1 1 0 3 0.10 0.14 0.07 < 1 1 2 -3 0.33 0.14 0.07 < 1 1 2 -2 0.18 0.14 0.14 < 1 1 2 -1 8.01 7.41 0.35 o 1 1 2 0 319.67 367.09 3.43 o 1 1 2 1 11.11 13.29 0.62 o 1 1 2 2 2.38 3.32 0.42 o 1 1 2 3 0.00 0.07 0.14 < 1 1 4 -3 0.01 0.07 0.14 < 1 1 4 -2 1.19 1.94 0.28 o 1 1 4 -1 1.20 1.59 0.28 o 1 1 4 0 402.03 449.58 4.47 o 1 1 4 1 1.16 1.66 0.21 o 1 1 4 2 2.55 2.42 0.28 o 1 1 4 3 0.08 0.07 0.14 < 1 1 6 -3 0.46 0.76 0.21 < 1 1 6 -2 1.23 1.31 0.21 o 1 1 6 -1 0.18 0.21 0.14 < 1 1 6 0 226.08 172.88 3.89 o 1 1 6 1 0.54 0.48 0.21 < 1 1 6 2 1.85 0.97 0.35 < 1 2 1 -3 23.37 23.20 0.28 o 1 2 1 -2 0.19 0.48 0.07 o 1 2 1 -1 1278.34 1009.55 6.81 o 1 2 1 0 216689.00 199107.00 1655.84 o 1 2 1 1 1015.56 763.36 5.11 o 1 2 1 2 1.14 1.38 0.14 o 1 2 1 3 9.67 9.20 0.35 o 1 2 3 -3 27.73 28.60 0.90 o 1 2 3 -2 0.45 0.69 0.14 o 1 2 3 -1 895.39 1091.15 12.41 o 1 2 3 0 156844.00 169799.00 332.50 o 1 2 3 1 803.84 1069.22 8.67 o 1 2 3 2 1.28 1.80 0.21 o 1 2 3 3 27.00 30.81 1.45 o 1 2 5 -3 1.02 1.04 0.21 o 1 2 5 -2 3.71 3.87 0.48 o 1 2 5 -1 324.12 350.58 3.83 o 1 2 5 0 101299.00 103861.00 746.61 o 1 2 5 1 248.98 237.12 3.27 o 1 2 5 2 0.96 1.04 0.21 o 1 2 5 3 1.09 0.97 0.35 < 1 3 0 1 27.90 25.28 0.35 o 1 3 0 2 0.44 0.42 0.07 o 1 3 0 3 0.04 0.00 0.07 < 1 3 2 -3 0.10 0.07 0.07 < 1 3 2 -2 0.40 0.42 0.07 o 1 3 2 -1 6.48 6.16 0.28 o 1 3 2 0 185.16 232.04 4.45 o 1 3 2 1 0.04 0.07 0.14 < 1 3 2 2 1.21 1.11 0.14 o 1 3 2 3 0.37 0.07 0.28 < 1 3 4 -3 1.14 0.83 0.21 < 1 3 4 -2 0.66 0.76 0.21 < 1 3 4 -1 6.86 6.71 0.42 o 1 3 4 0 261.47 374.91 4.52 o 1 3 4 1 3.99 4.22 0.35 o 1 3 4 2 2.47 2.35 0.28 o 1 3 4 3 0.21 0.14 0.14 < 1 3 6 -3 0.16 0.21 0.14 < 1 3 6 -2 1.09 0.83 0.21 < 1 3 6 0 197.67 145.45 3.61 o 1 4 1 -3 5.95 5.95 0.14 o 1 4 1 -2 0.12 0.21 0.07 < 1 4 1 -1 426.10 326.48 2.45 o 1 4 1 0 1365.91 1448.10 9.98 o 1 4 1 1 572.50 613.63 4.22 o 1 4 1 2 0.02 0.42 0.07 o 1 4 1 3 11.30 11.49 0.48 o 1 4 3 -3 1.37 0.90 0.14 o 1 4 3 -2 0.09 0.14 0.14 < 1 4 3 -1 326.48 340.51 3.28 o 1 4 3 0 2332.43 2427.78 37.08 o 1 4 3 1 185.19 222.44 2.64 o 1 4 3 2 0.01 0.42 0.21 < 1 4 3 3 0.52 0.21 0.21 < 1 4 5 -3 4.38 4.77 0.35 o 1 4 5 -2 0.46 0.07 0.21 < 1 4 5 -1 149.92 172.85 3.88 o 1 4 5 0 4356.87 3732.05 40.21 o 1 4 5 1 162.63 184.37 3.54 o 1 4 5 2 0.24 0.35 0.28 < 1 4 5 3 5.17 4.98 0.62 o 1 5 0 1 1.82 2.35 0.14 o 1 5 0 2 0.13 0.14 0.07 < 1 5 0 3 0.06 0.00 0.07 < 1 5 2 -3 0.48 0.55 0.07 o 1 5 2 -2 0.48 0.35 0.07 o 1 5 2 -1 13.87 15.78 0.35 o 1 5 2 0 117.49 174.86 1.53 o 1 5 2 1 8.93 9.55 0.42 o 1 5 2 2 0.41 0.35 0.14 < 1 5 2 3 0.14 -0.07 0.21 < 1 5 4 -3 0.32 0.07 0.21 < 1 5 4 -2 1.57 1.31 0.35 < 1 5 4 -1 7.12 6.64 0.62 o 1 5 4 0 188.54 228.29 4.65 o 1 5 4 1 0.11 -0.14 0.21 < 1 5 4 3 0.46 0.42 0.28 < 1 5 6 -3 1.18 1.31 0.35 < 1 5 6 -2 1.12 0.83 0.35 < 1 5 6 -1 3.05 4.36 0.55 o 1 6 1 -2 0.12 0.35 0.21 < 1 6 1 -1 540.18 581.30 7.21 o 1 6 1 0 97487.70 80459.30 797.84 o 1 6 1 1 315.54 325.70 5.99 o 1 6 1 3 5.02 4.36 0.42 o 1 6 3 -3 6.95 7.96 0.55 o 1 6 3 -2 0.65 0.76 0.28 < 1 6 3 -1 279.93 293.44 6.40 o 1 6 3 0 80570.90 79088.90 837.53 o 1 6 3 1 372.43 361.92 6.34 o 1 6 3 3 8.95 8.23 0.83 o 1 6 5 -3 1.58 1.52 0.35 o 1 6 5 -2 3.10 2.84 0.90 < 2 0 0 0 212788.00 216958.00 3123.11 o 2 0 0 1 4605.61 6244.15 82.63 o 2 0 0 2 9.48 9.62 0.55 o 2 0 0 3 101.51 102.81 1.95 o 2 0 2 -3 33.02 30.62 0.97 o 2 0 2 -2 2.70 1.94 0.28 o 2 0 2 0 237742.00 215271.00 2187.88 o 2 0 2 1 2954.48 2702.43 34.24 o 2 0 2 2 10.33 10.66 0.69 o 2 0 2 3 38.90 35.94 1.45 o 2 0 4 -3 46.35 41.91 1.59 o 2 0 4 -2 0.02 0.21 0.21 < 2 0 4 -1 1990.49 1783.21 30.50 o 2 0 4 0 111873.00 107446.00 1093.74 o 2 0 4 2 5.64 5.33 0.55 o 2 0 4 3 43.35 40.16 1.59 o 2 0 6 -3 11.17 13.15 0.90 o 2 0 6 -2 1.88 2.14 0.55 < 2 0 6 -1 810.88 876.68 15.13 o 2 0 6 0 77077.30 72110.70 734.32 o 2 0 6 1 868.30 792.65 10.09 o 2 1 1 -3 0.35 0.14 0.07 < 2 1 1 -2 0.01 0.00 0.07 < 2 1 1 -1 0.35 0.35 0.14 < 2 1 1 0 64.27 67.34 1.04 o 2 1 1 1 4.78 4.98 0.28 o 2 1 1 2 0.79 0.42 0.21 < 2 1 1 3 0.36 0.28 0.21 < 2 1 3 -3 0.67 0.42 0.14 < 2 1 3 -2 0.90 0.62 0.14 o 2 1 3 -1 2.36 2.77 0.28 o 2 1 3 0 9.01 8.44 0.48 o 2 1 3 1 1.20 1.18 0.28 o 2 1 3 2 1.07 1.73 0.28 o 2 1 3 3 0.22 0.14 0.14 < 2 1 5 -3 1.76 1.45 0.28 o 2 1 5 -2 1.37 0.97 0.28 < 2 1 5 -1 6.38 5.33 0.48 o 2 1 5 0 7.75 7.54 0.48 o 2 1 5 1 0.78 0.35 0.28 < 2 1 5 2 1.38 1.38 0.28 o 2 1 5 3 0.32 0.28 0.21 < 2 2 0 0 1831.17 1951.04 29.66 o 2 2 0 1 1796.69 1936.20 14.70 o 2 2 0 2 6.06 6.50 0.35 o 2 2 0 3 11.43 9.90 0.42 o 2 2 2 -3 31.78 31.03 0.69 o 2 2 2 -2 3.96 3.25 0.35 o 2 2 2 -1 1811.07 1480.60 11.43 o 2 2 2 0 2164.47 2275.88 35.40 o 2 2 2 1 1898.77 1835.63 14.16 o 2 2 2 2 4.02 4.43 0.35 o 2 2 2 3 29.60 24.30 0.97 o 2 2 4 -3 3.89 4.01 0.35 o 2 2 4 -2 0.27 0.14 0.14 < 2 2 4 -1 732.67 694.50 6.25 o 2 2 4 0 1030.88 1131.32 13.62 o 2 2 4 1 846.80 805.62 6.96 o 2 2 4 2 1.07 0.76 0.28 < 2 2 4 3 7.58 8.23 0.83 o 2 2 6 -3 4.61 3.67 0.42 o 2 2 6 -2 0.08 0.00 0.28 < 2 2 6 -1 376.70 362.63 4.45 o 2 2 6 0 7054.47 6960.49 84.81 o 2 2 6 1 445.80 413.06 8.63 o 2 3 1 -3 0.09 0.07 0.14 < 2 3 1 -2 0.06 -0.14 0.14 < 2 3 1 -1 1.41 1.04 0.14 o 2 3 1 0 145.27 153.82 1.81 o 2 3 1 1 0.11 0.28 0.14 < 2 3 1 2 0.06 0.00 0.14 < 2 3 1 3 0.02 0.14 0.14 < 2 3 3 -3 1.79 1.59 0.28 o 2 3 3 -2 0.81 0.76 0.14 o 2 3 3 -1 5.91 5.26 0.48 o 2 3 3 0 94.53 88.81 1.87 o 2 3 3 1 4.28 5.47 0.42 o 2 3 3 2 1.13 1.94 0.62 < 2 3 3 3 0.68 0.07 0.21 < 2 3 5 -3 0.62 0.48 0.21 < 2 3 5 -2 2.16 1.25 0.28 o 2 3 5 -1 2.47 2.14 0.35 o 2 3 5 0 70.10 59.78 1.32 o 2 3 5 1 0.04 -0.07 0.14 < 2 3 5 2 0.28 0.55 0.28 < 2 3 5 3 0.07 0.07 0.28 < 2 4 0 0 139523.00 134324.00 1368.03 o 2 4 0 1 2542.73 2572.46 18.98 o 2 4 0 2 4.79 4.36 0.28 o 2 4 0 3 51.48 47.66 0.83 o 2 4 2 -3 24.00 22.98 0.69 o 2 4 2 -2 0.55 0.62 0.14 o 2 4 2 -1 1781.41 1630.20 12.53 o 2 4 2 0 147579.00 147701.00 1060.80 o 2 4 2 1 1880.29 1878.92 23.32 o 2 4 2 2 5.39 4.01 0.35 o 2 4 2 3 27.41 28.11 0.76 o 2 4 4 -3 26.56 30.18 0.83 o 2 4 4 -2 0.01 0.14 0.14 < 2 4 4 -1 1276.97 1746.78 26.76 o 2 4 4 0 84676.80 94680.80 728.03 o 2 4 4 1 1357.62 1462.64 24.70 o 2 4 4 2 3.06 3.53 0.55 o 2 4 4 3 27.80 26.51 1.32 o 2 4 6 -3 8.44 9.76 0.83 o 2 4 6 -2 2.34 2.42 0.48 o 2 4 6 -1 571.06 570.16 11.44 o 2 5 1 -3 0.56 0.42 0.07 o 2 5 1 -2 0.13 0.00 0.07 < 2 5 1 -1 1.39 1.38 0.14 o 2 5 1 0 190.81 141.65 1.95 o 2 5 1 1 4.50 5.26 0.28 o 2 5 1 2 0.47 0.48 0.14 < 2 5 1 3 0.54 0.28 0.14 < 2 5 3 -3 0.04 0.21 0.14 < 2 5 3 -2 0.54 0.42 0.28 < 2 5 3 -1 0.12 0.76 0.28 < 2 5 3 0 94.26 121.49 2.98 o 2 5 3 1 0.06 0.35 0.28 < 2 5 3 2 0.11 0.07 0.28 < 2 5 3 3 0.01 -0.07 0.21 < 2 5 5 -3 1.40 1.25 0.42 < 2 5 5 -2 0.86 0.62 0.35 < 2 5 5 -1 5.21 5.19 0.69 o 2 5 5 1 1.71 2.84 0.55 o 2 6 2 -2 1.14 2.08 0.62 < 2 6 2 -1 603.80 518.78 9.51 o 2 6 2 0 2561.86 2689.95 43.62 o 2 6 2 1 652.03 585.76 11.48 o 2 6 2 2 0.69 0.42 0.28 < 2 6 2 3 8.17 8.58 0.76 o 2 6 4 -3 1.71 1.87 0.69 < 2 6 4 -2 0.04 -0.21 0.35 < 3 0 1 -3 56.96 67.22 1.59 o 3 0 1 -2 25.16 27.63 1.18 o 3 0 1 -1 4320.97 5001.82 59.25 o 3 0 1 0 3893.93 4310.46 45.46 o 3 0 1 1 3924.12 4138.79 62.22 o 3 0 1 2 26.95 25.13 1.04 o 3 0 1 3 40.33 39.20 1.32 o 3 0 3 -3 47.25 41.35 1.32 o 3 0 3 -2 11.39 13.36 0.76 o 3 0 3 -1 3014.49 3045.10 32.51 o 3 0 3 0 4433.85 4248.63 62.35 o 3 0 3 1 2526.40 2757.90 42.96 o 3 0 3 2 18.15 17.44 1.04 o 3 0 3 3 47.86 48.13 1.59 o 3 0 5 -3 3.94 4.98 0.55 o 3 0 5 -2 2.34 2.42 0.48 o 3 0 5 0 6552.07 6474.50 80.77 o 3 0 5 1 916.61 1027.08 17.19 o 3 0 5 2 6.58 5.19 0.69 o 3 0 5 3 5.44 6.50 0.62 o 3 1 0 1 41.07 49.67 1.04 o 3 1 0 2 3.64 3.60 0.28 o 3 1 0 3 0.24 0.07 0.14 < 3 1 2 -3 0.19 0.21 0.14 < 3 1 2 -2 0.66 0.42 0.14 < 3 1 2 -1 4.79 3.94 0.28 o 3 1 2 0 144.53 134.14 1.87 o 3 1 2 1 22.09 23.12 0.69 o 3 1 2 2 3.21 3.25 0.28 o 3 1 2 3 0.18 0.14 0.14 < 3 1 4 -3 0.95 1.04 0.21 o 3 1 4 -2 0.10 0.07 0.14 < 3 1 4 -1 3.19 2.49 0.28 o 3 1 4 0 243.15 236.84 3.34 o 3 1 4 1 13.14 14.95 0.62 o 3 1 4 2 3.09 2.42 0.28 o 3 1 4 3 0.01 0.00 0.14 < 3 1 6 -3 0.43 1.04 0.28 < 3 1 6 -2 0.11 -0.14 0.14 < 3 1 6 -1 0.94 0.35 0.21 < 3 1 6 0 157.64 120.04 2.84 o 3 2 1 -3 121.26 139.17 1.94 o 3 2 1 -2 22.82 23.68 0.76 o 3 2 1 -1 6461.52 7992.52 74.43 o 3 2 1 0 134639.00 137064.00 984.58 o 3 2 1 1 6241.32 6418.55 47.04 o 3 2 1 2 30.64 26.17 0.76 o 3 2 1 3 133.02 116.53 2.01 o 3 2 3 -3 66.73 65.41 1.25 o 3 2 3 -2 6.65 6.71 0.42 o 3 2 3 -1 4407.00 4436.12 37.62 o 3 2 3 0 105299.00 119718.00 862.38 o 3 2 3 1 3684.23 4037.94 30.20 o 3 2 3 2 24.95 22.43 0.76 o 3 2 3 3 55.28 59.63 1.80 o 3 2 5 -3 57.53 51.87 1.25 o 3 2 5 -2 0.43 1.31 0.35 < 3 2 5 -1 2528.42 2625.09 20.30 o 3 2 5 0 73520.70 78687.40 566.96 o 3 2 5 1 2177.49 1877.07 14.44 o 3 2 5 2 15.62 13.36 0.76 o 3 2 5 3 56.39 52.14 1.73 o 3 3 0 1 6.41 7.13 0.35 o 3 3 0 2 1.20 1.11 0.21 o 3 3 0 3 0.16 0.00 0.14 < 3 3 2 -3 0.75 0.76 0.14 o 3 3 2 -2 1.49 1.04 0.21 o 3 3 2 -1 24.75 22.84 0.90 o 3 3 2 0 109.00 129.96 1.80 o 3 3 2 1 33.44 33.09 0.83 o 3 3 2 2 4.21 3.32 0.42 o 3 3 2 3 0.00 -0.14 0.14 < 3 3 4 -3 0.05 0.07 0.14 < 3 3 4 -2 0.00 0.14 0.14 < 3 3 4 -1 1.64 1.18 0.21 o 3 3 4 0 179.43 156.85 3.19 o 3 3 4 1 5.95 4.84 0.42 o 3 3 4 2 1.71 1.73 0.28 o 3 3 4 3 0.24 0.35 0.28 < 3 3 6 -3 1.73 1.87 0.28 o 3 3 6 -2 0.02 0.42 0.28 < 3 4 1 -3 31.61 34.06 0.83 o 3 4 1 -2 11.50 12.18 0.48 o 3 4 1 -1 2626.85 2803.84 21.32 o 3 4 1 0 4478.19 5062.19 37.61 o 3 4 1 1 2184.46 2176.46 22.48 o 3 4 1 2 16.49 13.91 0.69 o 3 4 1 3 23.32 22.57 0.69 o 3 4 3 -3 22.74 21.04 0.69 o 3 4 3 -2 7.23 7.61 0.42 o 3 4 3 -1 1698.26 1699.67 19.48 o 3 4 3 0 5314.64 4370.60 70.96 o 3 4 3 1 1599.89 1588.86 15.08 o 3 4 3 2 9.19 9.83 0.48 o 3 4 3 3 26.26 24.36 1.32 o 3 4 5 -3 2.90 2.63 0.42 o 3 4 5 -2 0.99 1.94 0.42 o 3 4 5 -1 771.08 682.72 12.60 o 3 4 5 0 6749.30 6929.83 73.26 o 3 4 5 1 569.39 608.35 9.98 o 3 5 0 1 27.41 26.37 0.76 o 3 5 0 2 1.24 1.18 0.21 o 3 5 0 3 0.07 0.35 0.14 < 3 5 2 -3 0.01 -0.07 0.07 < 3 5 2 -2 0.01 -0.07 0.14 < 3 5 2 -1 0.23 0.00 0.14 < 3 5 2 0 58.41 60.05 1.73 o 3 5 2 1 5.23 2.84 0.42 o 3 5 2 2 0.44 0.00 0.21 < 3 5 2 3 0.30 0.28 0.21 < 3 5 4 -3 1.21 2.63 0.42 o 3 5 4 -2 0.02 -0.07 0.21 < 3 5 4 -1 6.39 8.23 1.11 o 3 5 4 0 117.04 176.82 4.78 o 3 5 4 1 8.93 10.73 0.76 o 3 5 4 2 1.37 0.69 0.35 < 3 5 4 3 0.16 -0.21 0.21 < 4 0 0 0 140147.00 133797.00 1923.53 o 4 0 0 1 7076.64 7841.53 81.61 o 4 0 0 2 62.78 59.52 1.94 o 4 0 0 3 103.82 116.43 2.50 o 4 0 2 -3 164.53 175.88 3.82 o 4 0 2 -2 44.91 42.38 1.45 o 4 0 2 -1 7058.58 7055.12 87.90 o 4 0 2 0 94256.20 91774.90 935.16 o 4 0 2 1 7231.53 7981.69 83.37 o 4 0 2 3 162.06 149.48 3.40 o 4 0 4 -3 54.10 55.82 1.59 o 4 0 4 -2 17.92 17.30 0.90 o 4 0 4 -1 3782.40 3997.82 64.57 o 4 0 4 0 85140.00 105062.00 1065.57 o 4 0 4 1 4062.61 4417.08 56.66 o 4 0 4 2 35.55 39.11 1.45 o 4 0 4 3 71.14 77.43 2.91 o 4 0 6 -3 51.88 52.35 2.49 o 4 1 1 -3 0.01 0.00 0.14 < 4 1 1 -2 0.12 0.21 0.14 < 4 1 1 -1 1.80 2.42 0.28 o 4 1 1 0 12.48 14.74 0.55 o 4 1 1 1 0.42 0.69 0.21 < 4 1 1 2 0.60 0.76 0.21 < 4 1 1 3 0.12 0.14 0.14 < 4 1 3 -3 1.53 1.38 0.21 o 4 1 3 -2 0.02 0.28 0.21 < 4 1 3 -1 17.99 18.06 0.76 o 4 1 3 0 4.05 3.67 0.35 o 4 1 3 1 2.74 3.18 0.28 o 4 1 3 2 1.40 2.14 0.28 o 4 1 3 3 1.02 1.38 0.35 < 4 1 5 -3 1.53 2.01 0.28 o 4 1 5 -2 0.07 -0.14 0.14 < 4 1 5 -1 17.11 15.99 0.69 o 4 1 5 0 39.87 30.74 0.90 o 4 1 5 1 0.43 0.28 0.28 < 4 2 0 0 7889.63 7894.05 94.91 o 4 2 0 1 4009.88 4444.49 47.55 o 4 2 0 2 46.91 51.53 1.11 o 4 2 0 3 65.58 74.55 1.39 o 4 2 2 -3 16.31 17.23 0.62 o 4 2 2 -2 37.76 34.27 0.90 o 4 2 2 -1 2532.86 2451.72 19.68 o 4 2 2 0 3241.23 3041.79 23.28 o 4 2 2 1 2749.77 2658.56 22.40 o 4 2 2 2 35.97 37.25 1.11 o 4 2 2 3 23.97 27.76 0.83 o 4 2 4 -3 24.74 27.20 0.83 o 4 2 4 -2 21.81 27.96 0.83 o 4 2 4 -1 1784.34 2005.36 17.31 o 4 2 4 0 10704.00 11448.80 118.87 o 4 2 4 1 1986.43 2347.24 20.11 o 4 2 4 2 17.49 23.53 0.83 o 4 2 4 3 31.20 31.77 1.04 o 4 2 6 -3 1.67 3.18 0.48 o 4 2 6 -2 6.88 6.37 0.90 o 4 3 1 -3 0.63 0.62 0.14 o 4 3 1 -2 0.03 0.00 0.14 < 4 3 1 -1 7.86 8.37 0.48 o 4 3 1 0 51.99 50.49 1.11 o 4 3 1 1 3.63 3.94 0.35 o 4 3 1 2 0.42 0.42 0.14 < 4 3 1 3 1.17 0.83 0.21 < 4 3 3 -3 0.12 0.35 0.14 < 4 3 3 -2 0.13 0.00 0.14 < 4 3 3 -1 5.39 8.44 0.69 o 4 3 3 0 61.77 76.81 1.45 o 4 3 3 1 0.18 0.21 0.28 < 4 3 3 2 0.41 0.83 0.21 < 4 3 3 3 0.14 0.14 0.21 < 4 3 5 -3 2.77 3.18 0.35 o 4 3 5 -2 0.07 0.14 0.14 < 4 3 5 -1 21.92 18.13 0.90 o 4 4 0 0 95148.60 88411.30 901.40 o 4 4 0 1 4716.81 4844.62 42.26 o 4 4 0 2 36.86 32.40 0.90 o 4 4 0 3 74.46 75.31 1.39 o 4 4 2 -3 97.89 105.28 1.73 o 4 4 2 -2 28.37 26.17 0.83 o 4 4 2 -1 4551.81 4860.61 68.87 o 4 4 2 0 71735.00 67436.70 486.67 o 4 4 2 1 4710.83 4853.56 35.96 o 4 4 2 2 34.42 32.81 0.90 o 4 4 2 3 102.29 103.47 2.15 o 4 4 4 -3 40.56 53.45 2.42 o 4 4 4 -2 9.71 8.51 0.83 o 4 4 4 -1 2656.36 2777.87 36.21 o 4 4 4 1 2882.54 3071.32 33.67 o 4 4 4 2 24.04 23.67 1.18 o 4 5 1 -3 0.40 0.07 0.14 < 4 5 1 -2 0.06 0.14 0.14 < 4 5 1 -1 0.60 0.42 0.21 < 4 5 1 0 78.74 99.69 2.42 o 4 5 1 1 1.07 0.14 0.35 < 4 5 1 2 0.11 0.35 0.21 < 4 5 1 3 0.03 0.14 0.21 < 4 5 3 -3 1.71 2.21 0.42 o 4 5 3 -2 0.03 -0.14 0.21 < 4 5 3 -1 14.79 18.75 1.04 o 4 5 3 0 30.82 27.90 1.25 o 4 5 3 1 5.99 9.48 0.76 o 4 5 3 2 0.96 1.52 0.35 o 4 5 3 3 1.39 0.97 0.35 < 4 5 5 -3 0.30 0.76 0.28 < 5 0 1 -3 54.47 53.19 1.66 o 5 0 1 -2 77.56 82.59 2.15 o 5 0 1 -1 4136.36 4636.69 49.30 o 5 0 1 0 11987.90 12645.90 171.37 o 5 0 1 1 3937.11 3885.00 54.92 o 5 0 1 2 89.58 89.60 2.70 o 5 0 1 3 61.36 55.13 1.73 o 5 0 3 -3 26.03 23.81 1.11 o 5 0 3 -2 44.49 47.22 1.59 o 5 0 3 -1 2758.46 2943.93 32.24 o 5 0 3 0 12700.30 13318.00 194.46 o 5 0 3 1 2358.22 2350.37 39.24 o 5 0 3 3 24.72 36.34 1.38 o 5 0 5 -3 16.17 15.85 0.97 o 5 1 0 1 32.63 33.44 0.90 o 5 1 0 2 3.63 4.01 0.35 o 5 1 0 3 0.07 0.07 0.14 < 5 1 2 -3 0.25 0.14 0.14 < 5 1 2 -2 3.41 3.18 0.35 o 5 1 2 -1 28.13 24.57 0.83 o 5 1 2 0 55.23 54.64 1.25 o 5 1 2 1 36.32 39.32 1.45 o 5 1 2 2 4.04 4.29 0.42 o 5 1 2 3 0.01 0.14 0.21 < 5 1 4 -3 0.20 0.90 0.21 o 5 1 4 -2 0.88 1.31 0.28 o 5 1 4 -1 5.63 5.74 0.62 o 5 1 4 0 113.08 114.14 1.87 o 5 1 4 1 13.66 15.29 0.90 o 5 2 1 -3 155.60 156.59 2.22 o 5 2 1 -2 76.25 72.88 1.66 o 5 2 1 -1 7597.72 8277.56 61.04 o 5 2 1 0 66659.60 62738.50 515.30 o 5 2 1 1 7149.32 7328.12 54.13 o 5 2 1 2 96.74 87.25 1.59 o 5 2 1 3 142.16 138.78 3.05 o 5 2 3 -3 125.57 111.90 1.87 o 5 2 3 -2 40.65 41.33 1.52 o 5 2 3 -1 5901.10 5944.32 48.17 o 5 2 3 0 58823.20 61932.30 469.65 o 5 2 3 1 5358.54 5212.12 54.33 o 5 2 3 2 82.90 87.91 1.66 o 5 2 3 3 131.72 139.96 2.15 o 5 2 5 -3 54.81 59.89 1.38 o 5 2 5 -2 11.58 17.44 1.04 o 5 3 0 1 42.84 43.27 1.11 o 5 3 0 2 5.15 4.98 0.42 o 5 3 0 3 0.06 -0.14 0.14 < 5 3 2 -3 0.02 -0.07 0.14 < 5 3 2 -2 1.60 1.59 0.28 o 5 3 2 -1 8.95 8.93 0.69 o 5 3 2 0 38.26 37.52 1.04 o 5 3 2 1 19.57 15.43 0.83 o 5 3 2 2 2.04 2.56 0.28 o 5 3 2 3 0.09 -0.14 0.14 < 5 3 4 -3 0.67 0.69 0.28 < 5 3 4 -2 1.65 1.80 0.28 o 5 3 4 -1 12.81 13.42 0.90 o 5 3 4 0 92.32 138.14 4.09 o 5 4 1 -3 31.02 32.05 0.97 o 5 4 1 -2 52.39 54.57 1.25 o 5 4 1 -1 2529.10 2560.50 21.60 o 5 4 1 0 10633.10 10222.20 87.45 o 5 4 1 1 2552.87 2601.62 32.82 o 5 4 1 2 53.57 53.80 1.25 o 5 4 1 3 36.11 34.96 0.97 o 5 4 3 -3 16.08 16.26 0.83 o 5 4 3 -2 26.28 32.46 1.59 o 5 4 3 -1 1828.81 2268.03 36.11 o 5 4 3 0 11529.80 13252.70 137.23 o 5 4 3 1 1471.91 1775.02 30.10 o 5 4 3 2 44.96 57.60 1.87 o 5 5 2 -3 0.24 -0.14 0.35 < 5 5 2 -2 1.95 1.45 0.48 < 5 5 2 -1 21.70 20.76 1.52 o 5 5 2 0 34.98 45.55 2.28 o 5 5 2 1 23.76 22.70 1.32 o 5 5 2 2 2.34 3.04 0.55 o 5 5 2 3 0.02 0.07 0.35 < 5 5 4 -3 0.03 1.38 0.48 < 6 0 0 0 40745.50 36698.30 530.62 o 6 0 0 1 6957.13 6916.53 82.55 o 6 0 0 2 114.31 112.42 2.63 o 6 0 0 3 187.45 182.57 3.61 o 6 0 2 -2 93.53 88.76 3.40 o 6 0 2 -1 5207.58 5518.33 75.94 o 6 0 2 0 47757.70 42754.70 482.67 o 6 0 2 1 5429.16 4934.38 52.01 o 6 0 2 2 103.06 94.86 2.36 o 6 1 1 -3 0.01 0.00 0.14 < 6 1 1 -2 0.06 0.42 0.21 < 6 1 1 -1 15.79 16.61 0.69 o 6 1 1 0 0.86 0.42 0.28 < 6 1 1 1 1.49 1.31 0.35 < 6 1 1 2 0.12 0.55 0.21 < 6 1 1 3 0.58 1.04 0.28 < 6 1 3 -3 0.06 0.14 0.21 < 6 1 3 -2 0.04 0.28 0.21 < 6 1 3 -1 24.94 26.51 1.18 o 6 2 0 0 8931.61 10260.20 106.64 o 6 2 0 1 2207.82 1882.41 15.16 o 6 2 0 2 87.78 91.94 2.36 o 6 2 0 3 22.96 18.27 0.97 o 6 2 2 -3 39.95 39.60 1.80 o 6 2 2 -2 78.14 81.04 1.66 o 6 2 2 -1 2216.79 1999.76 18.37 o 6 2 2 0 14130.30 13067.20 109.88 o 6 2 2 1 2338.02 2202.55 17.38 o 6 2 2 2 70.19 80.41 2.22 o 6 3 1 -2 0.08 0.14 0.35 < 6 3 1 -1 4.76 5.40 0.55 o 6 3 1 0 31.88 33.85 1.18 o 6 3 1 1 4.26 4.29 0.35 o 6 3 1 2 0.06 0.21 0.21 < 6 3 1 3 0.01 0.07 0.14 < 6 3 3 -3 0.77 1.11 0.21 o 6 3 3 -2 0.05 -0.07 0.21 < 6 3 3 -1 34.61 30.66 1.32 o 6 4 0 0 30930.30 29911.70 348.23 o 6 4 0 1 4704.37 4569.71 37.41 o 6 4 0 2 77.15 79.24 1.73 o 6 4 0 3 121.40 120.46 2.29 o 6 4 2 -3 70.98 69.47 2.42 o 6 4 2 -2 61.35 54.78 1.80 o 6 4 2 -1 3663.79 3645.74 53.52 o