#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200044.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2200044_Fobs
loop_
_publ_author_name
'Bryan, Jeffrey C.'
'Marchand, Alan P.'
'Hazlewood, Anna'
_publ_section_title
;
 <i>N</i>,<i>N</i>'-Diacetyl-1,13-diaza-24-crown-8
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o13
_journal_page_last               o15
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                98.953
_cell_angle_beta                 105.103
_cell_angle_gamma                108.424
_cell_length_a                   7.4145
_cell_length_b                   8.1451
_cell_length_c                   10.2995
_exptl_crystal_F_000             236.00
_reflns_d_resolution_high        0.7579
_[local]_cod_data_source_file    na6001Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' ah33 in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            74.09
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 0.40 0.31 0.24 o
2 0 0 619.47 615.50 4.46 o
3 0 0 16.53 18.53 1.22 o
4 0 0 189.17 203.00 2.58 o
5 0 0 80.55 72.48 1.14 o
6 0 0 6.72 5.79 0.30 o
7 0 0 6.73 6.17 0.33 o
8 0 0 3.55 2.61 0.38 o
-9 1 0 0.12 0.78 0.43 o
-8 1 0 62.43 66.37 1.73 o
-7 1 0 109.68 111.97 1.95 o
-6 1 0 74.51 77.97 1.29 o
-5 1 0 5.88 6.55 0.72 o
-4 1 0 99.44 95.06 1.08 o
-3 1 0 160.38 146.25 1.38 o
-2 1 0 753.16 697.25 1.94 o
-1 1 0 2242.17 1975.72 16.39 o
0 1 0 173.63 177.06 2.41 o
2 1 0 385.30 397.79 10.92 o
3 1 0 1164.13 1204.05 15.82 o
4 1 0 0.31 0.02 0.21 o
5 1 0 4.35 6.42 0.31 o
6 1 0 86.96 79.96 1.43 o
7 1 0 68.51 63.53 1.43 o
8 1 0 66.09 66.19 1.60 o
-9 2 0 2.20 2.52 0.49 o
-8 2 0 30.55 31.65 2.75 o
-7 2 0 117.35 115.34 2.51 o
-6 2 0 0.45 -0.01 0.48 o
-5 2 0 311.49 306.50 3.08 o
-4 2 0 2.22 1.98 0.15 o
-3 2 0 9.21 9.01 0.35 o
-2 2 0 1713.37 1613.29 53.94 o
-1 2 0 381.11 381.94 3.98 o
0 2 0 2984.57 2944.25 67.20 o
1 2 0 9.94 10.04 0.36 o
2 2 0 5.66 6.98 0.33 o
3 2 0 304.20 297.87 3.35 o
4 2 0 360.03 387.40 5.18 o
5 2 0 8.26 10.16 0.51 o
6 2 0 105.66 95.03 1.66 o
7 2 0 1.18 0.84 0.51 o
-9 3 0 53.00 56.01 1.48 o
-8 3 0 0.50 0.71 0.50 o
-7 3 0 2.23 2.03 0.25 o
-6 3 0 258.76 247.42 2.17 o
-5 3 0 172.55 173.40 3.08 o
-4 3 0 301.49 296.02 3.19 o
-3 3 0 45.23 44.77 0.69 o
-2 3 0 376.92 392.54 2.63 o
-1 3 0 172.40 196.16 1.20 o
0 3 0 49.07 54.08 1.31 o
1 3 0 19.06 22.61 0.54 o
2 3 0 68.82 68.63 0.99 o
3 3 0 265.88 266.69 4.84 o
4 3 0 7.67 8.61 0.43 o
5 3 0 16.70 19.05 0.84 o
6 3 0 1.66 1.23 0.42 o
7 3 0 31.76 28.22 1.18 o
-9 4 0 0.59 0.55 0.40 o
-8 4 0 0.92 0.99 0.32 o
-7 4 0 1.44 0.23 0.46 o
-6 4 0 255.50 233.32 6.08 o
-5 4 0 268.32 260.50 6.22 o
-4 4 0 6.27 6.74 0.33 o
-3 4 0 209.11 216.18 1.96 o
-2 4 0 25.85 26.94 0.74 o
-1 4 0 50.53 54.81 0.97 o
0 4 0 640.30 699.42 10.98 o
1 4 0 0.66 0.25 0.30 o
2 4 0 74.26 79.26 1.94 o
3 4 0 4.44 3.88 0.37 o
4 4 0 12.34 12.16 0.52 o
5 4 0 67.40 61.18 1.38 o
6 4 0 12.85 11.20 0.57 o
-9 5 0 11.68 13.83 0.63 o
-8 5 0 1.09 1.91 0.50 o
-7 5 0 10.71 11.13 0.84 o
-6 5 0 13.37 10.58 0.53 o
-5 5 0 174.78 165.85 1.72 o
-4 5 0 73.59 75.37 1.42 o
-3 5 0 19.28 18.83 0.58 o
-2 5 0 9.62 12.59 0.61 o
-1 5 0 122.89 128.46 4.48 o
0 5 0 8.29 11.32 0.87 o
1 5 0 1.60 2.18 0.24 o
2 5 0 370.10 383.64 2.69 o
3 5 0 44.44 42.51 1.08 o
4 5 0 24.93 21.35 1.64 o
5 5 0 0.70 0.77 0.62 o
6 5 0 4.55 4.18 0.44 o
-9 6 0 3.33 3.36 0.68 o
-8 6 0 25.40 29.11 1.06 o
-7 6 0 19.80 18.65 1.02 o
-6 6 0 511.06 485.53 10.64 o
-5 6 0 193.80 186.77 4.70 o
-4 6 0 176.19 174.86 2.53 o
-3 6 0 84.22 81.21 2.51 o
-2 6 0 47.77 41.81 0.91 o
-1 6 0 0.26 0.51 0.22 o
0 6 0 14.67 14.86 0.89 o
1 6 0 0.49 1.77 0.28 o
2 6 0 34.89 32.11 0.97 o
3 6 0 135.80 136.81 1.97 o
4 6 0 8.60 7.87 0.84 o
5 6 0 6.83 7.35 0.47 o
-8 7 0 7.99 7.57 0.41 o
-7 7 0 1.17 0.32 0.36 o
-6 7 0 292.11 290.98 2.66 o
-5 7 0 159.74 155.23 1.87 o
-4 7 0 91.95 90.23 1.41 o
-3 7 0 491.96 483.70 4.83 o
-2 7 0 63.06 67.61 2.39 o
-1 7 0 0.55 0.61 0.44 o
0 7 0 45.71 41.25 1.62 o
1 7 0 105.89 108.43 1.67 o
2 7 0 0.04 0.72 0.54 o
3 7 0 0.00 0.06 0.75 o
4 7 0 0.13 -0.02 0.70 o
-8 8 0 20.99 20.62 0.94 o
-7 8 0 8.36 9.97 0.57 o
-6 8 0 52.47 54.30 1.32 o
-5 8 0 208.68 203.66 2.29 o
-4 8 0 52.30 52.66 1.21 o
-3 8 0 34.02 32.52 1.01 o
-2 8 0 335.49 326.92 3.57 o
-1 8 0 14.14 16.57 0.79 o
0 8 0 2.83 2.47 0.32 o
1 8 0 23.50 21.63 1.65 o
2 8 0 23.93 22.99 2.19 o
3 8 0 13.75 14.93 2.06 o
-7 9 0 2.24 2.27 1.06 o
-6 9 0 2.09 1.98 0.35 o
-5 9 0 2.67 2.59 0.32 o
-4 9 0 1.10 1.17 0.62 o
-3 9 0 324.96 315.26 2.96 o
-2 9 0 54.52 50.72 2.15 o
-1 9 0 73.37 75.32 1.56 o
0 9 0 26.84 24.25 1.08 o
1 9 0 25.69 21.93 0.99 o
-6 10 0 0.24 0.72 0.36 o
-5 10 0 11.34 12.74 0.59 o
-4 10 0 13.29 12.47 0.57 o
-3 10 0 20.70 19.97 1.51 o
-2 10 0 11.31 12.59 0.63 o
-1 10 0 9.05 8.98 0.50 o
0 -10 1 8.56 6.85 0.50 o
1 -10 1 1.21 0.70 0.68 o
2 -10 1 1.47 0.65 0.77 o
3 -10 1 27.12 28.12 1.13 o
4 -10 1 2.42 2.76 0.89 o
5 -10 1 0.17 0.98 0.82 o
6 -10 1 41.99 41.27 2.20 o
-1 -9 1 20.39 17.74 0.84 o
0 -9 1 24.18 21.58 0.92 o
1 -9 1 0.96 0.89 0.40 o
2 -9 1 1.03 -0.15 0.59 o
3 -9 1 2.74 3.79 0.35 o
4 -9 1 82.52 81.93 3.71 o
5 -9 1 34.76 36.20 1.31 o
6 -9 1 27.44 29.65 1.11 o
7 -9 1 35.09 39.96 1.29 o
-3 -8 1 0.18 -0.69 0.73 o
-2 -8 1 8.49 8.72 0.44 o
-1 -8 1 2.79 3.36 0.34 o
0 -8 1 17.68 15.58 0.75 o
1 -8 1 35.01 28.75 1.85 o
2 -8 1 96.76 105.49 1.95 o
3 -8 1 84.77 82.45 1.51 o
4 -8 1 161.08 152.32 1.93 o
5 -8 1 25.71 27.14 0.98 o
6 -8 1 2.10 1.31 0.29 o
7 -8 1 71.03 74.67 1.58 o
8 -8 1 9.92 11.03 0.82 o
-4 -7 1 63.25 64.46 1.77 o
-3 -7 1 120.13 114.47 6.67 o
-2 -7 1 0.01 -0.60 0.60 o
-1 -7 1 133.81 120.53 1.73 o
0 -7 1 12.34 12.79 0.67 o
1 -7 1 17.03 16.24 0.73 o
2 -7 1 122.25 120.82 3.54 o
3 -7 1 126.77 132.06 1.63 o
4 -7 1 4.00 3.65 0.26 o
5 -7 1 24.49 23.25 0.82 o
6 -7 1 50.36 53.89 1.90 o
7 -7 1 82.30 80.63 1.57 o
8 -7 1 23.84 26.10 1.11 o
-5 -6 1 1.99 1.55 0.48 o
-4 -6 1 62.24 62.42 3.67 o
-3 -6 1 42.96 41.94 1.17 o
-2 -6 1 26.62 26.00 0.88 o
-1 -6 1 191.04 194.64 2.10 o
0 -6 1 54.65 62.51 2.21 o
1 -6 1 7.74 6.85 0.36 o
2 -6 1 28.96 36.74 0.92 o
3 -6 1 253.28 249.69 2.05 o
4 -6 1 17.43 16.72 0.64 o
5 -6 1 0.00 0.99 0.54 o
6 -6 1 1.27 0.47 0.48 o
7 -6 1 65.45 65.95 1.73 o
8 -6 1 6.93 7.87 0.63 o
9 -6 1 15.93 17.06 0.94 o
-6 -5 1 6.74 6.13 0.45 o
-5 -5 1 18.74 19.84 0.92 o
-4 -5 1 13.83 14.99 1.24 o
-3 -5 1 32.89 29.84 1.14 o
-2 -5 1 64.57 60.91 1.13 o
-1 -5 1 0.62 2.52 0.62 o
0 -5 1 597.01 666.12 14.27 o
1 -5 1 20.15 24.39 0.63 o
2 -5 1 112.77 112.05 1.27 o
3 -5 1 91.26 98.14 2.98 o
4 -5 1 10.24 11.83 0.53 o
5 -5 1 149.40 144.09 3.43 o
6 -5 1 109.87 111.80 1.55 o
7 -5 1 25.26 21.99 0.85 o
8 -5 1 8.78 8.24 0.44 o
9 -5 1 11.83 12.69 0.66 o
-7 -4 1 0.99 1.54 0.40 o
-6 -4 1 24.04 21.12 0.97 o
-5 -4 1 9.55 9.05 0.48 o
-4 -4 1 75.93 71.08 1.75 o
-3 -4 1 72.96 81.82 3.59 o
-2 -4 1 175.45 172.40 1.60 o
-1 -4 1 82.14 96.87 1.99 o
0 -4 1 211.09 235.14 3.67 o
1 -4 1 131.55 155.26 1.65 o
2 -4 1 469.69 529.13 2.31 o
3 -4 1 3.60 3.58 0.20 o
4 -4 1 58.62 63.17 0.95 o
5 -4 1 18.65 18.95 1.20 o
6 -4 1 31.35 27.94 0.92 o
7 -4 1 4.22 4.45 0.34 o
8 -4 1 86.00 85.10 1.63 o
9 -4 1 4.97 5.30 0.41 o
-7 -3 1 73.95 68.42 1.61 o
-6 -3 1 4.49 3.69 0.33 o
-5 -3 1 127.68 114.07 1.66 o
-4 -3 1 5.12 3.55 0.26 o
-3 -3 1 8.00 12.19 0.85 o
-2 -3 1 1164.89 1205.15 3.77 o
-1 -3 1 6.24 6.88 0.51 o
0 -3 1 208.53 205.81 3.61 o
1 -3 1 26.73 27.75 0.57 o
2 -3 1 606.78 617.02 11.14 o
3 -3 1 60.36 66.49 0.84 o
4 -3 1 150.54 138.70 1.33 o
5 -3 1 35.52 31.88 0.77 o
6 -3 1 148.00 143.81 2.07 o
7 -3 1 108.83 104.71 2.63 o
8 -3 1 0.02 -0.17 0.51 o
9 -3 1 58.65 61.16 1.76 o
-8 -2 1 3.89 3.65 0.42 o
-7 -2 1 11.11 10.02 0.49 o
-6 -2 1 166.80 149.69 2.57 o
-5 -2 1 6.34 5.79 0.29 o
-4 -2 1 3.98 6.25 0.47 o
-3 -2 1 147.67 160.43 3.22 o
-2 -2 1 274.84 294.63 1.72 o
-1 -2 1 641.30 671.04 2.09 o
0 -2 1 15.69 17.27 0.40 o
1 -2 1 5489.78 5016.07 30.61 o
2 -2 1 107.42 113.92 3.02 o
3 -2 1 674.34 678.81 12.81 o
4 -2 1 14.80 14.21 0.56 o
5 -2 1 19.69 18.63 0.63 o
6 -2 1 488.42 477.53 3.07 o
7 -2 1 73.84 72.54 1.40 o
8 -2 1 10.98 10.44 0.50 o
9 -2 1 66.99 71.36 1.70 o
-8 -1 1 13.85 13.66 0.66 o
-7 -1 1 36.36 41.60 1.17 o
-6 -1 1 78.28 85.08 1.42 o
-5 -1 1 0.07 -0.08 0.26 o
-4 -1 1 36.08 35.29 0.76 o
-3 -1 1 238.06 247.65 1.64 o
-2 -1 1 38.93 33.04 0.91 o
-1 -1 1 122.71 108.58 0.74 o
0 -1 1 125.40 124.98 0.99 o
1 -1 1 2093.77 1870.60 12.80 o
2 -1 1 1576.73 1537.30 16.78 o
3 -1 1 45.27 41.48 0.66 o
4 -1 1 1.95 2.07 0.16 o
5 -1 1 7.57 10.16 0.46 o
6 -1 1 71.92 70.54 1.26 o
7 -1 1 325.23 316.46 2.87 o
8 -1 1 0.18 -0.07 0.58 o
-8 0 1 2.06 1.98 0.30 o
-7 0 1 7.92 8.25 0.40 o
-6 0 1 105.17 98.80 4.00 o
-5 0 1 8.26 9.87 0.46 o
-4 0 1 732.13 741.31 3.03 o
-3 0 1 0.49 1.34 0.24 o
-2 0 1 26.62 25.86 0.44 o
-1 0 1 719.25 709.42 8.99 o
0 0 1 41.45 38.82 0.30 o
1 0 1 1.64 0.19 0.24 o
2 0 1 301.06 317.39 4.41 o
3 0 1 0.52 1.74 0.15 o
4 0 1 42.06 42.11 1.01 o
5 0 1 14.72 17.79 1.22 o
6 0 1 14.71 11.96 0.56 o
7 0 1 25.76 24.50 1.61 o
8 0 1 1.22 0.44 0.79 o
-9 1 1 8.97 11.77 1.35 o
-8 1 1 141.58 148.06 2.10 o
-7 1 1 9.42 8.36 0.41 o
-6 1 1 13.75 15.43 0.64 o
-5 1 1 49.30 53.47 2.58 o
-4 1 1 27.85 26.57 0.61 o
-3 1 1 1266.88 1259.03 17.14 o
-2 1 1 762.78 722.70 6.33 o
-1 1 1 105.61 112.94 1.46 o
0 1 1 35.85 43.08 0.45 o
1 1 1 1733.11 1809.27 13.43 o
2 1 1 31.38 34.71 0.95 o
3 1 1 219.15 233.61 3.55 o
4 1 1 7.42 4.65 0.28 o
5 1 1 23.62 23.57 1.00 o
6 1 1 22.53 24.63 0.91 o
7 1 1 62.76 60.75 1.43 o
8 1 1 17.96 19.72 2.20 o
-9 2 1 9.92 10.40 0.50 o
-8 2 1 51.89 48.37 1.23 o
-7 2 1 0.10 0.50 0.46 o
-6 2 1 537.18 536.87 10.87 o
-5 2 1 32.95 30.74 0.72 o
-4 2 1 237.88 240.85 1.63 o
-3 2 1 72.49 76.28 1.47 o
-2 2 1 1.44 0.61 0.21 o
-1 2 1 0.50 0.18 0.41 o
0 2 1 521.32 582.58 7.36 o
1 2 1 57.90 60.98 0.73 o
2 2 1 75.91 78.21 0.95 o
3 2 1 10.48 11.50 0.52 o
4 2 1 145.62 148.62 1.68 o
5 2 1 7.48 7.23 0.35 o
6 2 1 93.13 92.50 3.37 o
7 2 1 33.73 35.19 1.21 o
-9 3 1 0.00 -0.54 0.55 o
-8 3 1 10.84 10.48 0.51 o
-7 3 1 5.16 5.21 0.34 o
-6 3 1 11.50 10.03 0.48 o
-5 3 1 118.80 117.18 1.33 o
-4 3 1 13.87 10.92 0.44 o
-3 3 1 240.69 254.20 4.05 o
-2 3 1 61.00 62.90 0.75 o
-1 3 1 275.39 295.64 4.24 o
0 3 1 68.10 67.66 0.81 o
1 3 1 211.73 239.06 2.45 o
2 3 1 0.14 0.37 0.32 o
3 3 1 68.65 74.32 1.20 o
4 3 1 15.13 14.97 0.68 o
5 3 1 15.51 14.28 0.66 o
6 3 1 4.82 4.61 0.90 o
7 3 1 15.84 17.06 1.36 o
-9 4 1 2.98 2.34 0.90 o
-8 4 1 76.90 75.00 1.46 o
-7 4 1 2.56 2.15 0.33 o
-6 4 1 0.15 0.37 0.37 o
-5 4 1 347.91 336.74 12.33 o
-4 4 1 375.74 352.10 2.12 o
-3 4 1 4.49 4.78 0.24 o
-2 4 1 387.97 432.02 6.84 o
-1 4 1 2.32 3.16 0.18 o
0 4 1 131.86 146.00 1.33 o
1 4 1 55.23 55.96 1.13 o
2 4 1 4.42 4.49 0.33 o
3 4 1 130.57 124.69 1.64 o
4 4 1 29.38 28.58 0.94 o
5 4 1 41.15 37.10 1.17 o
6 4 1 13.04 14.84 0.73 o
-9 5 1 4.33 4.39 0.37 o
-8 5 1 52.73 49.79 2.80 o
-7 5 1 57.70 53.13 1.18 o
-6 5 1 2.63 2.49 0.39 o
-5 5 1 354.99 339.54 2.40 o
-4 5 1 72.99 68.80 1.06 o
-3 5 1 174.64 173.94 4.58 o
-2 5 1 101.97 106.11 1.70 o
-1 5 1 8.76 5.42 0.29 o
0 5 1 5.01 6.89 0.60 o
1 5 1 310.07 327.67 2.38 o
2 5 1 443.19 436.02 2.94 o
3 5 1 209.35 200.91 3.98 o
4 5 1 10.32 10.83 0.46 o
5 5 1 7.10 7.41 0.88 o
-9 6 1 0.01 0.03 0.61 o
-8 6 1 0.32 0.11 0.49 o
-7 6 1 2.56 2.47 0.27 o
-6 6 1 32.28 31.20 1.34 o
-5 6 1 60.37 67.12 1.41 o
-4 6 1 247.00 250.60 4.25 o
-3 6 1 0.25 0.27 0.27 o
-2 6 1 29.06 23.88 0.75 o
-1 6 1 219.04 218.36 2.43 o
0 6 1 39.12 43.05 2.65 o
1 6 1 123.15 117.89 3.90 o
2 6 1 6.15 6.99 0.60 o
3 6 1 6.29 7.19 0.43 o
4 6 1 317.71 300.83 6.10 o
-9 7 1 0.09 0.29 0.84 o
-8 7 1 4.92 5.40 0.38 o
-7 7 1 1.59 1.78 0.40 o
-6 7 1 5.10 6.81 0.37 o
-5 7 1 0.63 0.79 0.47 o
-4 7 1 24.01 22.42 0.80 o
-3 7 1 0.61 0.09 0.47 o
-2 7 1 8.87 9.57 0.50 o
-1 7 1 56.88 50.59 1.50 o
0 7 1 148.50 143.80 6.79 o
1 7 1 15.34 15.99 0.82 o
2 7 1 34.82 31.73 2.07 o
3 7 1 97.96 87.82 3.22 o
-8 8 1 2.98 3.75 0.37 o
-7 8 1 31.44 31.90 1.07 o
-6 8 1 14.10 13.34 0.69 o
-5 8 1 0.22 0.49 0.48 o
-4 8 1 0.60 1.19 0.89 o
-3 8 1 186.11 177.19 2.08 o
-2 8 1 10.67 9.34 0.47 o
-1 8 1 3.17 3.31 0.33 o
0 8 1 12.09 10.52 0.58 o
1 8 1 68.26 61.27 2.03 o
2 8 1 1.02 1.24 0.86 o
-7 9 1 1.82 2.48 0.36 o
-6 9 1 3.54 2.78 0.37 o
-5 9 1 5.44 5.59 0.38 o
-4 9 1 99.52 100.81 1.74 o
-3 9 1 8.75 8.41 0.49 o
-2 9 1 23.63 24.62 1.07 o
-1 9 1 1.05 1.21 0.34 o
0 9 1 30.68 30.47 1.22 o
1 9 1 1.40 0.25 0.74 o
-6 10 1 1.14 1.30 0.48 o
-5 10 1 3.15 3.55 0.42 o
-4 10 1 0.62 0.46 0.88 o
-3 10 1 4.07 4.43 0.45 o
-2 10 1 52.86 55.07 1.52 o
-1 10 1 6.22 6.52 0.48 o
0 -10 2 43.65 40.26 1.32 o
1 -10 2 1.95 1.94 0.46 o
2 -10 2 54.09 51.54 1.41 o
3 -10 2 5.38 4.56 0.43 o
4 -10 2 147.39 150.88 2.26 o
5 -10 2 122.29 131.51 2.37 o
6 -10 2 4.38 3.17 1.27 o
-2 -9 2 24.71 24.80 1.14 o
-1 -9 2 12.65 9.96 0.52 o
0 -9 2 5.92 4.72 0.37 o
1 -9 2 6.24 7.05 0.67 o
2 -9 2 24.85 26.33 0.99 o
3 -9 2 88.70 85.89 1.83 o
4 -9 2 11.94 13.13 0.63 o
5 -9 2 8.52 8.91 0.47 o
6 -9 2 6.44 4.58 0.39 o
7 -9 2 3.99 4.84 1.17 o
-3 -8 2 9.50 8.60 0.51 o
-2 -8 2 13.88 13.12 0.63 o
-1 -8 2 8.43 6.38 0.50 o
0 -8 2 103.68 89.42 1.57 o
1 -8 2 28.07 27.45 0.95 o
2 -8 2 7.88 7.21 0.41 o
3 -8 2 133.83 135.07 1.80 o
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