#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200064.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200064_Fobs loop_ _publ_author_name 'Baba, Ibrahim' 'Farina, Yang' 'Othman, A. Hamid' 'Razak, Ibrahim Abdul' 'Fun, Hoong-Kun' 'Ng, Seik Weng' _publ_section_title ; Bis(N-cyclohexyl-N-ethyldithiocarbamato-S,S')lead(II) ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m35 _journal_page_last m36 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.586 _cell_angle_beta 92.978 _cell_angle_gamma 99.142 _cell_length_a 9.7180 _cell_length_b 10.1871 _cell_length_c 11.8751 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.6494 _[local]_cod_data_source_file na6024Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' na6024 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 193.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l 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11 1 0 574.74 618.44 49.59 o 12 1 0 220.67 183.86 35.02 o -14 2 0 53.13 99.18 40.10 o -13 2 0 3.76 0.95 28.50 o -11 2 0 170.43 157.37 31.46 o -10 2 0 1655.88 1513.95 83.91 o -9 2 0 7.63 -0.31 19.05 o -8 2 0 4916.49 4996.07 231.74 o -7 2 0 1189.43 1147.46 59.09 o -6 2 0 3799.52 3844.12 127.80 o -5 2 0 7213.08 7371.55 238.53 o -4 2 0 8825.29 9016.22 289.91 o -3 2 0 16495.84 14312.64 456.85 o -2 2 0 4691.39 4497.11 118.19 o -1 2 0 8829.40 9215.95 251.97 o 0 2 0 1183.11 1347.66 74.31 o 1 2 0 19867.67 19767.10 913.83 o 3 2 0 11317.02 11222.19 523.22 o 4 2 0 1086.01 1241.38 66.14 o 5 2 0 9673.58 10866.85 510.22 o 7 2 0 2731.16 2868.52 143.79 o 8 2 0 1988.86 2005.74 106.72 o 9 2 0 2023.19 1947.31 136.02 o 10 2 0 677.23 587.47 46.20 o 11 2 0 28.71 79.48 30.47 o 12 2 0 569.09 469.94 50.70 o 13 2 0 36.38 48.56 34.34 o -14 3 0 129.15 138.22 40.23 o -12 3 0 647.19 699.64 58.57 o -10 3 0 868.18 874.35 58.11 o -9 3 0 341.50 385.32 38.92 o -8 3 0 832.06 900.34 56.68 o -7 3 0 5192.14 4783.77 221.40 o 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4045.13 159.90 o 1 4 0 7797.93 8309.97 519.57 o 2 4 0 4830.87 4775.54 229.24 o 3 4 0 436.11 428.42 33.16 o 4 4 0 3696.52 3622.93 178.13 o 5 4 0 421.56 460.86 35.19 o 6 4 0 4996.72 5144.04 251.29 o 7 4 0 198.80 167.96 27.83 o 8 4 0 1136.70 1242.40 77.41 o 9 4 0 30.58 -1.83 24.09 o 11 4 0 3.30 -17.28 23.81 o 12 4 0 100.77 38.46 30.94 o 13 4 0 65.88 38.75 35.13 o -14 5 0 14.73 32.34 32.73 o -13 5 0 21.85 -10.06 26.27 o -12 5 0 14.06 -3.16 27.08 o -11 5 0 128.30 160.65 34.29 o -10 5 0 31.89 11.69 22.05 o -9 5 0 839.89 741.04 38.49 o -8 5 0 2.13 30.77 15.38 o -7 5 0 2082.14 2005.84 72.90 o -6 5 0 89.70 122.62 13.21 o -5 5 0 4491.71 4326.41 117.61 o -4 5 0 2452.68 2427.19 68.87 o -3 5 0 2847.38 3038.48 84.23 o -2 5 0 5714.54 5157.75 216.94 o -1 5 0 2024.00 2253.47 64.72 o 0 5 0 2671.95 2519.18 71.58 o 1 5 0 43.42 58.26 12.16 o 2 5 0 10438.23 11948.57 561.81 o 3 5 0 4.82 12.41 15.46 o 4 5 0 2754.83 2846.43 145.80 o 5 5 0 58.19 57.96 20.51 o 6 5 0 1809.50 1985.45 110.43 o 7 5 0 55.32 81.25 27.97 o 8 5 0 640.04 805.79 62.98 o 9 5 0 570.85 513.70 49.04 o 10 5 0 253.00 349.64 48.61 o 11 5 0 33.61 -19.83 19.83 o 12 5 0 24.45 42.08 37.43 o 13 5 0 92.26 65.69 39.43 o -13 6 0 62.55 29.82 31.55 o -12 6 0 0.54 12.21 29.64 o -11 6 0 81.11 57.13 30.67 o -10 6 0 3.86 -7.41 22.85 o -9 6 0 1420.42 1387.08 82.60 o -8 6 0 223.45 192.11 21.63 o -7 6 0 334.48 350.90 29.36 o -6 6 0 1856.59 1650.12 62.36 o -5 6 0 985.41 1066.58 37.65 o -4 6 0 2322.36 2354.09 68.37 o -3 6 0 216.50 246.50 15.79 o -2 6 0 8959.17 9262.08 244.44 o -1 6 0 163.63 172.33 14.52 o 0 6 0 810.41 882.37 38.39 o 1 6 0 554.03 479.95 25.89 o 2 6 0 3954.23 4139.15 204.52 o 3 6 0 116.25 132.37 25.02 o 4 6 0 2304.43 2540.66 135.24 o 5 6 0 986.68 980.80 67.29 o 6 6 0 1247.46 1472.04 90.56 o 7 6 0 344.70 379.65 47.15 o 8 6 0 271.37 295.98 44.85 o 9 6 0 588.16 627.76 60.90 o 10 6 0 79.74 153.29 40.78 o 12 6 0 0.64 10.32 33.82 o -14 7 0 1.49 -20.70 32.70 o -13 7 0 207.73 273.84 48.72 o -12 7 0 27.77 -2.84 30.05 o -11 7 0 124.36 165.57 39.75 o -10 7 0 442.87 413.21 46.13 o -9 7 0 189.23 179.24 35.96 o -8 7 0 431.95 435.10 44.49 o -7 7 0 213.54 273.93 55.10 o -6 7 0 4498.10 4237.34 152.73 o -5 7 0 0.21 9.37 11.43 o -4 7 0 524.78 513.49 23.68 o -3 7 0 53.29 53.81 12.11 o -2 7 0 3410.30 3518.78 99.27 o -1 7 0 163.33 153.86 20.06 o 0 7 0 2785.44 2741.56 97.56 o 1 7 0 1541.74 1480.86 82.41 o 2 7 0 2700.68 2529.98 132.03 o 3 7 0 994.22 966.82 63.86 o 4 7 0 1455.10 1347.19 82.28 o 5 7 0 1788.51 1881.20 108.35 o 6 7 0 267.36 277.78 40.21 o 7 7 0 926.98 911.55 68.36 o 8 7 0 2.55 17.50 28.04 o 9 7 0 476.78 526.12 61.03 o 10 7 0 3.66 5.40 32.37 o 12 7 0 10.56 32.62 34.72 o -13 8 0 39.17 39.52 31.59 o -12 8 0 77.29 135.47 38.26 o -11 8 0 36.01 31.61 30.13 o -10 8 0 262.74 212.69 39.75 o -9 8 0 15.94 15.69 28.65 o -8 8 0 316.16 368.22 42.85 o -7 8 0 23.48 34.34 17.85 o -6 8 0 686.12 728.51 38.97 o -5 8 0 13.81 -5.46 12.81 o -4 8 0 1823.64 1902.57 59.42 o -3 8 0 894.61 869.48 34.16 o -2 8 0 642.15 682.22 39.02 o -1 8 0 2004.47 2039.81 63.86 o 0 8 0 2206.09 2384.91 88.71 o 1 8 0 1730.00 2185.73 122.39 o 2 8 0 34.39 28.95 22.54 o 3 8 0 2200.71 1930.21 106.73 o 4 8 0 57.56 43.40 25.79 o 5 8 0 961.58 1025.13 72.66 o 6 8 0 52.74 21.18 30.20 o 7 8 0 698.36 784.73 67.65 o 8 8 0 38.13 32.68 31.90 o 9 8 0 71.63 49.54 37.35 o 10 8 0 96.82 138.44 55.51 o -13 9 0 6.60 5.93 34.34 o -12 9 0 28.62 -17.75 29.65 o -10 9 0 117.17 104.46 38.40 o -9 9 0 51.08 70.41 37.03 o -8 9 0 297.48 332.25 44.68 o -7 9 0 137.74 111.56 36.95 o -6 9 0 224.70 282.76 37.99 o -5 9 0 622.91 665.70 38.05 o -4 9 0 607.70 682.23 32.20 o -3 9 0 1925.72 2017.34 66.23 o -2 9 0 8.17 1.50 14.20 o -1 9 0 3191.00 3237.51 116.61 o 0 9 0 14.44 11.06 17.67 o 1 9 0 1794.73 1859.54 106.83 o 2 9 0 389.13 449.53 48.68 o 3 9 0 1149.80 1167.73 80.97 o 4 9 0 311.72 312.75 46.63 o 5 9 0 335.93 293.04 45.62 o 6 9 0 301.35 229.55 44.98 o 7 9 0 238.06 233.70 50.76 o 8 9 0 213.40 284.60 57.87 o 9 9 0 14.97 28.29 45.92 o 10 9 0 189.73 180.49 50.49 o -12 10 0 47.84 52.53 39.42 o -11 10 0 6.83 52.98 38.78 o -10 10 0 97.74 163.20 44.59 o -9 10 0 141.40 157.49 43.37 o -8 10 0 147.17 264.50 49.41 o -7 10 0 478.95 474.02 52.93 o -6 10 0 6.51 33.64 29.65 o -5 10 0 1203.91 1310.41 60.03 o -4 10 0 21.38 9.76 17.09 o -3 10 0 1055.22 1123.67 44.22 o -2 10 0 158.72 185.80 22.22 o -1 10 0 1085.53 1115.76 69.59 o 0 10 0 381.89 380.25 42.09 o 1 10 0 354.24 302.74 42.80 o 2 10 0 329.43 267.93 41.34 o 3 10 0 443.31 351.15 47.88 o 4 10 0 649.34 677.23 61.42 o 5 10 0 50.11 86.54 38.93 o 6 10 0 303.93 340.39 53.61 o 7 10 0 23.92 69.53 42.23 o 8 10 0 168.32 171.91 49.16 o 9 10 0 0.22 -24.20 37.09 o -12 11 0 14.68 102.49 45.51 o -11 11 0 52.98 73.03 46.24 o -10 11 0 0.04 10.69 33.32 o -9 11 0 91.03 159.25 43.22 o -8 11 0 1.49 -3.23 33.45 o -7 11 0 272.18 358.26 51.68 o -6 11 0 125.80 144.53 44.61 o -5 11 0 269.03 284.46 31.86 o -4 11 0 195.70 175.86 37.21 o -3 11 0 81.80 25.63 20.56 o -2 11 0 225.53 225.73 29.36 o -1 11 0 190.54 179.54 59.97 o 0 11 0 807.08 770.53 64.77 o 1 11 0 64.65 49.87 28.70 o 2 11 0 333.95 264.50 41.46 o 4 11 0 216.81 172.00 42.17 o 6 11 0 188.82 253.71 55.17 o 7 11 0 82.42 163.60 52.46 o 8 11 0 61.20 57.04 41.65 o -11 12 0 45.17 -11.64 38.52 o -10 12 0 37.98 150.79 54.07 o -9 12 0 10.51 61.90 41.06 o -8 12 0 75.06 164.56 53.85 o -4 12 0 325.61 333.15 46.65 o -3 12 0 36.91 72.27 24.60 o -2 12 0 197.55 249.80 32.83 o -1 12 0 2.82 -21.06 23.37 o 0 12 0 339.81 307.04 46.08 o 1 12 0 0.83 2.61 29.36 o 2 12 0 261.83 294.31 52.81 o 3 12 0 159.15 226.76 47.96 o 4 12 0 109.84 134.05 47.33 o 5 12 0 83.47 125.42 48.71 o 6 12 0 33.35 102.58 49.38 o 7 12 0 82.00 12.26 41.78 o -3 13 0 2.57 41.27 39.68 o -2 13 0 117.05 150.26 44.88 o -1 13 0 51.39 71.15 40.10 o 0 13 0 78.16 65.47 40.87 o 1 13 0 74.26 23.40 31.22 o 2 13 0 42.38 26.09 40.35 o 3 13 0 81.80 104.91 42.35 o 4 13 0 9.51 4.24 36.51 o 5 13 0 71.69 105.19 47.96 o -1 14 0 49.21 24.29 38.57 o 0 14 0 0.91 14.13 35.94 o 1 14 0 72.09 105.48 49.97 o 2 14 0 1.18 -4.99 35.97 o 3 14 0 58.16 28.71 36.91 o -1 15 0 21.70 12.35 38.20 o 0 15 0 2.20 -18.20 37.58 o 1 15 0 27.01 29.41 43.09 o -1 -15 1 30.68 -15.21 38.02 o 0 -15 1 1.73 53.43 42.41 o 1 -15 1 22.38 18.46 43.78 o 2 -15 1 7.24 -11.62 34.42 o -4 -14 1 0.49 12.29 37.40 o -3 -14 1 45.86 47.47 42.12 o -2 -14 1 4.63 4.25 38.34 o -1 -14 1 53.29 93.16 45.36 o 0 -14 1 10.48 -33.10 33.10 o 1 -14 1 73.94 92.76 42.02 o 2 -14 1 20.72 18.78 40.26 o -5 -13 1 52.02 60.90 41.25 o -4 -13 1 5.77 4.29 33.48 o -3 -13 1 66.66 48.56 36.05 o -2 -13 1 45.21 -5.43 32.05 o -1 -13 1 23.79 38.35 37.27 o 0 -13 1 183.69 151.77 46.61 o 1 -13 1 60.09 81.69 40.79 o 2 -13 1 122.28 151.38 46.76 o 3 -13 1 0.16 8.36 32.36 o 9 -13 1 11.18 11.42 38.59 o 10 -13 1 0.64 -21.49 41.67 o -7 -12 1 54.11 106.21 52.58 o -6 -12 1 51.22 13.66 37.22 o -5 -12 1 16.05 -4.86 33.02 o -4 -12 1 202.11 189.42 42.91 o -3 -12 1 44.73 74.95 41.45 o -2 -12 1 307.01 345.85 50.71 o -1 -12 1 3.09 45.31 32.28 o 0 -12 1 479.50 451.72 56.26 o 1 -12 1 0.31 -23.24 24.95 o 2 -12 1 225.86 204.85 40.28 o 3 -12 1 59.17 64.16 24.89 o 4 -12 1 196.08 202.36 43.05 o 5 -12 1 122.51 159.29 49.50 o 6 -12 1 43.63 38.64 41.15 o 7 -12 1 49.22 131.89 46.80 o 8 -12 1 10.88 36.27 40.20 o 9 -12 1 16.86 6.39 37.17 o 10 -12 1 11.27 4.15 42.69 o 11 -12 1 43.53 63.62 43.80 o -8 -11 1 78.56 120.71 52.00 o -7 -11 1 28.65 85.27 44.05 o -6 -11 1 275.09 244.86 51.32 o -5 -11 1 7.63 -10.23 29.10 o -4 -11 1 379.05 394.14 55.22 o -3 -11 1 0.94 -14.83 26.19 o -2 -11 1 375.77 408.64 50.76 o -1 -11 1 73.75 156.12 39.40 o 0 -11 1 389.14 379.16 48.52 o 1 -11 1 398.83 322.61 41.63 o 2 -11 1 173.88 148.21 25.26 o 3 -11 1 84.56 103.06 20.04 o 4 -11 1 106.07 79.12 18.88 o 5 -11 1 192.35 237.28 48.72 o 6 -11 1 58.25 28.99 33.53 o 7 -11 1 177.69 276.30 52.16 o 8 -11 1 3.72 67.67 36.77 o 9 -11 1 94.85 171.86 46.92 o 10 -11 1 0.12 25.38 34.47 o 11 -11 1 41.94 97.08 44.79 o 12 -11 1 16.42 -19.66 41.63 o -9 -10 1 0.34 -30.76 30.76 o -8 -10 1 80.41 116.58 44.14 o -7 -10 1 68.06 26.22 32.21 o -6 -10 1 268.22 279.31 46.97 o -5 -10 1 93.50 97.35 34.97 o -4 -10 1 304.87 361.19 47.99 o -3 -10 1 747.39 767.51 63.22 o -2 -10 1 126.60 114.97 32.79 o -1 -10 1 106.76 104.63 35.12 o 0 -10 1 44.09 31.39 27.61 o 1 -10 1 1273.91 1178.44 76.73 o 2 -10 1 198.28 168.26 20.77 o 3 -10 1 502.99 557.18 31.48 o 4 -10 1 136.66 156.47 19.45 o 5 -10 1 438.12 488.30 52.73 o 6 -10 1 6.26 -4.95 29.69 o 7 -10 1 228.16 215.67 43.88 o 8 -10 1 208.96 276.30 49.09 o 9 -10 1 99.28 140.15 45.84 o 10 -10 1 51.44 95.51 42.17 o 11 -10 1 3.13 -12.94 33.53 o 12 -10 1 40.78 22.32 38.90 o -10 -9 1 121.89 150.57 46.40 o -9 -9 1 52.90 103.57 42.61 o -8 -9 1 156.83 132.78 49.86 o -7 -9 1 401.76 406.70 52.25 o -6 -9 1 141.64 90.76 35.06 o -5 -9 1 286.79 261.98 40.98 o -4 -9 1 65.31 82.33 31.72 o -3 -9 1 1383.65 1434.40 90.92 o -2 -9 1 88.73 44.30 27.44 o -1 -9 1 1409.70 1362.11 83.11 o 0 -9 1 62.24 61.61 28.64 o 1 -9 1 1452.61 1508.02 61.29 o 2 -9 1 6.16 11.08 17.66 o 3 -9 1 1481.63 1511.07 52.37 o 4 -9 1 466.95 521.62 27.61 o 5 -9 1 339.74 389.14 24.70 o 6 -9 1 708.82 803.84 64.41 o 7 -9 1 45.53 50.04 31.38 o 8 -9 1 267.22 323.76 49.70 o 9 -9 1 8.27 -24.37 24.37 o 10 -9 1 126.98 69.00 41.06 o 11 -9 1 0.10 8.26 35.14 o 12 -9 1 5.23 -17.89 34.60 o 13 -9 1 1.75 23.51 38.93 o -10 -8 1 43.31 -8.01 33.97 o -9 -8 1 95.99 64.20 38.49 o -8 -8 1 61.07 46.01 40.69 o -7 -8 1 530.36 553.98 58.44 o -6 -8 1 50.32 85.69 38.43 o -5 -8 1 957.47 1023.55 75.48 o -4 -8 1 33.93 51.42 38.00 o -3 -8 1 1850.33 1753.00 100.51 o -2 -8 1 7.46 19.24 21.00 o -1 -8 1 2048.49 2068.93 113.28 o 0 -8 1 583.36 655.49 52.55 o 1 -8 1 168.23 183.52 18.70 o 2 -8 1 1217.27 1380.13 46.81 o 3 -8 1 550.21 570.06 28.07 o 4 -8 1 890.81 1031.02 38.66 o 5 -8 1 8.00 -5.47 12.42 o 6 -8 1 688.19 755.21 38.78 o 8 -8 1 100.56 140.40 40.78 o 9 -8 1 0.29 2.86 23.87 o 10 -8 1 168.34 158.44 40.80 o 11 -8 1 4.96 7.20 30.74 o 12 -8 1 15.21 1.20 32.48 o 13 -8 1 19.53 26.36 37.36 o -10 -7 1 1.60 14.12 33.33 o -9 -7 1 405.84 489.26 58.21 o -8 -7 1 22.32 -0.09 28.32 o 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